CN111419726A - Plant dried orange peel tobacco-flavored oral cavity atomized liquid and preparation method thereof - Google Patents
Plant dried orange peel tobacco-flavored oral cavity atomized liquid and preparation method thereof Download PDFInfo
- Publication number
- CN111419726A CN111419726A CN202010361196.2A CN202010361196A CN111419726A CN 111419726 A CN111419726 A CN 111419726A CN 202010361196 A CN202010361196 A CN 202010361196A CN 111419726 A CN111419726 A CN 111419726A
- Authority
- CN
- China
- Prior art keywords
- oral cavity
- atomized liquid
- orange peel
- dried orange
- plant
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000007788 liquid Substances 0.000 title claims abstract description 80
- 210000000214 mouth Anatomy 0.000 title claims abstract description 70
- 238000002360 preparation method Methods 0.000 title claims description 16
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 47
- 241000196324 Embryophyta Species 0.000 claims abstract description 45
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 45
- 235000006679 Mentha X verticillata Nutrition 0.000 claims abstract description 34
- 235000002899 Mentha suaveolens Nutrition 0.000 claims abstract description 34
- 235000001636 Mentha x rotundifolia Nutrition 0.000 claims abstract description 34
- 239000000796 flavoring agent Substances 0.000 claims abstract description 32
- 235000019634 flavors Nutrition 0.000 claims abstract description 29
- 239000002994 raw material Substances 0.000 claims abstract description 29
- 235000020682 bottled natural mineral water Nutrition 0.000 claims abstract description 28
- 239000003205 fragrance Substances 0.000 claims abstract description 28
- 235000019804 chlorophyll Nutrition 0.000 claims abstract description 21
- 229930002875 chlorophyll Natural products 0.000 claims abstract description 21
- ATNHDLDRLWWWCB-AENOIHSZSA-M chlorophyll a Chemical compound C1([C@@H](C(=O)OC)C(=O)C2=C3C)=C2N2C3=CC(C(CC)=C3C)=[N+]4C3=CC3=C(C=C)C(C)=C5N3[Mg-2]42[N+]2=C1[C@@H](CCC(=O)OC\C=C(/C)CCC[C@H](C)CCC[C@H](C)CCCC(C)C)[C@H](C)C2=C5 ATNHDLDRLWWWCB-AENOIHSZSA-M 0.000 claims abstract description 21
- 241001116389 Aloe Species 0.000 claims abstract description 19
- 244000228451 Stevia rebaudiana Species 0.000 claims abstract description 19
- 235000011399 aloe vera Nutrition 0.000 claims abstract description 19
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical class CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 claims abstract description 17
- 244000223014 Syzygium aromaticum Species 0.000 claims abstract description 14
- 235000016639 Syzygium aromaticum Nutrition 0.000 claims abstract description 14
- HELXLJCILKEWJH-NCGAPWICSA-N rebaudioside A Chemical compound O([C@H]1[C@H](O)[C@@H](CO)O[C@H]([C@@H]1O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O HELXLJCILKEWJH-NCGAPWICSA-N 0.000 claims abstract description 11
- 240000004510 Agastache rugosa Species 0.000 claims abstract description 6
- 244000062241 Kaempferia galanga Species 0.000 claims abstract description 5
- 235000013421 Kaempferia galanga Nutrition 0.000 claims abstract description 5
- 235000000177 Indigofera tinctoria Nutrition 0.000 claims abstract description 3
- 229940097275 indigo Drugs 0.000 claims abstract description 3
- COHYTHOBJLSHDF-UHFFFAOYSA-N indigo powder Natural products N1C2=CC=CC=C2C(=O)C1=C1C(=O)C2=CC=CC=C2N1 COHYTHOBJLSHDF-UHFFFAOYSA-N 0.000 claims abstract description 3
- 241000208125 Nicotiana Species 0.000 claims description 42
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 30
- 238000000034 method Methods 0.000 claims description 20
- 238000003756 stirring Methods 0.000 claims description 20
- QQILFGKZUJYXGS-UHFFFAOYSA-N Indigo dye Chemical compound C1=CC=C2C(=O)C(C3=C(C4=CC=CC=C4N3)O)=NC2=C1 QQILFGKZUJYXGS-UHFFFAOYSA-N 0.000 claims description 16
- 235000003599 food sweetener Nutrition 0.000 claims description 16
- 239000000243 solution Substances 0.000 claims description 16
- 239000003765 sweetening agent Substances 0.000 claims description 16
- 241001529821 Agastache Species 0.000 claims description 15
- 239000011521 glass Substances 0.000 claims description 15
- 238000005303 weighing Methods 0.000 claims description 15
- 235000002722 Dioscorea batatas Nutrition 0.000 claims description 13
- 235000006536 Dioscorea esculenta Nutrition 0.000 claims description 13
- 240000001811 Dioscorea oppositifolia Species 0.000 claims description 13
- 235000003416 Dioscorea oppositifolia Nutrition 0.000 claims description 13
- 230000001954 sterilising effect Effects 0.000 claims description 11
- 241001162994 Rugosus Species 0.000 claims description 10
- UEDUENGHJMELGK-HYDKPPNVSA-N Stevioside Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O UEDUENGHJMELGK-HYDKPPNVSA-N 0.000 claims description 10
- 238000009835 boiling Methods 0.000 claims description 10
- OSVXSBDYLRYLIG-UHFFFAOYSA-N dioxidochlorine(.) Chemical compound O=Cl=O OSVXSBDYLRYLIG-UHFFFAOYSA-N 0.000 claims description 10
- 239000003814 drug Substances 0.000 claims description 10
- 229940013618 stevioside Drugs 0.000 claims description 10
- OHHNJQXIOPOJSC-UHFFFAOYSA-N stevioside Natural products CC1(CCCC2(C)C3(C)CCC4(CC3(CCC12C)CC4=C)OC5OC(CO)C(O)C(O)C5OC6OC(CO)C(O)C(O)C6O)C(=O)OC7OC(CO)C(O)C(O)C7O OHHNJQXIOPOJSC-UHFFFAOYSA-N 0.000 claims description 10
- 235000019202 steviosides Nutrition 0.000 claims description 10
- 239000011550 stock solution Substances 0.000 claims description 10
- 239000000341 volatile oil Substances 0.000 claims description 10
- 238000001816 cooling Methods 0.000 claims description 9
