CN110575411A

CN110575411A - spray mask composition

Info

Publication number: CN110575411A
Application number: CN201910895755.5A
Authority: CN
Inventors: 刘东泰; 王奎荣; 张宏伟
Original assignee: Individual
Current assignee: Individual
Priority date: 2019-09-21
Filing date: 2019-09-21
Publication date: 2019-12-17

Abstract

The invention relates to a spray mask composition, which comprises a tank A and a tank B, wherein the tank A is a cleaning tank and comprises the components of carboxymethyl chitosan, EDTA disodium, jade powder, a mint extract and high-boron deuterium-depleted water; the jar B is a maintenance jar, and comprises Margarita powder, Bombyx Batryticatus, radix Angelicae Dahuricae, rhizoma Bletillae, radix Ampelopsis, Atractylodis rhizoma, Poria, stigma croci Sativi, Aloe Barbadensis Miller, Lac Caprae Seu Ovis extract, collagen polypeptide, hyaluronic acid, glycerol, nicotinamide, vitamin E, flos Rosae Rugosae extract, and high-boron deuterium-depleted water, and is prepared by micronizing Chinese medicinal components, mixing with other nutritional components, pressurizing, and packaging to make into spray. The facial mask adopts a mode of cleaning and then maintaining, the tank A is sprayed firstly to adsorb heavy metal ions on the face, dirt and mites in pores are removed, the skin is deeply cleaned, cells are activated, and the tank B is sprayed secondly, nano-scale traditional Chinese medicine particles can be directly absorbed through skin, so that the effects of whitening, moisturizing, aging resistance and the like of the facial mask are extremely exerted, and the facial mask is convenient to use and has better effect due to the spraying form.

Description

Spray mask composition

Technical Field

the invention belongs to the field of skin care products, and particularly relates to a spray mask composition.

Background

With the improvement of living standard of people, the facial mask is not only sought by women who love beauty, but also collected in bags by many men. The huge market demand promotes the vigorous development of the mask market, the mask is diversified, the whitening, moisturizing, anti-wrinkle, oil control and the like almost cover all facial problems, the production process is mature day by day, but the problems of low absorption rate, slow effect and the like still exist. The mask base cloth fixed by the most common mask paste at present is not suitable for the face shape of all people, so that part of the mask is wrinkled or uncovered, and the use form is also one of the reasons of low absorption rate and slow effect of the nutrient components of the mask.

disclosure of Invention

In view of the above technical background, the technical problem to be solved by the present invention is to provide a spray mask composition, which adopts a mode of cleaning and then maintaining to remove pore dirt and the like, activates cells and then supplies nutrient substances, wherein nano-scale traditional Chinese medicine particles can be directly absorbed through skin, so that the effects of whitening, moisturizing, aging resistance and the like of the mask are brought into full play, and the spray form is convenient to use and has a better effect.

In order to solve the technical problems, the invention adopts the technical scheme that:

A spray mask composition characterized by: comprises a tank A and a tank B, wherein the tank A is a cleaning tank and comprises the components of carboxymethyl chitosan, EDTA disodium, jade powder, mint extracts and high-boron deuterium-depleted water; the jar B is a maintenance jar, and comprises Margarita powder, Bombyx Batryticatus, radix Angelicae Dahuricae, rhizoma Bletillae, radix Ampelopsis, Atractylodis rhizoma, Poria, stigma croci Sativi, Aloe Barbadensis Miller, Lac Caprae Seu Ovis extract, collagen polypeptide, hyaluronic acid, glycerol, nicotinamide, vitamin E, flos Rosae Rugosae extract, and deuterium depleted water.

Preferably, the components are mixed according to the parts by weight:

and (4) tank A:

And (4) tank B:

A preparation method of a spray mask composition is characterized by comprising the following steps: the method comprises the following steps:

S01: preparing a first intermediate solution: weighing aloe vera according to the weight part ratio, peeling, placing in a juicer for squeezing, centrifuging the obtained juice to remove impurities, and obtaining a first intermediate solution;

S02: preparing a second intermediate solution: weighing jade powder, pearl powder, white muscardine silkworm, angelica dahurica, bletilla striata, ampelopsis japonica, bighead atractylodes rhizome, white poria and saffron crocus traditional Chinese medicine components according to the weight part ratio, cleaning, adding high-boron deuterium-depleted water together with the first intermediate solution, and crushing at a low temperature below 25 ℃ by adopting a chromium carbide air knife technology to obtain suspension containing traditional Chinese medicine particles as a second intermediate solution, wherein the particle size of the particles is nano-scale;

s03: blending and homogenizing: weighing other components according to the weight part ratio, putting the other components and the second intermediate liquid into a homogenizing tank, adding an emulsifier accounting for 0.1-1% of the total mass, stirring, heating to 25-35 ℃, and stirring the mixed liquid into a homogeneous system;

s04: and (3) sterilization and filling: short-time microwave sterilization and pressurized filling.

preferably, the emulsifier described in S03 is one or more of cetearyl alcohol, glyceryl stearate, cetearyl glucoside, hydrogenated lecithin, cetyl alcohol and isopropyl myristate.

