CN108560149A - A kind of processing technology of high-performance antibiosis polypropylene spunbond non-woven fabrics - Google Patents
A kind of processing technology of high-performance antibiosis polypropylene spunbond non-woven fabrics Download PDFInfo
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- CN108560149A CN108560149A CN201810258619.0A CN201810258619A CN108560149A CN 108560149 A CN108560149 A CN 108560149A CN 201810258619 A CN201810258619 A CN 201810258619A CN 108560149 A CN108560149 A CN 108560149A
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H3/00—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length
- D04H3/005—Synthetic yarns or filaments
- D04H3/007—Addition polymers
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
- D01F1/103—Agents inhibiting growth of microorganisms
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H3/00—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length
- D04H3/08—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating
- D04H3/14—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating with bonds between thermoplastic yarns or filaments produced by welding
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H3/00—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length
- D04H3/08—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating
- D04H3/16—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating with bonds between thermoplastic filaments produced in association with filament formation, e.g. immediately following extrusion
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/44—Oxides or hydroxides of elements of Groups 2 or 12 of the Periodic System; Zincates; Cadmates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/18—Synthetic fibres consisting of macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/20—Polyalkenes, polymers or copolymers of compounds with alkenyl groups bonded to aromatic groups
Abstract
The invention discloses a kind of processing technologys of high-performance antibiosis polypropylene spunbond non-woven fabrics, are related to non-woven fabrics processing technique field, including following operating procedure:(1) preparation of carboxyted polypropylene, (2) are polyacrylic antibacterial modified, the processing of (3) web, (4) nonwoven molding with cloth.The made polypropylene spunbond non-woven fabrics of the present invention not only has significant anti-microbial property, while anti-microbial property is stablized, and antibacterial timeliness is long;And the mechanical strength of made polypropylene spunbond non-woven fabrics is high, and good permeability is non-toxic to humans, suitable for being processed into operation clothing, sheet, diaper, isolation clothes, visiting the medical and hygiene articles such as clothes.
Description
Technical field:
The present invention relates to non-woven fabrics processing technique fields, and in particular to a kind of high-performance antibiosis polypropylene spunbond non-woven fabrics adds
Work technique.
Background technology:
Polypropylene spunbond non-woven fabrics is one kind of non-woven fabrics, be with polypropylene is raw material, polymerize networking by high temperature wire drawing,
Then reusable heat rolls the one kind of method bonding at cloth.It is wide at present since technological process is simple, yield is big, non-toxic to humans
The various fields such as general application hygienic material.
Since polypropylene spunbond non-woven fabrics is chiefly used in the processing of hygienic material, in order to improve the safety in utilization of hygienic material,
Need polypropylene spunbond non-woven fabrics that there is anti-microbial property.But rapidoprint polypropylene of polypropylene spunbond non-woven fabrics itself does not have anti-
Bacterium acts on, thus antibacterial polypropylene spunbond non-woven fabrics currently on the market largely using chemical mode, photocatalyst or nano silver from
Subprocessing technology carries out antibacterial processing, but deficiency is individually present:Though chemical mode can antibacterial, most of chemicals itself is easy
Human body is damaged;Though photocatalyst is safe and effective, cost is higher;Though nano silver has bacteriostasis, antibacterial ability weaker.
Invention content:
Technical problem to be solved by the present invention lies in provide one kind to be conducive to improve non-woven fabrics safety in utilization and antibacterial
The processing technology for the high-performance antibiosis polypropylene spunbond non-woven fabrics that significant effect, anti-microbial property are stablized.
