EP1088907B1 - Method for producing a plating for a metal component - Google Patents

Method for producing a plating for a metal component Download PDF

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Publication number
EP1088907B1
EP1088907B1 EP00120803A EP00120803A EP1088907B1 EP 1088907 B1 EP1088907 B1 EP 1088907B1 EP 00120803 A EP00120803 A EP 00120803A EP 00120803 A EP00120803 A EP 00120803A EP 1088907 B1 EP1088907 B1 EP 1088907B1
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Prior art keywords
slurry
layer
powder
component
application
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EP00120803A
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German (de)
French (fr)
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EP1088907A1 (en
Inventor
Thomas Dr. Cosack
Gerhard Wydra
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MTU Aero Engines AG
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MTU Aero Engines GmbH
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    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C10/00Solid state diffusion of only metal elements or silicon into metallic material surfaces
    • C23C10/28Solid state diffusion of only metal elements or silicon into metallic material surfaces using solids, e.g. powders, pastes
    • C23C10/34Embedding in a powder mixture, i.e. pack cementation
    • C23C10/52Embedding in a powder mixture, i.e. pack cementation more than one element being diffused in one step
    • C23C10/54Diffusion of at least chromium
    • C23C10/56Diffusion of at least chromium and at least aluminium
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C10/00Solid state diffusion of only metal elements or silicon into metallic material surfaces
    • C23C10/28Solid state diffusion of only metal elements or silicon into metallic material surfaces using solids, e.g. powders, pastes
    • C23C10/34Embedding in a powder mixture, i.e. pack cementation
    • C23C10/52Embedding in a powder mixture, i.e. pack cementation more than one element being diffused in one step

Definitions

  • the invention relates to a method for producing an armor for a metallic Component provided on its surface.
  • Armor or scratches are e.g. on engine components, e.g. seal tips of labyrinth seals or blade tips, provided to their Counteract processing during touch-ups during operation. Since the Efficiency of a compressor or turbine to a large extent on the gap size between the rotating and the stationary component, he is with increasing processing, e.g. the blade tips, reduced.
  • engine components e.g. seal tips of labyrinth seals or blade tips
  • the armor works in the operation of the engine usually in an inlet lining an opposite, second component.
  • Such inlet linings are abradable and usually consist of a corrosion and erosion resistant layer.
  • An armor of the engine component is required in particular when the Strength and hardness of the inlet coverings to increase erosion and temperature resistance is increased and the processing of engine components in addition strengthened. By the armor is achieved that the Anstreifvorgang a minimum Gap between the armor and the inlet lining is formed.
  • an MCrAlY powder is used applied by electroplating on the component to be coated, wherein in the bath, the required hard particles, e.g. BN, are included. These Particles are etched free after application.
  • Such a method is expensive and consuming.
  • the subsequent etching is due to the lack of Environmental compatibility and the required covering of the component disadvantageous.
  • JP 55-82765 A which consists of a Ni or Co base alloy Substrate first with a mixture of ceramic, Al and metal powder To coat, the heat resistance of the long-lasting high temperature loaded Layer to improve. Then follows a layer of one with a Binder provided by Ni powder, a heat treatment and an Alit Schlu by Pack process. In this case, the first layer of the mixture containing ceramic prevent Al from penetrating the layer into the substrate and thus the layer through the depletion of Al loses its heat resistance.
  • JP 55-082759 A discloses a method for improving the thermal resistance a coating applied to a substrate of a Ni or Co base alloy is applied, wherein during coating a metal or an alloy powder mixed with ceramic elements and then applied to the substrate becomes. It can be a binder used and a subsequent heat treatment be performed. The method is applied to components of e.g. Used gas turbines, which are exposed to hot gas corrosion.
  • the object of the present invention is to provide a method for manufacturing To create an armor of the type described above, which is manufacturing technology easy to carry out and a high-quality armor results.
  • the advantage of this method is that the armor with a manufacturing technology simple method can be applied to the component.
  • the hard particles are the Slip before application on the surface to be coated mixed. To this Way, the particles are uniform in the slurry present in a suspension distributed.
  • the hard particles after application in the slip layer is used, resulting e.g. a special arrangement of the particles on the surface to be clad.
  • the starting powder consists of MCrAlY, the starting powder - like the adding powder - preferably in a grain size distribution of 5 to 120 microns is present.
  • the M stands for at least one of the elements Ni or Co. Instead of Y, Hf or Ce can also be used.
  • the application of the slurry on the surface to be coated of the component takes place preferably by spraying, brushing or dipping, whereby the process manufacturing technology easy and inexpensive to do.
  • Applying can be easily localized layers also on geometric Apply complicated components. Moreover, no expensive and elaborate Spraying or evaporation systems required.
  • the slip layer be coated in inert gas, e.g. in argon, or im Vacuum is heat treated, wherein the heat treatment of the layer about 1-4 Hours, preferably over about 2 hours, are performed to the slip layer to connect with the component and the hard particles via diffusion.
  • inert gas e.g. in argon, or im Vacuum is heat treated, wherein the heat treatment of the layer about 1-4 Hours, preferably over about 2 hours, are performed to the slip layer to connect with the component and the hard particles via diffusion.
  • the metallic component is preferably made of a nickel or cobalt-based alloy, wherein the component is an engine building, e.g. a turbine blade, his can, on whose blade tip the armor is applied.
  • the addition powder makes up to 35% by weight of the total weight of starting materials. and adding powder.
  • an MCrAlY powder with an addition powder mixed into a suspension with a conventional inorganic binder In the Suspension is the binder with 5-10 wt .-% and additionally water with 5-7 Wt .-% before.
  • the particle sizes of the powder particles are between 5 and 120 ⁇ m.
  • These flowable and sprayable mass are introduced BN particles whose size is above that of the powder particles.
  • the particle-containing Slip e.g. also with a brush to form a layer on the blade tip be applied.
  • the suspension is in suspension, still moist slurry or the slip layer at room temperature dried for about 1.5 hours.
  • the dried slurry layer is then vacuumed at 1000 ° C for about 2 hours heat treated, in order to connect the slip layer with the material of the Turbine blade and to achieve with the hard particles by diffusion. While sintering the spherical MCrAlY particles at least partially together. In addition, Ni can also escape from the base material and into the Schlikker harsh diffuse. After heat treatment are the ceramic hard particles from BN od. Like. Outward on the slip before and can this and protect the blade tip during operation.
  • the BN particles are firmly connected to the blade tip via the slip layer and may during operation of the gas turbine when rubbing in an opposite Cut in the inlet lining to avoid damage in this way To prevent the blade tip and the gap size between the rotating and keep the standing component as low as possible.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Other Surface Treatments For Metallic Materials (AREA)
  • Turbine Rotor Nozzle Sealing (AREA)
  • Extrusion Moulding Of Plastics Or The Like (AREA)
  • Laminated Bodies (AREA)

