CN113548663A - Production method of environment-friendly activated carbon - Google Patents

Production method of environment-friendly activated carbon Download PDF

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Publication number
CN113548663A
CN113548663A CN202110895403.7A CN202110895403A CN113548663A CN 113548663 A CN113548663 A CN 113548663A CN 202110895403 A CN202110895403 A CN 202110895403A CN 113548663 A CN113548663 A CN 113548663A
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China
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activated carbon
chemical treatment
cylinder
hydrochloric acid
distilled water
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CN202110895403.7A
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Chinese (zh)
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钟小青
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Individual
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    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/30Active carbon
    • C01B32/39Apparatus for the preparation thereof
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/30Active carbon
    • C01B32/312Preparation
    • C01B32/318Preparation characterised by the starting materials
    • C01B32/324Preparation characterised by the starting materials from waste materials, e.g. tyres or spent sulfite pulp liquor
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/30Active carbon
    • C01B32/312Preparation
    • C01B32/342Preparation characterised by non-gaseous activating agents

Abstract

The invention relates to the technical field of activated carbon, in particular to an environment-friendly activated carbon production method, which adopts environment-friendly activated carbon production equipment. The invention can absorb the gas and water generated in the process of heating walnut shell and carbonizing in time, thereby preventing the influence on the quality of the active carbon; neutralizing acid water generated in the carbon particle acid adding treatment, discharging the neutralized acid water out of the reaction cylinder, and cooling the neutralized acid water; separating the active carbon blocks, storing the active carbon blocks for use, and absorbing the powder in time.

Description

Production method of environment-friendly activated carbon
Technical Field
The invention relates to the technical field of activated carbon, in particular to a production method of environment-friendly activated carbon.
Background
One typical use of activated carbon is to remove pollutants from water, other liquids, gases, land and soil, etc. by adsorption. Activated carbon is widely used. The existing activated carbon production method can not treat gas generated in the activated carbon heating process in time, can not chemically neutralize sewage generated after chemical reaction, and can not treat powdery activated carbon after the activated carbon is dried.
Disclosure of Invention
The invention aims to provide a method for producing environment-friendly activated carbon, aiming at the problems in the prior art.
In order to achieve the purpose, the invention adopts the following technical scheme: the environment-friendly active carbon production method adopts the following environment-friendly active carbon production equipment, the environment-friendly active carbon production equipment comprises a box body, a feeding funnel is arranged above one end of the box body, a grinding and conveying part is arranged below the funnel of the box body, a control feeding part is arranged below the rear side of the grinding and conveying part, a chemical treatment part is arranged below the control feeding part, a separation part is arranged towards the feeding funnel of the chemical treatment part, and a discharge hole is formed in one side of the separation part.
Preferably, the grinding and conveying part comprises a first motor, the first motor is fixed on one side of the box body facing the discharge port, the first motor rotates towards the direction of the feeding hopper and is provided with a first linkage shaft, one side, close to the first motor, of the first linkage shaft is fixedly provided with a first gear, the rear side of the first linkage shaft is provided with a second linkage shaft, the second linkage shaft is rotatably connected to two sides of the box body, one side, close to the first motor, of the second linkage shaft is fixedly provided with a second gear, the second gear is meshed with the first gear and is matched with the first gear, the first linkage shaft is far away from the direction of the first gear and is fixedly provided with a first grinding wheel, and the second linkage shaft is far away from the direction of the second gear and is fixedly provided with a second grinding wheel.
Preferably, second coupling shaft below is equipped with first transmission shaft, first transmission wheel one end is rotated and is connected in the box to one side of first motor, first transmission wheel top is equipped with the conveying deflector, the below is rotated and is equipped with the second axis of rotation in the middle of the conveying deflector, the second axis of rotation is kept away from first transmission shaft direction and is equipped with the third axis of rotation, the third axis of rotation passes the conveying deflector and rotates to be connected in the box to first motor one side, first motor one end is kept away from to first motor of first axis of rotation has set firmly first transmission wheel, first transmission wheel and second grinding miller transmission cooperation, the first transmission wheel one end of second axis of rotation has set firmly the second transmission wheel, second transmission wheel and first transmission wheel transmission cooperation, the one end of third axis of rotation second transmission wheel direction has set firmly the transmission cam, transmission cam and second transmission wheel transmission cooperation.
Preferably, the control feeding part comprises a metering funnel, the metering funnel is located below a third rotating shaft, a first baffle is arranged in the middle of the metering funnel in a rotating mode, a first metering hydraulic device is fixedly arranged below the first baffle, the metering funnel is rotatably arranged in a direction away from the first baffle, a second baffle is arranged in a rotating mode, a second metering hydraulic device is fixedly arranged below the second baffle, and an opening and closing device is arranged at the bottom of the metering funnel.
