CN110477792A - A kind of nonalcoholic wet tissue and preparation method thereof can be used for breathing mask cleaning-sterilizing - Google Patents
A kind of nonalcoholic wet tissue and preparation method thereof can be used for breathing mask cleaning-sterilizing Download PDFInfo
- Publication number
- CN110477792A CN110477792A CN201910834407.7A CN201910834407A CN110477792A CN 110477792 A CN110477792 A CN 110477792A CN 201910834407 A CN201910834407 A CN 201910834407A CN 110477792 A CN110477792 A CN 110477792A
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- Prior art keywords
- wet tissue
- disinfection
- sterilizing
- soak
- breathing mask
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
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- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/08—Oxygen or sulfur directly attached to an aromatic ring system
- A01N31/14—Ethers
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- A—HUMAN NECESSITIES
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- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
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- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
- A01N33/02—Amines; Quaternary ammonium compounds
- A01N33/12—Quaternary ammonium compounds
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- A—HUMAN NECESSITIES
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- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
- A01N47/30—Derivatives containing the group >N—CO—N aryl or >N—CS—N—aryl
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- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides
- A01N47/42—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides containing —N=CX2 groups, e.g. isothiourea
- A01N47/44—Guanidine; Derivatives thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
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Abstract
The present invention is used for the wet tissue of breathing mask cleaning-sterilizing, it is made of the non-woven fabrics of disinfection soak and carrying disinfection soak with cleaning function, wherein, the disinfection soak contains based on every 100 parts by weight: (1) 0.1~3.0% compounding disinfectant；(2) 0.0~10.0% dissolution aids；(3) 0.05~1.0% Radix et Caulis Opuntiae Dillenii extract；(4) 0.0~1.0% dirt detergent；(5) 0.05~0.5% stabilizer；(6) surplus is pure water.Disinfection Effect of the present invention is stablized；It is suitble to the cleaning-sterilizing of the medical instruments such as CPAP ventilator mask, fire-fighting oxygen mask；Product formula is mild, non-stimulated, corrosion-free, and stability is good, no pollution to the environment, safety and environmental protection；Product is also suitable for the disinfection of different hard surface materials；Performance is stablized, long shelf-life, and safety is without side-effects, and spirituosity, consumer are not easy to use comfortably.
Description
Technical field
The invention belongs to disposable sanitary articles fields, and in particular to one kind can be used for CPAP ventilator mask, fire-fighting oxygen
The wet tissue and preparation method thereof of gas mask cleaning-sterilizing.
Background technique
Wet tissue (wet sanitary napkins) is a kind of relatively common Disposable Sanitary Accessory, with living standards of the people and is defended
The raising that business is known, people start to focus more on the product of safety and sanitation, cleaning-sterilizing.
Due to the regulation of " sterile products label specification management regulation ", only allow to have wet tissue and health wet on domestic market
Towel.But it is not to say that, wet tissue cannot have sterilizing function, and in brief, wet tissue requires to accomplish to clean, and wet sanitary napkins require to accomplish
Cleaning sterilization, pasteurization towelette require to accomplish cleaning-sterilizing；The pasteurization towelette country exists only in medical institutions, is voluntarily made by hospital
Make, mostly high effect disinfectants ingredient, the shelf-life is shorter, and when use needs wearing gloves, extremely inconvenient；In health care, fire-fighting
First aid field etc., will form after the CPAP ventilator mask that patient wears for a long time, the oxygen mask after fireman's use grease stain,
Dirt, steam etc., many users are that gauze, paper handkerchief or wet tissue is taken to wipe, and can not play high-effective cleansing and effectively disappear
The effect of poison；So to reduce cross-infection when using, carry out the cleaning of the objects table such as mask with disinfection be it is highly important,
Wet tissue with sterilizing function will have disinfectant irreplaceable easy to use excellent in fields such as daily civilian and health cares
Gesture.
In conjunction with the background in current disinfectant field, mainly have containing the brominated disinfectant of class containing iodine of chlorine, peroxide disinfectant,
Alcohol disinfectant, disinfectant phenolic, quaternary ammonium disinfectant, guanidine disinfectant, disinfection agent of chlorine dioxide etc., and press disinfecting power
It is divided into bactericidal agent, high effect disinfectants, middle effect disinfectants, low effect disinfectants.They are in hospital, school, public place, family etc.
It is used widely.Potent chemicals in disinfectant can play disinfection, but often irritant to human body, to metal
Be corrosive, have to dry goods it is Bleachability etc., so, the Legal Regulation of pasteurization towelette can be stringent, and test request can be higher how
Disinfectant ingredient is effectively combined with wet tissue, under the premise of guaranteeing Disinfection Effect, it is ensured that use is safe, is current wet tissue industry
Key technology difficulty.
Notification number is the Chinese invention of CN105560129B, discloses a kind of preparation side of pure natural draft pasteurization towelette
Method, the disinfectant are tea tree ethereal oil；Its antiseptic property and stability are obviously worth verifying.
