CN207576428U - A kind of zeolite molecular sieve dynamic, static dual-purpose crystallization device - Google Patents
A kind of zeolite molecular sieve dynamic, static dual-purpose crystallization device Download PDFInfo
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- CN207576428U CN207576428U CN201721695349.7U CN201721695349U CN207576428U CN 207576428 U CN207576428 U CN 207576428U CN 201721695349 U CN201721695349 U CN 201721695349U CN 207576428 U CN207576428 U CN 207576428U
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- China
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- permanent magnet
- electrical heating
- reaction kettle
- heating sleeve
- molecular sieve
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- Silicates, Zeolites, And Molecular Sieves (AREA)
Abstract
The utility model is related to equipment of chemical industry technical field, specially a kind of zeolite molecular sieve dynamic, static dual-purpose crystallization device, including electrical heating sleeve；Electric heating cover is provided in electrical heating sleeve, synthesis reaction vessel is provided in electric heating cover, synthesis reaction vessel upper and lower ends are respectively arranged with reaction kettle end cap and reaction kettle pedestal, single side permanent magnet is fixedly installed above reaction kettle end cap, two-sided permanent magnet is provided with above single side permanent magnet, two-sided permanent magnet is arranged on one group of magnet torsion shaft, magnet torsion shaft one end is fixedly connected across electrical heating sleeve with one group of turn drive motor main shaft, resetting spring is provided with below reaction kettle pedestal, the resetting spring other end is fixedly connected with reactor base；The utility model drives the movement of reaction kettle and stopping by setting single side permanent magnet and one group of two-sided permanent magnet driven by driving motor above synthesis reaction vessel, ensures that device can realize dynamic, static two kinds of reactivenesses.
Description
Technical field
The utility model is related to equipment of chemical industry technical field more particularly to a kind of zeolite molecular sieve dynamic, static state two
With crystallization device.
Background technology
Zeolite molecular sieve is the hydrate of crystalline alumino metal salt, is unique absorption with shape selective, catalysis
Material, not only can be by selective catalysis to reduce the generation of byproduct, improve the utilization rate of reaction raw materials, but also can pass through
The means such as structural adjustment, loaded modified form the function catalysis material needed for production, thus it is more and more it is studied use it is all
Multi-field, use is also more and more extensive.At present, the synthesis mode of zeolite molecular sieve is mainly divided to two classes, be static monitor respectively with
Dynamic synthesizes.Correspondingly, the device of static monitor is mainly reaction kettle and baking oven, by synthesis materials such as silicon source, silicon source, templates
It is added in synthesis reactor, then will be placed into baking oven in reactor.Entire synthetic reaction process remains static；It is dynamic
State synthetic method is mainly that the synthesis reactor with heating unit is furnished with agitating device again.It is generally used in both of which experiment
Method, different synthesis modes also have an impact zeolite molecular sieve product, during routine experimentation, if investigated static and dynamic
Influence of the state synthetic method to zeolite molecular sieve will often prepare two sets of synthesizers, increase equipment cost, more complicated.
Invention content
The utility model overcomes above-mentioned the deficiencies in the prior art, and it is dual-purpose to provide a kind of zeolite molecular sieve dynamic, static state
Crystallization device.The utility model above synthesis reaction vessel by setting single side permanent magnet and one group to be driven by driving motor
Two-sided permanent magnet drive the movement of reaction kettle and stopping, ensureing that device can realize dynamic, static two kinds of reactivenesses.
The technical solution of the utility model：
A kind of zeolite molecular sieve dynamic, static dual-purpose crystallization device, including electrical heating sleeve, socket cover, electric heating cover,
Synthesis reaction vessel；The electrical heating sleeve is arranged in the reactor base, and electrical heating is provided in the electrical heating sleeve
It covers, is machined with sliding slot in the electric heating cover, the synthesis reaction vessel, the synthesis reaction vessel are movably set in the sliding slot
Top is provided with reaction kettle end cap, and reaction kettle pedestal is provided with below the synthesis reaction vessel, and the reaction kettle end cap top is solid
Surely single side permanent magnet is provided with, is provided with two-sided permanent magnet above the single side permanent magnet, the two-sided permanent magnet is arranged on one
On group magnet torsion shaft, described magnet torsion shaft one end is fixed across the electrical heating sleeve with one group of turn drive motor main shaft
Connection, the reaction kettle pedestal lower section are provided with resetting spring, and the resetting spring other end is fixed with the reactor base
Connection, the electrical heating sleeve upper end is provided with electric heating cover cover.
Further, the turn drive motor is arranged on the electric machine support, and the electric machine support adds with the electricity
Hot jacket drum outer wall is fixedly connected.
Further, the single side permanent magnet is N poles permanent magnetic iron bar.
Further, the two-sided permanent magnet is the two-sided different poles permanent magnet items of N/S.
The utility model has the advantages that relative to the prior art：
The utility model drives the two-sided different poles permanent magnet items of N/S to rotate by turn drive motor, repelled by homopolarity,
The heteropolar attracting N poles permanent magnet covered with reaction kettle interacts, and driving synthesis reaction vessel moves up and down in sliding slot, realizes
Zeolite molecular sieve dynamic synthesizes；When experiment needs static monitor, do not start motor, you can realize static reaction；Electric heating cover
The achievable building-up process temperature of cylinder is precisely controlled；Furthermore it is possible to by the way that turn drive motor rotating speed is controlled to control mixing rate；It is brilliant
Heating mantle cover can be opened after being combined to, realizes charging, takes out the cleaning of synthetic product and reaction kettle；
The utility model strong applicability, simple in structure, easily operated, device volume is small, saves space；
The up and down motion of the synthesis reaction vessel of the utility model can be uniformly mixed reaction raw materials, and up and down motion amplitude
Less, just meet the required condition for mitigating mixing of zeolite molecular sieve growth, be conducive to the growth of molecular sieve；
The utility model synthesis reaction vessel improves leakproofness, ensure that the pressure in kettle without built-in agitating device, simultaneous
Have zeolite molecular sieve dynamic, static dual-purpose reaction kettle, easily experiment condition is provided for zeolite molecular sieve compound experiment, it is full respectively
Requirement of experiment under sufficient different situations.
Description of the drawings
Fig. 1 is the structure diagram of the utility model；
Fig. 2 is the vertical view of the synthesis reaction vessel of the utility model.
1- electrical heating sleeve in figure；2- electric heating cover covers；3- electric heating covers；4- synthesis reaction vessels；41- reaction kettles end
Lid；42- reaction kettle pedestals；5- reactor bases；6- sliding slots；7- single side permanent magnets；The two-sided permanent magnets of 8-；9- magnet torsion shafts；
10- turn drive motors；11- resetting springs；12- electric machine supports.
Specific embodiment
The utility model is described in detail below with reference to attached drawing.
Show with reference to Fig. 1-Fig. 2, a kind of zeolite molecular sieve dynamic, static dual-purpose crystallization device, packet disclosed in the present embodiment
Include electrical heating sleeve 1, electric heating cover cover 2, electric heating cover 3, synthesis reaction vessel 4；The electrical heating sleeve 1 is arranged on described anti-
It answers on device pedestal 5, electric heating cover 3 is provided in the electrical heating sleeve 1, sliding slot 6 is machined in the electric heating cover 3, it is described
The synthesis reaction vessel 4 is movably set in sliding slot 6,4 top of synthesis reaction vessel is provided with reaction kettle end cap 41, the conjunction
4 lower section of reaction kettle is provided with reaction kettle pedestal 42,41 top of reaction kettle end cap is fixedly installed single side permanent magnet 7, institute
It states 7 top of single side permanent magnet and is provided with two-sided permanent magnet 8, the two-sided permanent magnet 8 is arranged on one group of magnet torsion shaft 9, institute
It states 9 one end of magnet torsion shaft to be fixedly connected with one group of 10 main shaft of turn drive motor across the electrical heating sleeve 1, the reaction
Seat 4 lower section in bottom is provided with resetting spring 11, and 11 other end of resetting spring is fixedly connected with the reactor base 5, institute
It states 1 upper end of electrical heating sleeve and is provided with electric heating cover cover 2.
Specifically, the turn drive motor 10 is arranged on the electric machine support 12, the electric machine support 12 with it is described
1 outer wall of electrical heating sleeve is fixedly connected.
More specifically, the single side permanent magnet 7 is N poles permanent magnetic iron bar；The two-sided permanent magnet 8 is two-sided heteropolar for N/S
Permanent magnetic iron bar.
