CN110663985A - Reconstituted tobacco with low combustion speed and preparation method thereof - Google Patents

Reconstituted tobacco with low combustion speed and preparation method thereof Download PDF

Info

Publication number
CN110663985A
CN110663985A CN201911118213.3A CN201911118213A CN110663985A CN 110663985 A CN110663985 A CN 110663985A CN 201911118213 A CN201911118213 A CN 201911118213A CN 110663985 A CN110663985 A CN 110663985A
Authority
CN
China
Prior art keywords
tobacco
reconstituted tobacco
concentrated solution
waste material
solution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201911118213.3A
Other languages
Chinese (zh)
Other versions
CN110663985B (en
Inventor
刘雄斌
王凤兰
罗广丰
胡念武
汪丹
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Tobacco Hubei Industrial LLC
Hubei Xinye Tobacco Sheet Development Co Ltd
Original Assignee
China Tobacco Hubei Industrial LLC
Hubei Xinye Tobacco Sheet Development Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Tobacco Hubei Industrial LLC, Hubei Xinye Tobacco Sheet Development Co Ltd filed Critical China Tobacco Hubei Industrial LLC
Priority to CN201911118213.3A priority Critical patent/CN110663985B/en
Publication of CN110663985A publication Critical patent/CN110663985A/en
Application granted granted Critical
Publication of CN110663985B publication Critical patent/CN110663985B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/14Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/24Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Tobacco Products (AREA)

Abstract

The invention discloses reconstituted tobacco with low burning speed, which comprises a composite additive component for reducing the burning speed, wherein the composite additive comprises the following components: 10-90 parts of diammonium hydrogen phosphate and 10-90 parts of sodium bicarbonate, and also provides a preparation method of the reconstituted tobacco with low combustion speed, which is characterized by comprising the following steps: s1, extracting and concentrating a tobacco waste material through an extracting solution to obtain a tobacco waste material concentrated solution; s2, adding a composite additive into the concentrated solution of the tobacco waste material, stirring and filtering to obtain a filtered concentrated solution, wherein the composite additive comprises diammonium hydrogen phosphate and sodium bicarbonate; s3, obtaining a coating liquid mixed with the filtering concentrated solution; and S4, coating the coating liquid on the substrate, drying and slicing to obtain the reconstituted tobacco with low combustion speed, reducing the combustion speed of the reconstituted tobacco, ensuring the complete combustion of the reconstituted tobacco, and having soft taste and mellow fragrance.

