CN109704439A - Toolroom machine method for treating waste liquid - Google Patents

Toolroom machine method for treating waste liquid Download PDF

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Publication number
CN109704439A
CN109704439A CN201711006769.4A CN201711006769A CN109704439A CN 109704439 A CN109704439 A CN 109704439A CN 201711006769 A CN201711006769 A CN 201711006769A CN 109704439 A CN109704439 A CN 109704439A
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CN
China
Prior art keywords
waste liquid
toolroom machine
water
packed bed
oil
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Pending
Application number
CN201711006769.4A
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Chinese (zh)
Inventor
陈奕宏
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Haiqi Technology Co.,Ltd.
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National Taipei University of Technology
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Priority to CN201711006769.4A priority Critical patent/CN109704439A/en
Publication of CN109704439A publication Critical patent/CN109704439A/en
Pending legal-status Critical Current

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Abstract

A kind of toolroom machine method for treating waste liquid, the toolroom machine waste liquid contains oil-water emulsion, the processing method includes: the toolroom machine waste liquid is introduced the internal rotary packed bed for negative pressure, under the centrifugal force effect that rotary packed bed rotation generates, water in the toolroom machine waste liquid is vaporized separation from the toolroom machine waste liquid, and the oil-water emulsion is made to form the water-in-oil emulsion that moisture content is lower than 10%.The toolroom machine method for treating waste liquid can quickly make oil-water emulsion form the low water-in-oil emulsion of moisture content, and the moisture content in toolroom machine waste liquid is effectively reduced.