Abstract

Production of a cladding for a metallic component comprises forming a slip by mixing a binder solution with a starting powder containing Al and/or Cr and an additional powder containing Al, Pt, Pd or Si, where the additional powder comprises no Al when the starting powder contains exclusively Al; applying the slip to the surface to be clad; adding ceramic hard particles to the slip before or after applying the slip; drying the slip layer at a temperature of room temperature to 450 degrees C and heat treating the slip layer at 750-1250 degrees C.

Description

Die Erfindung betrifft ein Verfahren zum Herstellen einer Panzerung für ein metallisches Bauteil, die auf dessen Oberfläche vorgesehen wird.The invention relates to a method for producing an armor for a metallic Component provided on its surface.

Panzerungen bzw. Anstreifbeläge werden z.B. an Triebwerksbauteilen, wie z.B. Dichtungsspitzen von Labyrinthdichtungen oder Schaufelspitzen, vorgesehen, um deren Abarbeitung bei Anstreifvorgängen während des Betriebs entgegenzuwirken. Da der Wirkungsgrad eines Verdichters oder einer Turbine in hohem Maße von der Spaltgröße zwischen dem rotierenden und dem stehenden Bauteil abhängt, wird er mit zunehmender Abarbeitung, z.B. der Schaufelspitzen, vermindert.Armor or scratches are e.g. on engine components, e.g. seal tips of labyrinth seals or blade tips, provided to their Counteract processing during touch-ups during operation. Since the Efficiency of a compressor or turbine to a large extent on the gap size between the rotating and the stationary component, he is with increasing processing, e.g. the blade tips, reduced.