Description

Reconstituted tobacco with low combustion speed and preparation method thereof
Technical Field
The invention relates to the field of paper-making reconstituted tobacco, in particular to low-burning-speed reconstituted tobacco and a preparation method thereof.
Background
The paper-making method reconstituted tobacco is a sheet-shaped or thread-shaped regenerated product prepared by taking waste tobacco stems, tobacco powder, low-grade tobacco leaves and the like in the cigarette production process as raw materials through the same flow as paper making. The additive is added into cigarettes, so that on one hand, the cost of the cigarettes can be properly reduced; on the other hand, the physical properties and chemical components of the cigarette can be adjusted to a certain degree, and the tar content is reduced, so that the quality of the cigarette is improved.
The preparation process comprises the steps of paper-making reconstituted tobacco, namely, tobacco stems, tobacco powder and low-grade tobacco leaves are used as raw materials, the extracted raw materials and an extraction liquid are separated after soaking and extraction, the extracted raw materials are added with fibers and then pulped, a paper machine is used for preparing a substrate with a high filling value by a method similar to paper making, meanwhile, the extraction liquid is concentrated to form a concentrated solution, essence and spice are added and then coated on the formed substrate, and the reconstituted tobacco is prepared after drying and slicing.
The reconstituted tobacco is finally added into a cigarette containing tobacco leaves or cut tobacco according to a certain proportion for combustion, the combustion speed of the cigarette is too high, which can cause incomplete combustion of the tobacco leaves, and the smoking time of consumers with too high combustion speed is short, the experience is poor.
Disclosure of Invention
In order to solve the problems, the invention provides the reconstituted tobacco with low combustion speed and the preparation method thereof, which reduce the combustion speed of the reconstituted tobacco, prolong the smoking time of the reconstituted tobacco, ensure the complete combustion of the tobacco leaves or tobacco shreds in cigarettes, remove the limitation of the doping proportion of combustible tobacco leaves, enrich the cigarette product categories and improve the use experience of consumers.
The technical scheme of the invention is that the low-burning-speed reconstituted tobacco comprises a composite additive component for reducing burning speed, wherein the composite additive comprises the following components: 10-90 parts of diammonium hydrogen phosphate and 10-90 parts of sodium bicarbonate.
Preferably, the composite additive comprises 10wt% to 90wt% of diammonium hydrogen phosphate, or comprises 10wt% to 90wt% of sodium bicarbonate, based on 100wt% of the mass of the composite additive.
The preparation method of the reconstituted tobacco with low burning speed is also provided, and is characterized by comprising the following steps:
s1, extracting and concentrating a tobacco waste material through an extracting solution to obtain a tobacco waste material concentrated solution;
s2, adding a composite additive into the concentrated solution of the tobacco waste material, stirring and filtering to obtain a filtered concentrated solution, wherein the composite additive comprises diammonium hydrogen phosphate and sodium bicarbonate;
s3, obtaining a coating liquid mixed with the filtering concentrated solution;
and S4, coating the coating liquid on the substrate, drying and slicing to obtain the reconstituted tobacco with low combustion speed.
Preferably, the extracting solution comprises one or more of EDTA aqueous solution, urea-coated agent aqueous solution and complex enzyme solution, the extracting temperature is 40-60 ℃, and the extracting time is 4-6 h.
Preferably, the composite additive comprises 10wt% to 90wt% of diammonium hydrogen phosphate, or comprises 10wt% to 90wt% of sodium bicarbonate, based on 100wt% of the mass of the composite additive.
Preferably, the concentration of the tobacco waste material concentrated solution is 35-45%.
Preferably, the feeding ratio of the composite additive to the tobacco waste material is 5-20: 50.
Preferably, the stirring speed of S2 is 300-500r/min, and the stirring time is at least 5 min.
The scheme is that a mixture of diammonium hydrogen phosphate and sodium bicarbonate is added into a tobacco waste material concentrated solution as a composite additive for reducing the combustion speed so as to reduce the combustion speed of cigarettes, and the mechanism is that the diammonium hydrogen phosphate has a boiling point of 155 ℃ and is decomposed at the temperature, the tobacco shred temperature is 230 plus one year when the cigarettes are lit, decomposition products are phosphoric acid and ammonia gas, the phosphoric acid and phosphorus pentoxide form a gas film to block oxygen and reduce the combustion speed, the phosphoric acid and the sodium bicarbonate react to generate carbon dioxide and water, the temperature of moisture is reduced, the combustion speed is reduced, meanwhile, combustion byproducts form a layer of non-combustible protective film to cover on tobacco leaves, and air is isolated so as to reduce the combustion speed.
The invention has the beneficial effects that:
1. the mixed additive is added in the preparation process of the coating liquid, so that the burning speed of the reconstituted tobacco is reduced, the burning speed of the cigarette is reduced, the smoking time of the cigarette is prolonged, and the tobacco leaves or tobacco shreds in the cigarette can be more fully burned;
3. by adjusting the addition amount of the composite additive and controlling the combustion speed, the limit of the mixing proportion or variety of combustible tobacco leaves is removed, the cigarette product categories are enriched, the selection diversity of the flavor and the taste of the cigarette is increased, and the use experience of consumers is improved;
4. the burning speed of the cigarette is controlled by independently regulating and controlling the burning speed of the reconstituted tobacco, and factors such as cigarette paper materials and the like do not need to be prepared, so that the process is simplified, and the production efficiency is improved.
Detailed Description
In order to make the present invention more comprehensible, the technical solutions of the present invention are further described below with reference to specific embodiments, but the present invention is not limited thereto.
