CN110346391B - Multidimensional stress loading experimental device for neutron diffraction measurement - Google Patents

Multidimensional stress loading experimental device for neutron diffraction measurement Download PDF

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Publication number
CN110346391B
CN110346391B CN201910685280.7A CN201910685280A CN110346391B CN 110346391 B CN110346391 B CN 110346391B CN 201910685280 A CN201910685280 A CN 201910685280A CN 110346391 B CN110346391 B CN 110346391B
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supporting frame
cross beam
loading
moving cross
side supporting
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CN110346391A (en
Inventor
庞蓓蓓
孙光爱
孙雪飞
王虹
李建
杨钊龙
潘建
张昌盛
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Institute of Nuclear Physics and Chemistry China Academy of Engineering Physics
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Institute of Nuclear Physics and Chemistry China Academy of Engineering Physics
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/02Details
    • G01N3/04Chucks
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N23/00Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
    • G01N23/20Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by using diffraction of the radiation by the materials, e.g. for investigating crystal structure; by using scattering of the radiation by the materials, e.g. for investigating non-crystalline materials; by using reflection of the radiation by the materials
    • G01N23/20008Constructional details of analysers, e.g. characterised by X-ray source, detector or optical system; Accessories therefor; Preparing specimens therefor
    • G01N23/20025Sample holders or supports therefor
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N23/00Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
    • G01N23/20Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by using diffraction of the radiation by the materials, e.g. for investigating crystal structure; by using scattering of the radiation by the materials, e.g. for investigating non-crystalline materials; by using reflection of the radiation by the materials
    • G01N23/207Diffractometry using detectors, e.g. using a probe in a central position and one or more displaceable detectors in circumferential positions
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/08Investigating strength properties of solid materials by application of mechanical stress by applying steady tensile or compressive forces
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E30/00Energy generation of nuclear origin
    • Y02E30/30Nuclear fission reactors

Abstract

The invention discloses a multidimensional stress loading experimental device for neutron diffraction measurement. The device can be used for carrying out neutron diffraction measurement on a sample, and simultaneously providing pulling, pressing, torsion, pulling and torsion, pressing and torsion for the sample and the composite loading of the mechanical loading and the temperature field. The device adopts a three-column structure, has stable and reliable structure, and reserves a large space for the operations of sample loading and unloading, temperature loading cavity installation and the like. The device also adopts non-contact video deformation measurement to directly measure the deformation of the sample, and solves the problems that the contact extensometer is complex to install or is not suitable for torsion measurement in neutron diffraction application. The multidimensional stress loading experimental device for neutron diffraction measurement has the characteristics of multifunction, simple operation and high measurement precision, can be used in combination with a neutron stress spectrometer, can realize neutron stress distribution measurement of a sample under a service condition, and provides an effective and reliable test means for revealing mechanical properties, damage and fracture mechanism research of materials.

