JP2003315588A - Method for manufacturing glass hollow optical fiber - Google Patents

Method for manufacturing glass hollow optical fiber

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Publication number
JP2003315588A
JP2003315588A JP2002116801A JP2002116801A JP2003315588A JP 2003315588 A JP2003315588 A JP 2003315588A JP 2002116801 A JP2002116801 A JP 2002116801A JP 2002116801 A JP2002116801 A JP 2002116801A JP 2003315588 A JP2003315588 A JP 2003315588A
Authority
JP
Japan
Prior art keywords
optical fiber
glass
fiber
hollow optical
hollow
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP2002116801A
Other languages
Japanese (ja)
Other versions
JP3877152B2 (en
Inventor
Yuji Matsuura
祐司 松浦
Mitsunobu Miyagi
光信 宮城
Takashi Katagiri
崇史 片桐
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Miyagi Mitsunobu
Original Assignee
Miyagi Mitsunobu
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Miyagi Mitsunobu filed Critical Miyagi Mitsunobu
Priority to JP2002116801A priority Critical patent/JP3877152B2/en
Publication of JP2003315588A publication Critical patent/JP2003315588A/en
Application granted granted Critical
Publication of JP3877152B2 publication Critical patent/JP3877152B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Abstract

<P>PROBLEM TO BE SOLVED: To provide such a method that a hollow fiber adaptive not only in an IR wavelength region but in a wide wavelength region can be manufactured at a low cost. <P>SOLUTION: In the method for manufacturing a hollow optical fiber by heating, fusing and drawing a glass tube, the thickness of the glass is controlled by using the interference effect of light in the glass of the optical fiber, so as to obtain an optical fiber showing low loss property in the wavelength region of the purpose. Preferably, a metal layer is added to the outer surface of the glass hollow optical fiber. <P>COPYRIGHT: (C)2004,JPO

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【発明の属する技術分野】本発明は,光伝送用の中空フ
ァイバに関するものである.
TECHNICAL FIELD The present invention relates to a hollow fiber for optical transmission.

【0002】[0002]

【従来の技術】ガラスや樹脂のチューブ内面に金属薄膜
を形成して,チューブ内面における反射率を向上させ,
さらにその表面にポリマーや無機物などの誘電体を成膜
し,誘電体薄膜における光の干渉効果により,内面反射
率をさらに増大させた低損失中空ファイバは,炭酸ガス
レーザ,エルビウムヤグなどの赤外レーザの伝送路とし
て開発が進んでいる.また,この中空ファイバは空気や
ガスをコアとして用いるため,端面破壊の可能性も低
く,また端面での反射がないので大きな光電力の伝送に
適しており,上記レーザ以外にも,石英系ファイバが使
用可能な波長帯でも,さまざまな分野への応用が展開さ
れている.
2. Description of the Related Art A thin metal film is formed on the inner surface of a glass or resin tube to improve the reflectance on the inner surface of the tube.
Furthermore, a low-loss hollow fiber with a dielectric material such as a polymer or an inorganic material deposited on its surface and the internal reflectance further increased by the optical interference effect in the dielectric thin film is used for infrared lasers such as carbon dioxide laser and erbium yag. Is being developed as a transmission line for the. Moreover, since this hollow fiber uses air or gas as the core, the possibility of end face destruction is low, and since there is no reflection at the end face, it is suitable for transmission of large optical power. Even in the wavelength range where can be used, applications are being developed in various fields.

【0003】一方,ある種の酸化物ガラスの屈折率が赤
外の特定波長域において,1より小さくなり,空気との
界面で高い反射率を示すことを利用し,酸化物ガラスを
線引法によりチューブ状に加工し,中空光ファイバを製
造する方法についても提案されている.
On the other hand, the fact that the refractive index of a certain type of oxide glass is smaller than 1 in a specific wavelength region of infrared and shows a high reflectance at the interface with air is utilized to draw an oxide glass. A method of manufacturing a hollow optical fiber by processing it into a tube has been proposed.

【0004】しかし,チューブ内面に複数の薄膜を生成
するという前者の手法では,製造工程が複雑化するため
に製造コストが高くなり,またチューブ内に液体等を流
入させて薄膜を形成するため,より高い可撓性をもつ口
径の小さな中空ファイバの製造においても難点があっ
た.
However, in the former method of forming a plurality of thin films on the inner surface of the tube, the manufacturing process is complicated and thus the manufacturing cost is high. Further, since a liquid or the like is introduced into the tube to form the thin films, There was also a problem in the production of hollow fibers with higher flexibility and small diameter.