Notification number is the Chinese invention of CN103520029B, discloses a kind of dry towel manufacturing method of disinfection, process characteristic
It is in the production process of spunlace non-woven cloth, adds antibacterial finish liquid, and heat cure is handled, and is obtained sterilizing dry towel, is convenient for
It saves；But it is not easy to directly wipe and certain ingredients of antibacterial finish liquid is not suitable for directly contact skin.
Notification number is the Chinese invention of CN103222992B, is disclosed a kind of water-soluble by leaf of Chinese ilex water extract and chlorine dioxide
Liquid mixing, then the pasteurization towelette made of sterilizing non-woven fabrics dipping, which is chlorine dioxide, belongs to high effect disinfectants,
Its experimental result also turns out that there is certain irritations for product；Because chlorine dioxide is a strong oxidizer, chemical property is not
Stablize, there are incompatibility.
The Chinese invention of notification number CN105010379B discloses a kind of biguanides fungicide, but the pH value of product is
11.5~13.5 and polar organic solvent methanol synergy exist, hence it is evident that be not suitable for human skin disinfection, there are certain harm
Property；The alkaline condition of its bactericidal property and product has compared with Important Relations bactericidal effect.
In conjunction with " disinfection technology standard " (version in 2002) to the regulation and WS/T 512-2016 " medical institutions' ring of disinfectant
Border surface cleaning and Disinfectant management specification " to the regulation of pasteurization towelette: it is with non-woven cloth, fabric, dust-free paper or other raw materials
Carrier, purified water are industrial water, the raw material such as appropriate addition disinfectant, the manufactured product with cleaning with disinfection,
Suitable for human body, general body surface, medical apparatus surface and other body surfaces.And WS 575-2017 " defend by wet sanitary napkins
It is raw to require " Pharmacopoeia of the People's Republic of China and " cosmetics safety technical specification will be met to bactericidal active ingredient, preservative
(version in 2015) " limitation requirement, with the upgrading of security legislation, the technology of foregoing invention patent also will be eliminated gradually.
Nowadays, safe and environment-friendly, health idea is all being advocated in the whole world, and pasteurization towelette is also in the ingredient for finding safety and low toxicity
Potent chemicals is substituted, in view of current guanidine disinfectant has been suitable for hospital surgery hand, skin, mucous membrane, body surface, medical treatment
The disinfection such as instrument, safety is preferable, to mucocutaneous nonirritant advantage, so, guanidine disinfectant is applied to human body, object table
Dual-purpose pasteurization towelette is good selection.But since guanidine disinfectant such as chlorhexidine acetate is easy crystallization in liquid environment
It is precipitated, difficult long term storage generally requires ethyl alcohol or the isopropanol of 50%-80% to dissolve, and consumer often repels use and contains
The product of ethyl alcohol or isopropanol, so the pasteurization towelette of guanidine disinfectant does not have accomplished and promotes.
The disinfection sanitizer or novel technique for how passing through selection new material improve antiseptic property and stability, and do not add
The ingredient for adding alcohol (ethyl alcohol) or isopropanol etc. to be hazardous to the human body combines disinfection composition with wet tissue, and product can accord with
Close disinfectant regulation, and the professional standard of wet tissue can be met, ensure user it is healthy and safe under the premise of, it is ensured that wet tissue
Disinfection Effect is consumer there is an urgent need to.
Summary of the invention
For the above-mentioned problems in the prior art and deficiency, the purpose of the present invention, which first consists in, provides one kind without wine
Smart ingredient can be cleaned effectively, sterilizing, and consumer does not stimulate when directly using, and can be used for CPAP ventilator mask, fire-fighting
The wet tissue of the cleaning-sterilizings such as oxygen mask, overcomes problems of the prior art.In addition, the present invention also provides the masks
The preparation method of pasteurization towelette.
Purpose to realize the present invention, inventor provide the following technical solutions:
A kind of wet tissue of breathing mask cleaning-sterilizing, by disinfection soak and carrying disinfection soak with cleaning function
Non-woven fabrics composition, wherein the disinfection soak contains based on every 100 parts by weight:
(1) 0.1~3.0% compounding disinfectant；
(2) 0.0~10.0% dissolution aids；
(3) 0.05~1.0% Radix et Caulis Opuntiae Dillenii extract；
(4) 0.0~1.0% dirt detergent；
(5) 0.05~0.5% stabilizer；
(6) surplus is pure water.
Preferably, the compounding disinfectant is that guanidine disinfectant is composed with other disinfection sanitizers；Described
Guanidine disinfectant can be selected from polyaminopropyl biguanide, chlorhexidine gluconate or chlorhexidine acetate；Other disinfection sanitizers can be selected from
Benzalkonium chloride, benzethonium chloride, triclosan, triclocarban, Chlorphenesin or Cetylpyridinium Chloride.
