CN110477436A - A kind of preparation method and application of flavouring essence for tobacco sustained-release particle - Google Patents
A kind of preparation method and application of flavouring essence for tobacco sustained-release particle Download PDFInfo
- Publication number
- CN110477436A CN110477436A CN201910698872.2A CN201910698872A CN110477436A CN 110477436 A CN110477436 A CN 110477436A CN 201910698872 A CN201910698872 A CN 201910698872A CN 110477436 A CN110477436 A CN 110477436A
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- China
- Prior art keywords
- tobacco
- preparation
- sustained
- flavouring essence
- release particle
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
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- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The present invention provides a kind of preparation methods of flavouring essence for tobacco sustained-release particle, comprising the following steps: tobacco aromaticss are added in polarity or solvent containing emulsifier S1., are uniformly mixed, obtain preparation liquid；S2. stationary phase carrier is prepared；S3. preparation liquid and stationary phase carrier are mixed, so that stationary phase fully absorbs preparation liquid；S4. stationary phase carrier residual solvent in step S3 is removed.Sustained-release particle of the invention includes essence particle, and heating process slow release fragrance position is uniformly distributed it, forms mellow in taste sensory experience.
Description
Technical field
The present invention relates to cigarette additive manufacturing fields, and in particular to a kind of preparation method of flavouring essence for tobacco sustained-release particle.
Background technique
Flavors and fragrances is added in cigarette, its role is to improve the physicochemical property of cigarette, mellow and full fragrance, modification cigarette perfume
Taste improves the style inhaled taste, establish product, affects smell, the sense of taste and the tactile of consumer to a certain extent, promotes and produce
The acceptability of product.Tobacco aromaticss can be directly added into tobacco component, also may be added to filter tip, cigarette paper, packing timber
Material.Tobacco aromaticss source is broadly divided into 3 types, the fragrance from tobacco itself, non-tobacco natural perfume material and people at present
The fragrance of work synthesis.Tobacco essence oil can be extracted with multi-solvents at different temperature；Non-tobacco natural perfume material refers to from removing
Various plants other than tobacco or the extract in animal, are such as extracted from the flower of various plants, fruit, leaf, stem, root or skin
Essential oil or water out, alcohol steep object such as medicinal extract, can agent etc..Artificial synthesized fragrance is chemical products.
Tobacco aromaticss are a kind of special commodity, in use should be in view of the influence to cigarette product, again
The health of smoker is considered, no matter therefore which kind of approach should all have certain perfume (or spice) using essence, fragrance by tobacco
Type and fragrance characteristic can transmit graceful fragrance in smoking process and inhale taste, furthermore have corresponding adaptability and steady to tobacco
It is qualitative, and with matrix or ingredient phase harmony.Meanwhile existing processing technology should be met, and to avoid a larger increase of cost,
Unless really need and invest relatively rationally, flavouring essence for tobacco reply improve production quality and reduce cost should have it is certain significantly
Contribution, becomes more readily available and satisfactory quality, processing and use all securely and reliably should not damage human health, and
Internal and international related regulation is not violated.
Summary of the invention
Technical problems to be solved: the invention discloses a kind of preparation method of flavouring essence for tobacco sustained-release particle, main purposes
It is to solve that flavouring essence for tobacco is volatile in use leads to problems such as later period line effect not good enough.By the present invention in that using polarity
Or tobacco aromaticss are formed evenly dispersed system by emulsified solvent, prepare preparation liquid.Stationary phase well prepared in advance is carried
Body comes into full contact with therewith, into stationary phase inside or is incorporated in micropore system, and solvent removal is obtained compact sustained release
Particle.This particle includes essence particle, and heating process slow release fragrance position is uniformly distributed it, forms mellow in taste sense
Official's experience.
A kind of technical solution: preparation method of flavouring essence for tobacco sustained-release particle, comprising the following steps:
S1. tobacco aromaticss are added in polarity or solvent containing emulsifier, are uniformly mixed, obtain preparation liquid；
S2. stationary phase carrier is prepared；
S3. preparation liquid and stationary phase carrier are mixed, so that stationary phase fully absorbs preparation liquid；
S4. stationary phase carrier residual solvent in step S3 is removed.
Further, the mass ratio of tobacco aromaticss described in step S1 and solvent is 1:1-10, and the solution is that dispersion is equal
Even solution or coarse dispersion system, dispersed phase ionic diameter is 1-100um in the coarse dispersion system.
Further, polar solvent described in step S1 is the strong alcohols of polarity, lipid, ethers or ketone, wherein lipid
For in soybean lecithin or lecithin any one or both mixture.
Further, emulsifier described in step S1 is cholesterol, poly yamanashi esters, polyoxyethylene fatty acid ester or polyoxy
In ethylene polyoxypropylene copolymeric body class any one or both mixture.