【0005】一方,後者の手法ではガラス線引法を用い
るため,製造コストが低く抑えられ,かつ,きわめて口
径の小さなファイバを製造可能という利点があるが,伝
送可能な波長帯が材料によって決定されてしまうため,
波長選択の自由度に限界があった.数種類のガラスを混
合することにより対応波長域をシフトさせることは可能
だが,複素屈折率の実部が1を下回る領域でもわずかに
存在する吸収係数のために,吸収損失が生じて完全反射
とはならない.そのため,十分に高いファイバの伝送効
率を得るのが難しく,実用化には至らなかった.
On the other hand, in the latter method, since the glass drawing method is used, there are advantages that the manufacturing cost is kept low and a fiber having an extremely small diameter can be manufactured, but the wavelength band that can be transmitted is determined by the material. Because,
There was a limit to the degree of freedom in wavelength selection. It is possible to shift the corresponding wavelength range by mixing several kinds of glass, but due to the absorption coefficient that exists even in the region where the real part of the complex refractive index is less than 1, absorption loss occurs and perfect reflection is not possible. It won't. Therefore, it was difficult to obtain a sufficiently high fiber transmission efficiency, and it was not possible to put it into practical use.

【0006】[0006]

【発明が解決しようとする課題】そこで本発明の目的
は,赤外波長域をはじめとする広範囲の波長域に適応可
能な中空ファイバを,低いコストで製造可能な手法を実
現することにある.
SUMMARY OF THE INVENTION An object of the present invention is to realize a method capable of manufacturing a hollow fiber which can be adapted to a wide wavelength range including an infrared wavelength range at a low cost.

【0007】[0007]

【課題を解決するための手段】本発明は上記の目的を達
成するために,ガラス管を加熱溶融し,線引して中空光
ファイバを製造する方法において,上記光ファイバのガ
ラス内部での光の干渉効果を利用し,目的波長帯域にお
いて低損失性を示す光ファイバが得られるように,上記
光ファイバのガラス肉厚を調整することを特徴とするガ
ラス中空光ファイバの製造方法を提供する.
In order to achieve the above-mentioned object, the present invention provides a method for producing a hollow optical fiber by heating and melting a glass tube and drawing the optical fiber inside the glass. A glass hollow optical fiber manufacturing method characterized by adjusting the glass wall thickness of the optical fiber so that an optical fiber exhibiting low loss in a target wavelength band can be obtained by utilizing the interference effect of.

【0008】ここで前記中空光ファイバの外面に金属層
を装荷することを特徴とする,ガラス中空光ファイバの
製造方法であってもよい.
A method for manufacturing a glass hollow optical fiber may be characterized in that a metal layer is loaded on the outer surface of the hollow optical fiber.

【0009】ここで前記中空光ファイバの外面に誘電体
多層膜を形成したことを特徴とする,ガラス中空光ファ
イバの製造方法の製造方法であってもよい.
A method of manufacturing a glass hollow optical fiber may be characterized in that a dielectric multilayer film is formed on the outer surface of the hollow optical fiber.

【0010】ここで前記中空光ファイバの外面に誘電体
多層膜を形成し,さらにその外面に金属層を装荷したこ
とを特徴とする,ガラス中空光ファイバの製造方法であ
ってもよい.
A method for manufacturing a glass hollow optical fiber may be characterized in that a dielectric multilayer film is formed on the outer surface of the hollow optical fiber, and a metal layer is loaded on the outer surface.

【0011】そして,このような本発明の中空光ファイ
バの製造方法であれば,紫外から赤外にわたる広範囲の
波長の光に対して低損失性を示し,かつ可撓性に富んだ
口径の小さな中空光ファイバを低コストで製造可能とな
る.
According to the method for manufacturing a hollow optical fiber of the present invention as described above, a low loss property is exhibited with respect to light having a wide range of wavelengths from ultraviolet to infrared, and flexibility is small and a diameter is small. Hollow optical fibers can be manufactured at low cost.