Preferably, the chemical treatment part includes a chemical treatment section of thick bamboo, a chemical treatment section of thick bamboo is located measurement funnel below, a chemical treatment section of thick bamboo is close to the upper end and is equipped with the sponge that absorbs water in switching device below, sponge top one side that absorbs water is equipped with gas treatment device, it is equipped with the lift filter to slide in the chemical treatment section of thick bamboo in the sponge below that absorbs water, lift filter below chemical treatment bobbin base portion evenly is equipped with a plurality of heat conduction pieces, heat conduction piece below is equipped with heating device in a chemical treatment section of thick bamboo below, the heating device below is equipped with the heating energy source chamber.
Preferably, the chemical treatment cylinder is provided with a first hydraulic device in the direction away from the gas treatment device, the first hydraulic device is fixed on the box body, a distilled water cylinder is arranged below the first hydraulic device, a first piston rod is arranged below the first hydraulic device, the first piston rod penetrates through the lower end of the distilled water cylinder and is fixedly provided with a first piston plate, the first piston plate is arranged in the distilled water cylinder in a sliding and sealing manner, a distilled water storage cavity is arranged below the distilled water cylinder, a distilled water inlet pipe is connected between one side of the distilled water cylinder above the first piston plate and the distilled water storage cavity, a distilled water outlet pipe is connected between one side of the distilled water cylinder above the first piston plate and the lower part of a water absorption sponge in the chemical treatment cylinder, a second hydraulic device is arranged on one side of the chemical treatment cylinder away from the grinding and conveying part and is fixed on the box body, a second piston rod is arranged below the hydraulic device, and a hydrochloric acid cylinder is arranged below the second piston rod, a second piston rod penetrates through the lower end of the top of the hydrochloric acid cylinder and is fixedly provided with a second piston plate, the second piston plate is arranged in the hydrochloric acid cylinder in a sliding and sealing manner, a hydrochloric acid storage cavity is arranged below the hydrochloric acid cylinder, a hydrochloric acid inlet pipe is connected between the hydrochloric acid storage cavity and the hydrochloric acid cylinder, a hydrochloric acid outlet pipe is connected between the hydrochloric acid cylinder and the chemical treatment cylinder, the chemical treatment cylinder is provided with a third hydraulic device towards the direction of the grinding and conveying part, the third hydraulic device is fixed on the box body, a pressing plate is arranged below the third hydraulic device, a third piston rod is arranged below the pressing plate, an alkaline solution cylinder is arranged below the third piston rod, a third piston plate is arranged at the lower end of the top of the alkaline solution cylinder and penetrates through the third piston plate, the third piston plate is arranged in the alkaline solution cylinder in a sliding and sealing manner, an alkaline solution storage cavity is arranged below the alkaline solution cylinder, an alkaline solution inlet pipe is connected between the alkaline solution storage cavity and the alkaline solution cylinder, and an alkaline solution outlet pipe is connected with an alkaline solution, the top of the lifting filter plate below the pressing plate is provided with two push rods, the stirrer is arranged near the bottom in the middle of the chemical treatment barrel, a PH value test bar is arranged on one side of the stirrer, a cooling cavity is arranged on the periphery of the bottom of the chemical treatment barrel, a first sewage outlet pipe is connected between the cooling cavity and the chemical treatment barrel, and a sewage cavity is arranged on one side of the distilled water storage cavity away from the heating energy cavity.
Preferably, the separation part includes active carbon absorption device, active carbon absorption device is located grinds the transfer unit below, it is equipped with the straw to grind transfer unit and chemical treatment section of thick bamboo and be connected between the sponge top of absorbing water, keep away from straw one side in the active carbon absorption device and set firmly the second motor, the second motor is equipped with the motor axis of rotation to the straw direction, the motor axis of rotation is equipped with the commentaries on classics board to the straw direction, the commentaries on classics board is equipped with the filter to the straw direction, the filter is fixed in the middle of active carbon absorption device is inside, the filter is equipped with the active carbon piece chamber to straw direction below, the filter is equipped with the active carbon powder chamber to second motor direction below.
Preferably, the production method of the environment-friendly activated carbon specifically comprises the following steps:
s1 feed grind transfer: putting the walnut shells into a device, grinding the walnut shells into powder, and conveying to the next step;
s2 metered feed: weighing 5-10 g of the crushed powder and feeding the crushed powder into a chemical cylinder;
s3, heating and carbonizing: heating by a heating device to uniformly heat the walnut shell fragments, treating a large amount of gas and generated water until no gas is generated or the carbon particles are heated to red, closing the heating device, and treating according to the following steps after the chemical cylinder is cooled;
acid treatment of the S4 carbon pellets: adding 50mL of 2mol/L hydrochloric acid, heating and boiling for 15 minutes by using a heating device, neutralizing and discharging the solution in the cup, and pouring 50mL of 2mol/L hydrochloric acid and boiling for 15 minutes to remove impurities in the carbon particles; cooling, filtering, washing with distilled water for three times, boiling a clean chemical cylinder in a beaker containing 50mL of distilled water for 15 minutes, discarding the solution in the beaker, boiling with new distilled water for several times, checking with a pH bar, and making the aqueous solution acidic and neutral; filtering the solution containing the carbon particles;
s5 drying activated carbon: heating the filtered wet carbon granules, continuously stirring until the carbon granules are completely baked, cutting off the carbon granules to burn, closing the heating device, and cooling;
s6, separating the active carbon block powder: absorbing the activated carbon, and separating the activated carbon into block powder by filtration.