Guanidine disinfectant is stronger to the disinfection of bacterium, other disinfection sanitizers be containing " chlorine " disinfectant, can be to fungi
The disinfection of mould is stronger, and the disinfectant compounding of two kinds of different Disinfect mechanisms can dramatically increase sterilization, Disinfection Effect, drops simultaneously
The low usage amount of disinfection sanitizer, reduces the allergy risk and toxic side effect of user.Water-soluble preferable disinfectant can be with
It is used directly to compound；Water-soluble poor disinfectant is used in compounding after must first being dissolved with dissolution aids.It selects as far as possible at least
A kind of preferable disinfectant of water solubility, reduces the usage amount of dissolution aids, reduces cost.
Polyaminopropyl biguanide, also known as hexamethylene, No. CAS: 133029-32-0；Liquid, 20% activity
Content, it is water-soluble preferable；It is broad-spectrum antiseptic, low concentration, high-effect.
Chlorhexidine gluconate also known as chlorhexidine gluconate, No. CAS: 18472-51-0, it is common medical type external application
Disinfectant, liquid, 20% active quantities are water-soluble preferable, can kill staphylococcus aureus, Escherichia coli and Candida albicans
Bacterium.
Chlorhexidine acetate also known as chlorhexidine acetate are common medical type disinfectant for external use, can kill golden yellow grape
Coccus, No. CAS: 56-95-1；White powder, it is water-soluble poor, it needs to be dissolved by heating with propylene glycol or dipropylene glycol, large intestine bar
Bacterium and Candida albicans.
Benzalkonium chloride, No. CAS: 2001-54-5；White powder, wide-spectrum bactericide.
Benzethonium chloride, No. CAS: 121-54-0；White powder, it is water-soluble preferable；Cidex-7.
Triclosan, No. CAS: 3380-34-5；White powder, it is water-soluble poor, it needs to be heated with propylene glycol or dipropylene glycol
Dissolution.High-efficiency broad spectrum antibacterial agent has killing and inhibiting effect to gram-positive bacteria, negative bacterium, yeast and virus.
Triclocarban, No. CAS: 101-20-2, white powder is water-soluble poor, a kind of efficient, wide spectrum, safety novel
Antibacterial agent, the extensive application in medical disinfectant.
Chlorphenesin, No. CAS: 104-29-0；White powder, it is water-soluble poor, need hot water or propylene glycol or dipropyl two
Alcohol dissolves by heating；The chemicals preservative of wide spectrum.
Cetylpyridinium Chloride, No. CAS: 121-54-0；White powder, it is water-soluble preferable；Disinfection sanitizer.
Preferably, the dissolution aids are the one or more of propylene glycol, dipropylene glycol or CO40 rilanit special
Mixing, they are completely harmless, can be that disinfection soak keeps clear molten with the water-soluble poor disinfection sanitizer of hydrotropy
The key of liquid, effective disinfection composition for releasing wet tissue extrusion liquid.
Preferably, the Radix et Caulis Opuntiae Dillenii extract is Cactus Pedicel Aqueous extracts, rich in triterpene, malic acid, succinic acid etc.
Determination of Organic Acids has suppression to staphylococcus aureus, proteus, Escherichia coli, bacillus subtilis, Bacillus cercus
Production is used.Applicants have found that Radix et Caulis Opuntiae Dillenii extract is used together with disinfectant is compounded, disinfection effect can be enhanced,
Chemosterilant is reduced to the irritation of human skin.
Make preferably, the dirt detergent can predominantly play cleaning dirt in entirely disinfection soak system
With, and the nonionic surfactant or amphoteric surfactant of disinfectant bactericidal activity are not reduced, such as alkyl glycosides APG, sweet tea
Dish alkali CAB, cocounut oil 2C etc..
Preferably, the stabilizer is EDTA-2 sodium or EDTA-4 sodium.It must be added in right amount in disinfection soak steady
Agent is determined to increase the stability of product, can effectively solve after the disinfection soak of wet tissue contacts for a long time with non-woven fabrics, wet tissue
The problem of slowly turning to be yellow；The presence of stabilizer will not reduce the active constituent content of disinfection soak, can guarantee squeezing for wet tissue
Active constituent content can effectively release in liquid out, will not reduce sterilizing rate or Disinfection Effect.
Preferably, the pure water is the purified water that pasteurization towelette requires, the pure water of the present patent application is that RO is reverse osmosis
Water treatment facilities production, the water without any additive meets the purified water of pasteurization towelette through the detection of third party testing agency
It is required that；
Preferably, the non-woven fabrics is that pure cotton non-woven fabrics or full non-woven viscose fabric or bamboo fiber nonwovens or wood pulp are multiple
Non-woven fabrics or viscose glue terylene compound nonwoven cloth etc. are closed, non-woven fabrics the grammes per square metre scope used is in 40-55g/m2It is advisable.It is of the present invention
Disinfection soak can be used for disinfection wet tissue.
Obviously in the present invention, other raw materials can also be added by sterilizing in soak, such as extracting solution, hydrosol, freshener, be disappeared
The ingredients such as infusion, essence, the addition of these raw materials realize its respective function substantially, usually will not influence basic nature of the invention
Energy.Those skilled in the art are i.e. implementable without involving an inventive effort.