【0012】[0012]

【本発明の実施の形態】以下,本発明の実施の形態の一
例を詳述する.まず母材となるガラスチューブは適用し
ようとする波長域における吸収係数が十分低い必要があ
る.紫外,可視,赤外のどの波長においても高い透明度
をもつ石英ガラスが好ましい材料のひとつである.ま
た,ガラス軟化温度が低いパイレックスガラスや,ソー
ダガラスは簡易な炉でも溶融が可能であるため,低コス
ト製造という観点からは望ましい材料である.一方,カ
ルコゲナイドガラスなどの中赤外波長域で高い透明性を
もつガラスを用いれば,波長3ミクロン以上の長波長域
においても高透過率を示すファイバを製造可能となる.
BEST MODE FOR CARRYING OUT THE INVENTION Hereinafter, an example of an embodiment of the present invention will be described in detail. First, the glass tube that is the base material must have a sufficiently low absorption coefficient in the wavelength range to be applied. Quartz glass, which has high transparency at all wavelengths of ultraviolet, visible, and infrared, is one of the preferable materials. In addition, Pyrex glass and soda glass, which have a low glass softening temperature, can be melted even in a simple furnace, so they are desirable materials from the viewpoint of low-cost manufacturing. On the other hand, if glass with high transparency in the mid-infrared wavelength range such as chalcogenide glass is used, it is possible to manufacture a fiber with high transmittance even in the long-wavelength range of 3 μm or more.

【0013】母材ガラスチューブを管状電気炉などの高
温雰囲気中で溶融,軟化させたうえで張力を加えて線引
きすることにより中空ファイバを製造する.通常の状態
で線引きを行えば,母材の外径とガラス肉厚の比は,線
引されるファイバのそれに一致するため,設計値に近い
形状の母材を使用することが望ましい.また,母材内部
に圧力をかけるなどして,管の内外に圧力差を与えなが
ら張力を加えることにより,線引されるファイバの肉厚
を制御することが可能である.
Hollow fibers are manufactured by melting and softening a preform glass tube in a high-temperature atmosphere such as a tubular electric furnace, and then applying tension to draw it. When the wire is drawn in a normal state, the ratio of the outer diameter of the base material to the glass thickness matches that of the fiber to be drawn, so it is desirable to use a base material with a shape close to the design value. In addition, the wall thickness of the drawn fiber can be controlled by applying tension to the inside and outside of the tube by applying pressure to the inside of the base material.

【0014】図1は本発明の中空光ファイバの製造方法
で製作されたファイバの一実施形態を示す断面図であ
る.本例ではファイバの透過率を向上させる目的で,線
引したファイバの外面に金属層を形成している.また金
属層の付加により,ファイバを伝送する光が,ファイバ
外部の環境から受ける影響を除去することが可能なう
え,ファイバの強度を向上させることができる.金属層
の材料としては,適用する波長域で高い反射率をしめす
ものが望ましく,紫外域ではアルミニウム,可視域では
銀,赤外域では銀,金,モリブデン,ニッケルなどが好
適である.また金属層を付加する方法としては,メッキ
法,真空蒸着法,スパッタリング法や溶融金属を付着さ
せる方法,およびこれらの組合せによる方法が望まし
い.また,ガラスの強度は線引後に劣化することがある
ため,線引直後に金属層を付加することができるよう
に,線引炉の直下に金属層形成装置を配置することが望
ましい.
FIG. 1 is a sectional view showing an embodiment of a fiber manufactured by the method for manufacturing a hollow optical fiber of the present invention. In this example, a metal layer is formed on the outer surface of the drawn fiber in order to improve the transmittance of the fiber. In addition, by adding a metal layer, it is possible to remove the influence of the light transmitted through the fiber from the environment outside the fiber and improve the strength of the fiber. As a material for the metal layer, a material exhibiting a high reflectance in the applicable wavelength range is desirable, and aluminum in the ultraviolet range, silver in the visible range, silver, gold, molybdenum, nickel in the infrared range are suitable. As a method of adding a metal layer, a plating method, a vacuum deposition method, a sputtering method, a method of depositing molten metal, or a combination thereof is preferable. Since the strength of glass may deteriorate after drawing, it is desirable to place a metal layer forming device directly below the drawing furnace so that a metal layer can be added immediately after drawing.

