CN110465250A - A kind of microcapsules compound wall materials, microcapsule essence and its preparation method and application - Google Patents
A kind of microcapsules compound wall materials, microcapsule essence and its preparation method and application Download PDFInfo
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- CN110465250A CN110465250A CN201910732563.2A CN201910732563A CN110465250A CN 110465250 A CN110465250 A CN 110465250A CN 201910732563 A CN201910732563 A CN 201910732563A CN 110465250 A CN110465250 A CN 110465250A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/94—Mixtures with anionic, cationic or non-ionic compounds
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/34—Organic compounds containing sulfur
- C11D3/349—Organic compounds containing sulfur additionally containing nitrogen atoms, e.g. nitro, nitroso, amino, imino, nitrilo, nitrile groups containing compounds or their derivatives or thio urea
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
- C11D3/502—Protected perfumes
- C11D3/505—Protected perfumes encapsulated or adsorbed on a carrier, e.g. zeolite or clay
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/29—Sulfates of polyoxyalkylene ethers
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/667—Neutral esters, e.g. sorbitan esters
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/90—Betaines
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Abstract
The present invention provides a kind of microcapsules compound wall materials, microcapsule essence and its preparation method and application; the microcapsules compound wall materials include xanthan gum, chitosan oligosaccharide, deionized water and preservative; they form both effectiveness wall material and protect outer layer, and the solubilizer and essence of wrapping inner layer form microcapsule essence.Not only can to avoid destruction of the equipment whipping process to essence microcapsule in production, but also can to avoid fragrance matter directly heated, light influence and cause oxidation deterioration, avoid the volatilization of effective component, effectively control the release of fragrance matter, improve the stability of fragrance.By the addition of chitosan oligosaccharide, essence protective bulkhead film is on the one hand formed, another aspect has apparent moisturizing again, activates body cell, prevents pachylosis and aging, inhibit the growth of skin surface harmful bacteria, antibacterial antidermatosis and absorb ultraviolet light function and other effects.
Description
Technical field
The present invention relates to micro-capsule package technology field, a kind of microcapsules compound wall materials and preparation method thereof are particularly related to,
And microcapsule essence with the microcapsules compound wall materials and its preparation method and application.
Background technique
Microcapsules technology is that finely dispersed solid matter particle, drop or gas are completely enclosed in a tunic, shape
At a kind of technology of microcapsules.Essence microcapsule is one of the important branch and microcapsules technology in microcapsules technology
A rather typical application.Essence microcapsule is to be wrapped up using natural or synthetic high molecular material essence, can be with
Avoid fragrance matter is directly heated, influence of light and cause oxidation deterioration, avoid the volatilization of effective component, effectively control flavor
The release of matter improves the stability of fragrance.How to protect microcapsule essence in process of production not to be destroyed, in essence and clothing
Firm connection is set up between object, assigns clothing fragrance and fragrance remaining time is more lasting, it is washable on clothing to improve essence
Performance is washed, is that current laundry liquid flavoring will solve the problems, such as.The common method of essence microcapsule is up to more than 200 kinds at present, compared with
The technology of mature essence microcapsule mainly has: spray drying, extrusion, molecule embedding hair, polymerization, coacervation and object
Manage absorption method etc..
When selecting essence microcapsule wall material, generally require that material property is stable, safe and non-toxic, nonirritant, free from extraneous odour；
It can be compatible with essence but chemically react；Have permeability appropriate, dissolubility etc., and wall material solution meet high concentration and
The requirement of low viscosity.Often beta-cyclodextrin, Arabic gum, protein, starch and its derivative is selected to prepare as spray drying process
The wall material of essence microcapsule product.
At this stage in Cosmetic Manufacture, essence causes oxidation deterioration because of directly heated, light influence, fragrant in whipping process
Essence is more easily damaged, and Mobyneb moisturizing, crease-resistant, sun-proof, antipruritic skin care preparation is short.How essence is protected in process of production
It is not destroyed, firm connection is set up between essence and skin, assign skin fragrance and fragrance remaining time is more lasting, improve
The washing resistance performance of essence on the skin is currently to solve the problems, such as.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of microcapsules compound wall materials, microcapsule essence and preparation method thereof
And application, the microcapsules compound wall materials are natural or synthetic high molecular material, it can be straight to avoid fragrance matter after essence package
Receive hot, light influence and cause oxidation deterioration, avoids the volatilization of effective component, effectively control the release of fragrance matter, improve
The stability of fragrance.