Has the advantages that:
1. can absorb and treat gas and water generated in the process of heating the walnut shell and carbonizing in time, and prevents the influence on the quality of the active carbon.
2. Acid water generated in the carbon particle acid-adding treatment is discharged out of the reaction cylinder after neutralization treatment, and then is used for cooling and finally discharged.
3. Separating the active carbon blocks, storing the active carbon blocks for use, and absorbing the powder in time.
Drawings
The invention is further explained below with reference to the figures and examples:
FIG. 1 is a process flow diagram of the present invention.
Fig. 2 is a schematic isometric view of the present invention.
Fig. 3 is a schematic top view of the present invention.
FIG. 4 is a top view, longitudinal section A-A, schematic structural view of the present invention.
Fig. 5 is an isometric cross-sectional view of the internal structure of the present invention.
FIG. 6 is a schematic top view of a chemical reaction part according to the present invention.
FIG. 7 is a top view of a chemical reaction component of the present invention in a schematic view along section B-B.
FIG. 8 is a schematic top view of a chemical reaction component of the present invention in cross-section view of a C-C structure.
In the figure, a box body 1, a grinding and conveying component 2, a control feeding component 3, a chemical treatment component 4, a separation component 5, a feeding funnel 101, a discharge port 102, a first motor 201, a first linkage shaft 202, a second linkage shaft 203, a first gear 204, a second gear 205, a first grinding wheel 206, a second grinding wheel 207, a first transmission wheel 208, a second transmission wheel 209, a transmission cam 210, a first rotating shaft 211, a second rotating shaft 212, a third rotating shaft 213, a transmission guide plate 214, a measuring funnel 301, a first baffle plate 302, a second baffle plate 303, a first measuring hydraulic device 304, a second measuring hydraulic device 305, an opening and closing device 306, a chemical treatment cylinder 401, a water absorption sponge 402, a gas treatment device 403, a lifting filter plate 404, a first hydraulic device 405, a first piston rod 406, a distilled water cylinder 407, a first piston plate 408, a distilled water inlet pipe 409, a distilled water outlet pipe 410, a second transmission wheel 209, a transmission wheel 210, a transmission wheel, a first rotating shaft 211, a third rotating shaft 212, a third rotating shaft 213, a third rotating shaft, a fourth rotating shaft, a fourth rotating shaft, a fourth rotating, Distilled water storage cavity 411, first sewage outlet pipe 412, second sewage outlet pipe 413, cooling cavity 414, sewage cavity 415, heating device 416, heating energy cavity 417, second hydraulic device 418, second piston rod 419, second piston plate 420, hydrochloric acid cylinder 421, hydrochloric acid inlet pipe 422, hydrochloric acid outlet pipe 423, hydrochloric acid storage cavity 424, third hydraulic device 425, third piston rod 426, alkali solution cylinder 427, alkali solution inlet pipe 428, alkali solution outlet pipe 429, third piston plate 430, pressing plate 431, heat conducting block 432, push rod 433, stirrer 434, pH value testing rod 435, alkali solution storage cavity 436, activated carbon absorption device 501, second motor 502, motor rotating shaft 503, rotating plate 504, suction pipe 505, filter plate 506, activated carbon block cavity 507, activated carbon powder cavity 508.
Detailed Description
The following are specific embodiments of the present invention and are further described with reference to the drawings, but the present invention is not limited to these embodiments.
In the description of the present invention, it should be noted that the terms "inside", "below", and the like refer to orientations or positional relationships based on the orientations or positional relationships shown in the drawings or orientations or positional relationships that the products of the present invention conventionally place when used, and are used only for convenience in describing the present invention and simplifying the description, but do not indicate or imply that the devices or elements referred to must have a specific orientation, be constructed in a specific orientation, and be operated, and thus, should not be construed as limiting the present invention. Furthermore, the terms "first," "second," and the like are used merely to distinguish one description from another, and are not to be construed as indicating or implying relative importance.
Referring to fig. 1-8, a method for producing environment-friendly activated carbon, which uses an environment-friendly activated carbon production device comprising a box body 1, wherein a feeding funnel 101 is arranged above one end of the box body 1, a grinding and conveying part 2 is arranged below the funnel 101 of the box body 1, a control feeding part 3 is arranged below the rear side of the grinding and conveying part 2, a chemical treatment part 4 is arranged below the control feeding part 3, a separation part 5 is arranged in the direction of the feeding funnel 101 by the chemical treatment part 4, and a discharge port 102 is arranged on one side of the separation part 5.
