GB1212355A - Improvements in or relating to a method of manufacturing filaments - Google Patents

Improvements in or relating to a method of manufacturing filaments

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Publication number
GB1212355A
GB1212355A GB44659/67A GB4465967A GB1212355A GB 1212355 A GB1212355 A GB 1212355A GB 44659/67 A GB44659/67 A GB 44659/67A GB 4465967 A GB4465967 A GB 4465967A GB 1212355 A GB1212355 A GB 1212355A
Authority
GB
United Kingdom
Prior art keywords
filament
boron
jet
particles
molten
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB44659/67A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Raytheon Technologies Corp
Original Assignee
United Aircraft Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by United Aircraft Corp filed Critical United Aircraft Corp
Publication of GB1212355A publication Critical patent/GB1212355A/en
Expired legal-status Critical Current

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    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/62227Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres
    • C04B35/62272Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres based on non-oxide ceramics
    • C04B35/62277Fibres based on carbides
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22DCASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
    • B22D11/00Continuous casting of metals, i.e. casting in indefinite lengths
    • B22D11/005Continuous casting of metals, i.e. casting in indefinite lengths of wire
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B37/00Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
    • C03B37/01Manufacture of glass fibres or filaments
    • C03B37/02Manufacture of glass fibres or filaments by drawing or extruding, e.g. direct drawing of molten glass from nozzles; Cooling fins therefor
    • C03B37/0203Cooling non-optical fibres drawn or extruded from bushings, nozzles or orifices
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B37/00Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
    • C03B37/01Manufacture of glass fibres or filaments
    • C03B37/02Manufacture of glass fibres or filaments by drawing or extruding, e.g. direct drawing of molten glass from nozzles; Cooling fins therefor
    • C03B37/0203Cooling non-optical fibres drawn or extruded from bushings, nozzles or orifices
    • C03B37/0206Cooling non-optical fibres drawn or extruded from bushings, nozzles or orifices by contacting of the fibres with liquid or mist
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B37/00Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
    • C03B37/01Manufacture of glass fibres or filaments
    • C03B37/02Manufacture of glass fibres or filaments by drawing or extruding, e.g. direct drawing of molten glass from nozzles; Cooling fins therefor
    • C03B37/0203Cooling non-optical fibres drawn or extruded from bushings, nozzles or orifices
    • C03B37/0213Cooling non-optical fibres drawn or extruded from bushings, nozzles or orifices by forced gas cooling, i.e. blowing or suction
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    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/62227Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres
    • C04B35/62272Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres based on non-oxide ceramics
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    • C04B35/626Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/62605Treating the starting powders individually or as mixtures
    • C04B35/62645Thermal treatment of powders or mixtures thereof other than sintering
    • C04B35/62665Flame, plasma or melting treatment
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    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
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    • C04B35/626Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/628Coating the powders or the macroscopic reinforcing agents
    • C04B35/62844Coating fibres
    • C04B35/62847Coating fibres with oxide ceramics
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    • C04B35/62852Alumina or aluminates
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    • C04B2235/34Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3409Boron oxide, borates, boric acids, or oxide forming salts thereof, e.g. borax
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    • C04B2235/3418Silicon oxide, silicic acids, or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint
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    • C04B2235/46Gases other than oxygen used as reactant, e.g. nitrogen used to make a nitride phase
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    • C04B2235/50Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/52Constituents or additives characterised by their shapes
    • C04B2235/5208Fibers
    • C04B2235/5264Fibers characterised by the diameter of the fibers
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    • C04B2235/54Particle size related information
    • C04B2235/5418Particle size related information expressed by the size of the particles or aggregates thereof
    • C04B2235/5436Particle size related information expressed by the size of the particles or aggregates thereof micrometer sized, i.e. from 1 to 100 micron
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S264/00Plastic and nonmetallic article shaping or treating: processes
    • Y10S264/19Inorganic fiber