Die Panzerung arbeitet sich beim Betrieb des Triebwerks üblicherweise in einen Einlaufbelag eines gegenüberliegenden, zweiten Bauteils ein. Derartige Einlaufbeläge sind abreibbar und bestehen meist aus einer korrosions- und erosionsfesten Schicht. Eine Panzerung des Triebwerksbauteils ist insbesondere dann erforderlich, wenn die Festigkeit und Härte der Einlaufbeläge zur Steigerung der Erosions- und Temperaturbeständigkeit erhöht wird und sich die Abarbeitung der Triebwerksbauteile zusätzlich verstärkt. Durch die Panzerung wird erreicht, daß beim Anstreifvorgang ein minimaler Spalt zwischen der Panzerung und dem Einlaufbelag gebildet wird.The armor works in the operation of the engine usually in an inlet lining an opposite, second component. Such inlet linings are abradable and usually consist of a corrosion and erosion resistant layer. An armor of the engine component is required in particular when the Strength and hardness of the inlet coverings to increase erosion and temperature resistance is increased and the processing of engine components in addition strengthened. By the armor is achieved that the Anstreifvorgang a minimum Gap between the armor and the inlet lining is formed.

Bei einem bekannten Verfahren zum Herstellen einer Panzerung wird ein MCrAlY-Pulver durch galvanisches Auftragen auf das zu panzernde Bauteil aufgebracht, wobei in dem Bad die erforderlichen harten Partikel, wie z.B. BN, enthalten sind. Diese Partikel werden nach dem Auftragen freigeätzt. Ein solches Verfahren ist teuer und aufwendig. Insbesondere das anschließende Ätzen ist aufgrund der mangelnden Umweltverträglichkeit und dem erforderlichen Abdecken des Bauteils nachteilig.In one known method for making armor, an MCrAlY powder is used applied by electroplating on the component to be coated, wherein in the bath, the required hard particles, e.g. BN, are included. These Particles are etched free after application. Such a method is expensive and consuming. In particular, the subsequent etching is due to the lack of Environmental compatibility and the required covering of the component disadvantageous.

Bei einem anderen bekannten Verfahren wird eine an die Bauteilkontur angepaßte Lotfolie durch Kleben od dgl. an dem Bauteil befestigt. Danach werden BN-Partikel in die Lotfolie eingesetzt. Anschließend wird die Lotfolie durch Wärmebehandlung geschmolzen und die BN-Partikel darin eingebettet. Auch dieses Verfahren ist verhältnismäßig teuer und aufwendig. Zudem ist die Verbindung zwischen den Partikeln und dem Bauteil unzureichend.In another known method, one adapted to the component contour Lotfolie by gluing or the like. Attached to the component. Thereafter, BN particles in the solder foil used. Subsequently, the solder foil is melted by heat treatment and the BN particles embedded therein. This procedure is also proportionate expensive and expensive. In addition, the connection between the particles and the component is insufficient.

Aus der JP 55-82765 A ist es bekannt, das aus einer Ni- oder Co-Basislegierung bestehende Substrat zunächst mit einer Mischung aus Keramik-, Al- und Metallpulver zu beschichten, um die Wärmebeständigkeit der langandauernd hochtemperaturbelasteten Schicht zu verbessern. Anschließend folgt eine Schicht aus einem mit einem Binder versehenen Ni-Pulver, eine Wärmebehandlung und ein Alitieren durch ein Packverfahren. Dabei soll die erste Schicht aus der Keramik enthaltenden Mischung verhindern, daß Al von der Schicht in das Substrat eindringt und die Schicht mithin durch die Verarmung von Al ihre Wärmebeständigkeit einbüßt.It is known from JP 55-82765 A, which consists of a Ni or Co base alloy Substrate first with a mixture of ceramic, Al and metal powder To coat, the heat resistance of the long-lasting high temperature loaded Layer to improve. Then follows a layer of one with a Binder provided by Ni powder, a heat treatment and an Alitieren by Pack process. In this case, the first layer of the mixture containing ceramic prevent Al from penetrating the layer into the substrate and thus the layer through the depletion of Al loses its heat resistance.