In order to solve the above technical problems, of the invention is achieved by the following technical programs:
A kind of microcapsules compound wall materials, including xanthan gum, chitosan oligosaccharide and deionized water, wherein xanthan gum content be 2~
5 parts, chitosan oligosaccharide content is 0.5~1.5 part, and deionized water content is 55~60 parts.
It further, further include preservative in the microcapsules compound wall materials, the antiseptic content is 0.05~0.15
Part.
Further, the preservative is DMDM hydantoin.
The preparation method of microcapsules compound wall materials of the invention, includes the following steps:
S1, xanthan gum, chitosan oligosaccharide are add to deionized water and quickly stir 0.5 hour to being completely dissolved, obtain solution；
S2, the bubble removed in solution is vacuumized, is then cooled to 35 DEG C, this glue is microcapsules compound wall materials.
Further, in the step S1, the temperature for dissolving the deionized water of xanthan gum and chitosan oligosaccharide is 70~80 DEG C.
Further, in the step S2, preservative is added in solution after being cooled to 35 DEG C, and continues to stir to completely molten
Solution.
A kind of microcapsule essence wrapped up by microcapsules compound wall materials of the invention, including A phase, B phase and C phase, wherein
A phase includes 2~5 parts of xanthan gums, 0.5~1.5 part of chitosan oligosaccharide, 55~60 parts of deionized waters；
B phase includes 30-35 parts of essence, 6~7 parts of solubilizer；
C phase includes preservative.
Xanthan gum, chitosan oligosaccharide, deionized water, preservative form both effectiveness microcapsule wall material as protection outer layer, have
Water-wet behavior, internal layer are made of solubilizer and essence.By the addition of chitosan oligosaccharide, essence protective bulkhead film is on the one hand formed, it is another
Aspect has apparent moisture-keeping function again, while also having activation body cell, prevents pachylosis and aging, inhibits skin surface
Harmful bacteria growth, antibacterial antidermatosis and absorption ultraviolet light function and other effects.
Chitosan oligosaccharide is called Chitosan poly oligosaccharide, chitosan oligomer, is that chitosan is degraded through special biological enzyme technology
A kind of degree of polymerization oligosaccharide product between 2~20, molecular weight≤3200Da are that water solubility is preferable, function is big, bioactivity
High low molecular weight product.It has the unexistent higher solubility of chitosan, is dissolved in water entirely, while chitosan oligosaccharide has significantly
Moisturizing activates body cell, prevents pachylosis and aging, inhibits the growth of skin surface harmful bacteria, antibacterial antidermatosis and suction
Ultraviolet light function and other effects is received, in biomedicine field, field of fine chemical, field of health care food and agricultural herding field
It is applied, it has extremely wide application range and development prospect.
Further, the solubilizer is Cremophor RH40.
Further, the preservative is DMDM hydantoin.
Further, the partial size of the microcapsule essence is 2~30 μm.
The preparation method of microcapsule essence of the invention, includes the following steps:
S1, essence, the solubilizer in B phase stirred evenly for use in normal temperature condition in advance；
S2, xanthan gum, the chitosan oligosaccharide in A phase are added in 75 DEG C of deionized waters quickly stir it is molten to being completely dissolved to obtain
Liquid；
S3,35 DEG C are cooled to after solution to be vacuumized to de-bubble, C phase is added and stirs evenly, this glue is microcapsules composite
Material；
S4, will in S1 gained mixture be added S3 in microcapsules compound wall materials glue in, stir evenly to get.
The microcapsule essence can stir destruction to essence microcapsule not only to avoid equipment in production process, but also can be to avoid
Fragrance matter is directly heated, light influence and cause oxidation deterioration, avoid the volatilization of effective component, effectively control fragrance matter
Release, improves the stability of fragrance.
A kind of application of microcapsule essence in the preparation of shampoo, shower cream or laundry liquid product, the group of laundry liquid product
Divide and content is as follows:
When preparation,
1. relevant device, apparatus are cleaned；
2. cooling down after the stirring of A phase each component is warming up to 80-85 DEG C until dissolving, it is each that B phase is sequentially added when being down to 45 DEG C
It is stirred evenly after ingredient.
3. the inspection of semifinished product, discharging.
4. filling, product inspection, storage.
Microcapsule essence is added in liquid detergent, forms essence wall material outer layer, can directly be heated to avoid fragrance matter, light
Influence and cause oxidation deterioration, avoid the volatilization of effective component, effectively control fragrance matter release, improve the stabilization of fragrance
Property.Avoid fragrance in the loss and destruction of other raw materials to Flavor active ingredient of production storage process.Pass through special formula
Microcapsule essence is dispersed in more effectively in liquid detergent system with production technology.Reach effectively enhancing essence on clothing
Aroma retaining effect.Microcapsule essence is rested on after shower or washing on skin or hair or clothing, and microcapsules are fragrant in daily life
It was proficient in shake, friction triggering fragrance release, it is lasting to guarantee.