Abstract

1,212,355. Filaments; coating with glass. UNITED AIRCRAFT CORP. 2 Oct., 1967 [17 Oct., 1966], No. 44659/67. Headings C1A and C1M. [Also in Divisions B2, B3 and C7] In a method of manufacturing a filament of metal or metal compound from molten material the molten material is expelled through an orifice in a downwardly directed jet, the jet being electrically charged and being adjacent to, or surrounded by, one or more electrodes which are electrically charged opposite to the charge on the jet to create an electrostatic field. A heat exchange medium is passed into the electrostatic field and the velocity and volume of the medium and the voltage in the electrical charges in the jet and electrodes are correlated to maintain a rate of cooling of the jet between 0À001 to 0-04 calories per second per square centimetre per degree centrigrade. The filament may be produced from molten nickel, chromium stainless steel, beryllium, boron, titanium, aluminium, iron, tin, or of aluminium oxide, aluminium oxide with magnesium oxide and/or silicon dioxide, or aluminium oxide with calcium oxide and silicon dioxide. The filament may be treated to coat it, or form an alloy or compound, by supplying a reactant to the surface of the filament. Examples described include the formation of a molten boron jet which is reacted with graphite particles or methane to produce a boron carbide filament, the formation of a molten titanium (boron) jet which is reacted with boron (titanium) particles to produce a titanium boride filament, the formation of a molten boron jet which is partly reacted with propane/boron trichloride to give a boron carbide-coated boron filament which is subsequently coated with silica from a finely powdered quartz aerosol (Example 3), boron coated with silica or carbon and chromium or nickel coated with a silica powder to form a glass coating. Fig. 1 shows the filament being cooled by a horizontal gas flow of an inert or reactant gas, the filament being retained in position in the gas flow by electrostatic forces created by a voltage across the filament and a metal porous tube from which the gas flows. 'In an alternative embodiment (Fig. 2, not shown), a corona discharge is formed between the filament and surrounding electrodes that causes a cooling convection current in the surrounding gas or air. In a further embodiment (Fig. 3, not shown), a corona discharge is formed and a stream of flux particles are fed into its field and the particles are carried to the surface of the filament and absorb heat therefrom. The particles may be left on to form a coating or may be chemically removed. The flux particles may be added to stop a reaction at a given time. Flux materials used are Al 2 .O 3 , Si.O 2 , Mg.O, Mg.O+Al 2 0 3 , Ca.O +Mg.O, Ca.0+Al 2 0 3 , Na 2 O + Si.0 2 , Mg.O + Si.0 2 , Mg.O+Ti.O 2 , Pb.O + SiO 2 and Al 2 0 3 +SiO 2 .
GB44659/67A 1966-10-17 1967-10-02 Improvements in or relating to a method of manufacturing filaments Expired GB1212355A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US58700966A 1966-10-17 1966-10-17

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GB1212355A true GB1212355A (en) 1970-11-18

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GB44659/67A Expired GB1212355A (en) 1966-10-17 1967-10-02 Improvements in or relating to a method of manufacturing filaments

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US (1) US3461943A (en)
DE (1) DE1583715C3 (en)
FR (1) FR1551091A (en)
GB (1) GB1212355A (en)
SE (1) SE327787B (en)

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US3834847A (en) * 1970-01-16 1974-09-10 Du Pont Open cell foam device for gas distribution in filament quenching chimneys
US3824052A (en) * 1971-04-15 1974-07-16 Deering Milliken Res Corp Apparatus to produce nonwoven fabric
US3856513A (en) * 1972-12-26 1974-12-24 Allied Chem Novel amorphous metals and amorphous metal articles
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US4736789A (en) * 1978-07-28 1988-04-12 Kennecott Corporation Apparatus and method for continuous casting of metallic strands at exceptionally high speeds using an oscillating mold assembly
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US4441542A (en) * 1981-06-10 1984-04-10 Olin Corporation Process for cooling and solidifying continuous or semi-continuously cast material
CA1191015A (en) * 1981-09-29 1985-07-30 Tsuyoshi Masumoto Method of manufacturing thin metal wire
US4557742A (en) * 1984-07-02 1985-12-10 Polaroid Corporation Polarized optical fiber and method of forming same
US7626122B2 (en) * 2006-08-25 2009-12-01 David Levine Lightweight composite electrical wire
IL231729B (en) 2014-03-26 2018-06-28 Umzen Ltd Nut and method for fixing an object to a building structure
CN107324816A (en) * 2017-07-25 2017-11-07 云南省科学技术院 The preparation method and Preparation equipment of a kind of high temperature resistant high purity aluminium oxide cotton

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Publication number Publication date
DE1583715C3 (en) 1974-10-10
US3461943A (en) 1969-08-19
DE1583715A1 (en) 1970-08-20
SE327787B (en) 1970-08-31
DE1583715B2 (en) 1973-06-28
FR1551091A (en) 1968-12-27

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PS Patent sealed [section 19, patents act 1949]
PCNP Patent ceased through non-payment of renewal fee