DK0550448T3 - Process for preparing rhamnose from rhamnolipids - Google Patents
Process for preparing rhamnose from rhamnolipidsInfo
- Publication number
- DK0550448T3 DK0550448T3 DK91914055.8T DK91914055T DK0550448T3 DK 0550448 T3 DK0550448 T3 DK 0550448T3 DK 91914055 T DK91914055 T DK 91914055T DK 0550448 T3 DK0550448 T3 DK 0550448T3
- Authority
- DK
- Denmark
- Prior art keywords
- rhamnose
- rhamnolipids
- separated
- further processed
- preparing
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H3/00—Compounds containing only hydrogen atoms and saccharide radicals having only carbon, hydrogen, and oxygen atoms
- C07H3/02—Monosaccharides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H3/00—Compounds containing only hydrogen atoms and saccharide radicals having only carbon, hydrogen, and oxygen atoms
- C07H3/08—Deoxysugars; Unsaturated sugars; Osones
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Saccharide Compounds (AREA)
- Body Structure For Vehicles (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
Abstract
The invention relates to a process for the production of rhamnose from rhamnolipids in which an acid emulsion of the rhamnolipid is hydrolysed at 100 to 200 C and then cooled, the aqueous phase of the hydrolysate produced is separated from the lipid phase, its pH is raised by the addition of a basic compound, any remaining precipitate is separated, the remaining solution condensed and either further processed directly or chromatographed via an ion exchange resin. The eluate comprises rhamnose-containing fractions which can be further processed as such or converted into crystalline rhamnose monohydrate.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE4030262A DE4030262A1 (en) | 1990-09-25 | 1990-09-25 | METHOD FOR PRODUCING RHAMNOSE FROM RHAMNOLIPID |
Publications (1)
Publication Number | Publication Date |
---|---|
DK0550448T3 true DK0550448T3 (en) | 1994-09-26 |
Family
ID=6414911
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DK91914055.8T DK0550448T3 (en) | 1990-09-25 | 1991-07-30 | Process for preparing rhamnose from rhamnolipids |
Country Status (9)
Country | Link |
---|---|
EP (1) | EP0550448B1 (en) |
JP (1) | JP3140775B2 (en) |
AT (1) | ATE106083T1 (en) |
DE (2) | DE4030262A1 (en) |
DK (1) | DK0550448T3 (en) |
ES (1) | ES2054501T3 (en) |
FI (1) | FI103119B (en) |
NO (1) | NO179176C (en) |
WO (1) | WO1992005182A1 (en) |
Families Citing this family (39)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
SG54274A1 (en) | 1992-11-27 | 1998-11-16 | Hoechst Ag | Alpha-l-rhamnosidase for obtaining rhamnose a process for its preparation and its use |
ES2291036T3 (en) * | 1998-02-24 | 2008-02-16 | Paradigm Biomedical, Inc. | USE OF RAMNOLIPIDS AS COSMETICS. |
US20040121335A1 (en) | 2002-12-06 | 2004-06-24 | Ecker David J. | Methods for rapid detection and identification of bioagents associated with host versus graft and graft versus host rejections |
US7666588B2 (en) | 2001-03-02 | 2010-02-23 | Ibis Biosciences, Inc. | Methods for rapid forensic analysis of mitochondrial DNA and characterization of mitochondrial DNA heteroplasmy |
US20030027135A1 (en) | 2001-03-02 | 2003-02-06 | Ecker David J. | Method for rapid detection and identification of bioagents |
US7226739B2 (en) | 2001-03-02 | 2007-06-05 | Isis Pharmaceuticals, Inc | Methods for rapid detection and identification of bioagents in epidemiological and forensic investigations |
US8073627B2 (en) | 2001-06-26 | 2011-12-06 | Ibis Biosciences, Inc. | System for indentification of pathogens |
US7217510B2 (en) | 2001-06-26 | 2007-05-15 | Isis Pharmaceuticals, Inc. | Methods for providing bacterial bioagent characterizing information |
EP1578399A4 (en) | 2002-12-06 | 2007-11-28 | Isis Pharmaceuticals Inc | Methods for rapid identification of pathogens in humans and animals |
US8057993B2 (en) | 2003-04-26 | 2011-11-15 | Ibis Biosciences, Inc. | Methods for identification of coronaviruses |
US8158354B2 (en) | 2003-05-13 | 2012-04-17 | Ibis Biosciences, Inc. | Methods for rapid purification of nucleic acids for subsequent analysis by mass spectrometry by solution capture |
US7964343B2 (en) | 2003-05-13 | 2011-06-21 | Ibis Biosciences, Inc. | Method for rapid purification of nucleic acids for subsequent analysis by mass spectrometry by solution capture |
US8546082B2 (en) | 2003-09-11 | 2013-10-01 | Ibis Biosciences, Inc. | Methods for identification of sepsis-causing bacteria |
US7956175B2 (en) | 2003-09-11 | 2011-06-07 | Ibis Biosciences, Inc. | Compositions for use in identification of bacteria |
US8097416B2 (en) | 2003-09-11 | 2012-01-17 | Ibis Biosciences, Inc. | Methods for identification of sepsis-causing bacteria |
US8163895B2 (en) | 2003-12-05 | 2012-04-24 | Ibis Biosciences, Inc. | Compositions for use in identification of orthopoxviruses |