Die JP 55-082759 A offenbart ein Verfahren zur Verbesserung der thermischen Beständigkeit einer Beschichtung, die auf ein Substrat aus einer Ni- oder Co-Basislegierung aufgebracht wird, wobei beim Beschichten ein Metall- oder ein Legierungspulver mit Keramikelementen gemischt und dann auf das Substrat aufgebracht wird. Es kann ein Bindemittel eingesetzt und eine anschließende Wärmebehandlung durchgeführt werden. Das Verfahren wird bei Bauteilen von z.B. Gasturbinen eingesetzt, die der Heißgaskorrosion ausgesetzt sind.JP 55-082759 A discloses a method for improving the thermal resistance a coating applied to a substrate of a Ni or Co base alloy is applied, wherein during coating a metal or an alloy powder mixed with ceramic elements and then applied to the substrate becomes. It can be a binder used and a subsequent heat treatment be performed. The method is applied to components of e.g. Used gas turbines, which are exposed to hot gas corrosion.

Die Aufgabe der vorliegenden Erfindung besteht darin, ein Verfahren zum Herstellen einer Panzerung der eingangs beschriebenen Gattung zu schaffen, das sich fertigungstechnisch möglichst einfach durchführen läßt und eine hochwertige Panzerung ergibt.The object of the present invention is to provide a method for manufacturing To create an armor of the type described above, which is manufacturing technology easy to carry out and a high-quality armor results.

Diese Aufgabe ist erfindungsgemäss durch das Verfahren gemäss Anspruch 1 gelöst. This object is achieved by the method solved according to claim 1.

Der Vorteil dieses Verfahrens liegt darin, daß die Panzerung mit einem fertigungstechnisch einfachen Verfahren auf das Bauteil aufgebracht werden kann. Zudem sind die keramischen Hartpartikel in der Schlickerschicht sicher eingebettet und mit dem Bauteil fest verbunden.The advantage of this method is that the armor with a manufacturing technology simple method can be applied to the component. In addition are the ceramic hard particles embedded in the slip layer safely and with the Component firmly connected.

In einer bevorzugten Ausgestaltung des Verfahrens werden die Hartpartikel dem Schlicker vor dem Auftragen auf die zu panzernde Oberfläche zugemischt. Auf diese Weise sind die Partikel in dem in einer Suspension vorliegenden Schlicker gleichmäßig verteilt.In a preferred embodiment of the method, the hard particles are the Slip before application on the surface to be coated mixed. To this Way, the particles are uniform in the slurry present in a suspension distributed.

In einer alternativen Ausgestaltung werden die Hartpartikel nach dem Auftragen in die Schlickerschicht eingesetzt, wodurch sich z.B. eine spezielle Anordnung der Partikel auf der zu panzernden Oberfläche erzielen läßt.In an alternative embodiment, the hard particles after application in the slip layer is used, resulting e.g. a special arrangement of the particles on the surface to be clad.

Ferner ist bevorzugt, daß das Ausgangspulver aus MCrAlY besteht, wobei das Ausgangspulver - wie das Zugabepulver - bevorzugt in einer Komgrößenverteilung von 5 bis 120 µm vorliegt. Das M steht dabei für wenigstens eines der Elemente Ni oder Co. Anstelle von Y kann auch Hf oder Ce verwendet werden.It is further preferred that the starting powder consists of MCrAlY, the starting powder - like the adding powder - preferably in a grain size distribution of 5 to 120 microns is present. The M stands for at least one of the elements Ni or Co. Instead of Y, Hf or Ce can also be used.

Das Auftragen des Schlickers auf die zu panzernde Oberfläche des Bauteils erfolgt bevorzugt durch Spritzen, Pinseln oder Tauchen, wodurch sich das Verfahren fertigungstechnisch einfach und kostengünstig durchführen läßt. Durch diese Art des Auftragens lassen sich auf einfache Weise lokal begrenzte Schichten auch auf geometrisch komplizierten Bauteilen aufbringen. Zudem sind keine teuren und aufwendigen Spritz- oder Verdampfungsanlagen erforderlich. The application of the slurry on the surface to be coated of the component takes place preferably by spraying, brushing or dipping, whereby the process manufacturing technology easy and inexpensive to do. By this kind of Applying can be easily localized layers also on geometric Apply complicated components. Moreover, no expensive and elaborate Spraying or evaporation systems required.

Bevorzugt wird das Trocknen des Schlickers, der zusammen mit dem organischen oder anorganischen Bindemittel in einer Suspension vorliegt, über 0,5 - 4 Stunden durchgeführt, wobei sich eine Dauer von 1 - 2 Stunden als besonders vorteilhaft wiesen hat.Preference is given to drying the slurry, which together with the organic or inorganic binder in suspension, over 0.5 to 4 hours carried out, with a duration of 1 - 2 hours as particularly advantageous has meadows.