The present invention also provides a kind of preparation methods of the wet tissue of above-mentioned breathing mask cleaning-sterilizing, including walk as follows
It is rapid:
A) preparation disinfection soak
According to the proportion of wet tissue disinfection soak, first pure water is quantitatively adding in stainless steel stirred tank A, in stirring
Under, successively it is slowly added to guanidine disinfectant, (water-soluble poor disinfectant needs first dissolution aids to be taken to heat for other disinfectants
It is dissolved by heating in formula stainless steel stirred tank B, stand-by after cooling and standings), sequentially add Radix et Caulis Opuntiae Dillenii extract, dirt detergent
And disinfection soak is made after mixing evenly in stabilizer；The pH value general control of the solution is in 4.5~8.0 ranges, appearance
Must clear, no solid is precipitated or residual, set aside for use, it is ensured that after being added to non-woven fabrics, the disinfection of wet tissue extrusion liquid at
Point can effectively release, will not because of physical characteristics such as fibers adsorption or crystallizations, cause disinfectant effective component can not release or
The phenomenon that releasing on a small quantity causes Disinfection Effect insufficient.
B) wet tissue of breathing mask cleaning-sterilizing is prepared
Non-woven fabrics is passed through to the humidifier shower humidification of wet tissue machine with the disinfection soak of a) step, and controls wet tissue
Liquid content is 3.5~5.0 times, obtains the wet tissue.Wet tissue product for breathing mask cleaning-sterilizing of the invention, mainly
Including two kinds of manner of packings: one is bagged wet tissues, and one is barreled wet tissues.
Bagged wet tissue mainly uses following production method: the production of bagged wet tissue carries out on full-automatic wet tissue production line,
Nonwoven cloth material is first subjected to de- packet, previous ultraviolet sterilization is replaced with ozone disinfection, is disappeared to nonwoven cloth material
Poison, then upper machine auto-folder form, spray liquid feeding, are quantitatively adding above-mentioned disinfection soak, and controlling wet tissue liquid content is 3.5
It~4.5 times, cuts off in flakes, stacks, packaging seal after humidification, a kind of wet tissue of the invention has just been made after packaging, and (sack is wet
Towel).
Barreled wet tissue mainly uses following production method: the production of barreled wet tissue carries out on barreled wet tissue production line, with
The production technology of bagged wet tissue is different, and nonwoven cloth material is carried out de- packet, previous disinfection by ultraviolet light is replaced with ozone disinfection
Method carries out disinfection to nonwoven cloth material, then answers a pager's call through dry towel volume and carry out point off, rewinding, and cutting is packed into the wet tissue that ozonization is crossed
Tank bucket is quantitatively adding above-mentioned disinfection soak through automatic liquid feeder liquid filling, and controlling wet tissue liquid content is 4.0~5.0
Times, automatic sealing covers, and pastes circle mark, a kind of wet tissue of the invention (barreled wet tissue) has just been made after heat shrinkable package.Because of production
The difference of liquid feeding mode, barreled wet tissue liquid content need higher than bagged wet tissue liquid content, it is ensured that entire volume non-woven fabrics can all moisten
It is wet, facilitate wiping, guarantees cleaning and Disinfection Effect.
C) stability test: carrying out stability test to disinfection soak and wet tissue respectively, select 37 DEG C of Acceleration study method,
90d and/or 54 DEG C, 14d method assessment, it is ensured that disinfection soak and wet tissue will not turn yellow, crystallize or be precipitated solid component, guarantee
Disinfection composition validity.The sanitary condition of raw material, water quality and operating environment also has a significant impact to the shelf-life of product, if former
Material and operating environment polluted bacterium, be easy the effective component of consumption disinfectant, shorten the shelf-life, the presence of Radix et Caulis Opuntiae Dillenii extract
This defect can be made up.
Current barreled wet tissue of the present invention is usually used in medical and health organization；Bagged wet tissue is usually used in fire-fighting first aid and family
Front yard nursing.
Compared with prior art, the beneficial effects of the present invention are:
1, wide sterilization spectrum, Disinfection Effect are stablized: not only there is killing effect to bacterial propagule, saccharomytes, but also
There is killing effect to mould, bacterial spore, virus etc..It is detected through third party testing agency: to staphylococcus aureus, large intestine
The killing rate > 99.9% of the invasive organisms such as bacillus, Candida albicans.
2, it is suitble to the cleaning-sterilizing of the medical instruments such as CPAP ventilator mask, fire-fighting oxygen mask, dirt can be effectively removed
Dirt, grease stain, steam can effectively keep the health of mask, effectively prevent transmission.
3, product formula is mild, non-stimulated, corrosion-free, and stability is good, no pollution to the environment, safety and environmental protection.
4, product is also suitable for the disinfection of different hard surface materials, can be used for hospital, amusement park, Internet bar, supermarket, guest
The common objects surface sterilization in the places such as shop, office, family；The sanitizer formulations of low concentration can be adapted for human body hand, skin
The cleaning-sterilizing of skin, mucous membrane.