The grinding and conveying component 2 comprises a first motor 201, the first motor 201 is fixed on one side of the box body 1 facing the discharge hole 102, a first linkage shaft 202 is arranged on the first motor 201 in a rotating mode towards the direction of the feeding hopper 101, a first gear 204 is fixedly arranged on one side, close to the first motor 201, of the first linkage shaft 202, a second linkage shaft 203 is arranged on the rear side of the first linkage shaft 202, the second linkage shaft 203 is connected to two sides of the box body 1 in a rotating mode, a second gear 205 is fixedly arranged on one side, close to the first motor 201, of the second linkage shaft 203, the second gear 205 is in meshing fit with the first gear 204, a first grinding wheel 206 is fixedly arranged on the first linkage shaft 202 in a direction away from the first gear 204, and a second grinding wheel 207 is fixedly arranged on the second linkage shaft 203 in a direction away from the second gear 205.
A first transmission shaft 211 is arranged below the second coupling shaft 203, one end of the first transmission wheel 208 is rotatably connected to one side of the box body 1 facing the first motor 201, a transmission guide plate 214 is arranged above the first transmission wheel 208, a second rotation shaft 212 is rotatably arranged below the middle of the transmission guide plate 214, a third rotation shaft 213 is arranged on the second rotation shaft 212 in a direction away from the first transmission shaft 211, the third rotation shaft 213 penetrates through the transmission guide plate 214 and is rotatably connected to one side of the box body facing the first motor 201, a first transmission wheel 208 is fixedly arranged on one end of the first rotation shaft 211 away from the first motor 201, the first transmission wheel 208 is in transmission fit with the second grinding wheel 207, a second transmission wheel 209 is fixedly arranged on one end of the second rotation shaft 212 facing the first transmission wheel 208, the second transmission wheel 209 is in transmission fit with the first transmission wheel 208, a transmission cam 210 is fixedly arranged on one end of the third rotation shaft 213 facing the second transmission wheel 209, and the transmission cam 210 is in transmission fit with the second transmission wheel 209.
The control feeding part 3 comprises a metering funnel 301, the metering funnel 301 is located below a third rotating shaft 213, a first baffle 302 is rotatably arranged on one side in the middle of the metering funnel 301, a first metering hydraulic device 304 is fixedly arranged below the first baffle 302, the metering funnel 301 is rotatably arranged in the direction away from the first baffle 302 and is provided with a second baffle 303, a second metering hydraulic device 305 is fixedly arranged below the second baffle 303, and an opening and closing device 306 is arranged at the bottom of the metering funnel 301.
Chemical treatment component 4 includes a chemical treatment section of thick bamboo 401, a chemical treatment section of thick bamboo 401 is located measurement funnel 301 below, a chemical treatment section of thick bamboo 401 is close to the upper end and is equipped with the sponge 402 that absorbs water below switching device 306, sponge 402 top one side that absorbs water is equipped with gas treatment device 403, it is equipped with lift filter 404 to slide in a chemical treatment section of thick bamboo 401 in the sponge 402 below that absorbs water, lift filter 404 below chemical treatment section of thick bamboo 401 bottom evenly is equipped with a plurality of heat conduction pieces 432, heat conduction piece 432 below is equipped with heating device 416 in a chemical treatment section of thick bamboo 401 below, heating device 416 below is equipped with heating energy source chamber 417.