The technical problems to be solved by the invention are realized using technical solution below:
A kind of processing technology of high-performance antibiosis polypropylene spunbond non-woven fabrics, including following operating procedure:
(1) preparation of carboxyted polypropylene:Polypropylene powder and nitric acid are sufficiently mixed, 130 DEG C of heat preservations is again heated to and stirs
Reaction is mixed, after reaction by gained mixture cooled to room temperature, and nitric acid is removed through washing, finally vacuum dried,
Powder is made to get carboxyted polypropylene in crushing;
(2) polyacrylic antibacterial modified:Chitosan hydrochloride is dissolved in water, made carboxyted polypropylene is added, fills
Divide stirring, and dilute sulfuric acid is added dropwise and adjusts pH value to 5, the reaction of reflux state insulated and stirred is again heated to, after reaction by gained
Then mixture cooled to room temperature is added dropwise inorganic alkali solution and adjusts pH value to 7, filtering, water-washing desalting is most done through vacuum afterwards
Particle is made to get chitin modified polypropylene in dry, crushing;
(3) processing of web:Made chitin modified PP GRANULES is added in screw extruder and is melted, then through spray
Silk networking is to get web;
(4) nonwoven molding with cloth:By made web it is hot rolled at cloth to get antibacterial polypropylene spunbond non-woven fabrics.
The mass fraction of nitric acid is 65-70% in the step (1), and the mass ratio of polypropylene powder and nitric acid is 15-30:
1-10。
Chitosan hydrochloride in the step (2), carboxyted polypropylene mass ratio be 5-10:35-50.
In the step (2) inorganic base in sodium hydroxide, potassium hydroxide, sodium carbonate, potassium carbonate, sodium bicarbonate one
Kind.
The made web of the step (3) has also carried out at secondary antibacterial before entering step (4) non-woven fabrics processing and forming
Reason.
The concrete operations of the secondary antimicrobial treatment are:Web is preheated to 125-130 DEG C, and uniformly on web
Secondary antimicrobial treatment solution is sprayed, the amount of spraying is 30-50g/m2, it is then transferred to standing 3-5h, 55- in 105-110 DEG C of environment successively
It is stood in 2-3h, 5-10 DEG C of environment in 60 DEG C of environment and stands 3-5h.
The secondary antimicrobial treatment solution is made of carrier nano magnesia and Chinese medicine antibacterial extracting solution, and preparation method is:
20g nano magnesias are added in 1kg Chinese medicine antibacterial extracting solutions, 15-30min is stood after being sufficiently stirred, recycle microwave reaction
Device microwave return stirring 5min continues microwave return stirring 5min after stopping 5min, stops microwave return stirring again after 5min
5min so repeats, so that microwave return stirring total time is reached 30min, cooled to room temperature is to get secondary antimicrobial treatment
Liquid.
The average grain diameter of the nano magnesia is 50nm.
The Chinese medicine antibacterial extracting solution is made of Chinese medicine composition through water extraction, and preparation method is:By 30g the bark of the root or stem of the tree of heaven,
20g Verbena officinalis, 15g Kadsura Root-barks, 15g Siberian elm brak, 10g gold boiling grass, 5g Mongollian Thyme Herbs, 5g berberis poiretiis, 5g Ranunculus sceleratus, 3g Blumea balsamiferas,
2g potentilla chinensis, 0.5g styraxes are added in the water of 5 times of Chinese medicine gross weights, and reflux state insulated and stirred 3h, mistake are heated to after impregnating 12h
Filtrate is collected in filter, filter residue is added in the water of 3 times of Chinese medicine gross weights, is again heated to reflux state insulated and stirred 2h, is filtered, and is closed
And filtrate is to get Chinese medicine antibacterial extracting solution.
The beneficial effects of the invention are as follows:
(1) present invention introduces carboxyl using nitric acid to polypropylene molecule structure end carboxylated, recycles chitosan
Institute's hydroxyl and amino are reacted with amide condensed to be introduced on polypropylene with carboxyl generation esterification respectively in molecular structure
Chitosan, to assign polypropylene antibacterial performance using the antibacterial characteristics of chitosan;
(2) present invention is born when prepared by secondary antimicrobial treatment solution using nano magnesia as carrier using its absorption property
Chinese medicine antibacterial ingredient is carried, to introduce natural antibacterial ingredient on made non-woven fabrics, to strengthen the anti-microbial property of made non-woven fabrics;
(3) formula of Chinese medicine antibacterial extracting solution preparation Chinese medicine composition used of the present invention follows strictly the compatibility of monarch
Relationship, using pathogenic bacteria as controlling object, antimicrobial component directly acts on pathogenic bacteria, to show good anti-microbial property;
And the formula of the Chinese medicine composition is obtained by experiment sieving many times, wherein the addition and its dosage per a herb are all
By verifying repeatedly, to be the identical or close similar Chinese medicine of pharmacological property can not replace easily;
(4) nano magnesia of the present invention itself has antibacterial action, and because free hydroxyl is contained on its surface after as carrier
Base thus can with esterification or amidated carboxyl reacts to Chinese medicine antibacterial ingredient is firmly attached to poly- completely on polypropylene
On tacryl, and then significantly improve the anti-microbial property of made non-woven fabrics;
(5) the made polypropylene spunbond non-woven fabrics of the present invention not only has significant anti-microbial property, while anti-microbial property is stablized, and resists
Bacterium timeliness is long;And the mechanical strength of made polypropylene spunbond non-woven fabrics is high, and good permeability is non-toxic to humans, is suitable for adding
Work is made operation clothing, sheet, diaper, isolation clothes, visits the medical and hygiene articles such as clothes.