5, performance is stablized, long shelf-life, and safety is without side-effects, and spirituosity, consumer are not easy to use comfortably.
Specific embodiment
Below with reference to embodiment, the content of the present invention will be explained in more detail.It should be appreciated that implementation of the invention is not limited to
In the following examples, the accommodation in any form and/or change made to the present invention fall within the scope of the present invention.
In the present invention, if not refering in particular to, all parts, percentage are unit of weight, and all equipment and raw material etc. are equal
It is commercially available or the industry is common.If the method that embodiment uses is technology generally in the art without specializing.
The compounding disinfectant component that soak is sterilized in the present invention is selected according to table 1, is matched according to summary of the invention
It discloses part and gives any proportion.
1 disinfectant component compatibility table of table
Several exemplary embodiments are only enumerated below, and further explanation is made to the present invention:
Embodiment 1
A kind of wet tissue (bagged wet tissue) of breathing mask cleaning-sterilizing, by with cleaning function disinfection soak and carrying
Sterilize the non-woven fabrics composition of soak, wherein the disinfection soak contains based on every 100 parts by weight:
| Polyaminopropyl biguanide (20% content) | 0.5 |
| Benzalkonium chloride | 0.1 |
| Radix et Caulis Opuntiae Dillenii extract | 0.05 |
| Alkyl glycosides APG | 0.1 |
| EDTA-2 sodium | 0.05 |
| Pure water | Surplus |
The preparation method of this wet tissue (bagged wet tissue) includes the following steps:
A) preparation disinfection soak
According to the proportion of wet tissue disinfection soak, first pure water is quantitatively adding in stainless steel stirred tank A, in stirring
Under, be successively slowly added to polyaminopropyl biguanide, benzalkonium chloride, sequentially add Radix et Caulis Opuntiae Dillenii extract, alkyl glycosides APG and
Disinfection soak is made after mixing evenly in EDTA-2 sodium；Solution ph is about 6.5, clear, set aside for use.
B) wet tissue of breathing mask cleaning-sterilizing is prepared
The production of bagged wet tissue carries out on full-automatic wet tissue production line, nonwoven cloth material is first carried out de- packet, through ozone
After disinfection, upper machine auto-folder molding is quantitatively adding above-mentioned disinfection soak, and controlling wet tissue liquid content is 3.5 times, humidification
Cutting in flakes, stacks, packaging seal afterwards, and a kind of wet tissue of the invention, i.e. bagged wet tissue has just been made after packaging.
C) it sterilizes soak and bagged wet tissue passes through 37 DEG C of Acceleration study method, the stability test of 90d.
Embodiment 2
A kind of wet tissue of breathing mask cleaning-sterilizing (barreled wet tissue), by with cleaning function disinfection soak and carrying
Sterilize the non-woven fabrics composition of soak, wherein the disinfection soak contains based on every 100 parts by weight:
| Polyaminopropyl biguanide (20% content) | 1.0 |
| Triclosan | 0.3 |
| Propylene glycol | 3.0 |
| Radix et Caulis Opuntiae Dillenii extract | 0.05 |
| Glycine betaine CAB | 0.1 |
| EDTA-4 sodium | 0.05 |
| Pure water | Surplus |
The preparation method of this wet tissue (barreled wet tissue) includes the following steps:
A) preparation disinfection soak
According to the proportion of wet tissue disinfection soak, first pure water is quantitatively adding in stainless steel stirred tank A, in stirring
Under, it is successively slowly added to polyaminopropyl biguanide, triclosan and propylene glycol mixture and (first stirs propylene glycol addition heated type stainless steel
Kettle B is mixed, triclosan is added in stirring, after being heated to 50 DEG C of dissolutions, obtains clear liquid, stand-by after cooling and standings), then according to
Disinfection soak is made after mixing evenly in secondary addition Radix et Caulis Opuntiae Dillenii extract, glycine betaine CAB and EDTA-4 sodium；The pH value of solution is
6.0, clear, set aside for use.
B) wet tissue of breathing mask cleaning-sterilizing is prepared
The production of barreled wet tissue carries out on barreled wet tissue production line, different from the liquid feeding of bagged wet tissue sequence, first by nothing
Woven fabric material carries out de- packet, after ozonization, answers a pager's call through dry towel volume and carries out point off, and rewinding, cutting is packed into what ozonization was crossed
Wet tissue tank bucket, then through automatic liquid feeder liquid filling, it is quantitatively adding above-mentioned disinfection soak, and controlling wet tissue liquid content is 4.5
Times, automatic sealing covers, labeling, and a kind of wet tissue of the invention, i.e. barreled wet tissue has just been made after heat shrinkable package.Barreled is wet
Towel liquid content needs higher than bagged wet tissue liquid content, it is ensured that entire volume non-woven fabrics can be soaked all, facilitate wiping, guarantee cleaning and
Disinfection Effect.