A first hydraulic device 405 is arranged on the chemical treatment barrel 401 in the direction away from the gas treatment device 403, the first hydraulic device 405 is fixed on the box body 1, a distilled water barrel 407 is arranged below the first hydraulic device 405, a first piston rod 406 is arranged below the first hydraulic device 405, a first piston plate 408 is fixedly arranged on the first piston rod 406 passing through the lower end of the distilled water barrel 407, the first piston plate 408 is arranged in the distilled water barrel 407 in a sliding and sealing manner, a distilled water storage cavity 411 is arranged below the distilled water barrel 407, a distilled water inlet pipe 409 is connected between one side of the distilled water barrel 407 above the first piston plate 408 and the distilled water storage cavity 411, a distilled water outlet pipe 410 is connected between one side of the distilled water barrel 407 above the first piston plate 408 and the lower side of the water absorption sponge 402 in the chemical treatment barrel 401, a second hydraulic device 418 is arranged on one side of the chemical treatment barrel 401 away from the grinding and conveying component 2, the second hydraulic device 418 is fixed on the box body 1, a second piston rod 419 is arranged below the second hydraulic device 418, a hydrochloric acid cylinder 421 is arranged below the second piston rod 419, a second piston plate 420 is fixedly arranged on the second piston rod 419 through the lower end of the top of the hydrochloric acid cylinder 421, the second piston plate 420 is arranged in the hydrochloric acid cylinder 421 in a sliding sealing manner, a hydrochloric acid storage cavity 424 is arranged below the hydrochloric acid cylinder 421, a hydrochloric acid inlet pipe 422 is connected between the hydrochloric acid storage cavity 424 and the hydrochloric acid cylinder 421, a hydrochloric acid outlet pipe 423 is connected between the hydrochloric acid cylinder 421 and the chemical treatment cylinder 401, a third hydraulic device 425 is arranged in the chemical treatment cylinder 401 in the direction of the grinding and conveying part 2, the third hydraulic device 425 is fixed on the box body 1, a pressure plate 431 is arranged below the third hydraulic device 425, a third piston rod 426 is arranged below the pressure plate 431, an alkali solution cylinder 427 is arranged below the third piston rod 426, a third piston plate 430 is arranged on the third piston rod 426 through the lower end of the top of the alkali solution cylinder 427, and the third piston plate 430 is arranged in a sliding sealing manner in the alkali solution cylinder 427, an alkali solution storage cavity 436 is arranged below the alkali solution cylinder 427, an alkali solution inlet pipe 428 is connected between the alkali solution storage cavity 436 and the alkali solution cylinder 427, an alkali solution outlet pipe 429 is connected between the alkali solution cylinder 427 and the chemical treatment cylinder 401, two push rods 433 are arranged above the lifting filter plate 404 below the pressing plate 431, a stirrer 434 is arranged in the middle of the chemical treatment cylinder 401 near the bottom, a pH value test rod 435 is arranged on one side of the stirrer 434, a cooling cavity 414 is arranged on the periphery of the bottom of the chemical treatment cylinder 401, a first sewage outlet pipe 412 is connected between the cooling cavity 414 and the chemical treatment cylinder 401, and a sewage cavity 415 is arranged on one side, away from the distilled water storage cavity 411, of the heating energy cavity 417.
The separation part 5 comprises an active carbon absorption device 501, the active carbon absorption device 501 is positioned below the grinding and conveying part 2, a suction pipe 505 is connected between the grinding and conveying part 2 and the chemical treatment cylinder 401 above the water absorption sponge 402, a second motor 502 is fixedly arranged on one side, far away from the suction pipe 505, of the active carbon absorption device 501, a motor rotating shaft 503 is arranged in the direction towards the suction pipe 505 of the second motor 502, a rotating plate 504 is arranged in the direction towards the suction pipe 505 of the motor rotating shaft 503, a filter plate 506 is arranged in the direction towards the suction pipe 505 of the rotating plate 504, the filter plate 506 is fixed in the middle of the interior of the active carbon absorption device 501, an active carbon block cavity 507 is arranged below the direction towards the suction pipe 505 of the filter plate 506, and an active carbon powder cavity 508 is arranged below the filter plate 506 towards the direction towards the second motor 502 of the filter plate 506.
The production method of the environment-friendly active carbon specifically comprises the following steps:
s1 feed grind transfer: putting the walnut shells into a device, grinding the walnut shells into powder, and conveying to the next step;
s2 metered feed: weighing 5-10 g of the crushed powder and feeding the crushed powder into a chemical cylinder;
s3, heating and carbonizing: heating by a heating device to uniformly heat the walnut shell fragments, treating a large amount of gas and generated water until no gas is generated or the carbon particles are heated to red, closing the heating device, and treating according to the following steps after the chemical cylinder is cooled;
acid treatment of the S4 carbon pellets: adding 50mL of 2mol/L hydrochloric acid, heating and boiling for 15 minutes by using a heating device, neutralizing and discharging the solution in the cup, and pouring 50mL of 2mol/L hydrochloric acid and boiling for 15 minutes to remove impurities in the carbon particles; cooling, filtering, washing with distilled water for three times, boiling a clean chemical cylinder in a beaker containing 50mL of distilled water for 15 minutes, discarding the solution in the beaker, boiling with new distilled water for several times, checking with a pH bar, and making the aqueous solution acidic and neutral; filtering the solution containing the carbon particles;
s5 drying activated carbon: heating the filtered wet carbon granules, and continuously stirring until the carbon granules are completely baked, and cutting to avoid burning the carbon granules. Closing the heating device and cooling;
s6, separating the active carbon block powder: absorbing the activated carbon, and separating the activated carbon into block powder by filtration.
Principle of operation
The staff puts into box 1 through feed hopper 101 the walnut shell in, the walnut shell falls down to grind conveying unit 2 in, first motor 201 starts to drive first grinding miller 206 and second grinding miller 207 through first universal driving shaft 202 and second universal driving shaft 203 and rotates in opposite directions and smash the grinding effect to the walnut shell, the walnut shell after smashing falls down on conveying deflector 214, conveying deflector 214 is at first conveying wheel 208, second conveying wheel 209, the shake is carried out under the cooperation pivoted effect of conveying cam 210, walnut shell powder shake slope downwardly movement enters into in the control feeding unit 3.