Further, stationary phase carrier is phenolic resin, polyester resin, polyamide, active carbon, ceramics in step S2
In particle, offal or offal reconstructed particle any one or both mixture.
Further, the mixed method of preparation liquid and stationary phase carrier is mixing, Dynamic Adsorption or change in step S3
The combination of any one or two kinds and above method in crosslinking is learned, wherein reagent used in being chemically crosslinked is with double property bases
The crosslinking agent of group, such as glutaraldehyde.
Further, stationary phase carrier residual solvent minimizing technology is vacuum drying, freeze-drying or reagent in step S4
Any one in extraction.
Further, the grain diameter of flavouring essence for tobacco sustained-release particle is 50-1000um, and the material containing amount of sustained-release particle is 1-
50%。
Further, the Dynamic Adsorption includes chromatography scheme or supercritical fluid absorption.
Application of the flavouring essence for tobacco sustained-release particle of above-mentioned preparation method preparation in cigarette field.
The utility model has the advantages that tobacco sustained-release particle of the invention has the advantage that
The present invention, by the way that flavouring essence for tobacco to be fused in solid phase particles, is formed on existing tobacco essence raw material basis
The mitigation of flavor matter discharges, so that steady entire essence bring pessimal stimulation sense, alleviates sense organ strain and brought in the process
Preceding weight after light otherness, the slow-releasing granules of preparation can fit preferably by the steady mild of the volatile aroma of flavouring essence for tobacco
For being used in different tobacco products.
Specific embodiment
Embodiment 1
S1. 100g free nicotine is added in the ethanol solution of 100mL, 15min is mixed under the revolving speed of 150rpm, obtains
To preparation liquid；
S2. ceramic particle is taken, the particle that partial size is 50um is filtered out；
S3. the ceramic particle after screening in step S2 is fitted into chromatography column, diameter height compares for 1:5, then by step S1 system
Standby preparation liquid passes through in chromatographic column, flow velocity 1mL/min；
S4. after preparation liquid passes through completely, ceramic particle is taken out, vacuum drying obtains tobacco sustained-release particle.
It smokes panel test to finished cigarettes made of the present embodiment, through smokeing panel test, the soft exquisiteness of cigarette perfume, fragrance is naturally, pleasant impression is dry
It is net comfortable.
Embodiment 2
S1. 100g essential oil of tobaccos is added in the ethanol solution of 100mL, 15min is mixed under the revolving speed of 150rpm, obtains
To preparation liquid；
S2. tobacco reconstructed particle is taken, the particle that partial size is 1000um is filtered out；
S3. the tobacco reconstructed particle after screening in step S2 is fitted into chromatography column, diameter height compares for 1:10, then will walk
The preparation liquid of rapid S1 preparation is by the way that in chromatographic column, flow velocity 20mL/min iterates through chromatographic column, up to what is contained in preparation liquid
Essential oil of tobaccos content is lower；
S4. after preparation liquid passes through completely, tobacco reconstructed particle is taken out, freeze-drying obtains tobacco sustained-release particle.
Smoke panel test to finished cigarettes made of the present embodiment, through smokeing panel test, aroma substance release uniformly, without bad breath,
Fragrance lasting stability.
Embodiment 3
S1. 100g tobacco alcohol extract is added in the lecithin soln of 1000mL, is mixed under the revolving speed of 150rpm
15min obtains preparation liquid；
S2. tobacco reconstructed particle is taken, the particle that partial size is 500um is filtered out；
S3. the tobacco reconstructed particle after screening in step S2 is added in preparation liquid, is mixed, until containing in preparation liquid
Tobacco alcohol extract content it is lower；
S4. it filters, takes out tobacco reconstructed particle, freeze-drying obtains tobacco sustained-release particle.
It smokes panel test, is smoked panel test to finished cigarettes made of the present embodiment, adopting cigarette perfume can uniformly be released effectively, and aftertaste is continuous
It is long.
Embodiment 4
S1. 100g free nicotine is added in the cholesterol solution of 1000mL, 15min is mixed under the revolving speed of 200rpm,
Obtain preparation liquid；
S2. offal is taken, the particle that partial size is 500um is filtered out；
S3. the offal after screening in step S2 is added in preparation liquid, 5h is mixed, until what is contained in preparation liquid is free
Nicotine content is lower；
S4. it filters, takes out offal, freeze-drying obtains tobacco sustained-release particle.
It smokes panel test to finished cigarettes made of the present embodiment, through smokeing panel test, which can promote cigarette perfume
Gas is rich, improves aroma quality, reduces miscellaneous gas and irritation.