C) it sterilizes soak and barreled wet tissue passes through 37 DEG C of Acceleration study method, the stability test of 90d.
Embodiment 3
A kind of wet tissue (bagged wet tissue) of breathing mask cleaning-sterilizing, by with cleaning function disinfection soak and carrying
Sterilize the non-woven fabrics composition of soak, wherein the disinfection soak contains based on every 100 parts by weight:
The preparation method of this wet tissue (bagged wet tissue) includes the following steps:
A) preparation disinfection soak
According to the proportion of wet tissue disinfection soak, first pure water is quantitatively adding in stainless steel stirred tank A, in stirring
Under, chlorhexidine gluconate, triclocarban and CO40 hydrogenated castor oil mixture are successively slowly added to (first by CO40 hydrogenated castor
Heated type stainless steel stirred tank B is added in oil, is heated to 60 DEG C, triclocarban is added in stirring, after all dissolutions, is clarified
Transparency liquid, stand-by after cooling and standings), Radix et Caulis Opuntiae Dillenii extract and EDTA-2 sodium are added, after mixing evenly, disinfection is made and impregnates
Liquid；The pH value of solution is 6.0, clear, set aside for use.Because CO40 rilanit special itself has certain surface-active,
It can add or be not added dirt detergent in formula less.
B) wet tissue of breathing mask cleaning-sterilizing is prepared
The production of bagged wet tissue carries out on full-automatic wet tissue production line, nonwoven cloth material is first carried out de- packet, through ozone
After disinfection, upper machine folding forming is quantitatively adding above-mentioned disinfection soak, and controlling wet tissue liquid content is 4.0 times, is cut after humidification
It is broken into piece, is stacked, packaging seal, a kind of wet tissue of the invention, i.e. bagged wet tissue has just been made after packaging.
C) it sterilizes soak and bagged wet tissue passes through 37 DEG C of Acceleration study method, the stability test of 90d.
Embodiment 4
A kind of wet tissue of breathing mask cleaning-sterilizing (barreled wet tissue), by with cleaning function disinfection soak and carrying
Sterilize the non-woven fabrics composition of soak, wherein the disinfection soak contains based on every 100 parts by weight:
| Chlorhexidine gluconate (20% content) | 1.5 |
| Chlorphenesin | 0.3 |
| Dipropylene glycol | 3.0 |
| Radix et Caulis Opuntiae Dillenii extract | 0.1 |
| Cocounut oil 2C | 0.05 |
| EDTA-4 sodium | 0.05 |
| Pure water | Surplus |
The preparation method of this wet tissue (barreled wet tissue) includes the following steps:
A) preparation disinfection soak
According to the proportion of wet tissue disinfection soak, first pure water is quantitatively adding in stainless steel stirred tank A, in stirring
Under, it is successively slowly added to chlorhexidine gluconate, Chlorphenesin and dipropylene glycol mixture and (heated type first is added in dipropylene glycol
Chlorphenesin is added in stirring in stainless steel stirred tank B, after being heated to 50 DEG C of dissolutions, clear liquid is obtained, after cooling and standings
For use), Radix et Caulis Opuntiae Dillenii extract is sequentially added, disinfection soak is made after mixing evenly in cocounut oil 2C and EDTA-4 sodium；Solution
PH value is about 6.5, clear, set aside for use.
B) wet tissue of breathing mask cleaning-sterilizing is prepared
The production of barreled wet tissue carries out on barreled wet tissue production line, and nonwoven cloth material is first carried out de- packet, is disappeared through ozone
It after poison, answers a pager's call through dry towel volume and carries out point off, rewinding, cutting is packed into the wet tissue tank bucket that ozonization is crossed, then through automatic liquid feeder
Liquid filling is quantitatively adding above-mentioned disinfection soak, and controlling wet tissue liquid content is 4.5 times, and automatic sealing covers, and labeling, heat is received
A kind of wet tissue of the invention, i.e. barreled wet tissue has just been made after contracting packaging.Barreled wet tissue liquid content is needed than bagged wet tissue containing liquid
Amount wants high, it is ensured that entire volume non-woven fabrics can be soaked all, facilitate wiping, guarantee cleaning and Disinfection Effect.
C) it sterilizes soak and barreled wet tissue passes through 54 DEG C of Acceleration study method, the stability test of 14d.
