CN1194431C - Prepn of composite negative-pole graphite material for lithium ion battery, negative pole and battery - Google Patents
Prepn of composite negative-pole graphite material for lithium ion battery, negative pole and battery Download PDFInfo
- Publication number
- CN1194431C CN1194431C CNB021591660A CN02159166A CN1194431C CN 1194431 C CN1194431 C CN 1194431C CN B021591660 A CNB021591660 A CN B021591660A CN 02159166 A CN02159166 A CN 02159166A CN 1194431 C CN1194431 C CN 1194431C
- Authority
- CN
- China
- Prior art keywords
- lithium
- negative electrode
- ion battery
- lithium ion
- graphite
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 title claims abstract description 22
- 229910001416 lithium ion Inorganic materials 0.000 title claims abstract description 22
- 239000002131 composite material Substances 0.000 title claims description 27
- 239000007770 graphite material Substances 0.000 title description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 57
- 229910002804 graphite Inorganic materials 0.000 claims abstract description 41
- 239000010439 graphite Substances 0.000 claims abstract description 41
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims abstract description 20
- 238000000034 method Methods 0.000 claims abstract description 19
- 239000007773 negative electrode material Substances 0.000 claims abstract description 19
- 238000002360 preparation method Methods 0.000 claims abstract description 11
- 239000000243 solution Substances 0.000 claims abstract description 11
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims abstract description 9
- 239000010452 phosphate Substances 0.000 claims abstract description 9
- -1 polypropylene Polymers 0.000 claims abstract description 9
- 229910000314 transition metal oxide Inorganic materials 0.000 claims abstract description 7
- 229910003002 lithium salt Inorganic materials 0.000 claims abstract description 5
- 159000000002 lithium salts Chemical class 0.000 claims abstract description 5
- 239000012046 mixed solvent Substances 0.000 claims abstract description 5
- 239000004743 Polypropylene Substances 0.000 claims abstract description 4
- 229920001155 polypropylene Polymers 0.000 claims abstract description 4
- 229910000319 transition metal phosphate Inorganic materials 0.000 claims abstract description 3
- 229910052744 lithium Inorganic materials 0.000 claims description 18
- 239000000463 material Substances 0.000 claims description 14
- 239000003792 electrolyte Substances 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 12
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical class [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims description 11
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 claims description 10
- 238000005303 weighing Methods 0.000 claims description 8
- 239000000853 adhesive Substances 0.000 claims description 7
- 230000001070 adhesive effect Effects 0.000 claims description 7
- 239000006258 conductive agent Substances 0.000 claims description 7
- 229910019142 PO4 Inorganic materials 0.000 claims description 6
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 6
- OIFBSDVPJOWBCH-UHFFFAOYSA-N Diethyl carbonate Chemical compound CCOC(=O)OCC OIFBSDVPJOWBCH-UHFFFAOYSA-N 0.000 claims description 5
- 230000004888 barrier function Effects 0.000 claims description 5
- 229910021626 Tin(II) chloride Inorganic materials 0.000 claims description 4
- 239000006229 carbon black Substances 0.000 claims description 4
- 239000012065 filter cake Substances 0.000 claims description 4
- 239000012982 microporous membrane Substances 0.000 claims description 4
- 229920000642 polymer Polymers 0.000 claims description 4
- 150000003839 salts Chemical class 0.000 claims description 4
- 238000005406 washing Methods 0.000 claims description 4
- 229910010707 LiFePO 4 Inorganic materials 0.000 claims description 3
- IEJIGPNLZYLLBP-UHFFFAOYSA-N dimethyl carbonate Chemical compound COC(=O)OC IEJIGPNLZYLLBP-UHFFFAOYSA-N 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 229920001343 polytetrafluoroethylene Polymers 0.000 claims description 3
- 239000004810 polytetrafluoroethylene Substances 0.000 claims description 3
- QGHDLJAZIIFENW-UHFFFAOYSA-N 4-[1,1,1,3,3,3-hexafluoro-2-(4-hydroxy-3-prop-2-enylphenyl)propan-2-yl]-2-prop-2-enylphenol Chemical group C1=C(CC=C)C(O)=CC=C1C(C(F)(F)F)(C(F)(F)F)C1=CC=C(O)C(CC=C)=C1 QGHDLJAZIIFENW-UHFFFAOYSA-N 0.000 claims description 2
- KMTRUDSVKNLOMY-UHFFFAOYSA-N Ethylene carbonate Chemical compound O=C1OCCO1 KMTRUDSVKNLOMY-UHFFFAOYSA-N 0.000 claims description 2
- 229910002097 Lithium manganese(III,IV) oxide Inorganic materials 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims description 2
- 239000003513 alkali Substances 0.000 claims description 2
- MTAZNLWOLGHBHU-UHFFFAOYSA-N butadiene-styrene rubber Chemical compound C=CC=C.C=CC1=CC=CC=C1 MTAZNLWOLGHBHU-UHFFFAOYSA-N 0.000 claims description 2
- 229910017052 cobalt Inorganic materials 0.000 claims description 2