A method of using a spray mask composition, comprising: spraying the A tank to the face uniformly, forming a film on the face along with the evaporation of water, removing the film to clean the face, and spraying the B tank to massage the face lightly to make the components of the nutrient essence completely absorbed.

The invention has the advantages that:

(1) the facial mask composition A + B adopts a mode of cleaning firstly and then maintaining, the facial mask composition A + B firstly deeply cleans the face to remove pore dirt and the like, the nano-scale jade powder improves skin microcirculation, activates cells, supplies nutrient substances and is matched with other nano-scale traditional Chinese medicine particles for direct transdermal absorption;

(2) the facial mask composition adopts a spray form, and the essence components are pressurized and atomized into fine liquid drops which can uniformly act on the face, so that the effect is better, and the use is convenient.

Detailed Description

The technical solution of the present invention is described below clearly and completely with reference to specific embodiments, and it is obvious that the described embodiments are only some embodiments of the present invention. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

The invention provides a technical scheme that: a spray mask composition characterized by: comprises a tank A and a tank B, wherein the tank A is a cleaning tank and comprises the components of carboxymethyl chitosan, EDTA disodium, jade powder, mint extracts and high-boron deuterium-depleted water; the jar B is a maintenance jar, and comprises Margarita powder, Bombyx Batryticatus, radix Angelicae Dahuricae, rhizoma Bletillae, radix Ampelopsis, Atractylodis rhizoma, Poria, stigma croci Sativi, Aloe Barbadensis Miller, Lac Caprae Seu Ovis extract, collagen polypeptide, hyaluronic acid, glycerol, nicotinamide, vitamin E, flos Rosae Rugosae extract, and deuterium depleted water.

The components are mixed according to the parts by weight:

and (4) tank A:

And (4) tank B:

the main components have the following functions in the system:

Carboxymethyl chitosan: the cationic biological polysaccharide is the only cationic biological polysaccharide in nature, has good film forming property and adsorbability, and can be uniformly sprayed on the face to form a film, so that heavy metal ions on the face can be adsorbed, dirt in pores can be removed, and the pores can be opened; the protonated ammonium of carboxymethyl chitosan has the functions of resisting bacteria and infection, and the protonated ammonium of carboxymethyl chitosan acts on the negatively charged cell membrane of bacteria to adsorb and aggregate the bacteria, penetrates cell walls to enter cells simultaneously, disturbs the metabolism and synthesis of the bacteria, and can inhibit the growth of the bacteria on the surface of skin.

Jade powder: the compendium of materia Medica states that jade has: the traditional Chinese medicine has the effects of removing heat in stomach, relieving asthma and dysphoria, quenching thirst, moistening heart and lung, assisting sound and throat, nourishing hair, nourishing five internal organs, softening tendons and bones, calming soul, promoting blood circulation, improving eyesight and ears and the like. Modern researches show that the jade powder has far infrared microwave emission, can improve skin microcirculation, enhance cell activity, promote skin cell metabolism, remove waste in time, promote absorption of skin cells on nutrients, and achieve the purposes of moisturizing, whitening, increasing skin elasticity and delaying aging.

and (3) mint extract: refreshing and refreshing the mind and making the face feel fresh.

high-boron deuterium-depleted water: research shows that the deuterium-depleted water can promote the activity of enzymes in vivo, enhance the immunity of the organism, effectively remove acid wastes in blood, improve the internal environment, enhance the activity of cells, keep the skin in a young and healthy state, and delay the skin aging, and meanwhile, the boron ions have the effects of inhibiting bacteria and killing mites.

pearl powder: whitening, the pearl has the whitening effect from ancient times, and modern science finds that trace elements contained in the pearl can promote the increase of the quantity of SOD (superoxide dismutase) and enhance the activity, and the SOD can remove free radicals of a human body, improve skin color and make the skin naturally white; oil control, the nanometer pearl powder has extremely fine particle size and better adsorption capacity, can adsorb redundant oil on the nanometer pearl powder, and can control the secretion of the oil to dry and clean the skin; the speckle reduction, compendium of materia Medica, has long pointed out: the pearl can remove darkness, and a large amount of trace elements contained in the pearl powder can effectively suppress the increase of lipid peroxide, thereby effectively removing color spots; the pearl powder contains 18 amino acids required by human body, which can promote the growth of collagen cells, and the collagen cells are the main assistant and minister for promoting the regeneration of skin.