Embodiment 5
A kind of wet tissue (bagged wet tissue) of breathing mask cleaning-sterilizing, by with cleaning function disinfection soak and carrying
Sterilize the non-woven fabrics composition of soak, wherein the disinfection soak contains based on every 100 parts by weight:
| Chlorhexidine acetate | 0.3 |
| Propylene glycol | 2.0 |
| Benzethonium chloride | 0.1 |
| Radix et Caulis Opuntiae Dillenii extract | 0.05 |
| Alkyl glycosides APG | 0.1 |
| EDTA-2 sodium | 0.05 |
| Pure water | Surplus |
The preparation method of this wet tissue (bagged wet tissue) includes the following steps:
A) preparation disinfection soak
According to the proportion of wet tissue disinfection soak, first pure water is quantitatively adding in stainless steel stirred tank A, in stirring
Under, it sequentially adds chlorhexidine acetate and propylene glycol mixture and (propylene glycol is first added heated type stainless steel stirred tank B, in stirring
It is chlorhexidine acetate is added, after being heated to 50 DEG C of dissolutions, obtains clear liquid, stand-by after cooling and standings), benzethonium chloride it is slow
To pure water is added, Radix et Caulis Opuntiae Dillenii extract, alkyl glycosides APG and EDTA-2 sodium are sequentially added, after mixing evenly, disinfection leaching is made
Steep liquid；The pH value of solution is 6.0, clear, set aside for use.
B) wet tissue of breathing mask cleaning-sterilizing is prepared
The production of bagged wet tissue carries out on full-automatic wet tissue production line, nonwoven cloth material is first carried out de- packet, through ozone
After disinfection, upper machine folding forming is quantitatively adding above-mentioned disinfection soak, and controlling wet tissue liquid content is 4.0 times, is cut after humidification
It is broken into piece, is stacked, packaging seal, a kind of wet tissue of the invention, i.e. bagged wet tissue has just been made after packaging.
C) it sterilizes soak and bagged wet tissue passes through 54 DEG C of Acceleration study method, the stability test of 14d.
Embodiment 6
A kind of wet tissue of breathing mask cleaning-sterilizing (barreled wet tissue), by with cleaning function disinfection soak and carrying
Sterilize the non-woven fabrics composition of soak, wherein the disinfection soak contains based on every 100 parts by weight:
| Chlorhexidine acetate | 0.3 |
| Dipropylene glycol | 3.0 |
| Cetylpyridinium Chloride | 0.3 |
| Radix et Caulis Opuntiae Dillenii extract | 0.1 |
| Glycine betaine CAB | 0.1 |
| EDTA-4 sodium | 0.05 |
| Pure water | Surplus |
The preparation method of this wet tissue (barreled wet tissue) includes the following steps:
A) preparation disinfection soak
According to the proportion of wet tissue disinfection soak, first pure water is quantitatively adding in stainless steel stirred tank A, in stirring
Under, it is successively slowly added to chlorhexidine acetate and (first heated type stainless steel stirred tank is added in dipropylene glycol by dipropylene glycol mixture
Chlorhexidine acetate is added in stirring in B, after being heated to 50 DEG C of dissolutions, obtains clear liquid, stand-by after cooling and standings), western pyrrole
Oronain sequentially adds Radix et Caulis Opuntiae Dillenii extract, disinfection soak is made after mixing evenly in glycine betaine CAB and EDTA-4 sodium；It is molten
Liquid pH value is about 6.0, clear, set aside for use.
B) wet tissue of breathing mask cleaning-sterilizing is prepared
The production of barreled wet tissue carries out on barreled wet tissue production line, and nonwoven cloth material is first carried out de- packet, is disappeared through ozone
It after poison, answers a pager's call through dry towel volume and carries out point off, rewinding, cutting is packed into the wet tissue tank bucket that ozonization is crossed, then through automatic liquid feeder
Liquid filling is quantitatively adding above-mentioned disinfection soak, and controlling wet tissue liquid content is 5.0 times, and automatic sealing covers, and labeling, heat is received
A kind of wet tissue of the invention, i.e. barreled wet tissue has just been made after contracting packaging.Barreled wet tissue liquid content is needed than bagged wet tissue containing liquid
Amount wants high, it is ensured that entire volume non-woven fabrics can be soaked all, facilitate wiping, guarantee cleaning and Disinfection Effect.
C) it sterilizes soak and barreled wet tissue passes through 54 DEG C of Acceleration study method, the stability test of 14d.
The disinfection soak of above-described embodiment 1-6 can also be interchangeable with manner of packing (packed and barreled), not influenced
The preparation of product bactericidal effect and product.
Embodiment 7
In order to verify sterilizing effect of the invention, the disinfection soak of Example 1~6 carries out bactericidal effect survey
Examination.Method, result, the conclusion of test are as follows:
Test method: being tested, action time 2min, 5min by " disinfection technology standard " (version in 2002), is tested
Temperature is 19~21 DEG C.
Test result such as table 2:
Table 2 is averaged killing rate table
Test result: test sample to staphylococcus aureus, Escherichia coli, Candida albicans act on respectively 2min and
5min, average killing rate is 100%, has apparent sterilizing effect.
Rule to wet tissue made of embodiment, according to GB15979-2002 " Disposable Sanitary Accessory sanitary standard "
Provisioning request, to following project total number of bacterial colonies, fungus colony sum, coliform, Pseudomonas aeruginosa, Staphylococcus aureus
Bacterium, hemolytic streptococcus are examined, and are not detected, and testing result is all up to standard.
To wet tissue made of embodiment, product other technologies index subjet according to GB/T 27728-2011 " wet tissue "
Regulation, to following project: deviation, liquid content, package encapsulation, pH value, detergency, corrosivity, transportable property fluorescent brightening
Agent etc. is detected, and testing result is all up to standard.