- 239000010941 cobalt Substances 0.000 claims description 2
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims description 2
- 239000004816 latex Substances 0.000 claims description 2
- 229920000126 latex Polymers 0.000 claims description 2
- MHCFAGZWMAWTNR-UHFFFAOYSA-M lithium perchlorate Chemical group [Li+].[O-]Cl(=O)(=O)=O MHCFAGZWMAWTNR-UHFFFAOYSA-M 0.000 claims description 2
- 229910001486 lithium perchlorate Inorganic materials 0.000 claims description 2
- 239000003960 organic solvent Substances 0.000 claims description 2
- 238000001556 precipitation Methods 0.000 claims description 2
- 239000000376 reactant Substances 0.000 claims description 2
- 239000012266 salt solution Substances 0.000 claims description 2
- 229910001432 tin ion Inorganic materials 0.000 claims description 2
- IUTCEZPPWBHGIX-UHFFFAOYSA-N tin(2+) Chemical compound [Sn+2] IUTCEZPPWBHGIX-UHFFFAOYSA-N 0.000 claims description 2
- 239000007774 positive electrode material Substances 0.000 claims 1
- 229910044991 metal oxide Inorganic materials 0.000 abstract description 5
- 150000004706 metal oxides Chemical class 0.000 abstract description 5
- 150000001875 compounds Chemical class 0.000 abstract 4
- 239000003795 chemical substances by application Substances 0.000 abstract 2
- 239000008151 electrolyte solution Substances 0.000 abstract 2
- 239000012528 membrane Substances 0.000 abstract 2
- 239000013543 active substance Substances 0.000 abstract 1
- 230000005611 electricity Effects 0.000 abstract 1
- 239000002391 graphite-based active material Substances 0.000 abstract 1
- 229910052799 carbon Inorganic materials 0.000 description 10
- 230000002441 reversible effect Effects 0.000 description 10
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 239000002388 carbon-based active material Substances 0.000 description 2
- 239000012153 distilled water Substances 0.000 description 2
- 238000000227 grinding Methods 0.000 description 2
- 230000002427 irreversible effect Effects 0.000 description 2
- 239000010410 layer Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 235000011150 stannous chloride Nutrition 0.000 description 2
- 229910013684 LiClO 4 Inorganic materials 0.000 description 1
- 229910012851 LiCoO 2 Inorganic materials 0.000 description 1
- 229910013870 LiPF 6 Inorganic materials 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000005229 chemical vapour deposition Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 239000005486 organic electrolyte Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000002344 surface layer Substances 0.000 description 1
Images
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
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- Battery Electrode And Active Subsutance (AREA)
Abstract
Description
Claims (8)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNB021591660A CN1194431C (en) | 2002-12-30 | 2002-12-30 | Prepn of composite negative-pole graphite material for lithium ion battery, negative pole and battery |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNB021591660A CN1194431C (en) | 2002-12-30 | 2002-12-30 | Prepn of composite negative-pole graphite material for lithium ion battery, negative pole and battery |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1417876A CN1417876A (en) | 2003-05-14 |
CN1194431C true CN1194431C (en) | 2005-03-23 |
Family
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNB021591660A Expired - Lifetime CN1194431C (en) | 2002-12-30 | 2002-12-30 | Prepn of composite negative-pole graphite material for lithium ion battery, negative pole and battery |
Country Status (1)
Country | Link |
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CN (1) | CN1194431C (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2012022256A1 (en) * | 2010-08-19 | 2012-02-23 | Byd Company Limited | Method for preparing negative active material, negative electrode material and lithium ion battery |
Families Citing this family (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100570648B1 (en) * | 2004-01-26 | 2006-04-12 | 삼성에스디아이 주식회사 | Negative active material for lithium secondary battery, method of preparing same, and lithium secondary battery comprising same |
US20080032196A1 (en) | 2005-04-13 | 2008-02-07 | Lg Chem, Ltd. | Method of preparing material for lithium secondary battery of high performance |
US20070298512A1 (en) | 2005-04-13 | 2007-12-27 | Lg Chem, Ltd. | Material for lithium secondary battery of high performance |
US20070292761A1 (en) | 2005-04-13 | 2007-12-20 | Lg Chem, Ltd. | Material for lithium secondary battery of high performance |
CN101300696A (en) * | 2006-05-10 | 2008-11-05 | 株式会社Lg化学 | Material for lithium secondary battery of high performance |
KR100778450B1 (en) | 2006-11-22 | 2007-11-28 | 삼성에스디아이 주식회사 | Negative active material for rechargeable lithium battery, method of preparing same, and rechargeable lithium battery comprising same |