White muscardine silkworm: the Shen nong Ben Cao Jing (Shen nong's herbal classic) has the efficacy of removing black spots and making people have good complexion. Bombyx Batryticatus contains amino acids and active mercerizing agent, and has effects of nourishing skin and caring skin. The protein contained in the stiff silkworm can stimulate the sebaceous gland and regulate the secretion of sex hormone, so that the stiff silkworm has a certain curative effect on chloasma caused by female sexual hormone secretion disorder, and the active mercerizing hormone contained in the stiff silkworm can promote the neogenesis of skin cells, regulate sebum, improve skin microcirculation, whiten and prevent sunburn, eliminate pigmentation and keep skin elasticity.

aloe vera: the mucus contains polysaccharides such as arboran A Baloe mannasetin and various vitamins, is very beneficial to human skin, has the effects of astringing, softening, moisturizing, diminishing inflammation and whitening the skin, and can effectively prevent aging problems such as small wrinkles, eye bags, skin laxity and the like.

collagen polypeptide: the skin is bright, the skin luster depends on the water content, and the collagen polypeptide has good water retention capacity, so that the skin is moisturized and bright and emits healthy luster; skin tightening, after the collagen polypeptide enters the dermal tissue, the broken and aged elastic fiber net can be repaired, the skin tightness is increased, the skin tension is generated, pores are reduced, and the skin is tight and elastic; the anti-wrinkle leather has the advantages that the anti-wrinkle leather has a plump collagen layer in the dermis, can quickly fill local collapse, enables skin cells to be propped up, improves relaxation, tightens the skin, and reduces deep wrinkles and fine lines; lightening spots, wherein the collagen polypeptide can ensure that cells are more tightly bonded, the speed of generating new cells is accelerated, melanin and toxin are not gathered and hidden in the body, the skin color is white, and the spots are lightened; the collagen polypeptide can directly permeate into the bottom layer of the skin, has good affinity with surrounding tissues, can assist cells to produce collagen, and promotes the normal growth of skin cells.

hyaluronic acid: also known as hyaluronic acid, is an acidic mucopolysaccharide. It is an important basic substance for skin tenderness, is the substance found at present and has the best moisture retention in nature, and is called as an ideal natural moisture retention factor. It can improve skin nutrition metabolism, make skin tender and smooth, remove wrinkle, increase elasticity, and delay aging, and is good transdermal absorption promoter while keeping moisture, and can be used in combination with other nutritional ingredients to achieve ideal effect of promoting nutrition absorption.

Wherein the emulsifier in S03 is one or more of cetearyl alcohol, glyceryl stearate, cetearyl glucoside, hydrogenated lecithin, cetyl alcohol and isopropyl myristate.

The invention adopts chromium carbide air knife technology for traditional Chinese medicine components such as jade powder, pearl powder and the like, is ultramicro nanometer crushing technology, is researched and matured at present, and has the principle that an air knife is formed by utilizing high-speed air vortex, substances are ultramicro-granulated at the low temperature of below 25 ℃, the original molecular structure of the substances is not damaged, the efficacy of the substances is retained to the maximum extent, the particle size of the obtained traditional Chinese medicine is nanometer, the traditional Chinese medicine can be completely suspended in spray liquid, the diameter of pores is approximately 20-50 micrometers, nanometer traditional Chinese medicine particles can be completely absorbed through the pores in a transdermal manner, the permeability is good, and the problem that the particle size of common traditional Chinese medicine components is large and is not easy to absorb is solved.

the carboxymethyl chitosan in the tank A has good adsorbability, can adsorb heavy metal ions on the face, removes dirt in pores, opens the pores, is combined with high-boron deuterium-depleted water to create an acidic bacteriostatic environment, has the effects of bacteriostasis and killing mites, is matched with nanoscale jade powder to improve skin microcirculation, enhance cell activity, promote skin cell metabolism, promote absorption of nutrient substances by skin cells and enable the skin to present a high-activity absorption state; in addition, the nanometer Chinese medicinal components in the B tank can be completely absorbed through skin penetration, and the components of the nutrient essence can be efficiently absorbed based on the three steps of cleaning, activating and absorbing, so that the effects of whitening, moisturizing, resisting aging and the like of the mask can be fully exerted.