Embodiment 5
S1. 100g free nicotine is added in the cholesterol solution of 1000mL, 15min is mixed under the revolving speed of 200rpm,
Obtain preparation liquid；
S2. offal is taken, the particle that partial size is 500um is filtered out；
S3. the offal after screening in step S2 is added in preparation liquid, 1h is mixed, until what is contained in preparation liquid is free
Nicotine content is lower；
S4. it filters, takes out offal, freeze-drying obtains tobacco sustained-release particle.
Smoke panel test to finished cigarettes made of the present embodiment, through smokeing panel test, using the tobacco sustained-release particle cigarette from
Right cigarette perfume is pure, and aesthetic quality is excellent.
Embodiment 6
S1. 100g essential oil of tobaccos is added in the ethanol solution of 1000mL, 15min is mixed under the revolving speed of 200rpm, obtains
To preparation liquid；
S2. offal is taken, the particle that partial size is 500um is filtered out；
S3. the offal after screening in step S2 is added in preparation liquid, crosslinking agent glutaraldehyde, cross-linking reaction 5h is added；
S4. it filters, takes out offal, freeze-drying obtains tobacco sustained-release particle.
It smokes panel test to finished cigarettes made of the present embodiment, through smokeing panel test, cigarette perfume exquisiteness is soft, and fragrance is non-stimulated, pleasant impression
It is clean comfortable.
Embodiment 7
S1. 100g essential oil of tobaccos is added in the acetone soln of 1000mL, 15min is mixed under the revolving speed of 200rpm, obtains
To preparation liquid；
S2. offal is taken, the particle that partial size is 500um is filtered out,；
S3. the offal after screening in step S2 is added and is encased in overcritical two extractions kettle, be passed through CO2Fluid, by the liquid in S1
Adverse current sprays into an extraction kettle, and 25 DEG C of condition, pressure 35MPa, flow velocity 0.5L/min, two extract 40 DEG C of temperature in kettles, and pressure is
10MPa, flow velocity 5L/min；
S4. offal is taken out, tobacco sustained-release particle is obtained.
It smokes panel test to finished cigarettes made of the present embodiment, through smokeing panel test, fragrance is plentiful, and without miscellaneous, pleasant impression is completely comfortable.
Embodiment 8
S1. 100g essential oil of tobaccos is added in the acetone soln of 1000mL, 15min is mixed under the revolving speed of 150rpm, obtains
To preparation liquid；
S2. offal is taken, the particle that partial size is 300um is filtered out,；
S3. the offal after screening in step S2 is added and is encased in overcritical two extractions kettle, be passed through CO2Fluid, by the liquid in S1
Adverse current sprays into an extraction kettle, and 40 DEG C of condition, pressure 15MPa, flow velocity 5L/min, two extract 30 DEG C of temperature in kettles, and pressure is
15MPa, flow velocity 3L/min；
S4. offal is taken out, tobacco sustained-release particle is obtained.
It smokes panel test to finished cigarettes made of the present embodiment, through smokeing panel test, fragrance is sufficient, and non-stimulated, pleasant impression is pure comfortable.
Comparative example 1
S1. 100g free nicotine is added in the cholesterol solution of 1000mL, 15min is mixed under the revolving speed of 200rpm,
Obtain preparation liquid；
S2. offal is taken, the particle that partial size is 2000um is filtered out；
S3. the offal after screening in step S2 is added in preparation liquid, 1h is mixed, until what is contained in preparation liquid is free
Nicotine content is lower；
S4. it filters, takes out offal, freeze-drying obtains tobacco sustained-release particle.
It smokes panel test to finished cigarettes made of the present embodiment, through smokeing panel test, is filled using the cigarette perfume of the tobacco sustained-release particle
It is sufficient but slightly coarse, it is micro- to have miscellaneous gas.
Claims (10)
1. a kind of preparation method of flavouring essence for tobacco sustained-release particle, which comprises the following steps:
S1. tobacco aromaticss are added in polarity or solvent containing emulsifier, are uniformly mixed, obtain preparation liquid；
S2. stationary phase carrier is prepared；
S3. preparation liquid and stationary phase carrier are mixed, so that stationary phase fully absorbs preparation liquid；
S4. stationary phase carrier residual solvent in step S3 is removed.
2. a kind of preparation method of flavouring essence for tobacco sustained-release particle according to claim 1, it is characterised in that: institute in step S1
The mass ratio for stating tobacco aromaticss and solvent is 1:1-10, and the solution is finely dispersed solution or coarse dispersion system, described thick
Dispersed phase ionic diameter is 1-100um in dispersion.
3. a kind of preparation method of flavouring essence for tobacco sustained-release particle according to claim 1, it is characterised in that: institute in step S1
Stating polar solvent is the strong alcohols of polarity, lipid, ethers or ketone, and wherein lipid is any one in soybean lecithin or lecithin
Kind or both mixture.