【0015】図2は石英ガラスを線引して得られるファ
イバ,およびその外面に銀層を付加したファイバの伝送
損失の理論計算値である.想定したファイバの内径は2
80ミクロンであり,円形中空ファイバの最低次モード
であるHE11モードの伝送損失をファイバのガラス肉
厚の関数として示したものである.
FIG. 2 shows theoretical calculation values of the transmission loss of a fiber obtained by drawing quartz glass and a fiber having a silver layer added to its outer surface. The assumed fiber inner diameter is 2
The transmission loss of HE11 mode, which is 80 micron and is the lowest mode of the circular hollow fiber, is shown as a function of the glass thickness of the fiber.

【0016】低損失性を与えるガラス肉厚dは,金属層
を付加していないファイバの場合,ガラスの屈折率を
n,適用する波長をλとすれば次の数式で与えられる.
The glass thickness d giving the low loss property is the refractive index of glass in the case of a fiber having no metal layer added.
If n and the wavelength to be applied are λ, they are given by the following formula.

【0017】[0017]

【数1】 [Equation 1]

【0018】一方,金属層を付加した場合の最適ガラス
肉厚dは,次の数式で与えられる.
On the other hand, the optimum glass thickness d when the metal layer is added is given by the following equation.

【0019】[0019]

【数2】 [Equation 2]

【0020】ガラス層の厚さが極端に小さいとファイバ
の強度が低下し,また過剰に大きいとガラスにおける吸
収損失の影響が大きくなる.そのため,ガラス層の厚さ
は5ミクロンから20ミクロン程度であり,上記の数式
の条件をみたすものであることが望ましい.なお,上記
の数式で与えられるのは最適な膜厚であり,実際にファ
イバを製造する際には最適値から10パーセント程度の
誤差が許容される.
If the thickness of the glass layer is extremely small, the strength of the fiber will decrease, and if it is too large, the effect of absorption loss in the glass will increase. Therefore, the thickness of the glass layer is about 5 to 20 microns, and it is desirable to satisfy the conditions of the above formula. The optimum film thickness is given by the above equation, and an error of about 10% from the optimum value is allowed when actually manufacturing the fiber.

【0021】金属層の厚さが極端に小さいとファイバ中
を伝送する光を,ファイバ外部の環境から遮断すること
ができないため,0.1ミクロン以上の厚さが必要とな
る.また,十分な機械的強度をファイバに与えるために
は,金属層の厚さは10ミクロン以上であることが望ま
しいが,極端に厚い金属層はファイバの可撓性を低下さ
せるために,その厚さは200ミクロン以下であること
が望ましい.また,反射率を増大させるために光学的に
機能する0.1ミクロン以上の金属膜を形成した上に,
ファイバに機械的強度を与えるための別の保護層を付加
することも可能である.保護層の材質としては金属,樹
脂などが好適である.
When the thickness of the metal layer is extremely small, the light transmitted through the fiber cannot be shielded from the environment outside the fiber, so that a thickness of 0.1 micron or more is required. Further, in order to give sufficient mechanical strength to the fiber, it is desirable that the thickness of the metal layer be 10 microns or more, but an extremely thick metal layer reduces the flexibility of the fiber, It is desirable that the thickness is 200 microns or less. In addition, after forming a metal film of 0.1 micron or more that functions optically to increase the reflectance,
It is also possible to add another protective layer to give mechanical strength to the fiber. Metal, resin, etc. are suitable as the material of the protective layer.

【0022】また,線引したガラス中空ファイバの外面
に誘電体の多層膜を形成することにより,低損失性を向
上させたり,ファイバに波長選択性を持たせたりするこ
とも可能である.その際,多層膜の層数が少ない場合
は,多層膜の外面に金属層を付加することにより伝送効
率を向上させることができる.
Further, by forming a multi-layered film of a dielectric material on the outer surface of the drawn glass hollow fiber, it is possible to improve the low loss property and give the fiber wavelength selectivity. In that case, if the number of layers of the multilayer film is small, the transmission efficiency can be improved by adding a metal layer to the outer surface of the multilayer film.

【0023】[0023]

【発明の効果】以上要するに,本発明によれば次のよう
な優れた効果を発揮する.
In summary, according to the present invention, the following excellent effects are exhibited.