Description

Toolroom machine method for treating waste liquid
Technical field
The present invention relates to a kind of toolroom machine (machine tool) method for treating waste liquid, utilize rotation more particularly to a kind of Packed bed is come the toolroom machine method for treating waste liquid that carries out.
Background technique
Toolroom machine waste liquid (such as cutting waste fluid) containing oil-water emulsion is if be arbitrarily emitted into water body, oil therein Dirt is easy to be attached on the surface of organism in water body (such as: fish, shrimp, shellfish) or be ingested in vivo, is also easily destroyed hydrological landscape Or lead to bacteria breed, it needs by being properly recycled.Wherein, the oil bead diameter of the oil-water emulsion of oil-in-water form is only about It is 10-3- 10 μm, therefore can not be separated and simply standing (gravity) and being layered grease;And the grease cream of Water-In-Oil form Change liquid, often because the obstruction of gas-liquid quality transmission, causes the rate of water removal to be substantially limited when using distillation separation.
Such as the method for general toolroom machine waste liquid of the processing containing oil-in-water emulsion is the boundary by destroying oil droplet and water Face, make oil droplet can be close to each other and assemble, and then with water stratification and separate, the above process referred to as be demulsified (demulsification).The modes such as demulsifier, hyperfiltration (ultrafiltration), high voltage electric field are usually used to carry out Demulsification, but still face processing speed slowly, equipment and consumables cost is high, demulsifier pollution, still needs to subsequent other separation journeys The problems such as sequence.
Summary of the invention
The purpose of the present invention is to provide a kind of toolroom machine method for treating waste liquid, can overcome lacking for above-mentioned background technique Point.
Toolroom machine method for treating waste liquid containing oil-water emulsion of the invention includes that the toolroom machine waste liquid is introduced inside For the rotary packed bed of negative pressure, under the centrifugal force effect that rotary packed bed rotation generates, the water in the toolroom machine waste liquid is certainly It is vaporized separation in the toolroom machine waste liquid, and the oil-water emulsion is made to form the water-in-oil emulsion that moisture content is lower than 10%.
The beneficial effects of the present invention are: the toolroom machine method for treating waste liquid can quickly make oil-water emulsion form moisture content The moisture content in toolroom machine waste liquid is effectively reduced in water-in-oil emulsion lower than 10%.
It will be described in detail below with regard to the content of present invention:
Preferably, the pressure inside the rotary packed bed is less than 500torr.It is highly preferred that inside the rotary packed bed Pressure is between 110-470torr.In a specific embodiment of the present invention, the pressure inside the rotary packed bed is between 338- 469torr。
Preferably, in the rotary packed bed, the temperature of the toolroom machine waste liquid is greater than 55 DEG C and less than 100 DEG C.In this hair In bright specific embodiment, the temperature of the toolroom machine waste liquid is between 62.3-80 DEG C.
Preferably, inventive article machine method for treating waste liquid also includes the water-in-oil emulsion that the moisture content is lower than to 10% The rotary packed bed is exported, and after evenly mixing with the toolroom machine waste liquid, then leads back to the rotary packed bed.
Preferably, inventive article machine method for treating waste liquid also includes the aqueous vapor condensing recovery for isolating the vaporization.More Preferably, the temperature of the condensation is less than 40 DEG C.In a specific embodiment of the present invention, the temperature of the condensation is between 24-30 DEG C.
Preferably, the speed of rotary packed bed rotation is 300rpm or more.It is highly preferred that rotary packed bed rotation Speed is 300-3000rpm.
Preferably, the moisture content of the oil-water emulsion is 20% or more.
Preferably, the substance which is filled is selected from wire netting, glass marble, plastic filler, activity Carbon, zeolite, metal plate or combinations thereof.
In a specific embodiment of the present invention, which can make oil-water emulsion form moisture content low In 0.5% water-in-oil emulsion, or even form the water-in-oil emulsion that moisture content is lower than 0.3%.
Detailed description of the invention
Other features of the invention and effect will be clearly presented in the embodiment referring to attached drawing, in which:
Fig. 1 is configuration schematic diagram, illustrates the embodiment of inventive article machine method for treating waste liquid.
Specific embodiment
The present invention will be described further with regard to following embodiment, however, it should be noted that the embodiment is only to illustrate With, and it is not necessarily to be construed as the limitation that the present invention is implemented.
Refering to fig. 1, the embodiment of inventive article machine method for treating waste liquid includes that will contain the toolroom machine of oil-water emulsion Waste liquid (being formed by oil-in-water emulsion with 150kg water by 17kg cutting oil) is heated to 65 DEG C by heater 1, then with liquid The toolroom machine waste liquid is introduced into rotary packed bed 2 (substance of filling is wire netting) using constant power by body pump.
By being connected to the vacuum pump 3 of the rotary packed bed 2, make inside the rotary packed bed 2 for negative pressure, meanwhile, the rotation Turn packed bed 2 to rotate with the revolving speed of 652rpm, to generate centrifugal force effect to the toolroom machine waste liquid, make in the oil-water emulsion Water forms the low water-in-oil emulsion of moisture content after being removed, then flow out the rotary packed bed 2 and flow into the storage of toolroom machine waste liquid In slot 4, after evenly mixing with the toolroom machine waste liquid, then is heated by the heater 1 and lead back to the rotary packed bed 2.
While the rotary packed bed 2 rotation, the water in the toolroom machine waste liquid is vaporized point from the toolroom machine waste liquid From being subsequently introduced condenser 5 and condense and flow into recycle-water storage tank 6 and collect.Water temperature in the recycle-water storage tank 6 is about 24- 30℃。
After carrying out above-mentioned toolroom machine method for treating waste liquid 0.5h, 1h, 1.5h, 2h, 2.5h, 3h, 3.5h, 4h, 4.25h, The pressure inside the rotary packed bed 2 is all measured respectively, the fluid temperature being introduced into the rotary packed bed 2, introduces the rotary filling Fill the flow rate of liquid of bed 2, in the waste liquid moisture content (actual measurement) in the toolroom machine liquid waste tank 4, the water in the recycle-water storage tank 6 Weight, it is as a result as shown in table 1 below respectively.
Table 1
It can be seen from upper table 1 after the toolroom machine method for treating waste liquid 4h for carrying out the present embodiment, in the toolroom machine waste liquid Waste liquid moisture content in storage tank 4 can be reduced to 7.65%, show the toolroom machine waste liquid from the oil-in-water emulsion contained originally It is transformed into the water-in-oil emulsion that moisture content is lower than 10%;After the toolroom machine method for treating waste liquid 4.25h for carrying out the present embodiment, Waste liquid moisture content in the toolroom machine liquid waste tank 4 can be greatly reduced by 90.0% to 0.20% that (de-water ratio is up to 99.6%), show that the oil-water emulsion that the toolroom machine waste liquid contains has formed Water-In-Oil emulsification of the moisture content significantly lower than 10% Liquid.After the toolroom machine method for treating waste liquid 4.25h for carrying out the present embodiment, up to 88% can be recycled in the recycle-water storage tank 6 Water.In addition, the toolroom machine method for treating waste liquid of the present embodiment is not necessarily to discharge any waste liquid completely, the toolroom machine liquid waste tank 4 In liquid and the recycle-water storage tank 6 in water it is all recyclable recycle, and the liquid in the toolroom machine liquid waste tank 4 is above-mentioned Each time of measuring point is all homogeneous liquid phase (oil-free water stratification phenomenon).
It is lower than in conclusion inventive article machine method for treating waste liquid can quickly make oil-water emulsion form moisture content 10% water-in-oil emulsion eliminates using demulsifier, surpasses during processing without carrying out general common demulsification processing The modes such as filtering, high voltage electric field carry out the required problems faced that is demulsified.The present invention is sustainable to be effectively reduced a large amount of toolroom machine waste liquids In moisture content, and can continuous processing oil-in-water emulsion or water-in-oil emulsion, and can get the water of not oil-containing for recycling again It utilizes, so the purpose of the present invention can be reached really.
The above, only the embodiment of the present invention, when cannot be limited the scope of implementation of the present invention with this, i.e., it is all according to Simple equivalent changes and modifications, all still belong to the scope of the present invention made by claims of the present invention and description.