Description

Multidimensional stress loading experimental device for neutron diffraction measurement
Technical Field
The invention belongs to the technical field of neutron diffraction in-situ environment loading, and particularly relates to a multidimensional stress loading experimental device for neutron diffraction measurement.
Background
The multidimensional stress loading experimental device for neutron diffraction measurement is matched with a neutron stress spectrometer, can be used for measuring stress distribution conditions of component manufacturing materials such as aviation wings, engines and high-speed rail under the conditions of service conditions and temperature, and plays a guiding role in component material selection, aging mechanism, processing technology and the like. In order to accurately measure the deformation condition of a sample, a conventional material testing machine device often uses sensors such as an extensometer to directly measure, and in neutron diffraction measurement application, on one hand, an environment loading experimental device needs to reserve a neutron beam line channel, and meanwhile, the size of the device is limited by a sample table, the beam height and the like, so that the problem that the extensometer cannot be installed or is complicated to install is caused, and the deformation measurement of the sample can only be indirectly obtained through a driving motor end. The in-situ testing device (CN 207423647U) for mechanical properties of variable-temperature tension-torsion composite load materials disclosed in the Chinese patent literature library is not provided with a deformation measurement related sensor, and the deformation condition of a sample can be obtained only through the ends of driving motors. On the other hand, in the case of sealing loading such as oxidation resistance and ice resistance, the use of conventional measuring sensors such as extensometers can damage the sealing structure and cannot meet the requirements. The patent 'in-situ heating device for neutron diffraction' (ZL 201720225423.2) disclosed in the Chinese patent literature library proposes the structural design of an in-situ temperature loading device for strain measurement by using an extensometer, but the structure is not suitable for measuring torsional deformation, and the structure of arranging a measuring hole of the extensometer on a heating body cannot meet the requirement of sealing loading.
Disclosure of Invention
The invention aims to provide a multidimensional stress loading experimental device for neutron diffraction measurement.
The invention relates to a multidimensional stress loading experiment device for neutron diffraction measurement, which is characterized by comprising a base, a left side supporting frame, a right side supporting frame, a torsion driving motor, a tension and compression driving motor, a precise screw A, a precise screw B, a left side moving cross beam, a right side moving cross beam, a thrust bearing, a right loading rod, a guide post, a tension and torsion optical sensor, a left clamp, a right clamp, a temperature loading cavity and a deformation measuring camera; the left support frame and the right support frame are right triangular support plates which are symmetrically distributed left and right, the right angle position, the upper angle position, the lower angle position and the center position of the left support frame are respectively provided with mounting holes FLA, FLB, FLC and FLD, and the lower part of the FLD is provided with mounting holes FLE; the right angle position, the upper angle position, the lower angle position and the center position of the right side supporting frame are respectively provided with a mounting hole FRA, FRB, FRC and an FRD, and the lower part of the FRD is provided with a mounting hole FRE; the left side moving cross beam and the right side moving cross beam are right-left symmetrically distributed right triangular moving support plates which are respectively arranged on the inner sides of the left side supporting frame and the right side supporting frame, threaded holes MLA and MLB are respectively formed in the right angle position and the upper angle position of the left side moving cross beam, mounting holes MLC and MLD are respectively formed in the lower angle and the central position of the left side moving cross beam, threaded holes MRA and threaded holes MRB are respectively formed in the right angle position and the upper angle position of the right side moving cross beam, and mounting holes MRC and MRD are respectively formed in the lower angle and the central position of the right side moving cross beam;
the connection relation is as follows: the right-angle edges of the left support frame and the right support frame are symmetrically and fixedly connected to the left side and the right side of the base respectively; the pulling and pressing driving motor is fixedly arranged on the right side supporting frame, and an output shaft of the pulling and pressing driving motor is respectively connected with the precise screw A and the precise screw B through two groups of transmission gears; the torsion driving motor is fixedly arranged on the left side supporting frame; the precise screw rod A passes through the threaded hole MLA of the left side moving cross beam and the threaded hole MRA of the right side moving cross beam, and two ends of the precise screw rod A are respectively arranged at the FLA position of the left side supporting frame and the FRA position of the right side supporting frame; the precise lead screw B passes through the threaded hole MLB of the left side moving cross beam and the threaded hole MRB of the right side moving cross beam, and two ends of the precise lead screw B are respectively arranged at the FLB of the left side supporting frame and the FRB of the right side supporting frame; the outer ring of the thrust bearing is fixed on a mounting hole MLD of the left side moving cross beam, one side of the inner ring of the thrust bearing is fixedly