- 235000006092 Stevia rebaudiana Nutrition 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 8
- 241000628997 Flos Species 0.000 claims description 6
- 239000012535 impurity Substances 0.000 claims description 6
- 238000004659 sterilization and disinfection Methods 0.000 claims description 6
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 5
- 241000345998 Calamus manan Species 0.000 claims description 5
- 239000004155 Chlorine dioxide Substances 0.000 claims description 5
- 238000000889 atomisation Methods 0.000 claims description 5
- 235000019398 chlorine dioxide Nutrition 0.000 claims description 5
- 230000001877 deodorizing effect Effects 0.000 claims description 5
- 230000000249 desinfective effect Effects 0.000 claims description 5
- 238000000605 extraction Methods 0.000 claims description 5
- 238000011049 filling Methods 0.000 claims description 5
- 239000003456 ion exchange resin Substances 0.000 claims description 5
- 229920003303 ion-exchange polymer Polymers 0.000 claims description 5
- 238000004806 packaging method and process Methods 0.000 claims description 5
- 238000009928 pasteurization Methods 0.000 claims description 5
- 238000001556 precipitation Methods 0.000 claims description 5
- 239000012716 precipitator Substances 0.000 claims description 5
- 235000012950 rattan cane Nutrition 0.000 claims description 5
- 210000000582 semen Anatomy 0.000 claims description 5
- 238000000926 separation method Methods 0.000 claims description 5
- 238000003860 storage Methods 0.000 claims description 5
- 238000003809 water extraction Methods 0.000 claims description 5
- 238000009472 formulation Methods 0.000 claims description 2
- 238000007789 sealing Methods 0.000 claims 1
- 241000894006 Bacteria Species 0.000 abstract description 7
- 230000000694 effects Effects 0.000 abstract description 6
- 235000019640 taste Nutrition 0.000 abstract description 4
- 235000019658 bitter taste Nutrition 0.000 abstract description 2
- 238000009395 breeding Methods 0.000 abstract description 2
- 230000001488 breeding effect Effects 0.000 abstract description 2
- 244000061176 Nicotiana tabacum Species 0.000 abstract 3
- 230000002035 prolonged effect Effects 0.000 abstract 1
- 239000000047 product Substances 0.000 description 21
- 241000010428 Alpinia katsumadae Species 0.000 description 3
- 244000060696 Alpinia speciosa Species 0.000 description 3
- 235000013411 Alpinia speciosa Nutrition 0.000 description 3
- 206010006326 Breath odour Diseases 0.000 description 3
- 235000009508 confectionery Nutrition 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 206010012335 Dependence Diseases 0.000 description 2
- 208000032139 Halitosis Diseases 0.000 description 2
- 206010062717 Increased upper airway secretion Diseases 0.000 description 2
- 239000012263 liquid product Substances 0.000 description 2
- 208000026435 phlegm Diseases 0.000 description 2
- 230000000391 smoking effect Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 150000003568 thioethers Chemical class 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 241000675108 Citrus tangerina Species 0.000 description 1
- 206010010774 Constipation Diseases 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 208000002399 aphthous stomatitis Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 230000001680 brushing effect Effects 0.000 description 1
- 230000005802 health problem Effects 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 230000002147 killing effect Effects 0.000 description 1
- 231100000053 low toxicity Toxicity 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 230000007310 pathophysiology Effects 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 235000019605 sweet taste sensations Nutrition 0.000 description 1
- 230000001225 therapeutic effect Effects 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/046—Aerosols; Foams
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4926—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having six membered rings
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/87—Application Devices; Containers; Packaging
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Emergency Medicine (AREA)
- Dermatology (AREA)
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Oral & Maxillofacial Surgery (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses plant dried orange peel tobacco flavor type oral cavity atomized liquid which comprises the following components in percentage by mass: natural mineral water: 48-59%, nicotine salt 2-4%, mint: 4-6%, ethanol: 3-5%, dried leaves of stevia: 1-3%, wrinkled giant hyssop: 2-4%, aloe: 8-10%, chlorophyll: 6-8%, natural indigo: 1-2%, katsumade galangal seed: 1-1.5%, dried orange peel: 2-4% and clove: 1 to 1.5 percent. The plant dried orange peel tobacco fragrance type oral cavity atomized liquid is packaged by the atomizing bottle, so that people can conveniently carry the atomized liquid, the peculiar smell of the oral cavity can be inhibited to the greatest extent by adding the raw materials such as wrinkled giant hyssop, chlorophyll and dried orange peel, the ethanol has a certain effect of eliminating bacteria, the breeding speed of the bacteria is slowed down, the refreshing and maintaining time of the oral cavity all day is effectively prolonged, the taste of the plant dried orange peel tobacco fragrance type oral cavity atomized liquid is improved by adding the vine fragrance type edible essence, and the bitter taste of some raw materials can be effectively covered.