The walnut shell powder is blocked by the first baffle 302 and the second baffle 303 in the control feeding part 3, and 5-10 g of walnut shell powder is controlled to fall into the chemical treatment cylinder 401 through the first metering hydraulic device 304 and the second metering hydraulic device 305.
The walnut shell bits and pieces get into in the chemical treatment section of thick bamboo 401 closing device 306 and close, heating device 416 heats, make walnut shell bits and pieces thermally equivalent through agitator 434, can see soon that the pipe wall is attached with water, flow on the sponge 402 that absorbs water when the volume is many, the mouth of pipe has a large amount of gas to escape and in time absorbed the processing by gas treatment device 403, the interior walnut shell bits and pieces carbonization gradually, heating device 416 can be closed to no longer producing gas or seeing the heating of charcoal granule to red-red, add water in cooling chamber 414 and carry out the cooling action, treat the chemical treatment section of thick bamboo 401 after the cooling.
Performing acid treatment on carbon granules, wherein the carbon granules rise for a certain distance on a lifting filter plate 404 under the matching action of a first hydraulic device 405, a second hydraulic device 418 and a third hydraulic device 425 and then descend, hydrochloric acid in a hydrochloric acid storage cavity 424 enters a hydrochloric acid cylinder 421 through a hydrochloric acid inlet pipe 422, then is pressed into a hydrochloric acid outlet pipe 423 by a second piston plate 420 and enters a chemical treatment cylinder 401, a 50mL2mol/L hydrochloric acid heating device 416 is added to heat the solution to be light yellow, the lifting filter plate 404 lifts the carbon granules above the hydrochloric acid solution, an alkali solution in an alkali solution storage cavity 436 enters an alkali solution cylinder 427 and then is pressed into the chemical treatment cylinder 401 for neutralization reaction, the solution after the neutralization reaction enters a cooling cavity 414 through a first sewage outlet pipe 412 to perform a cooling action, and then enters a sewage cavity 415 through a second sewage outlet pipe 413; the filter plate 404 was lifted down and boiled for 15 minutes by adding 50mL of 2mol/L hydrochloric acid to remove impurities from the carbon particles.
The lifting filter plate 404 lifts the carbon particles above the hydrochloric acid solution, the alkali solution in the alkali solution storage cavity 436 enters the alkali solution cylinder 427 and then is pressed into the chemical treatment cylinder 401 for neutralization reaction, the solution after the neutralization reaction enters the cooling cavity 414 through the first sewage outlet pipe 412 for cooling, and then enters the sewage cavity 415 through the second sewage outlet pipe 413; after the chemical treatment cylinder 401 is cooled, the lifting filter plate 404 descends, is added into a 50mL distilled water heating device 416 to be heated to boiling for 15 minutes, then is boiled by replacing new distilled water for several times, and a pH value test rod is used for starting the aqueous solution to show acidity and finally shows neutrality; the solution containing the carbon granules was filtered.
Discharging water in the chemical treatment cylinder 401, drying the carbon granules, heating by the heating device 416, uniformly heating by the stirrer 434 until the carbon granules are completely baked, and cutting to avoid burning the carbon granules; the heating device 416 is turned off for cooling.
The second motor 502 is started to suck the activated carbon into the activated carbon absorption device 501 through the suction pipe 505, the blocky activated carbon is blocked by the filter plate 506 and enters the activated carbon block chamber 507, the powdery activated carbon enters the activated carbon powder chamber 508 through the filter plate 506 to be treated, and the blocky activated carbon is taken out for use through the discharge port 102.
The above description is only an embodiment of the present invention, and not intended to limit the scope of the present invention, and all modifications of equivalent structures and equivalent processes, which are made by using the contents of the present specification and the accompanying drawings, or directly or indirectly applied to other related technical fields, are included in the scope of the present invention.

Claims (8)

1. The environment-friendly activated carbon production method adopts the following environment-friendly activated carbon production equipment, the environment-friendly activated carbon production equipment comprises a box body (1), the box body (1) is provided with a feeding funnel (101) above the position close to one end, the environment-friendly activated carbon production method is characterized in that the box body (1) is provided with a grinding conveying part (2) below the funnel (101), a control feeding part (3) is arranged below the rear side of the grinding conveying part (2), a chemical treatment part (4) is arranged below the control feeding part (3), the chemical treatment part (4) is provided with a separation part (5) towards the direction of the feeding funnel (101), and a discharge hole (102) is formed in one side of the separation part (5).