connected with one end of the left clamp, and the other side of the inner ring of the thrust bearing is connected with an output shaft of the torsion driving motor through a transmission gear; the right loading rod is arranged on the mounting hole MRD of the right side moving cross beam and is fixedly connected with one end of the tension-torsion force sensor; the guide posts penetrate through the mounting holes MLC of the left side moving cross beam and the mounting holes MRC of the right side moving cross beam, and the two ends of the guide posts are fixed on the FLC of the left side supporting frame and the FRC of the right side supporting frame; one end of the right clamp is fixedly connected with the other end of the tension-torsion optical sensor; the other ends of the left clamp and the right clamp are connected to the two ends of the sample; the temperature loading cavity is fixedly arranged on the base; the deformation measuring camera is fixedly arranged on the left side supporting frame and the right side supporting frame through the bracket and is arranged right above the sample.
The base, the left side supporting frame and the right side supporting frame are made of aviation aluminum.
The screw threads at the two ends of the precise screw A and the precise screw B are opposite in direction and equal in screw pitch.
The temperature loading cavity is one of a high-temperature device, a low-temperature device and a high-temperature and low-temperature device, the left side and the right side of the temperature loading cavity are provided with clamp telescopic holes, the front side and the rear side are provided with neutron incidence windows, and a deformation measurement observation window is arranged right above the neutron incidence windows.
The working process of the multidimensional stress loading experimental device for neutron diffraction measurement comprises the following steps: controlling the pulling and pressing driving motor to rotate forward (or reversely); the precise screw A and the precise screw B rotate after passing through the transmission gear, and the left side moving cross beam and the right side moving cross beam move left and right (or right and left) on opposite threads, so that the thrust bearing and the right loading rod are driven to move left and right (or right and left), and finally the left clamp and the right clamp are driven to carry out stretching (or compression) loading on the sample. The torsion driving motor drives the left clamp to rotate through the transmission gear, so that the left clamp is driven to carry out torsion loading on the sample. And simultaneously, the tension-compression horizontal force and the torsion force of the sample are measured by the tension-compression force optical sensor, and the torsion deformation of the sample is measured by the deformation measuring camera.
The multidimensional stress loading experimental device for neutron diffraction measurement has the characteristics of multifunction, simple operation and high measurement precision. The device adopts a three-column structure of a double-precision screw rod and a guide shaft, has stable and reliable structure, and reserves a larger space for the operations of sample loading and unloading, temperature loading cavity installation and the like; meanwhile, the device adopts non-contact video deformation measurement to directly measure the deformation of the sample, and solves the problems of complex installation of a contact extensometer, inapplicability to torsion measurement, damage to a sealing structure and the like in neutron diffraction application. The multidimensional stress loading experimental device for neutron diffraction measurement is suitable for carrying out multimode loading of a sample under the conditions of pulling, pressing, twisting, high and low temperature and loading conditions, and realizes stress distribution measurement of a material under the condition of service, thereby providing an effective and reliable testing means for further revealing mechanical properties of the material and researching damage and fracture mechanisms.
Drawings
FIG. 1 is a schematic diagram of a multi-dimensional stress loading experimental apparatus for neutron diffraction measurement according to the present invention;
FIG. 2 is a left side view of a multi-dimensional stress loading experimental set-up for neutron diffraction measurement of the present invention;
FIG. 3 is a schematic diagram of the structure of a temperature loading chamber in a multi-dimensional stress loading experimental apparatus for neutron diffraction measurement of the present invention;
in the figure, 1, a base 2, a left side support frame 3, a right side support frame 4, a torsion driving motor 5, a tension driving motor 6, a precision screw A7, a precision screw B8, a left side moving cross beam 9, a right side moving cross beam 10, a thrust bearing 11, a right loading rod 12, a guide post 13, a tension torsion sensor 14, a left clamp 15, a right clamp 16, a temperature loading cavity 17 and a deformation measuring camera.
Detailed Description
The details of the present invention and its specific embodiments are further described below with reference to the accompanying drawings.