Although some commercially available facial masks also contain other components such as carboxymethyl chitosan, when one component acts on the face at the same time, the activity of other nutrient components is reduced by several times in the process of opening pores, and the components have large particle size and are not easy to absorb, so that the problems of low absorption rate, slow effect and the like are caused.

Example 1

The components are mixed according to the parts by weight:

And (4) tank A:

and (4) tank B:

s03: blending and homogenizing: weighing other components according to the weight part ratio, putting the other components and the second intermediate solution into a homogenizing tank, adding cetearyl alcohol with the total mass of 0.1%, opening and stirring, heating to 25-35 ℃, and stirring the mixed solution into a uniform system;

Example 2

A spray mask composition characterized by: the components are mixed according to the parts by weight:

And (4) tank A:

and (4) tank B:

S03: blending and homogenizing: weighing other components according to the weight part ratio, putting the other components and the second intermediate solution into a homogenizing tank, adding cetearyl glucoside with the total mass of 0.5%, opening and stirring, heating to 25-35 ℃, and stirring the mixed solution into a uniform system;

Example 3

And (4) tank A:

And (4) tank B:

S03: blending and homogenizing: weighing other components according to the weight part ratio, putting the other components and the second intermediate solution into a homogenizing tank, adding cetyl alcohol accounting for 1% of the total mass, starting stirring, heating to 25-35 ℃, and stirring the mixed solution into a uniform system;

the spray compositions prepared in examples 1 to 3 were compared with the spray mask compositions of comparative examples 1 to 3 for evaluation. The spray mask compositions of comparative examples 1 to 3 contained only the B can, and the others were the same.

Firstly, testing water replenishing and moisture preserving performance:

And (4) testing standard: the national light industry standard QB/T4256-.

testing the environmental temperature: 20-22 ℃; humidity: 40-60% and carrying out real-time dynamic monitoring.

Volunteer conditions:

25 female volunteers aged 18-65 years, without severe systemic diseases, immunodeficiency or autoimmune diseases, and without severe allergic history to skin care cosmetics.

testing an instrument: capacitance method skin moisture tester.

the determination step comprises:

(1) preparation before testing: any product (cosmetics or external medicine) cannot be used 2-3 days before the test of the tested part, and water cannot be contacted 2 hours before the test. Before testing, subjects uniformly wiped their inner forearms with dry facial tissue. Sit still for 30min in a standard environment during which time water and beverages cannot be drunk. The forearms were exposed and left in the test condition to remain relaxed.

Marking the inner side of the arm of the volunteer with 3 multiplied by 3cm²And (3) testing areas, wherein the interval between each testing area is at least 1cm, one arm of each volunteer marks 3 testing areas, and the same part of the other arm marks 3 testing areas. The spray mask compositions of examples 1 to 3 and comparative examples 1 to 3 were sprayed at random to test areas, and the spraying force and the distance degree were the same for each area, thereby ensuring that the spraying amounts were approximately equal.

(2) And (3) testing: the measurement was performed using a skin moisture tester, and the moisture value of each test area was measured at 3 time points (0h (i.e., before test), 2h, and 3h), respectively, and the test results are shown in table 1 below.

and (4) analyzing results: descriptive statistics are performed on the measurements for each test area, including quantity, mean, standard deviation, minimum, median, and maximum. The difference between the initial value of each test area and the measured value at the other time points (i.e., the value of the spray mask composition that increases the moisture of the skin) was calculated and the results are shown in table 2 below. If the test data is normal distribution, performing statistical analysis by adopting a t test method; and if the test data is in abnormal distribution, performing statistical analysis by adopting a rank sum test method.

TABLE 1 skin moisture values for each test area

	0h (before test)	2h	3h
				example 1 test area skin moisture value (n ═ 25)	30.4	34.4	35.0
Comparative example 1 test area skin moisture value (n ═ 25)	28.4	29.5	29.6
				Example 2 test area skin moisture value (n ═ 25)	29.3	34.0	34.4
comparative example 2 test area skin moisture value (n ═ 25)	28.6	29.9	30.0
				Example 3 test area skinSkin moisture value (n ═ 25)	29.7	34.6	35.0
Comparative example 3 test area skin moisture value (n ═ 25)	30.0	31.5	31.6

TABLE 2 skin moisture differential values for each test area

as is apparent from table 2, the spray mask compositions prepared in the respective examples had better moisturizing effects than the comparative examples, and 96% of 25 volunteers participating in the test responded that the skin was moisturized using the spray mask composition disclosed in the present invention.