Example 1
Carrying out manual impurity removal on the tobacco waste material, carrying out pretreatment of stem washing, and airing;
weighing 500g of raw materials after impurity removal, putting the raw materials into 5L of extracting solution, carrying out ultrasonic extraction at 40-60 ℃ with the extracting solution being 0.12% of EDTA aqueous solution, wherein the ultrasonic extraction frequency is 3KHz-5KHz, the extraction time is 4-6h, and carrying out solid-liquid separation treatment to obtain an extracting solution;
centrifuging the extract solution at 12000r/min by a butterfly centrifuge for 3-5min to reduce the residue content, and collecting the supernatant;
concentrating the purified extract liquor to 35% by using a double-effect climbing-film evaporator to obtain a concentrated solution;
uniformly stirring 50g of a mixture of diammonium hydrogen phosphate and sodium bicarbonate, then adding the concentrated solution, and continuously stirring for 5min, wherein the mass ratio of the diammonium hydrogen phosphate to the sodium bicarbonate is 1:9, so as to obtain a mixed concentrated solution;
filtering the mixed concentrated solution by a rectangular sieve of 200 meshes to obtain a filtered concentrated solution; and adding essence and spice into the filtered concentrated solution to prepare coating liquid according to paper-making reconstituted tobacco process specifications, and coating the coating liquid on a formed substrate to prepare the reconstituted tobacco, namely the low-combustion-speed reconstituted tobacco.
Example 2
Carrying out manual impurity removal on the tobacco waste material, carrying out pretreatment of stem washing, and airing;
weighing 500g of the raw materials after impurity removal, putting into 2.5L of extracting solution, wherein the extracting solution is 2% aqueous solution of a urea bag agent, carrying out ultrasonic extraction at 40-60 ℃, wherein the ultrasonic extraction frequency is 3KHz-5KHz, the extraction time is 4-6h, and carrying out solid-liquid separation treatment to obtain an extracting solution;
centrifuging the extract solution at 12000r/min by a butterfly centrifuge for 3-5min to reduce the residue content, and collecting the supernatant;
concentrating the purified extract liquor to 40% by using a double-effect climbing-film evaporator to obtain a concentrated solution;
uniformly stirring 100g of a mixture of diammonium hydrogen phosphate and sodium bicarbonate, then adding the concentrated solution, and continuously stirring for 5min, wherein the mass ratio of diammonium hydrogen phosphate to sodium bicarbonate is 1: 1, obtaining a mixed concentrated solution;
filtering the mixed concentrated solution by a rectangular sieve of 200 meshes to obtain a filtered concentrated solution; and adding essence and spice into the filtered concentrated solution to prepare coating liquid according to paper-making reconstituted tobacco process specifications, and coating the coating liquid on a formed substrate to prepare the reconstituted tobacco, namely the low-combustion-speed reconstituted tobacco.
Example 3
Carrying out manual impurity removal on the tobacco waste material, carrying out pretreatment of stem washing, and airing;
weighing 500g of raw materials after impurity removal, putting the raw materials into 1L of extracting solution, wherein the extracting solution is a complex enzyme solution, the complex enzyme comprises pectinase, glucoamylase and cellulase, carrying out ultrasonic extraction at 40-60 ℃, wherein the ultrasonic extraction frequency is 3KHz-5KHz, the extraction time is 4-6h, and carrying out solid-liquid separation treatment to obtain an extracting solution;
centrifuging the extract solution at 12000r/min by a butterfly centrifuge for 3-5min to reduce the residue content, and collecting the supernatant;
concentrating the purified extract liquor to 45% by using a double-effect climbing-film evaporator to obtain a concentrated solution;
uniformly stirring 200g of a mixture of diammonium hydrogen phosphate and sodium bicarbonate, adding the concentrated solution, and continuously stirring for 5min, wherein the mass ratio of the diammonium hydrogen phosphate to the sodium bicarbonate is 9: 1, obtaining a mixed concentrated solution;
filtering the mixed concentrated solution by a rectangular sieve of 200 meshes to obtain a filtered concentrated solution; and adding essence and spice into the filtered concentrated solution to prepare coating liquid according to paper-making reconstituted tobacco process specifications, and coating the coating liquid on a formed substrate to prepare the reconstituted tobacco, namely the low-combustion-speed reconstituted tobacco.
Example 4
Carrying out manual impurity removal on the tobacco waste material, carrying out pretreatment of stem washing, and airing;
weighing 500g of the raw materials after impurity removal, putting into 2.5L of extracting solution, wherein the extracting solution is 2% aqueous solution of a urea bag agent, carrying out ultrasonic extraction at 40-60 ℃, wherein the ultrasonic extraction frequency is 3KHz-5KHz, the extraction time is 4-6h, and carrying out solid-liquid separation treatment to obtain an extracting solution;
centrifuging the extract solution at 12000r/min by a butterfly centrifuge for 3-5min to reduce the residue content, and collecting the supernatant;
concentrating the purified extract liquor to 40% by using a double-effect climbing-film evaporator to obtain a concentrated solution;
filtering the concentrated solution by a rectangular sieve of 200 meshes to obtain filtered concentrated solution; and adding essence and spice into the filtered concentrated solution to prepare coating liquid according to paper-making reconstituted tobacco process specifications, and coating the coating liquid on a formed substrate to prepare the reconstituted tobacco, namely the low-combustion-speed reconstituted tobacco.
Example 5
The reconstituted tobacco finally obtained in the examples 1 to 4 is shredded and put into a constant temperature and humidity box for balancing for 24 hours to prepare cigarettes, and the test results are as follows:
sample (I) Burning rate (mm/min)
Example 1 9.72
Example 2 7.68
Example 3 6.5
Example 4 10.58
The above description is only a preferred embodiment of the present invention, and all equivalent changes and modifications made in accordance with the claims of the present invention should be covered by the present invention.