US7666592B2 (en) | 2004-02-18 | 2010-02-23 | Ibis Biosciences, Inc. | Methods for concurrent identification and quantification of an unknown bioagent |
ES2641832T3 (en) | 2004-05-24 | 2017-11-14 | Ibis Biosciences, Inc. | Mass spectrometry with selective ion filtration by setting digital thresholds |
US20050266411A1 (en) | 2004-05-25 | 2005-12-01 | Hofstadler Steven A | Methods for rapid forensic analysis of mitochondrial DNA |
US7811753B2 (en) | 2004-07-14 | 2010-10-12 | Ibis Biosciences, Inc. | Methods for repairing degraded DNA |
US8084207B2 (en) | 2005-03-03 | 2011-12-27 | Ibis Bioscience, Inc. | Compositions for use in identification of papillomavirus |
CA2600184A1 (en) | 2005-03-03 | 2006-09-08 | Isis Pharmaceuticals, Inc. | Compositions for use in identification of adventitious viruses |
JP2009502137A (en) | 2005-07-21 | 2009-01-29 | アイシス ファーマシューティカルズ インコーポレイティッド | Method for rapid identification and quantification of nucleic acid variants |
WO2008143627A2 (en) | 2006-09-14 | 2008-11-27 | Ibis Biosciences, Inc. | Targeted whole genome amplification method for identification of pathogens |
EP2126132B1 (en) | 2007-02-23 | 2013-03-20 | Ibis Biosciences, Inc. | Methods for rapid foresnsic dna analysis |
US9598724B2 (en) | 2007-06-01 | 2017-03-21 | Ibis Biosciences, Inc. | Methods and compositions for multiple displacement amplification of nucleic acids |
EP2347254A2 (en) | 2008-09-16 | 2011-07-27 | Ibis Biosciences, Inc. | Sample processing units, systems, and related methods |
EP2349549B1 (en) | 2008-09-16 | 2012-07-18 | Ibis Biosciences, Inc. | Mixing cartridges, mixing stations, and related kits, and system |
US8534447B2 (en) | 2008-09-16 | 2013-09-17 | Ibis Biosciences, Inc. | Microplate handling systems and related computer program products and methods |
WO2010093943A1 (en) | 2009-02-12 | 2010-08-19 | Ibis Biosciences, Inc. | Ionization probe assemblies |
US9194877B2 (en) | 2009-07-17 | 2015-11-24 | Ibis Biosciences, Inc. | Systems for bioagent indentification |
US8950604B2 (en) | 2009-07-17 | 2015-02-10 | Ibis Biosciences, Inc. | Lift and mount apparatus |
US9890408B2 (en) | 2009-10-15 | 2018-02-13 | Ibis Biosciences, Inc. | Multiple displacement amplification |
CN102766172A (en) * | 2011-09-19 | 2012-11-07 | 大庆沃太斯化工有限公司 | Industrial production method of rhamnolipid biosurfactant dry powder |
AU2016207008B2 (en) * | 2015-01-12 | 2019-09-26 | Stepan Company | Production of rhamnolipid compositions |
BR102017000578B1 (en) | 2017-01-11 | 2019-04-02 | Natura Cosméticos S.A. | PROCESS OF OBTAINING RAMNOLIPID PRODUCED BY PSEUDOMONAS OR ENTEROBACTER USING ANDIROBA OR MURUMURU SEED WASTE |
JP7022139B2 (en) * | 2017-02-06 | 2022-02-17 | ステパン カンパニー | Decolorization of concentrated ramnolipid composition |
CN108949850B (en) * | 2018-08-01 | 2021-07-23 | 万华化学集团股份有限公司 | Online separation and purification method of rhamnolipid fermentation liquor |
CN112225763A (en) * | 2020-11-16 | 2021-01-15 | 西安润嬴生物科技有限公司 | Separation and purification method of rhamnolipid |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4933281A (en) * | 1987-03-17 | 1990-06-12 | The University Of Iowa Research Foundation | Method for producing rhamnose |
DE3871491D1 (en) * | 1987-11-03 | 1992-07-02 | Nestle Sa | SELECTIVE HYDROLYSIS. |
GB8727221D0 (en) * | 1987-11-20 | 1987-12-23 | Unilever Plc | Glycoside hydrolysis |
-
1990
- 1990-09-25 DE DE4030262A patent/DE4030262A1/en not_active Withdrawn
-
1991
- 1991-07-30 EP EP91914055A patent/EP0550448B1/en not_active Expired - Lifetime
- 1991-07-30 DE DE59101734T patent/DE59101734D1/en not_active Expired - Fee Related
- 1991-07-30 WO PCT/EP1991/001426 patent/WO1992005182A1/en active IP Right Grant
- 1991-07-30 DK DK91914055.8T patent/DK0550448T3/en active
- 1991-07-30 ES ES91914055T patent/ES2054501T3/en not_active Expired - Lifetime
- 1991-07-30 AT AT91914055T patent/ATE106083T1/en not_active IP Right Cessation
- 1991-07-30 JP JP03512763A patent/JP3140775B2/en not_active Expired - Fee Related
-
1993
- 1993-02-18 FI FI930736A patent/FI103119B/en active
- 1993-03-11 NO NO930885A patent/NO179176C/en not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
JP3140775B2 (en) | 2001-03-05 |
EP0550448B1 (en) | 1994-05-25 |
JPH06500309A (en) | 1994-01-13 |
DE59101734D1 (en) | 1994-06-30 |
NO930885L (en) | 1993-03-11 |
NO179176B (en) | 1996-05-13 |
NO930885D0 (en) | 1993-03-11 |
EP0550448A1 (en) | 1993-07-14 |
FI930736A (en) | 1993-02-18 |
FI103119B1 (en) | 1999-04-30 |
ATE106083T1 (en) | 1994-06-15 |
FI930736A0 (en) | 1993-02-18 |
ES2054501T3 (en) | 1994-08-01 |
NO179176C (en) | 1996-08-21 |
DE4030262A1 (en) | 1992-03-26 |
FI103119B (en) | 1999-04-30 |
WO1992005182A1 (en) | 1992-04-02 |
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