Bevorzugt ist ferner, daß die Schlickerschicht in Schutzgas, z.B. in Argon, oder im Vakuum wärmebehandelt wird, wobei das Wärmebehandeln der Schicht über 1 - 4 Stunden, bevorzugt über etwa 2 Stunden, durchgeführt wird, um die Schlickerschicht mit dem Bauteil und den Hartpartikeln über Diffusion zu verbinden.It is further preferred that the slip layer be coated in inert gas, e.g. in argon, or im Vacuum is heat treated, wherein the heat treatment of the layer about 1-4 Hours, preferably over about 2 hours, are performed to the slip layer to connect with the component and the hard particles via diffusion.

Bevorzugt besteht das metallische Bauteil aus einer Legierung auf Nickel- oder Kobaltbasis, wobei das Bauteil ein Triebwerksbauteit, z.B. eine Turbinenschaufel, sein kann, auf deren Schaufelspitze die Panzerung aufgebracht wird.The metallic component is preferably made of a nickel or cobalt-based alloy, wherein the component is an engine building, e.g. a turbine blade, his can, on whose blade tip the armor is applied.

Bevorzugt macht das Zugabepulver bis zu 35 Gew.-% des Gesamtgewichts aus Ausgangs- und Zugabepulver aus.Preferably, the addition powder makes up to 35% by weight of the total weight of starting materials. and adding powder.

Im folgenden wird die Erfindung anhand eines Beispiels näher erläutert.In the following the invention will be explained in more detail by means of an example.

Bei einer Ausgestaltung des Verfahrens zum Herstellen einer Panzerung wird zunächst zur Herstellung eines Schlickers ein MCrAlY-Pulver mit einem Zugabepulver zu einer Suspension mit einem üblichen anorganischen Bindemittel gemischt. In der Suspension liegt das Bindemittel mit 5 - 10 Gew.-% und zusätzlich Wasser mit 5 - 7 Gew.-% vor. Die Korngrößen der Pulverpartikel liegen zwischen 5 und 120 µm. In diese fließfähige und spritzbare Masse werden BN-Partikel eingebracht, deren Größe über jener der Pulverpartikel liegt.In one embodiment of the method for producing an armor is first to prepare a slip, an MCrAlY powder with an addition powder mixed into a suspension with a conventional inorganic binder. In the Suspension is the binder with 5-10 wt .-% and additionally water with 5-7 Wt .-% before. The particle sizes of the powder particles are between 5 and 120 μm. In These flowable and sprayable mass are introduced BN particles whose size is above that of the powder particles.

In die Masse wird anschließend die Schaufelspitze einer Turbinenschaufel aus einer Nickelbasislegierung in der Weise eingetaucht, daß sich auf der zu panzernden Schaufelspitze eine Schlickerschicht bildet. Alternativ könnte der die Partikel enthaltende Schlicker z.B. auch mit einem Pinsel unter Bildung einer Schicht auf die Schaufelspitze aufgetragen werden. Im nächsten Schritt wird der in einer Suspension vorliegende, noch feuchte Schlicker bzw. die Schlickerschicht bei Raumtemperatur über etwa 1,5 Stunden getrocknet.In the mass then the blade tip of a turbine blade from a Nickel-based alloy immersed in such a way that on the to be armored Blade tip forms a slip layer. Alternatively, the particle-containing Slip e.g. also with a brush to form a layer on the blade tip be applied. In the next step, the suspension is in suspension, still moist slurry or the slip layer at room temperature dried for about 1.5 hours.

Die getrocknete Schlickerschicht wird dann bei 1000 °C etwa 2 Stunden im Vakuum wärmebehandelt, um eine Verbindung der Schlickerschicht mit dem Werkstoff der Turbinenschaufel und mit den Hartpartikeln durch Diffusion zu erzielen. Dabei sintern die in kugliger Form vorliegenden MCrAlY-Partikel wenigstens teilweise zusammen. Darüber hinaus kann auch Ni aus dem Grundwerkstoff austreten und in die Schlikkerschicht diffundieren. Nach dem Wärmebehandeln stehen die keramischen Hartpartikel aus BN od. dgl. nach außen über die Schlickerschicht vor und können diese sowie die Schaufelspitze beim Betrieb schützen.The dried slurry layer is then vacuumed at 1000 ° C for about 2 hours heat treated, in order to connect the slip layer with the material of the Turbine blade and to achieve with the hard particles by diffusion. While sintering the spherical MCrAlY particles at least partially together. In addition, Ni can also escape from the base material and into the Schlikkerschicht diffuse. After heat treatment are the ceramic hard particles from BN od. Like. Outward on the slip before and can this and protect the blade tip during operation.