Claims (8)

1. The reconstituted tobacco with low burning speed is characterized by comprising a composite additive component for reducing the burning speed, wherein the composite additive comprises the following components: 10-90 parts of diammonium hydrogen phosphate and 10-90 parts of sodium bicarbonate.
2. The reconstituted tobacco with low combustion speed according to claim 1, wherein the compound additive comprises 10wt% to 90wt% of diammonium hydrogen phosphate or 10wt% to 90wt% of sodium bicarbonate, based on 100wt% of the mass of the compound additive.
3. The method for preparing the reconstituted tobacco with low burning speed according to claim 1, which is characterized by comprising the following steps:
s1, extracting and concentrating a tobacco waste material through an extracting solution to obtain a tobacco waste material concentrated solution;
s2, adding a composite additive into the concentrated solution of the tobacco waste material, stirring and filtering to obtain a filtered concentrated solution, wherein the composite additive comprises diammonium hydrogen phosphate and sodium bicarbonate;
s3, obtaining a coating liquid mixed with the filtering concentrated solution;
and S4, coating the coating liquid on the substrate, drying and slicing to obtain the reconstituted tobacco with low combustion speed.
4. The method for preparing the reconstituted tobacco with the low combustion speed according to claim 3, wherein the extracting solution comprises one or more of EDTA (ethylene diamine tetraacetic acid) aqueous solution, urea-coated agent aqueous solution and complex enzyme solution, the extracting temperature is 40-60 ℃, and the extracting time is 4-6 h.
5. The method for preparing the reconstituted tobacco with low combustion speed according to claim 3, wherein the compound additive comprises 10wt% -90wt% of diammonium hydrogen phosphate or 10wt% -90wt% of sodium bicarbonate, wherein the mass of the compound additive is 100 wt%.
6. The method for preparing the reconstituted tobacco with the low combustion speed according to claim 3, wherein the concentration of the tobacco waste material concentrated solution is 35-45%.
7. The method for preparing the reconstituted tobacco with the low combustion speed according to claim 3, wherein the feeding ratio of the composite additive to the tobacco waste material is 5-20: 50.
8. The method for preparing the reconstituted tobacco with low burning speed as claimed in claim 3, wherein the stirring speed of S2 is 500r/min and the stirring time is at least 5 min.
CN201911118213.3A 2019-11-15 2019-11-15 Reconstituted tobacco with low combustion speed and preparation method thereof Active CN110663985B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201911118213.3A CN110663985B (en) 2019-11-15 2019-11-15 Reconstituted tobacco with low combustion speed and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201911118213.3A CN110663985B (en) 2019-11-15 2019-11-15 Reconstituted tobacco with low combustion speed and preparation method thereof