【0024】紫外から赤外の広い波長範囲に適応する
低損失性を有する中空ファイバを製造できる.
It is possible to manufacture a hollow fiber having a low loss property applicable to a wide wavelength range from ultraviolet to infrared.

【0025】可撓性に富む,口径の小さいファイバを
低コストで製造可能である.
It is possible to manufacture a flexible fiber having a small diameter and at a low cost.

【図面の簡単な説明】[Brief description of drawings]

【図1】本発明の一実施形態を示す断面図である.FIG. 1 is a sectional view showing an embodiment of the present invention.

【図2】本発明の効果を示す理論計算の結果を示す図で
ある.
FIG. 2 is a diagram showing the result of theoretical calculation showing the effect of the present invention.

【符号の説明】[Explanation of symbols]

1 中空ファイバ 2 ガラス層 3 金属層 4 保護層 5 中空領域 6 石英ガラス中空ファイバ 7 銀層を付加した石英ガラス中空ファイバ 1 hollow fiber 2 glass layers 3 metal layers 4 protective layer 5 Hollow area 6 Quartz glass hollow fiber 7 Silica glass hollow fiber with added silver layer

───────────────────────────────────────────────────── フロントページの続き (72)発明者 宮城 光信 宮城県仙台市青葉区荒巻字青葉(番地な し) 東北大学 (72)発明者 片桐 崇史 宮城県仙台市青葉区荒巻字青葉(番地な し) 東北大学 Fターム(参考) 2H050 AA06 AB02Y AB67Y AC36 AC64    ─────────────────────────────────────────────────── ─── Continued front page    (72) Inventor Mitsunobu Miyagi             Aoba, Aoba-ku, Sendai City, Miyagi Prefecture             Shi) Tohoku University (72) Inventor Takashi Katagiri             Aoba, Aoba-ku, Sendai City, Miyagi Prefecture             Shi) Tohoku University F-term (reference) 2H050 AA06 AB02Y AB67Y AC36                       AC64

Claims (4)

【特許請求の範囲】[Claims] 【請求項1】 ガラス管を加熱溶融し,線引して中空光
ファイバを製造する方法において,上記光ファイバのガ
ラス内部での光の干渉効果を利用し,目的波長帯域にお
いて低損失性を示す光ファイバが得られるように,上記
光ファイバのガラス肉厚を調整することを特徴とするガ
ラス中空光ファイバの製造方法.
1. A method for manufacturing a hollow optical fiber by heating and melting a glass tube and drawing the glass tube, utilizing the interference effect of light inside the glass of the optical fiber, and exhibiting low loss in a target wavelength band. A method for producing a glass hollow optical fiber, characterized in that the glass wall thickness of the optical fiber is adjusted so that an optical fiber can be obtained.
【請求項2】 前記中空光ファイバの外面に金属層を付
加することを特徴とする,請求項1に記載のガラス中空
光ファイバの製造方法.
2. The method for producing a glass hollow optical fiber according to claim 1, wherein a metal layer is added to the outer surface of the hollow optical fiber.
【請求項3】 前記中空光ファイバの外面に誘電体多層
膜を付加することを特徴とする,請求項1に記載のガラ
ス中空光ファイバの製造方法.
3. The method for producing a glass hollow optical fiber according to claim 1, wherein a dielectric multilayer film is added to the outer surface of the hollow optical fiber.
【請求項4】 前記中空光ファイバの外面に誘電体多層
膜を形成し,さらにその外面に金属層を付加したことを
特徴とする,請求項1に記載のガラス中空光ファイバの
製造方法.
4. The method for producing a glass hollow optical fiber according to claim 1, wherein a dielectric multilayer film is formed on the outer surface of the hollow optical fiber, and a metal layer is added to the outer surface.
JP2002116801A 2002-04-18 2002-04-18 Manufacturing method of glass hollow optical fiber Expired - Fee Related JP3877152B2 (en)

Priority Applications (1)

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Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2002116801A JP3877152B2 (en) 2002-04-18 2002-04-18 Manufacturing method of glass hollow optical fiber

Publications (2)

Publication Number Publication Date
JP2003315588A true JP2003315588A (en) 2003-11-06
JP3877152B2 JP3877152B2 (en) 2007-02-07

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Cited By (1)

* Cited by examiner, † Cited by third party
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