Die BN-Partikel sind über die Schlickerschicht fest mit der Schaufelspitze verbunden und können sich während des Betriebs der Gasturbine beim Anstreifen in einen gegenüberliegenden Einlaufbelag einschneiden, um auf diese Weise eine Beschädigung der Schaufelspitze zu verhindern und die Spaltgröße zwischen dem rotierenden und dem stehenden Bauteil möglichst gering zu halten.The BN particles are firmly connected to the blade tip via the slip layer and may during operation of the gas turbine when rubbing in an opposite Cut in the inlet lining to avoid damage in this way To prevent the blade tip and the gap size between the rotating and keep the standing component as low as possible.

Claims (12)

  1. Method for producing an armour-plating for a metal component, in particular for a turbine blade, that is provided on the surface of the component, characterised by the steps: production of a slurry by mixing a binding-agent solution with an Al- and/or Cr-containing starting powder and an additive powder that comprises at least one element selected from Al, Pt, Pd or Si, the additive powder not comprising any Al when the starting powder contains exclusively Al; application of the slurry to the surface that is to be plated; addition of ceramic hard particles of BN, SiC or Al2O3 to the slurry before or after the application of the slurry, the size of the particles being chosen so that after heat-treatment they jut out over the layer in such a way that during operation they can cut into run-in coatings or the like; drying of the slurry layer at a temperature of ambient temperature to 450°C; and heat-treatment of the slurry layer at temperatures of 750° to 1250°C.
  2. Method according to claim 1, characterised in that the hard particles are admixed with the slurry before the application.
  3. Method according to claim 1, characterised in that the hard particles are inserted into the slurry layer after the application.
  4. Method according to one of the preceding claims, characterised in that the starting powder consists of MCrAlY, when M stands for Ni, for Co or for a combination of Ni and Co.
  5. Method according to one of the preceding claims, characterised in that the powders each have a particle-size distribution of 5 to 120 µm.
  6. Method according to one of the preceding claims, characterised in that the application of the slurry is carried out by injection, painting or dipping.
  7. Method according to one of the preceding claims, characterised in that the drying of the slurry layer is carried out over 0.5 - 4 hours.
  8. Method according to one of the preceding claims, characterised in that the slurry layer is heat-treated in inert gas, in argon for example, or under vacuum.
  9. Method according to claim 8, characterised in that the heat-treatment is carried out over 1 to 4 hours, preferably over approximately 2 hours.
  10. Method according to one of the preceding claims, characterised in that the component consists of a nickel- or cobalt-based alloy.
  11. Method according to one of the preceding claims, characterised in that the component is a turbine blade, on whose blade tip the armour-plating is provided.
  12. Method according to one of the preceding claims, characterised in that the additive powder constitutes up to 35% by weight of the total weight of the starting powder and additive powder.
EP00120803A 1999-09-29 2000-09-23 Method for producing a plating for a metal component Expired - Lifetime EP1088907B1 (en)

Applications Claiming Priority (2)

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DE19946650A DE19946650C2 (en) 1999-09-29 1999-09-29 Process for the production of armor for a metallic component
DE19946650 1999-09-29

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EP1088907A1 EP1088907A1 (en) 2001-04-04
EP1088907B1 true EP1088907B1 (en) 2005-08-10

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AT (1) ATE301735T1 (en)
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DE102009008510A1 (en) * 2009-02-11 2010-08-12 Mtu Aero Engines Gmbh Coating and method for coating a workpiece

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DE102004034410A1 (en) * 2004-07-16 2006-02-02 Mtu Aero Engines Gmbh Protective layer for application to a substrate and method for producing a protective layer
EP2842662B1 (en) * 2013-09-03 2020-08-05 MTU Aero Engines GmbH Armour plating for a blade tip for titanium blades
CN109280955A (en) * 2018-11-20 2019-01-29 沈阳工学院 A kind of heat resistant and wear resistant MCrAlSiC composite coating

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EP1088907A1 (en) 2001-04-04
DE19946650A1 (en) 2001-09-13
ATE301735T1 (en) 2005-08-15
DE19946650C2 (en) 2003-11-27

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