Publications (2)

Publication Number Publication Date
CN110663985A true CN110663985A (en) 2020-01-10
CN110663985B CN110663985B (en) 2021-09-17

Family

ID=69087871

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201911118213.3A Active CN110663985B (en) 2019-11-15 2019-11-15 Reconstituted tobacco with low combustion speed and preparation method thereof

Country Status (1)

Country Link
CN (1) CN110663985B (en)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2196659A (en) * 1986-10-25 1988-05-05 Derek Aubrey Thacker Fire retardant composition
CN101766327A (en) * 2008-12-26 2010-07-07 湖北中烟工业有限责任公司 Extraction method of the tobacco thin slice production of paper process
CN106376971A (en) * 2016-09-22 2017-02-08 内蒙古昆明卷烟有限责任公司 Cigarette with cut tobaccos being cut reconstituted tobaccos and cut tobacco stems

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2196659A (en) * 1986-10-25 1988-05-05 Derek Aubrey Thacker Fire retardant composition
CN101766327A (en) * 2008-12-26 2010-07-07 湖北中烟工业有限责任公司 Extraction method of the tobacco thin slice production of paper process
CN106376971A (en) * 2016-09-22 2017-02-08 内蒙古昆明卷烟有限责任公司 Cigarette with cut tobaccos being cut reconstituted tobaccos and cut tobacco stems

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
刘志昌等: "尿包萃取在造纸法烟草薄片生产中的应用研究", 《化学与生物工程》 *

Also Published As

Publication number Publication date
CN110663985B (en) 2021-09-17

Similar Documents

Publication Publication Date Title
CN103211288B (en) Thin section for tobacco and cigarette
KR100385585B1 (en) Steam rupture method of tobacco stem
US9480283B2 (en) Process and apparatus for improving raw tobacco
CN101411544B (en) Corn husk tobacco thin sheet and method for producing the same
CN101966007B (en) Method for manufacturing tobacco sheet by using commingling paper-making method
WO2011127680A1 (en) Sheet for cigarette, preparation method thereof, and cigarette
CN103892436A (en) Method for improving use efficiency of tobacco raw materials in reconstituted tobacco production
CN105707970A (en) Preparation method of mixed type regenerated cut stems
CN103315377A (en) Method of preparing extracting solution of papermaking reconstituted tobacco
CN110663985B (en) Reconstituted tobacco with low combustion speed and preparation method thereof
CN108185506B (en) Preparation method of reconstituted tobacco
CN102960853B (en) Method of utilizing ammoniation technology to improve quality of tobacco stalk extracting solution
WO2011127681A1 (en) Cigarette flake and preparation method thereof, and the cigarette
CN108477662B (en) Manufacturing process of reconstituted tobacco with burley tobacco characteristics
CN104068463A (en) Method for preparing tobacco sheet with cane shoot leaves
CN103932380A (en) Tobacco stem soaking extracting processing method for tobacco stem reproducing technology
CN111000278A (en) Method for improving quality of paper-making reconstituted tobacco products
CN113826942B (en) Preparation method of sun-cured tobacco extract with sweet characteristic and processing method of sun-cured tobacco
CN113519883B (en) Novel flexible tobacco stem pulping process
CN102058150A (en) Method for improving quality of tobacco stalk extract and application thereof
CN102631022B (en) Method for reducing total sugar content in tobacco
CN101683181A (en) Method for preparing cut stems used for cigarettes
CN113679084A (en) Method for preparing paper-making reconstituted tobacco by using betel nut flower base fibers
CN113712239B (en) Preparation method of high-nicotine paper-making reconstituted tobacco with burley tobacco particles as filler
CN114698867B (en) Preparation method of reconstituted tobacco with accurate components and reconstituted tobacco

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant