CN109667153A - A kind of fabric anti-flaming dope and the flame retardant fabric using the anti-flaming dope - Google Patents
A kind of fabric anti-flaming dope and the flame retardant fabric using the anti-flaming dope Download PDFInfo
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- CN109667153A CN109667153A CN201811369041.2A CN201811369041A CN109667153A CN 109667153 A CN109667153 A CN 109667153A CN 201811369041 A CN201811369041 A CN 201811369041A CN 109667153 A CN109667153 A CN 109667153A
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- Prior art keywords
- parts
- flaming dope
- cloth
- fabric
- flame retardant
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- 239000004744 fabric Substances 0.000 title claims abstract description 108
- 239000003063 flame retardant Substances 0.000 title claims abstract description 50
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 title claims abstract description 36
- 229920002050 silicone resin Polymers 0.000 claims abstract description 28
- -1 Methyl Hydrogen Chemical compound 0.000 claims abstract description 24
- 229910000000 metal hydroxide Inorganic materials 0.000 claims abstract description 17
- 150000004692 metal hydroxides Chemical class 0.000 claims abstract description 17
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract description 17
- 239000002202 Polyethylene glycol Substances 0.000 claims abstract description 16
- YGCOKJWKWLYHTG-UHFFFAOYSA-N [[4,6-bis[bis(hydroxymethyl)amino]-1,3,5-triazin-2-yl]-(hydroxymethyl)amino]methanol Chemical compound OCN(CO)C1=NC(N(CO)CO)=NC(N(CO)CO)=N1 YGCOKJWKWLYHTG-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229940051841 polyoxyethylene ether Drugs 0.000 claims abstract description 16
- 229920000056 polyoxyethylene ether Polymers 0.000 claims abstract description 16
- 239000000835 fiber Substances 0.000 claims abstract description 15
- 239000001257 hydrogen Substances 0.000 claims abstract description 15
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 15
- 229920000742 Cotton Polymers 0.000 claims abstract description 14
- 150000002191 fatty alcohols Chemical class 0.000 claims abstract description 14
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims abstract description 12
- 229920001296 polysiloxane Polymers 0.000 claims abstract description 12
- 229920005573 silicon-containing polymer Polymers 0.000 claims abstract description 12
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000012530 fluid Substances 0.000 claims abstract description 11
- 229910052710 silicon Inorganic materials 0.000 claims abstract description 11
- 239000010703 silicon Substances 0.000 claims abstract description 11
- 239000002994 raw material Substances 0.000 claims abstract description 10
- 239000004952 Polyamide Substances 0.000 claims abstract description 9
- 229920002647 polyamide Polymers 0.000 claims abstract description 9
- 239000000203 mixture Substances 0.000 claims abstract description 8
- 229920004933 Terylene® Polymers 0.000 claims abstract description 3
- 239000005020 polyethylene terephthalate Substances 0.000 claims abstract description 3
- 239000011248 coating agent Substances 0.000 claims description 13
- 238000000576 coating method Methods 0.000 claims description 13
- 238000001035 drying Methods 0.000 claims description 11
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 10
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 claims description 8
- 239000000347 magnesium hydroxide Substances 0.000 claims description 8
- 229910001862 magnesium hydroxide Inorganic materials 0.000 claims description 8
- 238000010792 warming Methods 0.000 claims description 5
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims description 4
- 229910021502 aluminium hydroxide Inorganic materials 0.000 claims description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 2
- 239000004593 Epoxy Substances 0.000 claims 1
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 claims 1
- 229910021505 gold(III) hydroxide Inorganic materials 0.000 claims 1
- WDZVNNYQBQRJRX-UHFFFAOYSA-K gold(iii) hydroxide Chemical compound O[Au](O)O WDZVNNYQBQRJRX-UHFFFAOYSA-K 0.000 claims 1
- 150000002576 ketones Chemical class 0.000 claims 1
- 229920005989 resin Polymers 0.000 claims 1
- 239000011347 resin Substances 0.000 claims 1
- 239000000463 material Substances 0.000 abstract description 21
- 239000004753 textile Substances 0.000 abstract description 7
- 238000012545 processing Methods 0.000 abstract description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 14
- 239000001301 oxygen Substances 0.000 description 14
- 229910052760 oxygen Inorganic materials 0.000 description 14
- 230000000052 comparative effect Effects 0.000 description 13
- 239000003795 chemical substances by application Substances 0.000 description 8
- 230000000694 effects Effects 0.000 description 8
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 7
- 241000219146 Gossypium Species 0.000 description 7
- 238000000034 method Methods 0.000 description 7
- 238000012986 modification Methods 0.000 description 6
- 230000004048 modification Effects 0.000 description 6
- 239000010410 layer Substances 0.000 description 5
- 239000000314 lubricant Substances 0.000 description 5
- 239000000243 solution Substances 0.000 description 5
- 239000004902 Softening Agent Substances 0.000 description 4
- MCWXGJITAZMZEV-UHFFFAOYSA-N dimethoate Chemical compound CNC(=O)CSP(=S)(OC)OC MCWXGJITAZMZEV-UHFFFAOYSA-N 0.000 description 4
- 229920002545 silicone oil Polymers 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 239000007789 gas Substances 0.000 description 3
- 150000002431 hydrogen Chemical class 0.000 description 3
- 230000035699 permeability Effects 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 240000000047 Gossypium barbadense Species 0.000 description 2
- 235000009429 Gossypium barbadense Nutrition 0.000 description 2
- 230000006750 UV protection Effects 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 125000000217 alkyl group Chemical group 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 229920006231 aramid fiber Polymers 0.000 description 2
- 239000012752 auxiliary agent Substances 0.000 description 2
- 230000000740 bleeding effect Effects 0.000 description 2
- 150000001768 cations Chemical class 0.000 description 2
- 238000002485 combustion reaction Methods 0.000 description 2
- 239000003995 emulsifying agent Substances 0.000 description 2
- 238000004079 fireproofing Methods 0.000 description 2
- 239000003230 hygroscopic agent Substances 0.000 description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 2
- 238000010422 painting Methods 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 238000011056 performance test Methods 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 230000004224 protection Effects 0.000 description 2
- 239000002689 soil Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 230000009967 tasteless effect Effects 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 238000009941 weaving Methods 0.000 description 2
- FHVDTGUDJYJELY-UHFFFAOYSA-N 6-{[2-carboxy-4,5-dihydroxy-6-(phosphanyloxy)oxan-3-yl]oxy}-4,5-dihydroxy-3-phosphanyloxane-2-carboxylic acid Chemical compound O1C(C(O)=O)C(P)C(O)C(O)C1OC1C(C(O)=O)OC(OP)C(O)C1O FHVDTGUDJYJELY-UHFFFAOYSA-N 0.000 description 1
- 241001474374 Blennius Species 0.000 description 1
- XZMCDFZZKTWFGF-UHFFFAOYSA-N Cyanamide Chemical compound NC#N XZMCDFZZKTWFGF-UHFFFAOYSA-N 0.000 description 1
- 206010021143 Hypoxia Diseases 0.000 description 1
- 229920000877 Melamine resin Polymers 0.000 description 1
- AFCARXCZXQIEQB-UHFFFAOYSA-N N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CCNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 AFCARXCZXQIEQB-UHFFFAOYSA-N 0.000 description 1
- 229910007161 Si(CH3)3 Inorganic materials 0.000 description 1
- OLBVUFHMDRJKTK-UHFFFAOYSA-N [N].[O] Chemical compound [N].[O] OLBVUFHMDRJKTK-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- 230000003213 activating effect Effects 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 229940072056 alginate Drugs 0.000 description 1
- 229920000615 alginic acid Polymers 0.000 description 1
- 235000010443 alginic acid Nutrition 0.000 description 1
- OJMOMXZKOWKUTA-UHFFFAOYSA-N aluminum;borate Chemical compound [Al+3].[O-]B([O-])[O-] OJMOMXZKOWKUTA-UHFFFAOYSA-N 0.000 description 1
- 239000002216 antistatic agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 1
- 239000004327 boric acid Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000013065 commercial product Substances 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 229940008099 dimethicone Drugs 0.000 description 1
- 239000004205 dimethyl polysiloxane Substances 0.000 description 1
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 208000018875 hypoxemia Diseases 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 230000001535 kindling effect Effects 0.000 description 1
- 239000004816 latex Substances 0.000 description 1
- 229920000126 latex Polymers 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- OKKJLVBELUTLKV-UHFFFAOYSA-N methanol Natural products OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 238000011017 operating method Methods 0.000 description 1
- 125000006353 oxyethylene group Chemical group 0.000 description 1
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 235000019353 potassium silicate Nutrition 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000000979 retarding effect Effects 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
- 239000002344 surface layer Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 238000005829 trimerization reaction Methods 0.000 description 1
- BIKXLKXABVUSMH-UHFFFAOYSA-N trizinc;diborate Chemical compound [Zn+2].[Zn+2].[Zn+2].[O-]B([O-])[O-].[O-]B([O-])[O-] BIKXLKXABVUSMH-UHFFFAOYSA-N 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/44—Oxides or hydroxides of elements of Groups 2 or 12 of the Periodic Table; Zincates; Cadmates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/45—Oxides or hydroxides of elements of Groups 3 or 13 of the Periodic Table; Aluminates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/35—Heterocyclic compounds
- D06M13/355—Heterocyclic compounds having six-membered heterocyclic rings
- D06M13/358—Triazines
- D06M13/364—Cyanuric acid; Isocyanuric acid; Derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/368—Hydroxyalkylamines; Derivatives thereof, e.g. Kritchevsky bases
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/34—Polyamides
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/30—Flame or heat resistance, fire retardancy properties
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The present invention relates to the technical fields of textile material, more particularly to a kind of fabric anti-flaming dope, raw material including following parts by weight: 30-60 parts of silicone resin, 5-10 parts of metal hydroxides, 5-15 parts of hexamethylolmelamine, 10-20 parts of polyethylene glycol and 1-5 parts of fatty alcohol polyoxyethylene ether, the silicone resin is by dimethyl silicone polymer and Methyl Hydrogen Polysiloxane Fluid according to silicon mass content than being polymerized for the proportion of 3:1-8:1;To make anti-flaming dope of the invention be suitble to the processing of personal clothing or daily worn cotton or relatively soft clothing cloth, application range and applicability are stronger;A kind of flame retardant fabric of application anti-flaming dope is further related to, it is blended that the cloth is selected from cotton, terylene, polyamide fibre or polyester-cotton blend;Make cloth after using the anti-flaming dope, on the basis of keeping original comfort level and pliability, improves the flame retardant property of cloth.
Description
Technical field
The present invention relates to the technical fields of textile material, and in particular to a kind of fabric anti-flaming dope and applies the fire-retardant painting
The flame retardant fabric of material.
Background technique
Fabric is mostly all inflammable since it is at the reason being grouped as through being formed by weaving, even if encountering a little fire
Star is also easy kindling, or part is burnt out, gently then surface damage, heavy then burn hole etc., this has seriously affected it using imitating
Fruit, if anti-fire is bad, the use of fabric will receive significant limitation.
In order to improve the flame retardant property of fabric or cloth, occur many fire protection flame retarding clothes and fire prevention in the prior art
Clothes.In patent CN105220314B, resistance to 320~340 DEG C fire- resistance cloth of one kind and preparation method thereof is disclosed, weaving material is belonged to
Material and fireproofing technique field.Warp thread composition are as follows: (by mass percentage) poly- phosphamide fiber 30~70%, aramid fiber 30~
70%, weft yarn composition are as follows: long-staple cotton 1~30%, poly- phosphamide fiber 29~70%, alginate fibre 29~70%;In this application
It is blended at warp yarns with poly- phosphamide fiber and aramid fiber;With long-staple cotton, poly- phosphamide fiber and seaweed fiber blending at
Weft yarn;By warp thread in conjunction with weft yarn, using staggeredly weave, it is made into the fire- resistance cloth with certain density;It uses structure strong
It spends that the cloth hardness that biggish fiber is staggeredly mutually knitted is larger, and softness is not good enough, is unsuitable for making personal clothing or daily
Worn cotton or relatively soft clothing.
In patent CN105734958A, a kind of manufacturing method of fireproof cloth is disclosed, comprising the following steps: (1) take
Boric acid, zinc borate and aluminium borate, which are dissolved in the water, prepares solution, and woven cloth is placed in configured solution, impregnates 15
Hour or more, it every 5 hours, stirs, swipes cloth back and forth in design on fabric surface with brush;(2) by resulting cloth in temperature
It is dried in environment greater than 40 DEG C;(3) step (2) resulting cloth is immersed in pure acrylic latex in closed environment
In, 12 hours are impregnated, and take out, in environment of the temperature no more than 25 DEG C, the wind of 5.5m/s is not more than with wind speed, is blown
It is dry;(4) step (1) resulting fabric is immersed into water glass solution, impregnates 1.5 hours, after taking-up, entirely spreads out,
Three stackings are closed, and are extruded to shape with compression roller, and in gentle breeze, until fabric is dry.The method by soaking cloth three times
Bubble processing is affected to fabric itself original performance such as intensity, color fastness etc. to improve its fire protecting performance, and control is improper can
Fabric feeling can be made to harden, to influence whether the texture and quality of cloth.
Summary of the invention
In view of the deficienciess of the prior art, the first purpose of this invention is to provide a kind of suitable personal clothing or day
The often fabric anti-flaming dope of worn cotton or relatively soft clothing cloth.
The first purpose of this invention is achieved through the following technical solutions:
A kind of fabric anti-flaming dope, the raw material including following parts by weight: 30-60 parts of silicone resin, metal hydroxides 5-
10 parts, 5-15 parts of hexamethylolmelamine, 10-20 parts of polyethylene glycol and 1-5 parts of fatty alcohol polyoxyethylene ether, the silicone tree
Rouge is by dimethyl silicone polymer and Methyl Hydrogen Polysiloxane Fluid according to silicon mass content than being polymerized for the proportion of 3:1-8:1.
By using above-mentioned technical proposal, dimethyl silicone polymer is also referred to as dimethicone, colourless or light yellow liquid,
Tasteless, transparency is high, and it is small to have many advantages, such as that heat resistance, cold resistance, viscosity vary with temperature small, waterproofness, surface tension.Diformazan
Base silicone oil is non-toxic and tasteless, has physiological inertia and good chemical stability, electrical insulating property, weatherability, hydrophobicity are good, and have
There is very high anti-shear ability, can be used for a long time at -50 DEG C~200 DEG C.Methyl Hydrogen Polysiloxane Fluid is commonly called as containing hydrogen silicone oil, molecule
Formula are as follows: (CH3)3SiO[(CH3)(H)SiO]nSi(CH3)3, Methyl Hydrogen Polysiloxane Fluid is polymerize with linear dimethyl silicone polymer
To netted silicone resin, it had not only been able to maintain fabric original gas permeability and flexibility, but also the tearing strength of fabric, friction can be improved
Intensity and soil resistance, and have the function of more excellent UV resistance.Hexamethylolmelamine, in without acid aqueous solution
A couple of days can be kept to stablize, it can be shared with cation and non-ionic softening agent and bleeding agent.Metal hydroxides plays master
Fire-retardant effect is wanted, but needs to cooperate the hexamethylolmelamine in the present invention that can just give full play to it in anti-flaming dope
In fire retardation, then by netted silicone resin and metal hydroxides polymeric modification, auxiliary is to emulsify levelling agent fat
Alcohol polyoxyethylene ether, antistatic lubricant polyethylene glycol act synergistically between each other, and being formed has preferable flame retardant effect and fit
For the anti-flaming dope of soft or soft cloth, so as to be applied to personal clothing or daily worn cotton or relatively soft clothing
In the flame retardant treatment of cloth.
Preferably, including the raw material of following parts by weight: 40-50 parts of silicone resin, 6-8 parts of metal hydroxides, six
8-12 parts of melamine methylol, 12-16 parts of polyethylene glycol and 2-4 parts of fatty alcohol polyoxyethylene ether, the silicone resin is by gathering
Dimethyl siloxane and Methyl Hydrogen Polysiloxane Fluid are according to silicon mass content than being polymerized for the proportion of 5:1-7:1.
Preferably, the adduct number of the fatty alcohol polyoxyethylene ether ethylene oxide is 11-16.
By using above-mentioned technical proposal, fatty alcohol polyoxyethylene ether, RO(CH2CH2O)nH, R be generally be saturated or not
The C of saturation12~18Alkyl, be straight-chain alkyl, be also possible to branched alkyl;N is the adduct number of ethylene oxide, that is,
The number of oxyethylene group in surfactant molecule.N is bigger, and the oxygen on molecule hydrophilic group is more, can be formed more with water
Hydrogen bond is water-soluble better.When n=1 ~ 5, product can be dissolved in oil and not soluble in water, often as preparing sulfuric acid ester anionic surface
The raw material of activating agent.When n=6 ~ 8, it can be dissolved in water, be commonly used for the detergent and grease emulsifier of textile.When n=10 ~ 20, commonly use
Make emulsifier and levelling agent.By experimental results demonstrate cooperate other raw materials at n=11 ~ 16 in the present invention, treated cloth
Expect that color is best.
Preferably, the average molecular weight of the polyethylene glycol is 4000-6000.
By using above-mentioned technical proposal, polyethylene glycol, abbreviation PEG, PEG-4000,6000 be used as in textile industry it is anti-
Electrostatic agent, lubricant etc. play certain wettability, make silicone resin and metal applied in anti-flaming dope of the invention
It is easier to interpenetrate modification between hydroxide, improves the performance of the overall flame air-moisture-permeable of anti-flaming dope.
Preferably, the metal hydroxides is magnesium hydroxide or aluminium hydroxide.
Preferably, the average grain diameter of the metal hydroxides is 1-10 μm.
By using above-mentioned technical proposal, while guaranteeing that fire retardant matter plays a role, fire retardant matter particle is reduced, is reduced
Influence to cloth softness, to avoid causing the hardness of clothing to increase because using the anti-flaming dope, degree of comfort decreased
The problem of occur.
Preferably, further including 5-15 parts of triethanolamine.
By using above-mentioned technical proposal, triethanolamine, for being good solvent in textile industry, hygroscopic agent is to knit
The raw material of object softening agent.The flexibility of cloth processed can further be improved by adding suitable triethanolamine, to improve
Comfort level.
A second object of the present invention is to provide a kind of flame retardant fabric processed using above-mentioned fabrics with anti-flaming dope,
Make cloth after using the anti-flaming dope, on the basis of keeping original comfort level and pliability, improves the flame retardant property of cloth.
Second object of the present invention is achieved through the following technical solutions:
A kind of flame retardant fabric that fabric is processed with anti-flaming dope, it is blended that the cloth is selected from cotton, terylene, polyamide fibre or polyester-cotton blend.
It is obtained preferably, it is handled as follows:
(1) the two-sided of cloth to be processed is coated with insulating layer, drying obtains cloth germule;
(2) the two-sided of above-mentioned cloth germule is coated with the anti-flaming dope, coating thickness 1-2mm, up to fire-retardant after drying
Cloth.
Preferably, drying 20-40min at 80-95 DEG C in the step (1);In the step (2), prior to 100
1-3min is dried at DEG C, then is warming up at 180-195 DEG C and is dried 3-5min.
Fire-retardant painting of the invention is coated with after the surface layer of soft cloth is applied layer of cloth by using above-mentioned technical proposal
Material, drying.And the temperature and time of drying is controlled, especially the drying time after coating anti-flaming dope is shorter, drying
Temperature is relatively high, makes anti-flaming dope by " dodge dry " and is firmly coated on cloth, will not the property such as hardness to cloth itself
It can have adverse effect on, guarantee the soft comfort level of cloth.
In conclusion the invention has the following beneficial effects:
(1) silicone resin is compounded to obtain anti-flaming dope with fire proofing, has both the breathable moisture permeability and fire-retardant material of silicone resin
The flame retardant property of material, and other auxiliary agents are assisted, so that anti-flaming dope of the invention is suitable for soft cloth, to be suitble to daily clothing
The working process of object cloth, expands application range;
(2) anti-flaming dope of the invention is directly treated to processing cloth to be processed in the way of coating, is had
The flame retardant fabric of flame retardant property, limit oxygen index are up to 39.9%, are not affected in performances such as guarantee cloth itself pliabilitys
While, improve the flame retardant property of cloth.
Specific embodiment
Each auxiliary agent and raw material used are commercial product in the present invention.Anti-flaming dope in the present invention can be used for cotton, wash
In synthetic fibre, polyamide fibre or the blended fire-retardant working process of cloth of polyester-cotton blend, specific processing method is identical, carries out by taking polyamide fibre cloth as an example below
Explanation.
Embodiment 1
By silicone resin 60g, average grain diameter be 5 μm magnesium hydroxide 10g, hexamethylolmelamine 10g, average molecular weight be
The fatty alcohol polyoxyethylene ether 5g that 4000 polyethylene glycol 10g and the adduct number of ethylene oxide are 11 is thoroughly mixed, and is obtained
The anti-flaming dope of embodiment 1.Wherein, silicone resin is by dimethyl silicone polymer and Methyl Hydrogen Polysiloxane Fluid according to silicon mass content ratio
It is polymerized for the proportion of 3:1, the conventional technical means that polymerization polymerize with operating procedure for silicone resin is no longer superfluous herein
It states.
Embodiment 2
Embodiment 2 the difference from embodiment 1 is that: the anti-flaming dope in embodiment 2 is silicone resin 50g, average grain diameter is 10 μ
The aluminium hydroxide 8g of m, hexamethylolmelamine 12g, the polyethylene glycol 16g that average molecular weight is 4000 and ethylene oxide plus
It is thoroughly mixed and obtains for 16 fatty alcohol polyoxyethylene ether 4g at number.Wherein, silicone resin by dimethyl silicone polymer with
Methyl Hydrogen Polysiloxane Fluid is according to silicon mass content than being polymerized for the proportion of 7:1.
Embodiment 3
Embodiment 3 the difference from embodiment 1 is that: the anti-flaming dope in embodiment 3 is silicone resin 40g, average grain diameter is 1 μm
Magnesium hydroxide 6g, hexamethylolmelamine 8g, average molecular weight be 4000 polyethylene glycol 12g and ethylene oxide addition
Number is thoroughly mixed and obtains for 14 fatty alcohol polyoxyethylene ether 2g.Wherein, silicone resin is by dimethyl silicone polymer and first
Base containing hydrogen silicone oil is according to silicon mass content than being polymerized for the proportion of 5:1.
Embodiment 4
Embodiment 4 the difference from embodiment 1 is that: the anti-flaming dope in embodiment 4 is silicone resin 30g, average grain diameter is 5 μm
Magnesium hydroxide 5g, hexamethylolmelamine 5g, average molecular weight be 4000 polyethylene glycol 20g and ethylene oxide addition
Number is thoroughly mixed and obtains for 13 fatty alcohol polyoxyethylene ether 1g.Wherein, silicone resin is by dimethyl silicone polymer and first
Base containing hydrogen silicone oil is according to silicon mass content than being polymerized for the proportion of 8:1.
Embodiment 5
Embodiment 5 the difference from embodiment 1 is that: the anti-flaming dope in embodiment 5 is silicone resin 45g, average grain diameter is 5 μm
Magnesium hydroxide 8g, hexamethylolmelamine 15g, average molecular weight be 4000 polyethylene glycol 15g and ethylene oxide plus
It is thoroughly mixed and obtains for 14 fatty alcohol polyoxyethylene ether 3g at number.Wherein, silicone resin by dimethyl silicone polymer with
Methyl Hydrogen Polysiloxane Fluid is according to silicon mass content than being polymerized for the proportion of 6:1.
Embodiment 6
Embodiment 6 and the difference of embodiment 5 are: the triethanolamine of 5g is also added into the anti-flaming dope in embodiment 6.
Embodiment 7
Embodiment 7 and the difference of embodiment 5 are: the triethanolamine of 10g is also added into the anti-flaming dope in embodiment 7.
Embodiment 8
Embodiment 8 and the difference of embodiment 5 are: the triethanolamine of 15g is also added into the anti-flaming dope in embodiment 8.
The application examples of anti-flaming dope prepared by the present invention
Application examples 1
It is the double spread insulating layer of the polyamide fibre cloth of 5m by length and width, 40min is dried at 80 DEG C, then double spread is real again
Apply the anti-flaming dope of example 7, coating thickness 1-2mm, after coating uniformly, prior to 100 DEG C at dry 3min, then be warming up to 180 DEG C
Lower drying 5min, obtains the flame retardant fabric of application examples 1.
Application examples 2
Application examples 2 and the difference of application examples 1 are: the double spread that length and width are the polyamide fibre cloth of 5m insulating in application examples 2
Layer, dries 20min at 90 DEG C, and then the anti-flaming dope of double spread embodiment 7, coating thickness 1-2mm, coating are uniform again
Afterwards, prior to 100 DEG C at dry 1min, then be warming up at 195 DEG C and dry 3min, obtain the flame retardant fabric of application examples 2.
Application examples 3
Application examples 3 and the difference of application examples 1 are: the double spread that length and width are the polyamide fibre cloth of 5m insulating in application examples 3
Layer, dries 30min at 95 DEG C, and then the anti-flaming dope of double spread embodiment 7, coating thickness 1-2mm, coating are uniform again
Afterwards, prior to 100 DEG C at dry 2min, then be warming up at 190 DEG C and dry 2min, obtain the flame retardant fabric of application examples 3.
Application examples 4-10
Application examples 4-10 is that the anti-flaming dope of embodiment 1-6 and embodiment 8 are successively coated on polyamide cloth with the method for application examples 2
The flame retardant fabric of the application examples 4-10 obtained on material.
Comparative example 1
Comparative example 1 and the difference of application examples 2 are: hexamethylolmelamine is not added in flame retardant fabric.
Comparative example 2
Comparative example 2 and the difference of application examples 2 are: after anti-flaming dope coating uniformly, drying 5min at 100 DEG C, obtain comparative example 2
Flame retardant fabric.
Comparative example 3
Comparative example 3 and the difference of application examples 2 are: without magnesium hydroxide in anti-flaming dope, remaining is identical as application examples 2.
Blank group
The difference of blank group and application examples 2 is: the two-sided uncoated any anti-flaming dope of cloth, remaining is identical as application examples 2.
Performance test
Flame retardant property survey is carried out to the flame retardant fabric of application examples 1-10 and comparative example 1-2 according to the method for GB/T 5454-1997
Examination;Color variation after observing the color situation of each cloth and washing 50 times;And feel degree is detected, test result is shown in Table
Shown in 1.Wherein, limit oxygen index refers to the volume point of polymer oxygen when can just support its burning in oxygen and nitrogen mixture gas
Particle density.It is the index for characterizing material combustion behavior.It has been generally acknowledged that the substance can fire in air when limit oxygen index is 22
It burns.Limit oxygen index refers under the defined conditions, most hypoxemia needed for material carries out flaming combustion in oxygen-nitrogen mixture stream
Concentration.It is indicated with the numerical value of percentage by volume shared by oxygen.Oxygen index (OI) height indicates that material is nonflammable, the low expression material of oxygen index (OI)
Material is easy burning, it is considered that oxygen index (OI) < 22% belongs to combustible material, and oxygen index (OI) belongs to combustible material between 22%-27%, and oxygen refers to
Number > 27% belongs to nonflammable material.
The performance test results of each flame retardant fabric of table 1
As shown in Table 1, by anti-flaming dope of the invention treated cloth, excellent flame retardant property is all had,
Change it for nonflammable material by combustible material, and limit oxygen index is up to 39.9%, makes the flame retardant property of soft cloth
It is greatly improved.By blank group and application examples 1-3 and the Comparative result of application examples 9 and 10 it is found that resistance of the invention
Added with after triethanolamine in burning coating material, further improvement is obtained to the feel of cloth, has kept cloth more smooth, it is fine and smooth.
By the testing result of comparative example 1 it is found that flame retardant property of the hexamethylolmelamine to anti-flaming dope in the present invention
There is large effect, the flame retardant property of cloth substantially reduces if without hexamethylolmelamine, and becomes flammable from fire retardant.And
And comparative example 3 is combined it is found that metal hydroxides plays main fire-retardant effect, if being that the present invention is implemented without metal hydroxides
The presence of magnesium hydroxide and aluminium hydroxide in example, then the flame retardant property of resulting cloth substantially reduces, and becomes inflammable from fire retardant.
It is proved by comparative example 1 in conjunction with comparative example 3, the metal hydroxides in the present invention needs to cooperate the hexamethylol trimerization in the present invention
Cyanamide can just give full play to its fire retardation in anti-flaming dope, then by netted silicone resin and metal hydroxides
Polymeric modification, auxiliary is to emulsify levelling agent fatty alcohol polyoxyethylene ether, and antistatic lubricant polyethylene glycol, collaboration is made between each other
With, the anti-flaming dope that there is preferable flame retardant effect and be suitable for soft or soft cloth is formed, it is personal so as to be applied to
In the flame retardant treatment of clothing or daily worn cotton or relatively soft clothing cloth.
In the present invention, Methyl Hydrogen Polysiloxane Fluid is polymerize to obtain netted silicone resin with linear dimethyl silicone polymer,
Not only it had been able to maintain fabric original gas permeability and flexibility, but also the tearing strength, friction intensity and soil resistance of fabric can have been improved, and have
There is more excellent UV resistance function.Hexamethylolmelamine can keep a couple of days to stablize in without acid aqueous solution, it
It can be shared with cation and non-ionic softening agent and bleeding agent.Metal hydroxides plays main fire-retardant effect, still
Its fire retardation in anti-flaming dope can be given full play to by needing to cooperate the hexamethylolmelamine in the present invention, then
By netted silicone resin and metal hydroxides polymeric modification, assist resisting quiet to emulsify levelling agent fatty alcohol polyoxyethylene ether
Electric lubricant polyethylene glycol acts synergistically between each other, and being formed has preferable flame retardant effect and be suitable for soft or soft cloth
The anti-flaming dope of material, so as to be applied to the flame retardant treatment of personal clothing or daily worn cotton or relatively soft clothing cloth
In.In addition, PEG-4000,6000 are used as antistatic agent, lubricant etc. in textile industry, applied to anti-flaming dope of the invention
In, certain wettability is played, makes to be easier to interpenetrate modification between silicone resin and metal hydroxides, improve fire-retardant
The performance of the overall flame air-moisture-permeable of coating.Triethanolamine, for being good solvent in textile industry, hygroscopic agent is to knit
The raw material of object softening agent.Suitable triethanolamine is added in the present invention, can further improve the flexibility of cloth processed,
To improve comfort level.
This specific embodiment is only explanation of the invention, is not limitation of the present invention, those skilled in the art
Member can according to need the modification that not creative contribution is made to the present embodiment after reading this specification, but as long as at this
All by the protection of Patent Law in the scope of the claims of invention.
Claims (10)
1. a kind of fabric anti-flaming dope, which is characterized in that the raw material including following parts by weight: 30-60 parts of silicone resin, gold
Hydroxide 5-10 parts of category, 5-15 parts of hexamethylolmelamine, 10-20 parts of polyethylene glycol and fatty alcohol polyoxyethylene ether 1-5
Part, the silicone resin is by dimethyl silicone polymer and Methyl Hydrogen Polysiloxane Fluid according to silicon mass content than the proportion for 3:1-8:1
It is polymerized.
2. fabric anti-flaming dope according to claim 1, which is characterized in that the raw material including following parts by weight: silicon
40-50 parts of ketone resin, 6-8 parts of metal hydroxides, 8-12 parts of hexamethylolmelamine, 12-16 parts of polyethylene glycol and fat
2-4 parts of alcohol polyoxyethylene ether, the silicone resin is by dimethyl silicone polymer and Methyl Hydrogen Polysiloxane Fluid according to silicon mass content ratio
It is polymerized for the proportion of 5:1-7:1.
3. fabric anti-flaming dope according to claim 1, it is characterised in that: epoxy in the fatty alcohol polyoxyethylene ether
The adduct number of ethane is 11-16.
4. fabric anti-flaming dope according to claim 1, it is characterised in that: the average molecular weight of the polyethylene glycol is
4000-6000。
5. fabric anti-flaming dope according to claim 1, it is characterised in that: the metal hydroxides is magnesium hydroxide
Or aluminium hydroxide.
6. fabric anti-flaming dope according to claim 1, it is characterised in that: the average grain diameter of the metal hydroxides
It is 1-10 μm.
7. fabric anti-flaming dope according to claim 1, it is characterised in that: further include 5-15 parts of triethanolamine.
8. a kind of flame retardant fabric processed with the described in any item fabrics of claim 1-7 with anti-flaming dope, feature exist
In: it is blended that the cloth is selected from cotton, terylene, polyamide fibre or polyester-cotton blend.
9. flame retardant fabric according to claim 8, which is characterized in that it handles obtain as follows:
(1) the two-sided of cloth to be processed is coated with insulating layer, drying obtains cloth germule;
(2) the two-sided of above-mentioned cloth germule is coated with the anti-flaming dope, coating thickness 1-2mm, up to fire-retardant after drying
Cloth.
10. flame retardant fabric according to claim 9, it is characterised in that: in the step (1), dried at 80-95 DEG C
20-40min;In the step (2), prior to 100 DEG C at dry 1-3min, then be warming up at 180-195 DEG C and dry 3-5min.
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