The advantageous effects of the above technical solutions of the present invention are as follows:
The filming function of chitosan oligosaccharide, xanthan gum, using it as the wall material of microcapsule essence, this effect type microcapsule essence is
Sticky shape flowability mucus is directly added into cosmetic product base-material under room temperature.This muciform microcapsules of flowability
Essence can protect in the production process of target product itself not to be destroyed；It is set up between essence and skin firm
It connects, assigns skin fragrance and fragrance remaining time is more lasting, improve the washing resistance performance of essence on the skin；Microcapsules of the invention
Compound wall materials can to avoid fragrance matter directly heated, light influence and cause oxidation deterioration, avoid the volatilization of effective component, have
The release of effect control fragrance matter, improves the stability of fragrance.
Microcapsules compound wall materials of the invention and microcapsule essence, production method steps are succinct, without complicated processing,
It saves human and material resources.
Specific embodiment
To keep the technical problem to be solved in the present invention, technical solution and advantage clearer, below in conjunction with specific implementation
Example is described in detail.
Embodiment 1
A kind of microcapsules compound wall materials, including xanthan gum, chitosan oligosaccharide and deionized water, wherein xanthan gum content be 2~
5 parts, chitosan oligosaccharide content is 0.5~1.5 part, and deionized water content is 55~60 parts.
It further include preservative in the microcapsules compound wall materials, the preservative is DMDM hydantoin, content 0.05
~0.15 part.
The preparation method of the microcapsules compound wall materials, includes the following steps:
S1, xanthan gum, chitosan oligosaccharide are added in 70~80 DEG C of deionized water quickly stir 0.5 hour to completely it is molten
Solution, obtains solution；
S2, the bubble removed in solution is vacuumized, is then cooled to 35 DEG C, preservative is added afterwards, and continue to stir to complete
Fully dissolved.
Embodiment 2
A kind of microcapsule essence of microcapsules compound wall materials package, including A phase, B phase and C phase, wherein
A phase includes 2~5 parts of xanthan gums, 0.5~1.5 part of chitosan oligosaccharide, 55~60 parts of deionized waters；
B phase includes 30-35 parts of essence, 6~7 parts of solubilizer；
C phase includes preservative.
Xanthan gum, chitosan oligosaccharide, deionized water, preservative form both effectiveness microcapsule wall material as protection outer layer, internal layer by
Solubilizer and essence composition.By the addition of chitosan oligosaccharide, essence protective bulkhead film is on the one hand formed, on the other hand there is apparent guarantor again
Wet effect, while also there is activation body cell, pachylosis and aging are prevented, skin surface harmful bacteria is inhibited to breed, is antibacterial
Antidermatosis and absorption ultraviolet light function and other effects.
Further, the solubilizer is Cremophor RH40.
Further, the preservative is DMDM hydantoin.
Further, the partial size of the microcapsule essence is 2~30 μm；20~30 μm be suitable for fabric washing product, 2~
8 μm are suitable for washing hair products, personal nursing and skin care item.
The preparation method of the microcapsule essence, includes the following steps:
S1, essence, the solubilizer in B phase stirred evenly for use in normal temperature condition in advance；
S2, xanthan gum, the chitosan oligosaccharide in A phase are added in 75 DEG C of deionized waters quickly stir it is molten to being completely dissolved to obtain
Liquid；
S3,35 DEG C are cooled to after solution to be vacuumized to de-bubble, C phase is added and stirs evenly, this glue is microcapsules composite
Material；
S4, gained in S1 is added in the microcapsules compound wall materials glue in S3, is stirred evenly to obtain the final product.
The filming function of chitosan oligosaccharide, xanthan gum, using it as the wall material of microcapsule essence, the microcapsules that this method obtains are fragrant
Essence is sticky shape flowability mucus, is directly added into cosmetic product base-material under room temperature.This flowability is muciform micro-
Capsule essence can protect in the production process of target product itself not to be destroyed.
Embodiment 3
Microcapsule essence application can be added in shampoo, shower cream or laundry liquid product.
The component and content of the laundry liquid product of the present embodiment are as follows:
When preparation,
1. relevant device, apparatus are cleaned；
2. cooling down after the stirring of A phase each component is warming up to 80-85 DEG C until dissolving, it is each that B phase is sequentially added when being down to 45 DEG C
It is stirred evenly after ingredient.