Description
Technical Field
The invention relates to the technical field of atomized liquid, in particular to plant pericarpium citri reticulatae tobacco flavor type oral atomized liquid and a preparation method thereof.
Background
The oral odor is always a great trouble for some people, and for some patients with bad oral hygiene and bacteria, the oral odor can appear in the oral cavity, mainly because the bacteria are decomposed and fermented in the oral cavity and secrete substances with the oral odor, when people handle the oral odor, other effective and convenient modes are difficult to be provided except for frequent tooth brushing or medical treatment, and the people are very inconvenient for the people suffering from the oral odor.
Particularly for some smokers, how to relieve the smoking addiction, reduce the intake of nicotine and tar, and keep the oral health and fresh for a long time is a problem which needs to be solved urgently at present; most of oral cavity atomized liquid products on the market at present have the advantages of better taste and poor experience, and the oral cavity health problem still exists after the oral cavity atomized liquid products are used. Therefore, the plant tangerine peel and tobacco flavor type oral cavity atomized liquid and the preparation method thereof are provided.
Disclosure of Invention
Based on the technical problems in the background art, the invention provides plant pericarpium citri reticulatae tobacco flavor type oral cavity atomized liquid and a preparation method thereof.
The invention provides a plant dried orange peel tobacco fragrance type oral cavity atomized liquid and a preparation method thereof, wherein the oral cavity atomized liquid comprises the following components in percentage by mass: natural mineral water: 48-59%, nicotine salt 2-4%, dried orange peel: 2-4%, mint: 4-6%, ethanol: 3-5%, dried leaves of stevia: 1-3%, wrinkled giant hyssop: 2-4%, aloe: 8-10%, chlorophyll: 6-8%, natural indigo: 1-2%, katsumade galangal seed: 1-1.5%, clove: 1-1.5% of vine flavor edible essence: 6-8% of Chinese yam: 3 to 5 percent.
Preferably, the composition comprises the following components in percentage by mass: natural mineral water: 49% of nicotine salt: 3%, dried orange peel: 3% and mint: 5% and ethanol: 4%, dried leaves of stevia: 2%, agastache rugosus: 3% of aloe: 9% of chlorophyll: 7% and indigo naturalis: 1.5%, katsumade galangal seed 1.3%, clove: 1.2% and rattan-flavored edible essence: 7% and Chinese yam: 4 percent.
The preparation method comprises the following steps:
s1: raw material selection and pretreatment: directly obtaining high-quality natural mineral water from natural mountain spring, sterilizing natural mineral water with chlorine dioxide, and directly purchasing herba Menthae, ethanol, sweet stevia dry leaf, herba Agastaches, Aloe, chlorophyll, indigo naturalis, semen Alpinia zerumbet, pericarpium Citri Tangerinae, flos Caryophylli, caulis et folium Gaultheriae Yunnanensis edible essence, and rhizoma Dioscoreae.
S2: preparing a primary raw material: weighing a certain amount of dry stevia rebaudiana leaves, adopting a water extraction and alcohol precipitation method, removing impurities, decoloring and deodorizing the obtained solution by using a precipitator and ion exchange resin, recrystallizing the obtained solution by using methanol solution with a certain volume fraction and a certain concentration to obtain a pure stevioside white crystalline sweetener, then weighing a certain amount of mint, and performing subcritical low-temperature extraction on the mint to obtain mint essential oil.
S3: preparing a secondary raw material: and (3) quantitatively weighing the raw material in the S1, the stevioside white crystalline sweetener prepared in the S2 and the mint essential oil by using an electronic scale according to a required proportion in a sterile environment, and ensuring that the ratio reaches an expected standard.
S4: preparing stock solution: preparing a decocting pot, adding the natural mineral water weighed in the step S3 into the decocting pot for preheating, and after preheating for a period of time, putting the mint, the agastache rugosus, the aloe, the chlorophyll, the indigo naturalis, the katsumadai seed, the dried orange peel, the clove and the Chinese yam into the decocting pot to be decocted together with the natural mineral water to obtain the liquid medicine A.
S5: preparing a finished product liquid: and (4) after S4 is finished, injecting the liquid medicine A in S4 into a stirring pot, then adding the ethanol, the nicotine salt, the sweetening agent and the rattan flavor edible essence weighed in S3, stirring, naturally cooling the mixture in the stirring process, and obtaining the finished product of the plant dried orange peel tobacco flavor oral cavity atomized liquid B after a period of time.