Sample of the invention is measured through INTERTEK company, third party authority testing agency, detection method: according to
GB15979-2002 standard appendix C product bactericidal property, bacteriostasis property and stability test method.Test and result such as the following table 3:
3 sterilizing rate table of table
Currently, the technology has been applied to the P ü RDOUX CPAP MASK of Canadian Choice One Medical company
(3wipes) bagged wet tissue (3wipes and 10wipes), barreled wet tissue (70wipes)；Canadian Resplabs Medical
Inc. the barreled wet tissue The Original CPAP MASK WIPES (110wipes) of company；South America Tottus disinfection is wet
Towel: barreled wet tissue 35 and bagged wet tissue 40 etc..
Although inventor has done more detailed elaboration to technical solution of the present invention and has enumerated, it should be understood that right
For the those skilled in the art of this field one, above-described embodiment is modified and/or flexible or replaced using equivalent
Be for scheme it is obvious, cannot all be detached from the essence of spirit of that invention, the term occurred in the present invention is used for the technology of the present invention
The elaboration and understanding of scheme, can not be construed as limiting the invention.
Claims (10)
1. a kind of wet tissue for breathing mask cleaning-sterilizing, by the non-woven fabrics group of disinfection soak and carrying disinfection soak
At, which is characterized in that the disinfection soak contains based on every 100 parts by weight:
(1) 0.1~3.0% compounding disinfectant；
(2) 0.05~1.0% Radix et Caulis Opuntiae Dillenii extract；
(3) surplus is pure water.
2. a kind of wet tissue for breathing mask cleaning-sterilizing, by the non-woven fabrics group of disinfection soak and carrying disinfection soak
At, which is characterized in that the disinfection soak contains based on every 100 parts by weight:
(1) 0.1~3.0% compounding disinfectant；
(2) 0.0~10.0% dissolution aids；
(3) 0.05~1.0% Radix et Caulis Opuntiae Dillenii extract；
(4) 0.0~1.0% dirt detergent；
(5) 0.05~0.5% stabilizer；
(6) surplus is pure water.
3. the wet tissue of breathing mask cleaning-sterilizing as claimed in claim 1 or 2, which is characterized in that the compounding disinfectant
It is composed for guanidine disinfectant and other disinfection sanitizers.
4. the wet tissue of breathing mask cleaning-sterilizing as claimed in claim 3, which is characterized in that the guanidine disinfectant is optional
From polyaminopropyl biguanide, chlorhexidine gluconate or chlorhexidine acetate；Other disinfection sanitizers can be selected from benzalkonium chloride, benzyl rope chlorine
Ammonium, triclosan, triclocarban, Chlorphenesin or Cetylpyridinium Chloride.
5. the wet tissue of breathing mask cleaning-sterilizing as claimed in claim 1 or 2, which is characterized in that the cactus is extracted
Object is Cactus Pedicel Aqueous extracts.
6. the wet tissue of breathing mask cleaning-sterilizing as claimed in claim 2, which is characterized in that the dissolution aids are the third two
Any one or more mixing of -40 castor oil of alcohol, dipropylene glycol or polyethylene glycol.
7. the wet tissue of breathing mask cleaning-sterilizing as claimed in claim 2, which is characterized in that the dirt detergent is alkane
Base glucosides APG, glycine betaine CAB, cocounut oil 2C's is any.
8. the wet tissue of breathing mask cleaning-sterilizing as claimed in claim 2, which is characterized in that the stabilizer is EDTA-2
Sodium or EDTA-4 sodium.
9. the wet tissue of breathing mask cleaning-sterilizing as claimed in claim 2, which is characterized in that the non-woven fabrics be pure cotton without
Woven fabric, full non-woven viscose fabric, bamboo fiber nonwovens, wood pulp compound nonwoven cloth, viscose glue terylene compound nonwoven cloth it is any.
10. a kind of method for preparing wet tissue as claimed in claim 1 or 2, which is characterized in that the preparation method includes such as
Lower step:
A) preparation disinfection soak
According to the proportion of wet tissue disinfection soak, first pure water is quantitatively adding in stainless steel stirred tank A, under stirring, according to
It is secondary to be slowly added to guanidine disinfectant, other disinfectants, Radix et Caulis Opuntiae Dillenii extract, dirt detergent and stabilizer are sequentially added, is stirred
After mixing uniformly, disinfection soak is made；
B) wet tissue of breathing mask cleaning-sterilizing is prepared
Non-woven fabrics is passed through to the humidifier shower humidification of wet tissue machine with the disinfection soak of a) step, and controls wet tissue containing liquid
Amount is 3.5~5.0 times, obtains the wet tissue.
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| CN201910834407.7A CN110477792A (en) | 2019-09-05 | 2019-09-05 | A kind of nonalcoholic wet tissue and preparation method thereof can be used for breathing mask cleaning-sterilizing |
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