As shown in fig. 1 and 2, the multidimensional stress loading experimental device for neutron diffraction measurement of the present invention comprises a base 1, a left side supporting frame 2, a right side supporting frame 3, a torsion driving motor 4, a tension and compression driving motor 5, a precision screw A6, a precision screw B7, a left side moving beam 8, a right side moving beam 9, a thrust bearing 10, a right loading rod 11, a guide post 12, a tension and torsion sensor 13, a left clamp 14, a right clamp 15, a temperature loading cavity 16 and a deformation measuring camera 17; the left support frame 2 and the right support frame 3 are right triangular support plates which are symmetrically distributed left and right, the right angle position, the upper angle position, the lower angle position and the center position of the left support frame 2 are respectively provided with mounting holes FLA, FLB, FLC and FLD, and the lower part of the FLD is provided with mounting holes FLE; the right angle position, the upper angle position, the lower angle position and the center position of the right side supporting frame 3 are respectively provided with a mounting hole FRA, FRB, FRC and an FRD, and the lower part of the FRD is provided with a mounting hole FRE; the left side moving cross beam 8 and the right side moving cross beam 9 are right triangular moving support plates which are respectively arranged on the inner sides of the left side supporting frame 2 and the right side supporting frame 3 and are symmetrically distributed left and right, threaded holes MLA and MLB are respectively formed in the right angle position and the upper angle position of the left side moving cross beam 8, mounting holes MLC and MLD are respectively formed in the lower angle position and the central position of the right side moving cross beam 9, threaded holes MRA and threaded holes MRB are respectively formed in the right angle position and the upper angle position of the right side moving cross beam 9, and mounting holes MRC and MRD are respectively formed in the lower angle position and the central position of the right side moving cross beam;
the connection relation is as follows: the right side supporting frame 2 and the right side supporting frame 3 are symmetrically and fixedly connected to the left side and the right side of the base 1 respectively; the pulling and pressing driving motor 5 is fixedly arranged on the right side supporting frame 3, and an output shaft of the pulling and pressing driving motor 5 is respectively connected with the precise screw A6 and the precise screw B7 through two groups of transmission gears; the torsion driving motor 4 is fixedly arranged on the left supporting frame 2; the precise lead screw A6 passes through a threaded hole MLA of the left side moving cross beam 8 and a threaded hole MRA of the right side moving cross beam 9, and two ends of the precise lead screw A6 are respectively arranged at the FLA position of the left side supporting frame 2 and the FRA position of the right side supporting frame 3; the precise lead screw B7 passes through a threaded hole MLB of the left side moving cross beam 8 and a threaded hole MRB of the right side moving cross beam 9, and two ends of the precise lead screw B7 are respectively arranged at the FRB positions of the FLB of the left side supporting frame 2 and the FRB of the right side supporting frame 3; the outer ring of the thrust bearing 10 is fixed on a mounting hole MLD of the left side moving cross beam 8, one side of the inner ring of the thrust bearing 10 is fixedly connected with one end of the left clamp 14, and the other side of the inner ring of the thrust bearing 10 is connected with the output shaft of the torsion driving motor 4 through a transmission gear; the right loading rod 11 is arranged on the mounting hole MRD of the right side moving cross beam 9 and is fixedly connected with one end of the tension-torsion optical sensor 13; the guide post 12 passes through the mounting hole MLC of the left side moving cross beam 8 and the mounting hole MRC of the right side moving cross beam 9, and two ends of the guide post 12 are fixed on the FLC of the left side supporting frame 2 and the FRC of the right side supporting frame 3; one end of the right clamp 15 is fixedly connected with the other end of the tension-torsion optical sensor 13; the other ends of the left clamp 14 and the right clamp 15 are connected to the two ends of the sample; the temperature loading cavity 16 is fixedly arranged on the base 1; the deformation measuring camera 17 is fixedly arranged on the left side supporting frame 2 and the right side supporting frame 3 through brackets and is arranged right above the sample.
The base 1, the left support frame 2 and the right support frame 3 are manufactured by aviation aluminum.
The screw threads at the two ends of the precise screw A6 and the precise screw B7 are opposite in direction and equal in screw pitch.
As shown in fig. 3, the temperature loading cavity 16 is one of a high temperature device, a low temperature device and a high temperature device, the left side and the right side of the temperature loading cavity 16 are provided with clamp telescopic holes, the front side and the rear side are provided with neutron entrance windows, and the right side is provided with a deformation measurement observation window.
Example 1
The temperature loading cavity 16 in this embodiment is a high temperature device, the left and right sides of the temperature loading cavity 16 are provided with clamp telescopic holes, the front and rear sides are provided with neutron incident windows, and the right upper side is provided with a deformation measurement observation window.
After the implementation, the embodiment can carry out pulling, pressing, twisting, pulling and twisting, pressing and twisting and the composite loading of the mechanical loading and the high-temperature field on the sample at the same time of neutron diffraction measurement.
Example 2
The present embodiment has the same structure as that of embodiment 1, except that the temperature loading chamber is a low temperature device. After the implementation, the embodiment can carry out pulling, pressing, twisting, pulling and twisting, pressing and twisting and composite loading of the mechanical loading and the low-temperature field on the sample at the same time of neutron diffraction measurement.
Example 3
The present embodiment has the same structure as that of embodiment 1, except that the temperature loading chamber is a high-low temperature device. After the implementation, the embodiment can carry out pulling, pressing, twisting, pulling and twisting, pressing and twisting and the composite loading from the mechanical loading and the low temperature to Gao Wenchang on the sample at the same time of neutron diffraction measurement.