S6: and (3) disinfecting and storing the finished liquid: and (3) performing final sterilization on the finished product plant pericarpium citri reticulatae tobacco fragrance type oral cavity atomized liquid B by a pasteurization method, and then filling the finished product plant pericarpium citri reticulatae tobacco fragrance type oral cavity atomized liquid B into a total glass container and hermetically storing the total glass container.
S7: bottle separation and packaging: and (4) selecting an aseptic atomizing bottle, and injecting the finished product plant dried orange peel tobacco fragrance type oral cavity atomizing liquid B in the total glass container in the S6 into the atomizing bottle, so that the oral cavity atomizing liquid B can be normally used.
Preferably, in the S2, the volume fraction of methanol is 90%.
Preferably, in the step S4, the boiling temperature during the preparation of the stock solution is controlled at 105-113 ℃, and the boiling time is 45-60 min.
Preferably, in S5, the stirring time between the raw materials is 10-15min, and the natural cooling time is 80-110 min.
Preferably, in S6, the finished product plant pericarpium citri reticulatae tobacco flavor oral cavity atomized liquid B needs to be stored away from light, and the storage environment temperature is 20-30 ℃.
Preferably, in the S7, the capacity of the selected atomization bottle is 60 ml.
Discussion of the formulation:
the water phase of the natural mineral substance is purer than that of the traditional water, so that the purity of the atomized liquid is improved; the dried orange peel can reduce phlegm, and further has a certain inhibition effect on oral peculiar smell; the stem leaves on the mint have special fragrance, can be used for improving the peculiar smell of the oral cavity, also has the effects of clearing and benefiting the throat, and can further reduce the influence of thick phlegm impurities in the throat on the peculiar smell of the oral cavity; the ethanol can kill more bacteria and harmful fungi brought by residual residues in the oral cavity; the sweetener prepared from the dry leaves of the stevia rebaudiana can bring sweet taste to patients, and reduce the uncomfortable taste experience of the patients in use; the agastache rugosus has a sterilization function, and can further inhibit and eliminate the peculiar smell in the oral cavity when being sprayed to the oral cavity; the aloe has the functions of clearing away heat and toxic material and removing blood stasis, and can clear the bowels to relieve constipation and inhibit the condition of bad breath caused by pathophysiology; the chlorophyll can inhibit sulfides generated in the metabolic process of a human body, and can further well eliminate the peculiar smell of the oral cavity by reducing the generation of the sulfides; indigo naturalis can have certain therapeutic effect on aphtha; the katsumadai seed has the main effects of promoting the circulation of qi and relieving pain, and emits natural fragrance to make people feel comfortable after smelling; flos Caryophylli has effects of descending qi and lowering adverse qi, and can be used for relieving halitosis; the Chinese yam has certain effect of relieving halitosis like clove; the vine-flavored edible essence can bring certain fragrance to the spray, and the use experience of a patient is improved.
The invention has the beneficial effects that: the plant dried orange peel tobacco fragrance type oral cavity atomized liquid is packaged by the atomizing bottle, so that people can conveniently carry the atomized liquid, nicotine salt with low toxicity is added to relieve the smoking addiction of users, the peculiar smell of oral cavities can be inhibited to the greatest extent by the added raw materials such as wrinkled giant hyssop, chlorophyll and dried orange peel, ethanol has a certain killing effect on bacteria, the breeding speed of the bacteria is slowed down, the refreshing maintenance duration of the oral cavities all day is effectively improved, the taste of the plant dried orange peel tobacco fragrance type oral cavity atomized liquid is improved by the addition of the vine fragrance type edible essence, and the bitter taste of some raw materials can be effectively covered.
Detailed Description
The present invention will be further illustrated with reference to the following specific examples.
Example 1
The embodiment provides a plant dried orange peel tobacco flavor type oral cavity atomized liquid and a preparation method thereof, and the oral cavity atomized liquid comprises the following components in percentage by mass: natural mineral water: 59% of nicotine salt: 2%, dried orange peel: 4%, mint: 2% and ethanol: 3%, dried leaves of stevia: 1% and agastache rugosus: 2% and aloe: 8% of chlorophyll: 6% and indigo naturalis: 1%, alpinia katsumadai: 1% and dried orange peel: 2% and clove: 1% of vine-flavor edible essence: 6% and Chinese yam: 3 percent;
the manufacturing method comprises the following steps:
s1: raw material selection and pretreatment: directly obtaining high-quality natural mineral water from natural spring, sterilizing natural mineral water with chlorine dioxide, and directly purchasing nicotine salt, pericarpium Citri Tangerinae, herba Menthae, ethanol, dried leaves of stevia rebaudiana Bertoni, herba Agastaches, Aloe, chlorophyll, indigo naturalis, semen Alpiniae, flos Caryophylli, caulis et folium Gaultheriae Yunnanensis edible essence, and rhizoma Dioscoreae.
S2: preparing a primary raw material: weighing a certain amount of dry stevia rebaudiana leaves, adopting a water extraction and alcohol precipitation method, removing impurities, decoloring and deodorizing the obtained solution by using a precipitator and ion exchange resin, recrystallizing the obtained solution by using methanol solution with a certain volume fraction and a certain concentration to obtain a pure stevioside white crystalline sweetener, then weighing a certain amount of mint, and performing subcritical low-temperature extraction on the mint to obtain mint essential oil.