2. The method for producing environmentally friendly activated carbon according to claim 1, wherein: the grinding and conveying component (2) comprises a first motor (201), the first motor (201) is fixed on one side of the box body (1) towards the discharge hole (102), the first motor (201) is provided with a first linkage shaft (202) in a rotating way towards the direction of the feeding hopper (101), a first gear (204) is fixedly arranged on one side of the first linkage shaft (202) close to the first motor (201), a second linkage shaft (203) is arranged at the rear side of the first linkage shaft (202), the second linkage shaft (203) is rotatably connected to two sides of the box body (1), a second gear (205) is fixedly arranged on one side of the second linkage shaft (203) close to the first motor (201), the second gear (205) is meshed with the first gear (204), a first grinding wheel (206) is fixedly arranged on the first linkage shaft (202) in the direction away from the first gear (204), and a second grinding wheel (207) is fixedly arranged on the second linkage shaft (203) in the direction away from the second gear (205).
3. The method for producing environmentally friendly activated carbon according to claim 2, wherein: a first transmission shaft (211) is arranged below the second coupling shaft (203), one end of the first transmission wheel (208) is rotatably connected to one side of the box body (1) towards the first motor (201), a transmission guide plate (214) is arranged above the first transmission wheel (208), a second rotating shaft (212) is rotatably arranged below the middle of the transmission guide plate (214), the second rotating shaft (212) is far away from the first transmission shaft (211) and is provided with a third rotating shaft (213), the third rotating shaft (213) penetrates through the transmission guide plate (214) and is rotatably connected to one side of the box body towards the first motor (201), one end of the first rotating shaft (211) far away from the first motor (201) is fixedly provided with the first transmission wheel (208), the first transmission wheel (208) is in transmission fit with the second grinding wheel (207), and one end of the second rotating shaft (212) towards the first transmission wheel (208) is fixedly provided with the second transmission wheel (209), the second transmission wheel (209) is in transmission fit with the first transmission wheel (208), one end of the third rotating shaft (213) towards the second transmission wheel (209) is fixedly provided with a transmission cam (210), and the transmission cam (210) is in transmission fit with the second transmission wheel (209).
4. The method for producing environmentally friendly activated carbon according to claim 1, wherein: control feeding part (3) are including metering funnel (301), metering funnel (301) are located third axis of rotation (213) below, one side is rotated and is equipped with first baffle (302) in the middle of metering funnel (301), first baffle (302) below has set firmly first measurement hydraulic means (304), metering funnel (301) are kept away from first baffle (302) direction and are rotated and are equipped with second baffle (303), second baffle (303) below has set firmly second measurement hydraulic means (305), metering funnel (301) bottom is equipped with switching device (306).
5. The method for producing environmentally friendly activated carbon according to claim 1, wherein: chemical treatment part (4) are including chemical treatment section of thick bamboo (401), chemical treatment section of thick bamboo (401) are located measurement funnel (301) below, chemical treatment section of thick bamboo (401) are close to the upper end and are equipped with water absorption sponge (402) below switching device (306), water absorption sponge (402) top one side is equipped with gas treatment device (403), and it is equipped with lift filter (404) to slide in water absorption sponge (402) below chemical treatment section of thick bamboo (401), lift filter (404) below chemical treatment section of thick bamboo (401) bottom evenly is equipped with a plurality of heat conduction pieces (432), heat conduction piece (432) below is equipped with heating device (416) in chemical treatment section of thick bamboo (401) below, heating device (416) below is equipped with heating energy source chamber (417).
6. The method for producing environmentally friendly activated carbon according to claim 5, wherein: the chemical treatment tube (401) is far away from a gas treatment device (403) and is provided with a first hydraulic device (405), the first hydraulic device (405) is fixed on the box body (1), a distilled water tube (407) is arranged below the first hydraulic device (405), a first piston rod (406) is arranged below the first hydraulic device (405), a first piston plate (408) is fixedly arranged at the lower end of the first piston rod (406) penetrating through the distilled water tube (407), the first piston plate (408) is arranged in the distilled water tube (407) in a sliding sealing manner, a distilled water storage cavity (411) is arranged below the distilled water tube (407), a distilled water inlet tube (409) is connected between one side above the first piston plate (408) and the distilled water storage cavity (411) in the distilled water tube (407), and a distilled water outlet tube (410) is arranged between one side above the first piston plate (408) and the lower side of a water absorption sponge (402) in the chemical treatment tube (401) ) A second hydraulic device (418) is arranged on one side, away from the grinding and conveying component (2), of the chemical treatment cylinder (401), the second hydraulic device (418) is fixed on the box body (1), a second piston rod (419) is arranged below the second hydraulic device (418), a hydrochloric acid cylinder (421) is arranged below the second piston rod (419), the second piston rod (419) penetrates through the lower end of the top of the hydrochloric acid cylinder (421), a second piston plate (420) is fixedly arranged on the lower end of the top of the hydrochloric acid cylinder (421), the second piston plate (420) is