Specific implementation mode:
In order to make the technical means, the creative features, the aims and the efficiencies achieved by the present invention be easy to understand, tie below
Specific embodiment is closed, the present invention is further explained.
Embodiment 1
(1) preparation of carboxyted polypropylene:The nitric acid of 15g polypropylene powders and 5g mass fractions 70% is sufficiently mixed,
130 DEG C of insulated and stirred reactions are again heated to, after reaction by gained mixture cooled to room temperature, and nitre are removed through washing
Powder is made to get carboxyted polypropylene in acid, last vacuum dried, crushing;
(2) polyacrylic antibacterial modified:5g chitosan hydrochlorides are dissolved in water, the made carboxylated of 35g poly- third is added
Alkene is sufficiently stirred, and dilute sulfuric acid is added dropwise and adjusts pH value to 5, is again heated to the reaction of reflux state insulated and stirred, after reaction will
Then gained mixture cooled to room temperature is added dropwise sodium carbonate liquor and adjusts pH value to 7, filtering, water-washing desalting most passes through true afterwards
Sky is dry, particle is made to get chitin modified polypropylene in crushing;
(3) processing of web:Made chitin modified PP GRANULES is added in screw extruder and is melted, then through spray
Silk networking is to get web;
(4) nonwoven molding with cloth:By made web it is hot rolled at cloth to get antibacterial polypropylene spunbond non-woven fabrics.
Embodiment 2
(1) preparation of carboxyted polypropylene:The nitric acid of 20g polypropylene powders and 5g mass fractions 70% is sufficiently mixed,
130 DEG C of insulated and stirred reactions are again heated to, after reaction by gained mixture cooled to room temperature, and nitre are removed through washing
Powder is made to get carboxyted polypropylene in acid, last vacuum dried, crushing;
(2) polyacrylic antibacterial modified:8g chitosan hydrochlorides are dissolved in water, the made carboxylated of 50g poly- third is added
Alkene is sufficiently stirred, and dilute sulfuric acid is added dropwise and adjusts pH value to 5, is again heated to the reaction of reflux state insulated and stirred, after reaction will
Then gained mixture cooled to room temperature is added dropwise sodium carbonate liquor and adjusts pH value to 7, filtering, water-washing desalting most passes through true afterwards
Sky is dry, particle is made to get chitin modified polypropylene in crushing;
(3) processing of web:Made chitin modified PP GRANULES is added in screw extruder and is melted, then through spray
Silk networking is to get web;
(4) nonwoven molding with cloth:By made web it is hot rolled at cloth to get antibacterial polypropylene spunbond non-woven fabrics.
Embodiment 3
(1) preparation of carboxyted polypropylene:The nitric acid of 20g polypropylene powders and 5g mass fractions 70% is sufficiently mixed,
130 DEG C of insulated and stirred reactions are again heated to, after reaction by gained mixture cooled to room temperature, and nitre are removed through washing
Powder is made to get carboxyted polypropylene in acid, last vacuum dried, crushing;
(2) polyacrylic antibacterial modified:8g chitosan hydrochlorides are dissolved in water, the made carboxylated of 50g poly- third is added
Alkene is sufficiently stirred, and dilute sulfuric acid is added dropwise and adjusts pH value to 5, is again heated to the reaction of reflux state insulated and stirred, after reaction will
Then gained mixture cooled to room temperature is added dropwise sodium carbonate liquor and adjusts pH value to 7, filtering, water-washing desalting most passes through true afterwards
Sky is dry, particle is made to get chitin modified polypropylene in crushing;
(3) processing of web:Made chitin modified PP GRANULES is added in screw extruder and is melted, then through spray
Silk networking is to get web;
(4) secondary antimicrobial treatment:Web is preheated to 125-130 DEG C, and uniformly sprays secondary antibacterial on web
Treatment fluid, the amount of spraying are 50g/m2, then it is transferred to successively in 105-110 DEG C of environment and stands 2- in 3-5h, 55-60 DEG C of environment of standing
3-5h is stood in 3h, 5-10 DEG C of environment;
(5) nonwoven molding with cloth:By the web after secondary antimicrobial treatment it is hot rolled at cloth to get antibacterial polypropylene spunbond nonwoven
Cloth.
The preparation of secondary antimicrobial treatment solution:The extraction of 1kg Chinese medicine antibacterials is added in the nano magnesia of 20g average grain diameters 50nm
In liquid, 30min is stood after being sufficiently stirred, recycles microwave reactor microwave return stirring 5min, continues microwave after stopping 5min
Microwave return stirring 5min, such repetition make microwave return stirring total time reach again after return stirring 5min, stopping 5min
30min, cooled to room temperature is to get secondary antimicrobial treatment solution.
The preparation of Chinese medicine antibacterial extracting solution:By 30g the bark of the root or stem of the tree of heaven, 20g Verbena officinalis, 15g Kadsura Root-barks, 15g Siberian elm brak, 10g gold
Boil grass, 5g Mongollian Thyme Herbs, 5g berberis poiretiis, 5g Ranunculus sceleratus, 3g Blumea balsamiferas, 2g potentilla chinensis, 0.5g styraxes 5 times of Chinese medicine gross weights of addition
In water, it is heated to reflux state insulated and stirred 3h after impregnating 12h, is filtered, filtrate is collected, by filter residue 3 times of Chinese medicine gross weights of addition
In water, it is again heated to reflux state insulated and stirred 2h, is filtered, merging filtrate is to get Chinese medicine antibacterial extracting solution.
Reference examples
With reference to patent CN201410077137.7 embodiments 1.
Embodiment 4
Be utilized respectively embodiment 1-3 processing and prepare antibacterial polypropylene spunbond non-woven fabrics, wherein screw extruder melting, spinneret at
Net, the process condition for being rolled into cloth are identical, and test the anti-microbial property (dialogue of made antibacterial polypropylene spunbond non-woven fabrics
The 1h sterilizing rates of color candida albicans, staphylococcus aureus, Escherichia coli), test result is as shown in table 1.
The anti-microbial property of the 1 made antibacterial polypropylene spunbond non-woven fabrics of the present invention of table
Strain name | Embodiment 1 | Embodiment 2 | Embodiment 3 | Reference examples |
Candida albicans | 95-98% | 95-98% | > 99.9% | < 90% |
Staphylococcus aureus | 95-98% | 95-98% | > 99.9% | < 90% |
Escherichia coli | 95-98% | 95-98% | > 99.9% | < 90% |
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (9)
1. a kind of processing technology of high-performance antibiosis polypropylene spunbond non-woven fabrics, which is characterized in that including following operating procedure:
(1) preparation of carboxyted polypropylene:Polypropylene powder and nitric acid are sufficiently mixed, it is anti-to be again heated to 130 DEG C of insulated and stirreds
It answers, after reaction by gained mixture cooled to room temperature, and nitric acid, last vacuum dried, crushing is removed through washing
Powder is made to get carboxyted polypropylene;
(2) polyacrylic antibacterial modified:Chitosan hydrochloride is dissolved in water, made carboxyted polypropylene is added, fully stirs
It mixes, and dilute sulfuric acid is added dropwise and adjusts pH value to 5, be again heated to the reaction of reflux state insulated and stirred, after reaction mix gained
Then object cooled to room temperature is added dropwise inorganic alkali solution and adjusts pH value to 7, filters, water-washing desalting, finally vacuum dried,
Particle is made to get chitin modified polypropylene in crushing;
(3) processing of web:Made chitin modified PP GRANULES is added in screw extruder and is melted, then through spinneret at
Net is to get web;
(4) nonwoven molding with cloth:By made web it is hot rolled at cloth to get antibacterial polypropylene spunbond non-woven fabrics.
2. the processing technology of high-performance antibiosis polypropylene spunbond non-woven fabrics according to claim 1, it is characterised in that:The step
Suddenly the mass fraction of nitric acid is 65-70% in (1), and the mass ratio of polypropylene powder and nitric acid is 15-30:1-10.
3. the processing technology of high-performance antibiosis polypropylene spunbond non-woven fabrics according to claim 1, it is characterised in that:The step
Suddenly chitosan hydrochloride in (2), carboxyted polypropylene mass ratio be 5-10:35-50.
4. the processing technology of high-performance antibiosis polypropylene spunbond non-woven fabrics according to claim 1, it is characterised in that:The step
Suddenly the one kind of inorganic base in sodium hydroxide, potassium hydroxide, sodium carbonate, potassium carbonate, sodium bicarbonate in (2).
5. the processing technology of high-performance antibiosis polypropylene spunbond non-woven fabrics according to claim 1, it is characterised in that:The step
Suddenly (3) made web has also carried out secondary antimicrobial treatment before entering step (4) non-woven fabrics processing and forming.
6. the processing technology of high-performance antibiosis polypropylene spunbond non-woven fabrics according to claim 5, which is characterized in that described two
The concrete operations of secondary antimicrobial treatment are:Web is preheated to 125-130 DEG C, and is uniformly sprayed at secondary antibacterial on web
Liquid is managed, the amount of spraying is 30-50g/m2, then it is transferred in 105-110 DEG C of environment and is stood in 3-5h, 55-60 DEG C of environment of standing successively
3-5h is stood in 2-3h, 5-10 DEG C of environment.
7. the processing technology of high-performance antibiosis polypropylene spunbond non-woven fabrics according to claim 6, it is characterised in that:Described two
Secondary antimicrobial treatment solution is made of carrier nano magnesia and Chinese medicine antibacterial extracting solution, and preparation method is:By 20g nano magnesias
It is added in 1kg Chinese medicine antibacterial extracting solutions, 15-30min is stood after being sufficiently stirred, recycle microwave reactor microwave return stirring
5min continues microwave return stirring 5min after stopping 5min, stops microwave return stirring 5min again after 5min, so repeats,
Microwave return stirring total time is set to reach 30min, cooled to room temperature is to get secondary antimicrobial treatment solution.
8. the processing technology of high-performance antibiosis polypropylene spunbond non-woven fabrics according to claim 7, it is characterised in that:It is described to receive
The average grain diameter of rice magnesia is 50nm.
9. the processing technology of high-performance antibiosis polypropylene spunbond non-woven fabrics according to claim 7, it is characterised in that:In described
Medicine antibacterial extracting solution is made of Chinese medicine composition through water extraction, and preparation method is:30g the bark of the root or stem of the tree of heaven, 20g Verbena officinalis, 15g is purple
Chaste tree skin, 15g Siberian elm brak, 10g gold boiling grass, 5g Mongollian Thyme Herbs, 5g berberis poiretiis, 5g Ranunculus sceleratus, 3g Blumea balsamiferas, 2g potentilla chinensis, 0.5g peaces
Breath is fragrant to be added in the water of 5 times of Chinese medicine gross weights, is heated to reflux state insulated and stirred 3h after impregnating 12h, is filtered, collects filtrate, will
Filter residue is added in the water of 3 times of Chinese medicine gross weights, is again heated to reflux state insulated and stirred 2h, filters, merging filtrate is to get Chinese medicine
Antibacterial extracting solution.
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CN110894642A (en) * | 2019-12-16 | 2020-03-20 | 中科纺织研究院(青岛)有限公司 | Chitin modified PP spunbonded non-woven fabric |
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EP3786329A1 (en) | 2019-09-02 | 2021-03-03 | Bestee Material (Tsingtao) Co., Ltd. | Plant-based functional polypropylene spunbond non-woven fabric and preparation method thereof |
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