S3: preparing a secondary raw material: and (3) quantitatively weighing the raw material in the S1, the stevioside white crystalline sweetener prepared in the S2 and the mint essential oil by using an electronic scale according to a required proportion in a sterile environment, and ensuring that the ratio reaches an expected standard.
S4: preparing stock solution: preparing a decocting pot, adding the natural mineral water weighed in the step S3 into the decocting pot for preheating, and after preheating for a period of time, putting the dried orange peel, the mint, the agastache rugosus, the aloe, the chlorophyll, the indigo naturalis, the katsumadai seed, the clove and the Chinese yam into the decocting pot to be decocted together with the natural mineral water to obtain the liquid medicine A.
S5: preparing a finished product liquid: and (4) after S4 is finished, injecting the liquid medicine A in S4 into a stirring pot, then adding the ethanol, the nicotine salt, the sweetening agent and the rattan flavor edible essence weighed in S3, stirring, naturally cooling the mixture in the stirring process, and obtaining the finished product of the plant dried orange peel tobacco flavor oral cavity atomized liquid B after a period of time.
S6: and (3) disinfecting and storing the finished liquid: and (3) performing final sterilization on the finished product plant pericarpium citri reticulatae tobacco fragrance type oral cavity atomized liquid B by a pasteurization method, and then filling the finished product plant pericarpium citri reticulatae tobacco fragrance type oral cavity atomized liquid B into a total glass container and hermetically storing the total glass container.
S7: bottle separation and packaging: and (4) selecting an aseptic atomizing bottle, and injecting the finished product plant dried orange peel tobacco fragrance type oral cavity atomizing liquid B in the total glass container in the S6 into the atomizing bottle, so that the oral cavity atomizing liquid B can be normally used.
In S2, the volume fraction of methanol is 90%; s4, controlling the boiling temperature of the stock solution during preparation to be 105 ℃, and keeping the boiling time to be 45 min; in S5, the stirring time among the raw materials is 10min, and the natural cooling time is 80 min; in S6, the finished plant pericarpium citri reticulatae tobacco fragrance type oral cavity atomized liquid B needs to be stored in a dark place, and the storage environment temperature is 20-30 ℃; in S7, the capacity of the selected atomization bottle is 60 ml.
Example 2
The embodiment provides a plant dried orange peel tobacco flavor type oral cavity atomized liquid and a preparation method thereof, and the oral cavity atomized liquid comprises the following components in percentage by mass: natural mineral water: 56%, nicotine salt: 3%, dried orange peel: 5%, mint: 3% and ethanol: 3%, dried leaves of stevia: 1.5%, wrinkled giant hyssop: 2% and aloe: 8.5%, chlorophyll: 6% and indigo naturalis: 1.5%, Alpinia katsumadai: 1% and dried orange peel: 2.5%, clove: 1% of vine-flavor edible essence: 6% and Chinese yam: 3.5 percent;
the manufacturing method comprises the following steps:
s1: raw material selection and pretreatment: directly obtaining high-quality natural mineral water from natural mountain spring, sterilizing natural mineral water with chlorine dioxide, and directly purchasing herba Menthae, ethanol, sweet stevia dry leaf, herba Agastaches, Aloe, chlorophyll, indigo naturalis, semen Alpinia zerumbet, pericarpium Citri Tangerinae, flos Caryophylli, caulis et folium Gaultheriae Yunnanensis edible essence, and rhizoma Dioscoreae.
S2: preparing a primary raw material: weighing a certain amount of dry stevia rebaudiana leaves, adopting a water extraction and alcohol precipitation method, removing impurities, decoloring and deodorizing the obtained solution by using a precipitator and ion exchange resin, recrystallizing the obtained solution by using methanol solution with a certain volume fraction and a certain concentration to obtain a pure stevioside white crystalline sweetener, then weighing a certain amount of mint, and performing subcritical low-temperature extraction on the mint to obtain mint essential oil.
S3: preparing a secondary raw material: and (3) quantitatively weighing the raw material in the S1, the stevioside white crystalline sweetener prepared in the S2 and the mint essential oil by using an electronic scale according to a required proportion in a sterile environment, and ensuring that the ratio reaches an expected standard.
S4: preparing stock solution: preparing a decocting pot, adding the natural mineral water weighed in the step S3 into the decocting pot for preheating, and after preheating for a period of time, putting the dried orange peel, the mint, the agastache rugosus, the aloe, the chlorophyll, the indigo naturalis, the katsumadai seed, the clove and the Chinese yam into the decocting pot to be decocted together with the natural mineral water to obtain the liquid medicine A.
S5: preparing a finished product liquid: and (4) after S4 is finished, injecting the liquid medicine A in S4 into a stirring pot, then adding the ethanol, the nicotine salt, the sweetening agent and the rattan flavor edible essence weighed in S3, stirring, naturally cooling the mixture in the stirring process, and obtaining the finished product of the plant dried orange peel tobacco flavor oral cavity atomized liquid B after a period of time.
S6: and (3) disinfecting and storing the finished liquid: and (3) performing final sterilization on the finished product plant pericarpium citri reticulatae tobacco fragrance type oral cavity atomized liquid B by a pasteurization method, and then filling the finished product plant pericarpium citri reticulatae tobacco fragrance type oral cavity atomized liquid B into a total glass container and hermetically storing the total glass container.
S7: bottle separation and packaging: and (4) selecting an aseptic atomizing bottle, and injecting the finished product plant dried orange peel tobacco fragrance type oral cavity atomizing liquid B in the total glass container in the S6 into the atomizing bottle, so that the oral cavity atomizing liquid B can be normally used.
In S2, the volume fraction of methanol is 90%; s4, controlling the boiling temperature of the stock solution during preparation to be 109 ℃, and keeping the boiling time to be 50 min; in S5, the stirring time among the raw materials is 10min, and the natural cooling time is 90 min; in S6, the finished plant pericarpium citri reticulatae tobacco fragrance type oral cavity atomized liquid B needs to be stored in a dark place, and the storage environment temperature is 20-30 ℃; in S7, the capacity of the selected atomization bottle is 60 ml.
EXAMPLE III
The embodiment provides a plant dried orange peel tobacco flavor type oral cavity atomized liquid and a preparation method thereof, and the oral cavity atomized liquid comprises the following components in percentage by mass: natural mineral water: 50.5%, nicotine salt: 4%, dried orange peel: 6%, mint: 4% and ethanol: 3.5%, dried leaves of stevia: 2%, agastache rugosus: 2.5%, aloe: 9% of chlorophyll: 7% and indigo naturalis: 1.5%, Alpinia katsumadai: 1% and dried orange peel: 3.5%, clove: 1% of vine-flavor edible essence: 6.5% and Chinese yam: 3.5 percent;
the manufacturing method comprises the following steps:
s1: raw material selection and pretreatment: directly obtaining high-quality natural mineral water from natural mountain spring, sterilizing natural mineral water with chlorine dioxide, and directly purchasing herba Menthae, ethanol, sweet stevia dry leaf, herba Agastaches, Aloe, chlorophyll, indigo naturalis, semen Alpinia zerumbet, pericarpium Citri Tangerinae, flos Caryophylli, caulis et folium Gaultheriae Yunnanensis edible essence, and rhizoma Dioscoreae.
S2: preparing a primary raw material: weighing a certain amount of dry stevia rebaudiana leaves, adopting a water extraction and alcohol precipitation method, removing impurities, decoloring and deodorizing the obtained solution by using a precipitator and ion exchange resin, recrystallizing the obtained solution by using methanol solution with a certain volume fraction and a certain concentration to obtain a pure stevioside white crystalline sweetener, then weighing a certain amount of mint, and performing subcritical low-temperature extraction on the mint to obtain mint essential oil.
S3: preparing a secondary raw material: and (3) quantitatively weighing the raw material in the S1, the stevioside white crystalline sweetener prepared in the S2 and the mint essential oil by using an electronic scale according to a required proportion in a sterile environment, and ensuring that the ratio reaches an expected standard.
S4: preparing stock solution: preparing a decocting pot, adding the natural mineral water weighed in the step S3 into the decocting pot for preheating, and after preheating for a period of time, putting the dried orange peel, the mint, the agastache rugosus, the aloe, the chlorophyll, the indigo naturalis, the katsumadai seed, the clove and the Chinese yam into the decocting pot to be decocted together with the natural mineral water to obtain the liquid medicine A.
S5: preparing a finished product liquid: and (4) after S4 is finished, injecting the liquid medicine A in S4 into a stirring pot, then adding the ethanol, the nicotine salt, the sweetening agent and the rattan flavor edible essence weighed in S3, stirring, naturally cooling the mixture in the stirring process, and obtaining the finished product of the plant dried orange peel tobacco flavor oral cavity atomized liquid B after a period of time.
S6: and (3) disinfecting and storing the finished liquid: and (3) performing final sterilization on the finished product plant pericarpium citri reticulatae tobacco fragrance type oral cavity atomized liquid B by a pasteurization method, and then filling the finished product plant pericarpium citri reticulatae tobacco fragrance type oral cavity atomized liquid B into a total glass container and hermetically storing the total glass container.
S7: bottle separation and packaging: and (4) selecting an aseptic atomizing bottle, and injecting the finished product plant dried orange peel tobacco fragrance type oral cavity atomizing liquid B in the total glass container in the S6 into the atomizing bottle, so that the oral cavity atomizing liquid B can be normally used.
In S2, the volume fraction of methanol is 90%; s4, controlling the boiling temperature of the stock solution during preparation to be 112 ℃, and keeping the boiling time to be 58 min; in S5, the stirring time among the raw materials is 13min, and the natural cooling time is 105 min; in S6, the finished plant pericarpium citri reticulatae tobacco fragrance type oral cavity atomized liquid B needs to be stored in a dark place, and the storage environment temperature is 20-30 ℃; in S7, the capacity of the selected atomization bottle is 60 ml.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (8)
1. The plant dried orange peel tobacco flavor type oral cavity atomized liquid is characterized by comprising the following components in percentage by mass: natural mineral water: 48-59%, nicotine salt 2-4%, dried orange peel: 2-4%, mint: 4-6%, ethanol: 3-5%, dried leaves of stevia: 1-3%, wrinkled giant hyssop: 2-4%, aloe: 8-10%, chlorophyll: 6-8%, natural indigo: 1-2%, katsumade galangal seed: 1-1.5%, clove: 1-1.5% of vine flavor edible essence: 6-8% of Chinese yam: 3 to 5 percent.
2. The formulation of the plant pericarpium citri reticulatae tobacco flavor type oral cavity atomized liquid as claimed in claim 1, comprising the following components by mass percent: natural mineral water: 49% of nicotine salt: 3%, dried orange peel: 3% and mint: 5% and ethanol: 4%, dried leaves of stevia: 2%, agastache rugosus: 3% of aloe: 9% of chlorophyll: 7% and indigo naturalis: 1.5%, katsumade galangal seed 1.3%, and dried orange peel: 3% and clove: 1.2% and rattan-flavored edible essence: 7% and Chinese yam: 4 percent.
3. A preparation method of plant pericarpium citri reticulatae tobacco flavor type oral cavity atomized liquid is characterized by comprising the following steps:
s1: raw material selection and pretreatment: directly obtaining high-quality natural mineral water from natural spring, sterilizing natural mineral water with chlorine dioxide, and directly purchasing nicotine salt, pericarpium Citri Tangerinae, herba Menthae, ethanol, dried leaves of stevia rebaudiana Bertoni, herba Agastaches, Aloe, chlorophyll, indigo naturalis, semen Alpiniae, flos Caryophylli, caulis et folium Gaultheriae Yunnanensis edible essence, and rhizoma Dioscoreae;
s2: preparing a primary raw material: weighing a certain amount of dry stevia rebaudiana leaves, adopting a water extraction and alcohol precipitation method, removing impurities, decoloring and deodorizing the obtained solution by using a precipitator and ion exchange resin, recrystallizing the obtained solution by using a methanol solution with a certain volume fraction and a certain concentration to obtain a pure stevioside white crystalline sweetener, then weighing a certain amount of mint, and performing subcritical low-temperature extraction on the mint to obtain mint essential oil;
s3: preparing a secondary raw material: quantitatively weighing the raw material in S1, the stevioside white crystalline sweetener prepared in S2 and the mint essential oil by using an electronic scale according to a required proportion in an aseptic environment, and ensuring that the ratio reaches an expected standard;
s4: preparing stock solution: preparing a decocting pot, adding the natural mineral water weighed in the step S3 into the decocting pot for preheating, and after preheating for a period of time, putting the mint, the agastache rugosus, the aloe, the chlorophyll, the indigo naturalis, the katsumadai seed, the dried orange peel, the clove and the Chinese yam into the decocting pot to be decocted together with the natural mineral water to obtain a liquid medicine A;
s5: preparing a finished product liquid: after S4 is finished, the liquid medicine A in S4 is injected into a stirring pot, then the ethanol, the nicotine salt, the sweetening agent and the rattan flavor edible essence weighed in S3 are added, stirring is carried out, the mixture is naturally cooled in the stirring process, and after a period of time, the finished product of the plant dried orange peel tobacco flavor oral cavity atomized liquid B can be obtained;
s6: and (3) disinfecting and storing the finished liquid: performing final sterilization on the finished product plant pericarpium citri reticulatae tobacco fragrance type oral cavity atomized liquid B by a pasteurization method, then filling the finished product plant pericarpium citri reticulatae tobacco fragrance type oral cavity atomized liquid B into a total glass container, and sealing and storing the total glass container;
s7: bottle separation and packaging: and (4) selecting an aseptic atomizing bottle, and injecting the finished product plant dried orange peel tobacco fragrance type oral cavity atomizing liquid B in the total glass container in the S6 into the atomizing bottle, so that the oral cavity atomizing liquid B can be normally used.
4. The method for preparing the plant pericarpium citri reticulatae tobacco flavor oral cavity atomizing liquid according to claim 3, wherein the volume fraction of methanol in S2 is 90%.
5. The method for preparing the plant pericarpium citri reticulatae tobacco flavor type oral cavity atomized liquid as claimed in claim 3, wherein in S4, the boiling temperature of the stock solution during preparation is controlled at 105 ℃ and 113 ℃, and the boiling time is 45-60 min.
6. The method for preparing the plant pericarpium citri reticulatae tobacco flavor oral cavity atomized liquid according to claim 3, wherein in S5, the stirring time between the raw materials is 10-15min, and the natural cooling time is 80-110 min.
7. The method for preparing the plant pericarpium citri reticulatae tobacco flavor oral cavity atomized liquid according to claim 3, wherein in S6, the finished plant pericarpium citri reticulatae tobacco flavor oral cavity atomized liquid B needs to be stored in a dark place and the storage environment temperature is 20-30 ℃.