Secondly, testing whitening performance:

volunteer conditions:

Testing an instrument: a colorimeter.

the determination step comprises:

(1) Preparation before testing: the spray mask compositions of examples 1 to 3 and comparative examples 1 to 3 were randomly sprayed on the test area 2 times a day, the daily activities of the volunteers were almost indoor, the indoor temperature and humidity were approximately the same, and the other preparations were the same as above.

(2) And (3) testing: the measurement was performed using a colorimeter, and the chromaticity of each test area was measured at 3 time points (0h (i.e., before the test), 2d, and 3h), respectively, and the test results are shown in table 3 below.

And (4) analyzing results: the difference between the initial value of each test area and the measured value at the other time points (i.e., the spray mask composition reduced the skin color value) was calculated and the difference results are shown in table 4 below. If the test data is normal distribution, performing statistical analysis by adopting a t test method; and if the test data is in abnormal distribution, performing statistical analysis by adopting a rank sum test method.

TABLE 3 skin color values for each test area

	0h (before test)	2d	3d
				Example 1 test area skin chroma value (n ═ 25)	0.130	0.114	0.110
Comparative example 1 test regional skin tone value (n ═ 25)	0.128	0.125	0.122
				example 2 testing of regional skin tone colour values (n ═ 25)	0.129	0.110	0.108
comparative example 2 test regional skin tone value (n ═ 25)	0.128	0.124	0.121
				example 3 test area skin chroma value (n ═ 25)	0.129	0.109	0.106
Comparative example 3 test regional skin tone value (n ═ 25)	0.130	0.122	0.120

TABLE 4 skin chroma differences for each test area

as is apparent from table 4, the spray mask compositions prepared in the respective examples had better whitening effects than the comparative examples, and 96% of 25 volunteers participating in the test responded that the skin was whitened by using the spray mask composition disclosed in the present invention.

And thirdly, testing the effectiveness of other efficacies:

volunteer conditions:

25 female volunteers in each test group aged 18-65 years had no serious systemic diseases, no immunodeficiency or autoimmune diseases, and no history of severe allergy to skin care cosmetics.

test area: facial skin.

and (3) testing items: skin elasticity, wrinkle depth (crow's feet area), and speckle reduction.

the test mode is as follows: the spray mask compositions of examples 1 to 3 and comparative examples 1 to 3 were uniformly sprayed on the face 2 times a day for 3 weeks, and the results are shown in the following table, in which the data units are: a human.

Note: the validity judgment standard is as follows:

obvious effect-obvious elastic recovery, obviously shallow wrinkles and obviously lightened spots;

Effective-elasticity is slightly recovered, wrinkles are slightly lightened, and spots are slightly lightened;

Ineffective-the effect is not obvious or tends to be aggravated.

As can be seen from the above table, the spray mask compositions prepared in the examples have higher effective rates of restoring skin elasticity and lightening wrinkles and spots, which are all above 90%, compared with the comparative examples, i.e., the spray mask compositions of the present application have good improving effects in the above aspects.

The above-described embodiments merely represent some examples of the present invention and should not be construed as limiting the scope of the invention. It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the inventive concept, which falls within the scope of the present invention. The present invention is not limited to the above embodiments, and various modifications and changes may be made without departing from the spirit and scope of the present invention.

Claims

1. A spray mask composition characterized by: comprises a tank A and a tank B, wherein the tank A is a cleaning tank and comprises the components of carboxymethyl chitosan, EDTA disodium, jade powder, mint extracts and high-boron deuterium-depleted water; the jar B is a maintenance jar, and comprises Margarita powder, Bombyx Batryticatus, radix Angelicae Dahuricae, rhizoma Bletillae, radix Ampelopsis, Atractylodis rhizoma, Poria, stigma croci Sativi, Aloe Barbadensis Miller, Lac Caprae Seu Ovis extract, collagen polypeptide, hyaluronic acid, glycerol, nicotinamide, vitamin E, flos Rosae Rugosae extract, and deuterium depleted water.

2. A spray mask composition according to claim 1 wherein: the components are mixed according to the parts by weight:

and (4) tank A:

And (4) tank B:

3. The method for preparing a spray mask composition according to any one of claims 1 to 2, wherein: the method comprises the following steps:

4. the method of preparing a spray mask composition according to claim 3, wherein: the emulsifier in S03 is one or more of cetearyl alcohol, glyceryl stearate, cetearyl glucoside, hydrogenated soft phospholipid, cetyl alcohol and isopropyl myristate.

5. the method of using a spray mask composition according to any one of claims 1 to 2, wherein: spraying the A tank to the face uniformly, forming a film on the face along with the evaporation of water, removing the film to clean the face, and spraying the B tank to massage the face lightly to make the components of the nutrient essence completely absorbed.