More specifically, temperature sensor, the input of temperature sensor and one group of PLC controller are provided in synthesis reaction vessel
End electrical connection, the PLC controller are arranged in control panel, and several groups of control buttons, institute are provided on the control panel
Input terminal of the control button also with the PLC controller is stated to be electrically connected, the output terminal of the PLC controller also with the electrical heating
Set and turn drive motor electrical connection.
The utility model drives the two-sided different poles permanent magnet items of N/S to rotate by turn drive motor, repelled by homopolarity,
Heteropolar attracting and reaction kettle has covered N poles permanent magnet and has interacted, and synthesis reactor is driven to move up and down, and realizes that zeolite molecules sieve
State synthesizes；When experiment needs static monitor, do not start motor, removing the two-sided different poles permanent magnet electrical heating sleeves of N/S can
Realize that building-up process temperature is precisely controlled；In addition, can mixing rate be controlled by motor speed；It can open and add after crystallization synthesis
Hot jacket cover realizes charging, takes out the cleaning of synthetic product and reaction kettle.
Above example is only to the exemplary description of this patent does not limit its scope of protection, people in the art
Member can also be changed its part, as long as it does not exceed the essence of this patent, within the protection scope of the present patent.
Claims (4)
1. a kind of zeolite molecular sieve dynamic, static dual-purpose crystallization device, it is characterised in that：Add including electrical heating sleeve (1), electricity
Hot jacket cover (2), electric heating cover (3), synthesis reaction vessel (4)；The electrical heating sleeve (1) is arranged on the reactor base
(5) on, electric heating cover (3) is provided in the electrical heating sleeve (1), sliding slot (6), institute are machined in the electric heating cover (3)
It states and the synthesis reaction vessel (4) is movably set in sliding slot (6), reaction kettle end cap is provided with above the synthesis reaction vessel (4)
(41), reaction kettle pedestal (42) is provided with below the synthesis reaction vessel (4), is fixedly installed above the reaction kettle end cap (41)
There is single side permanent magnet (7), be provided with two-sided permanent magnet (8) above the single side permanent magnet (7), the two-sided permanent magnet (8) sets
It puts on one group of magnet torsion shaft (9), described magnet torsion shaft (9) one end passes through the electrical heating sleeve (1) and one group of overturning
Driving motor (10) main shaft is fixedly connected, and resetting spring (11), the reset bullet are provided with below the reaction kettle pedestal (42)
Spring (11) other end is fixedly connected with the reactor base (5), and electrical heating sleeve (1) upper end is provided with electrical heating sleeve
It covers (2).
2. a kind of zeolite molecular sieve dynamic according to claim 1, static dual-purpose crystallization device, which is characterized in that institute
It states turn drive motor (10) to be arranged on the electric machine support (12), the electric machine support (12) and the electrical heating sleeve
(1) outer wall is fixedly connected.
3. a kind of zeolite molecular sieve dynamic according to claim 2, static dual-purpose crystallization device, which is characterized in that institute
Single side permanent magnet (7) is stated as N poles permanent magnetic iron bar.
4. a kind of zeolite molecular sieve dynamic according to claim 3, static dual-purpose crystallization device, which is characterized in that institute
Two-sided permanent magnet (8) is stated as the two-sided different poles permanent magnet items of N/S.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721695349.7U CN207576428U (en) | 2017-12-07 | 2017-12-07 | A kind of zeolite molecular sieve dynamic, static dual-purpose crystallization device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721695349.7U CN207576428U (en) | 2017-12-07 | 2017-12-07 | A kind of zeolite molecular sieve dynamic, static dual-purpose crystallization device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207576428U true CN207576428U (en) | 2018-07-06 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721695349.7U Expired - Fee Related CN207576428U (en) | 2017-12-07 | 2017-12-07 | A kind of zeolite molecular sieve dynamic, static dual-purpose crystallization device |
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| Country | Link |
|---|---|
| CN (1) | CN207576428U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107824155A (en) * | 2017-12-07 | 2018-03-23 | 黑龙江省能源环境研究院 | A kind of zeolite molecular sieve dynamic, static dual-purpose crystallization device |
-
2017
- 2017-12-07 CN CN201721695349.7U patent/CN207576428U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107824155A (en) * | 2017-12-07 | 2018-03-23 | 黑龙江省能源环境研究院 | A kind of zeolite molecular sieve dynamic, static dual-purpose crystallization device |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180706 Termination date: 20201207 |