Claims (3)

1. A multidimensional stress loading experimental apparatus for neutron diffraction measurement, which is characterized in that: the loading experiment device comprises a base (1), a left side supporting frame (2), a right side supporting frame (3), a torsion driving motor (4), a tension-compression driving motor (5), a precise screw A (6), a precise screw B (7), a left side moving cross beam (8), a right side moving cross beam (9), a thrust bearing (10), a right loading rod (11), a guide column (12), a tension-torsion optical sensor (13), a left clamp (14), a right clamp (15), a temperature loading cavity (16) and a deformation measuring camera (17); the left side support frame (2) and the right side support frame (3) are right triangular support plates which are symmetrically distributed left and right, the right angle position, the upper angle position, the lower angle position and the central position of the left side support frame (2) are respectively provided with mounting holes FLA, FLB, FLC and FLD, and the lower part of the FLD is provided with mounting holes FLE; the right-angle position, the upper angle position, the lower angle position and the center position of the right-side supporting frame (3) are respectively provided with a mounting hole FRA, FRB, FRC and an FRD, and the lower part of the FRD is provided with a mounting hole FRE; the left side moving cross beam (8) and the right side moving cross beam (9) are right triangle-shaped moving support plates which are respectively arranged on the inner sides of the left side supporting frame (2) and the right side supporting frame (3) and are symmetrically distributed left and right, a right angle position and an upper angle position of the left side moving cross beam (8) are respectively provided with threaded holes MLA and MLB, a lower angle and a central position are respectively provided with mounting holes MLC and MLD, and a right angle position and an upper angle position of the right side moving cross beam (9) are respectively provided with threaded holes MRA and MRB, and a lower angle and a central position are respectively provided with mounting holes MRC and MRD; the base (1), the left side supporting frame (2) and the right side supporting frame (3) are manufactured by processing aviation aluminum;
the connection relation is as follows: one right-angle edge of the left support frame (2) and one right support frame (3) are respectively and symmetrically fixedly connected to the left side and the right side of the base (1); the pulling and pressing driving motor (5) is fixedly arranged on the right side supporting frame (3), and an output shaft of the pulling and pressing driving motor (5) is respectively connected with the precise screw A (6) and the precise screw B (7) through two groups of transmission gears; the torsion driving motor (4) is fixedly arranged on the left supporting frame (2); the precise screw rod A (6) passes through a threaded hole MLA of the left side moving cross beam (8) and a threaded hole MRA of the right side moving cross beam (9), and two ends of the precise screw rod A (6) are respectively arranged at the FLA position of the left side supporting frame (2) and the FRA position of the right side supporting frame (3); the precise lead screw B (7) passes through a threaded hole MLB of the left side moving cross beam (8) and a threaded hole MRB of the right side moving cross beam (9), and two ends of the precise lead screw B (7) are respectively arranged at the FRB positions of the FLB of the left side supporting frame (2) and the FRB of the right side supporting frame (3); the outer ring of the thrust bearing (10) is fixed on a mounting hole MLD of the left side moving cross beam (8), one side of the inner ring of the thrust bearing (10) is fixedly connected with one end of the left clamp (14), and the other side of the inner ring of the thrust bearing (10) is connected with an output shaft of the torsion driving motor (4) through a transmission gear; the right loading rod (11) is arranged on an installation hole MRD of the right side moving cross beam (9) and is fixedly connected with one end of the tension-torsion force sensor (13); the guide posts (12) penetrate through mounting holes MLC of the left side moving cross beam (8) and mounting holes MRC of the right side moving cross beam (9), and two ends of the guide posts (12) are fixed on the FLC of the left side supporting frame (2) and the FRC of the right side supporting frame (3); one end of the right clamp (15) is fixedly connected with the other end of the tension-torsion optical sensor (13); the other ends of the left clamp (14) and the right clamp (15) are connected to the two ends of the sample; the temperature loading cavity (16) is fixedly arranged on the base (1); the deformation measuring camera (17) is fixedly arranged on the left side supporting frame (2) and the right side supporting frame (3) through a bracket and is arranged right above the sample.
2. The multi-dimensional stress loading experimental set-up for neutron diffraction measurement according to claim 1, wherein: the screw threads at the two ends of the precise screw rod A (6) and the precise screw rod B (7) are opposite in direction and equal in screw pitch.
3. The multi-dimensional stress loading experimental set-up for neutron diffraction measurement according to claim 1, wherein: the temperature loading cavity (16) is one of a high-temperature device, a low-temperature device and a high-low temperature device, the left side and the right side of the temperature loading cavity (16) are provided with clamp telescopic holes, the front side and the rear side are provided with neutron incidence windows, and a deformation measurement observation window is arranged right above the neutron incidence windows.
CN201910685280.7A 2019-07-27 2019-07-27 Multidimensional stress loading experimental device for neutron diffraction measurement Active CN110346391B (en)

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Publication number Priority date Publication date Assignee Title
CN110715862A (en) * 2019-11-13 2020-01-21 吉林大学 Instrument and method for testing mechanical properties of material under tension-torsion composite-force-heat coupling working condition
CN113406691B (en) * 2021-06-23 2023-04-11 中国核动力研究设计院 Neutron fluence and deformation measuring device in test reactor

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