8. The method for preparing the plant pericarpium citri reticulatae tobacco flavor oral cavity atomized liquid according to claim 3, wherein the capacity of the selected atomization bottle in S7 is 60 ml.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010361196.2A CN111419726A (en) | 2020-04-30 | 2020-04-30 | Plant dried orange peel tobacco-flavored oral cavity atomized liquid and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010361196.2A CN111419726A (en) | 2020-04-30 | 2020-04-30 | Plant dried orange peel tobacco-flavored oral cavity atomized liquid and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN111419726A true CN111419726A (en) | 2020-07-17 |
Family
ID=71554935
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202010361196.2A Pending CN111419726A (en) | 2020-04-30 | 2020-04-30 | Plant dried orange peel tobacco-flavored oral cavity atomized liquid and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN111419726A (en) |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102186461A (en) * | 2008-10-14 | 2011-09-14 | 麦克内尔股份公司 | Multi portion intra-oral dosage form and use thereof |
| CN102397185A (en) * | 2011-11-05 | 2012-04-04 | 安徽省天旭茶业有限公司 | Oral freshener and preparation method thereof |
| CN103768435A (en) * | 2014-01-21 | 2014-05-07 | 江苏中烟工业有限责任公司 | Breath-freshening type tobacco oral cavity spray and preparation method thereof |
| CN103933276A (en) * | 2014-03-29 | 2014-07-23 | 胡侠 | Oral refresher and production method thereof |
| CN106307602A (en) * | 2016-09-12 | 2017-01-11 | 三峡大学 | Electronic cigarette liquid for freshening breath |
| CN110437204A (en) * | 2019-09-05 | 2019-11-12 | 深圳市真味生物科技有限公司 | A kind of electronics tobacco tar of nicotine salt and its preparation method and application the nicotine salt |
| CN110537724A (en) * | 2019-09-27 | 2019-12-06 | 铂德（深圳）科技有限公司 | Nicotine salt, electronic cigarette oil and production process thereof |
-
2020
- 2020-04-30 CN CN202010361196.2A patent/CN111419726A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102186461A (en) * | 2008-10-14 | 2011-09-14 | 麦克内尔股份公司 | Multi portion intra-oral dosage form and use thereof |
| CN102397185A (en) * | 2011-11-05 | 2012-04-04 | 安徽省天旭茶业有限公司 | Oral freshener and preparation method thereof |
| CN103768435A (en) * | 2014-01-21 | 2014-05-07 | 江苏中烟工业有限责任公司 | Breath-freshening type tobacco oral cavity spray and preparation method thereof |
| CN103933276A (en) * | 2014-03-29 | 2014-07-23 | 胡侠 | Oral refresher and production method thereof |
| CN106307602A (en) * | 2016-09-12 | 2017-01-11 | 三峡大学 | Electronic cigarette liquid for freshening breath |
| CN110437204A (en) * | 2019-09-05 | 2019-11-12 | 深圳市真味生物科技有限公司 | A kind of electronics tobacco tar of nicotine salt and its preparation method and application the nicotine salt |
| CN110537724A (en) * | 2019-09-27 | 2019-12-06 | 铂德（深圳）科技有限公司 | Nicotine salt, electronic cigarette oil and production process thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105106043B (en) | Fragrant mouthwash of a kind of peony anti-inflammatory deodorization and preparation method thereof | |
| CN105105314B (en) | Powder spray agent containing tobacco components and preparation method thereof | |
| KR101554072B1 (en) | The method of manufacturing foot bath additives using traditional Korean medicine | |
| CN111419726A (en) | Plant dried orange peel tobacco-flavored oral cavity atomized liquid and preparation method thereof | |
| CN105105315B (en) | A kind of clear throat type tobacco powder spray and preparation method thereof | |
| CN107661258A (en) | A kind of oral cleaning anti-inflammatory herbal mouthwash | |
| CN1457711A (en) | Incense rod for refreshment | |
| CN106618128A (en) | Green environmental protection joss stick and its preparation method thereof | |
| KR101175656B1 (en) | composition for korean herbal aromatic | |
| KR20140140787A (en) | Complex beauty Salt using solar salt processing environmentally friendly and manufacturing method thereof | |
| CN115721683A (en) | Electronic atomized liquid and preparation and use methods thereof | |
| CN1071305A (en) | The manufacture method of " Tianjing " tea | |
| KR100429141B1 (en) | health food beverage use mugwort and it's manufacture method | |
| CN110477157A (en) | A kind of deodorization body fragrance tea and preparation method thereof | |
| KR101025812B1 (en) | Manufacturing method of green tea with aloes | |
| CN105496857A (en) | Lemon flavor toilet water | |
| CN110433222A (en) | Composition of medicine for improving oral health and preparation method thereof, application method and purposes | |
| CN104782871A (en) | Chewing gum capable of replacing tobacco at initial stage of smoking cessation | |
| CN110279025A (en) | A kind of apple polyphenol health chewing gum and preparation method thereof | |
| KR101724825B1 (en) | Helpful agent contaiend chicory and aconitie tuber for prohibit smoking | |
| KR102548594B1 (en) | A White sage complex extract and its extraction method | |
| CN108354872A (en) | A kind of Chinese medicinal toothpaste and preparation method thereof | |
| KR101126279B1 (en) | Composition of mixed essential oils which is effective for stop smoking and its utiliztion | |
| KR102283663B1 (en) | Antimicrobial composition comprising extracts of herb | |
| KR102221423B1 (en) | Composition for inhibiting halitosis and enhancing oral hygiene |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20200717 |