arranged in the hydrochloric acid cylinder (421) in a sliding and sealing manner, a hydrochloric acid storage cavity (424) is arranged below the hydrochloric acid cylinder (421), a hydrochloric acid inlet pipe (422) is connected between the hydrochloric acid storage cavity (424) and the hydrochloric acid cylinder (421), a hydrochloric acid outlet pipe (423) is connected between the hydrochloric acid cylinder (421) and the chemical treatment cylinder (401), and a third hydraulic device (425) is arranged on the chemical treatment cylinder (401) in the direction of the grinding and conveying component (2), the third hydraulic device (425) is fixed on the box body (1), a pressure plate (431) is arranged below the third hydraulic device (425), a third piston rod (426) is arranged below the pressure plate (431), an alkali solution barrel (427) is arranged below the third piston rod (426), a third piston plate (430) is arranged at the lower end of the top of the alkali solution barrel (427) through the third piston rod (426), the third piston plate (430) is arranged in the alkali solution barrel (427) in a sliding and sealing manner, an alkali solution storage cavity (436) is arranged below the alkali solution barrel (427), an alkali solution inlet pipe (428) is connected between the alkali solution storage cavity (436) and the alkali solution barrel (427), an alkali solution outlet pipe (429) is connected between the alkali solution barrel (427) and the chemical treatment barrel (401), two push rods (433) are arranged above the lifting filter plate (404) below the pressure plate (431), be equipped with agitator (434) near the bottom in the middle of chemical treatment section of thick bamboo (401), agitator (434) one side is equipped with pH value test stick (435), chemical treatment section of thick bamboo (401) bottom periphery is equipped with cooling chamber (414), it is equipped with first sewage outlet pipe (412) to connect between cooling chamber (414) and the chemical treatment section of thick bamboo (401), heating energy source chamber (417) are kept away from distilled water and are stored chamber (411) one side and be equipped with sewage chamber (415).
7. The method for producing environmentally friendly activated carbon according to claim 1, wherein: the separation part (5) comprises an activated carbon absorption device (501), the activated carbon absorption device (501) is positioned below the grinding and conveying part (2), a suction pipe (505) is connected between the grinding and conveying part (2) and the chemical treatment cylinder (401) above the water absorption sponge (402), a second motor (502) is fixedly arranged on one side of the activated carbon absorption device (501) far away from the suction pipe (505), the second motor (502) is provided with a motor rotating shaft (503) towards the suction pipe (505), a rotating plate (504) is arranged on the rotating shaft (503) of the motor towards the suction pipe (505), the rotating plate (504) is provided with a filter plate (506) towards the suction pipe (505), the filter plate (506) is fixed in the middle inside the activated carbon absorption device (501), an activated carbon block cavity (507) is arranged below the filter plate (506) towards the suction pipe (505), and an activated carbon powder cavity (508) is arranged below the filter plate (506) towards the direction of the second motor (502).
8. The method for producing environmentally friendly activated carbon according to claim 1, wherein: the production method of the environment-friendly active carbon specifically comprises the following steps:
s1 feed grind transfer: putting the walnut shells into a device, grinding the walnut shells into powder, and conveying to the next step;
s2 metered feed: weighing 5-10 g of the crushed powder and feeding the crushed powder into a chemical cylinder;
s3, heating and carbonizing: heating by a heating device to uniformly heat the walnut shell fragments, treating a large amount of gas and generated water until no gas is generated or the carbon particles are heated to red, closing the heating device, and treating according to the following steps after the chemical cylinder is cooled;
acid treatment of the S4 carbon pellets: adding 50mL of 2mol/L hydrochloric acid, heating and boiling for 15 minutes by using a heating device, neutralizing and discharging the solution in the cup, and pouring 50mL of 2mol/L hydrochloric acid and boiling for 15 minutes to remove impurities in the carbon particles; cooling, filtering, washing with distilled water for three times, boiling a clean chemical cylinder in a beaker containing 50mL of distilled water for 15 minutes, discarding the solution in the beaker, boiling with new distilled water for several times, checking with a pH bar, and making the aqueous solution acidic and neutral; filtering the solution containing the carbon particles;
s5 drying activated carbon: heating the filtered wet carbon granules, continuously stirring until the carbon granules are completely baked, cutting off the carbon granules to burn, closing the heating device, and cooling;
s6, separating the active carbon block powder: absorbing the activated carbon, and separating the activated carbon into block powder by filtration.
CN202110895403.7A 2021-08-05 2021-08-05 Production method of environment-friendly activated carbon Withdrawn CN113548663A (en)

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Application Number Priority Date Filing Date Title
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114477177A (en) * 2022-03-04 2022-05-13 吉彩霞 Wooden columnar activated carbon production equipment
CN114920244A (en) * 2022-05-19 2022-08-19 王东营 Reaction box for activated carbon acidification treatment

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114477177A (en) * 2022-03-04 2022-05-13 吉彩霞 Wooden columnar activated carbon production equipment
CN114920244A (en) * 2022-05-19 2022-08-19 王东营 Reaction box for activated carbon acidification treatment
CN114920244B (en) * 2022-05-19 2024-03-05 深圳佰利安环保科技有限公司 Active carbon acidizing reaction box

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Application publication date: 20211026