Claims (10)

1. a kind of toolroom machine method for treating waste liquid, which contains oil-water emulsion, it is characterised in that the processing method Include: the toolroom machine waste liquid being introduced into the internal rotary packed bed for negative pressure, in the centrifugal force that rotary packed bed rotation generates Under effect, the water in the toolroom machine waste liquid is vaporized separation from the toolroom machine waste liquid, and it is aqueous to form the oil-water emulsion Rate is lower than 10% water-in-oil emulsion.
2. toolroom machine method for treating waste liquid according to claim 1, it is characterised in that: the pressure inside the rotary packed bed Less than 500torr.
3. toolroom machine method for treating waste liquid according to claim 2, it is characterised in that: the pressure inside the rotary packed bed Between 110-470torr.
4. toolroom machine method for treating waste liquid according to claim 1, it is characterised in that: in the rotary packed bed, the work The temperature of tool machine waste liquid is greater than 55 DEG C and less than 100 DEG C.
5. toolroom machine method for treating waste liquid according to claim 1, it is characterised in that: also comprising the moisture content to be lower than 10% water-in-oil emulsion exports the rotary packed bed, and after evenly mixing with the toolroom machine waste liquid, then leads back to the rotary filling Fill bed.
6. toolroom machine method for treating waste liquid according to claim 1, it is characterised in that: also include to isolate the vaporization Aqueous vapor condensing recovery.
7. toolroom machine method for treating waste liquid according to claim 6, it is characterised in that: the temperature of the condensation is less than 40 DEG C.
8. toolroom machine method for treating waste liquid according to claim 1, it is characterised in that: the speed of rotary packed bed rotation For 300rpm or more.
9. toolroom machine method for treating waste liquid according to claim 1, it is characterised in that: the moisture content of the oil-water emulsion is 20% or more.
10. toolroom machine method for treating waste liquid according to claim 1, it is characterised in that: what the rotary packed bed was filled Substance is selected from wire netting, glass marble, plastic filler, activated carbon, zeolite, metal plate or combinations thereof.
CN201711006769.4A 2017-10-25 2017-10-25 Toolroom machine method for treating waste liquid Pending CN109704439A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711006769.4A CN109704439A (en) 2017-10-25 2017-10-25 Toolroom machine method for treating waste liquid

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711006769.4A CN109704439A (en) 2017-10-25 2017-10-25 Toolroom machine method for treating waste liquid

Publications (1)

Publication Number Publication Date
CN109704439A true CN109704439A (en) 2019-05-03

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2123358U (en) * 1992-04-22 1992-12-02 渝州大学 High efficiency vacuum oil filtering equipment
CN2179188Y (en) * 1993-12-11 1994-10-12 山东省电力试验研究所 Vacuum oil-in-water separator
US6224716B1 (en) * 1998-03-18 2001-05-01 Oilquip, Inc. Apparatus for dehydrating oil
CN101265416A (en) * 2007-03-16 2008-09-17 中国人民解放军后勤工程学院 Lubricating oil composite dewatering technique
CN102652885A (en) * 2012-05-14 2012-09-05 周建伟 Vacuum-state centrifugal filtering and dehydrating device for lubricating oil

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2123358U (en) * 1992-04-22 1992-12-02 渝州大学 High efficiency vacuum oil filtering equipment
CN2179188Y (en) * 1993-12-11 1994-10-12 山东省电力试验研究所 Vacuum oil-in-water separator
US6224716B1 (en) * 1998-03-18 2001-05-01 Oilquip, Inc. Apparatus for dehydrating oil
CN101265416A (en) * 2007-03-16 2008-09-17 中国人民解放军后勤工程学院 Lubricating oil composite dewatering technique
CN102652885A (en) * 2012-05-14 2012-09-05 周建伟 Vacuum-state centrifugal filtering and dehydrating device for lubricating oil

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Effective date of registration: 20210104

Address after: 6th floor, Lane 38, Lane 358, Ruiguang Road, Neihu district, Taipei, China

Applicant after: Haiqi Technology Co.,Ltd.

Address before: No.1, section 3, Zhongxiao East Road, Taipei, Taiwan, China

Applicant before: National Taipei University of Technology

WD01 Invention patent application deemed withdrawn after publication
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20190503