4. a kind of preparation method of flavouring essence for tobacco sustained-release particle according to claim 1, it is characterised in that: institute in step S1
Stating emulsifier is appointing in cholesterol, poly yamanashi esters, polyoxyethylene fatty acid ester or polyoxyethylene polyoxypropylene copolymer class
Meaning one or both mixture.
5. a kind of preparation method of flavouring essence for tobacco sustained-release particle according to claim 1, it is characterised in that: solid in step S2
Determining phase carrier is in phenolic resin, polyester resin, polyamide, active carbon, ceramic particle, offal or offal reconstructed particle
Any one or both mixture.
6. a kind of preparation method of flavouring essence for tobacco sustained-release particle according to claim 1, it is characterised in that: pre- in step S3
The mixed method of standby liquid and stationary phase carrier be mixed, Dynamic Adsorption or any one or two kinds in being chemically crosslinked and with
The combination of upper method, wherein reagent used in being chemically crosslinked is the crosslinking agent with double property groups.
7. a kind of preparation method of flavouring essence for tobacco sustained-release particle according to claim 1, it is characterised in that: solid in step S4
Determining phase carrier residual solvent minimizing technology is any one in vacuum drying, freeze-drying or reagent extraction.
8. a kind of preparation method of flavouring essence for tobacco sustained-release particle according to claim 1, it is characterised in that: flavouring essence for tobacco is slow
The grain diameter for releasing particle is 50-1000um, and the material containing amount of sustained-release particle is 1-50%.
9. a kind of preparation method of flavouring essence for tobacco sustained-release particle according to claim 6, it is characterised in that: the dynamic
Absorption includes that chromatography scheme or supercritical fluid adsorb.
10. the flavouring essence for tobacco sustained-release particle of preparation method preparation according to claims 1-8 is in the application in cigarette field.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910698872.2A CN110477436A (en) | 2019-07-31 | 2019-07-31 | A kind of preparation method and application of flavouring essence for tobacco sustained-release particle |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910698872.2A CN110477436A (en) | 2019-07-31 | 2019-07-31 | A kind of preparation method and application of flavouring essence for tobacco sustained-release particle |
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| CN201910698872.2A Pending CN110477436A (en) | 2019-07-31 | 2019-07-31 | A kind of preparation method and application of flavouring essence for tobacco sustained-release particle |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110916240A (en) * | 2019-12-16 | 2020-03-27 | 云南中烟新材料科技有限公司 | Method for preparing cigarette filter stick aroma-enhancing pellets by using thin and short tobacco stems |
| CN113180274A (en) * | 2021-04-26 | 2021-07-30 | 河南中烟工业有限责任公司 | Reconstituted tobacco |
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| CN102823945A (en) * | 2012-09-17 | 2012-12-19 | 川渝中烟工业有限责任公司 | Essence particle additive as well as preparation method and application thereof |
| US20150080265A1 (en) * | 2013-09-18 | 2015-03-19 | The Werc Shop, LLC | Terpene-based compositions, processes, methodologies for creation and products thereby |
| CN105112162A (en) * | 2015-08-25 | 2015-12-02 | 东莞波顿香料有限公司 | Multifunctional essence slow-release carrier and preparation method thereof |
| CN108024572A (en) * | 2015-09-30 | 2018-05-11 | 菲利普莫里斯生产公司 | Aerosol generation product with dispersed spices |
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2019
- 2019-07-31 CN CN201910698872.2A patent/CN110477436A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102007043776A1 (en) * | 2007-09-13 | 2009-03-26 | Graner, Gerhard, Dr. | Use of microcapsules and microcapsules |
| CN102823945A (en) * | 2012-09-17 | 2012-12-19 | 川渝中烟工业有限责任公司 | Essence particle additive as well as preparation method and application thereof |
| US20150080265A1 (en) * | 2013-09-18 | 2015-03-19 | The Werc Shop, LLC | Terpene-based compositions, processes, methodologies for creation and products thereby |
| CN105112162A (en) * | 2015-08-25 | 2015-12-02 | 东莞波顿香料有限公司 | Multifunctional essence slow-release carrier and preparation method thereof |
| CN108024572A (en) * | 2015-09-30 | 2018-05-11 | 菲利普莫里斯生产公司 | Aerosol generation product with dispersed spices |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110916240A (en) * | 2019-12-16 | 2020-03-27 | 云南中烟新材料科技有限公司 | Method for preparing cigarette filter stick aroma-enhancing pellets by using thin and short tobacco stems |
| CN110916240B (en) * | 2019-12-16 | 2021-11-02 | 云南中烟新材料科技有限公司 | Method for preparing cigarette filter stick aroma-enhancing pellets by using thin and short tobacco stems |
| CN113180274A (en) * | 2021-04-26 | 2021-07-30 | 河南中烟工业有限责任公司 | Reconstituted tobacco |
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Application publication date: 20191122 |