3. the inspection of semifinished product, discharging.
4. filling, product inspection, storage.
Microcapsule essence is added in liquid detergent, forms essence wall material outer layer, can directly be heated to avoid fragrance matter, light
Influence and cause oxidation deterioration, avoid the volatilization of effective component, effectively control fragrance matter release, improve the stabilization of fragrance
Property.Avoid fragrance in the loss and destruction of other raw materials to Flavor active ingredient of production storage process.Pass through special formula
Microcapsule essence is dispersed in more effectively in liquid detergent system with production technology.Reach effectively enhancing essence on clothing
Aroma retaining effect.Microcapsule essence is rested on after shower or washing on skin or hair or clothing, and microcapsules are fragrant in daily life
It was proficient in shake, friction triggering fragrance release, it is lasting to guarantee.
The above is a preferred embodiment of the present invention, it is noted that for those skilled in the art
For, without departing from the principles of the present invention, several improvements and modifications can also be made, these improvements and modifications
It should be regarded as protection scope of the present invention.
Claims (10)
1. a kind of microcapsules compound wall materials, which is characterized in that including xanthan gum, chitosan oligosaccharide and deionized water, wherein xanthan gum
Content is 2~5 parts, and chitosan oligosaccharide content is 0.5~1.5 part, and deionized water content is 55~60 parts.
2. microcapsules compound wall materials according to claim 1, which is characterized in that further include in the microcapsules compound wall materials
Preservative, the preservative are DMDM hydantoin, and content is 0.05~0.15 part.
3. a kind of preparation method of microcapsules compound wall materials, which comprises the steps of:
S1,2~5 parts of xanthan gums, 0.5~1.5 part of chitosan oligosaccharide are added in 55~60 parts of deionized waters and are quickly stirred 0.5 hour
To being completely dissolved, solution is obtained；
S2, the bubble removed in solution is vacuumized, is then cooled to 35 DEG C, this glue is microcapsules compound wall materials.
4. the preparation method of microcapsules compound wall materials according to claim 3, which is characterized in that molten in the step S1
The temperature for solving the deionized water of xanthan gum and chitosan oligosaccharide is 70~80 DEG C.
5. the preparation method of microcapsules compound wall materials according to claim 3, which is characterized in that molten in the step S2
0.05~0.15 portion of preservative is added after being cooled to 35 DEG C in liquid, and continues stirring to being completely dissolved.
6. a kind of microcapsule essence of microcapsules compound wall materials package, which is characterized in that including A phase, B phase and C phase, wherein
A phase includes 2~5 parts of xanthan gums, 0.5~1.5 part of chitosan oligosaccharide, 55~60 parts of deionized waters；
B phase includes 30-35 parts of essence, 6~7 parts of solubilizer；
C phase includes preservative.
7. the microcapsule essence of microcapsules compound wall materials package according to claim 6, which is characterized in that the solubilizer
For Cremophor RH40；The preservative is DMDM hydantoin.
8. the preparation method of the microcapsule essence of microcapsules compound wall materials package according to claim 6, which is characterized in that
Include the following steps:
S1, essence, the solubilizer in B phase stirred evenly for use in normal temperature condition in advance；
S2, xanthan gum, the chitosan oligosaccharide in A phase are added in 75 DEG C of deionized waters and quickly stirred to being completely dissolved to obtain solution；
S3,35 DEG C are cooled to after solution to be vacuumized to de-bubble, C phase is added and stirs evenly, this glue is microcapsules compound wall materials；
S4, gained in S1 is added in the microcapsules compound wall materials glue in S3, is stirred evenly to obtain the final product.
9. microcapsule essence according to claim 6 or 7 answering in the preparation of shampoo, shower cream or laundry liquid product
With.
10. application according to claim 9, the component and content of the laundry liquid product are as follows:
When preparation, cools down after the stirring of A phase each component is warming up to 80-85 DEG C until dissolving, it is each that B phase is sequentially added when being down to 45 DEG C
It is stirred evenly after ingredient to obtain the final product.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111349526A (en) * | 2020-04-15 | 2020-06-30 | 惠州兆婷化妆品有限公司 | Kitchen heavy oil stain cleaning agent and preparation method thereof |
| CN113318137A (en) * | 2021-06-25 | 2021-08-31 | 东北林业大学 | Preparation method of water-soluble acanthopanax powder capsule |
| CN113502190A (en) * | 2021-07-13 | 2021-10-15 | 广州芬豪香精有限公司 | Manufacturing method of slow-volatilization fragrance-retaining essence |
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