KR100814880B1 (en) | 2006-11-22 | 2008-03-18 | 삼성에스디아이 주식회사 | Negative active material for rechargeable lithium battery, method of preparing thereof, and rechargeable lithium battery comprising the same |
KR100805123B1 (en) | 2007-02-15 | 2008-02-21 | 삼성에스디아이 주식회사 | Lithium secondary battery |
JP5511128B2 (en) | 2007-06-07 | 2014-06-04 | 三星エスディアイ株式会社 | Anode material for non-aqueous secondary battery and non-aqueous secondary battery |
KR100898291B1 (en) | 2007-09-12 | 2009-05-18 | 삼성에스디아이 주식회사 | Rechargeable lithium battery |
CN101510597B (en) * | 2008-12-05 | 2011-02-09 | 东莞新能源科技有限公司 | Lithium ion battery and isolating film |
CN102544444B (en) * | 2010-12-29 | 2015-01-14 | 比亚迪股份有限公司 | Preparation method for lithium ion battery anode active material |
CN103022432B (en) * | 2011-09-26 | 2015-08-26 | 比亚迪股份有限公司 | A kind of negative active core-shell material and preparation method thereof and a kind of lithium ion battery |
CN102610809B (en) * | 2012-03-14 | 2014-11-26 | 北大先行科技产业有限公司 | Ferroferric oxide/graphite lithium ion battery anode material and preparation method for ferroferric oxide/graphite lithium ion battery anode material |
CN102779988B (en) * | 2012-08-06 | 2016-04-27 | 常州大学 | A kind of method of modifying of composite cathode material for lithium ion cell plated film |
KR102228103B1 (en) * | 2013-03-26 | 2021-03-15 | 미쯔비시 케미컬 주식회사 | Carbonaceous material and nonaqueous secondary cell in which same is used |
CN104085923B (en) * | 2014-07-01 | 2016-07-06 | 中国科学技术大学 | Transition metal chalcogenide nano wire and preparation method thereof and stored energy application |
CN109524630B (en) * | 2017-09-20 | 2021-06-04 | 上海杉杉科技有限公司 | Preparation method of coated composite anode material |
CN109244392A (en) * | 2018-08-23 | 2019-01-18 | 武汉艾特米克超能新材料科技有限公司 | A kind of composite graphite negative electrode material and preparation method thereof and lithium ion battery |
CN111599995A (en) * | 2020-04-28 | 2020-08-28 | 惠州锂威新能源科技有限公司 | Cathode material, preparation method thereof and high-voltage lithium ion battery |
CN114335462B (en) * | 2021-12-24 | 2023-06-02 | 陕西煤业化工技术研究院有限责任公司 | Graphite negative electrode material for low temperature, preparation method thereof and lithium battery |
-
2002
- 2002-12-30 CN CNB021591660A patent/CN1194431C/en not_active Expired - Lifetime
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2012022256A1 (en) * | 2010-08-19 | 2012-02-23 | Byd Company Limited | Method for preparing negative active material, negative electrode material and lithium ion battery |
US9601753B2 (en) | 2010-08-19 | 2017-03-21 | Byd Company Limited | Negative active materials, lithium ion batteries, and methods thereof |
Also Published As
Publication number | Publication date |
---|---|
CN1417876A (en) | 2003-05-14 |
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Application publication date: 20030514 Assignee: PULEAD TAI'AN TECHNOLOGY INDUSTRY CO.,LTD. Assignor: PULEAD TECHNOLOGY INDUSTRY Co.,Ltd. Contract record no.: 2014990000235 Denomination of invention: Prepn of composite negative-pole graphite material for lithium ion battery, negative pole and battery Granted publication date: 20050323 License type: Exclusive License Record date: 20140423 |
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Denomination of invention: Prepn of composite negative-pole graphite material for lithium ion battery, negative pole and battery Effective date of registration: 20150817 Granted publication date: 20050323 Pledgee: Chinese bank Limited by Share Ltd. Xining Gan River Industrial Park Branch Pledgor: PULEAD TECHNOLOGY INDUSTRY Co.,Ltd.|PULEAD TAI'AN TECHNOLOGY INDUSTRY CO.,LTD. Registration number: 2015990000687 |
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Denomination of invention: Prepn of composite negative-pole graphite material for lithium ion battery, negative pole and battery Effective date of registration: 20170227 Granted publication date: 20050323 Pledgee: Chinese bank Limited by Share Ltd. Xining Gan River Industrial Park Branch Pledgor: PULEAD TAI'AN TECHNOLOGY INDUSTRY CO.,LTD.|PULEAD TECHNOLOGY INDUSTRY Co.,Ltd. Registration number: 2017990000126 |
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Denomination of invention: Preparation method, anode and battery of composite graphite anode material for lithium ion battery Effective date of registration: 20200812 Granted publication date: 20050323 Pledgee: Bank of China Limited by Share Ltd. Huangzhong County branch Pledgor: PULEAD TECHNOLOGY INDUSTRY Co.,Ltd. Registration number: Y2020990000946 |
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Effective date of registration: 20211201 Address after: No.139 Tong'an Road, Nanchuan Industrial Park, Xining, Qinghai 810000 Patentee after: QINGHAI TAIFENG PULEAD LITHIUM-ENERGY TECHNOLOGY Co.,Ltd. Address before: 102200, Beijing Changping science and Technology Park, super Road, No. 9 Patentee before: PULEAD TECHNOLOGY INDUSTRY Co.,Ltd. |
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