CN108143674A - A kind of lotion containing peony seed oil and preparation method thereof - Google Patents
A kind of lotion containing peony seed oil and preparation method thereof Download PDFInfo
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- CN108143674A CN108143674A CN201810187629.XA CN201810187629A CN108143674A CN 108143674 A CN108143674 A CN 108143674A CN 201810187629 A CN201810187629 A CN 201810187629A CN 108143674 A CN108143674 A CN 108143674A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Abstract
The invention discloses a kind of lotions containing peony seed oil and preparation method thereof, and the raw material of the lotion containing peony seed oil includes：Glycerine, hyaluronic acid, peony seed oil, grape pip essential oil, vitamin E, aloe, ginseng pulverate, astragalus membranaceus powder, matrimony vine, water；Preparation method includes：Matrimony vine is immersed in 50 60 DEG C of water 45 hours, solution A is obtained by filtration；Aloe is removed the peel, and Aloe mesophyll with solution A is mixed, squeezes the juice, obtains solution B；Glycerine, hyaluronic acid, ginseng pulverate, astragalus membranaceus powder are added in solution B, are uniformly mixing to obtain water phase liquid；Peony seed oil, grape pip essential oil, vitamin E are mixed, are uniformly mixing to obtain oil phase liquid；Oil phase liquid is added in water phase liquid, homogeneous 15 20 minutes obtains the lotion containing peony seed oil.Lotion provided by the invention containing peony seed oil enough rapidly permeates into human skin, has the effects that tender white, crease-resistant, anti-aging, lighten the stain, enhance elasticity of skin.
Description
Technical field
The present invention relates to peony seeds manufacture field more particularly to a kind of preparation methods of the lotion containing peony seed oil.
Background technology
With the progress of society and economic development and the continuous improvement of living standards of the people, people are to beauty and skin care
The requirement of cosmetic is also higher and higher, increasingly develops to the direction of " naturalization, nutrient laden, curative effect ".But currently on the market
Various beauty and skin care cosmetics in it is most of all containing harmful chemical substance, such as leaded, mercury venomous injurant
Matter, these skin care item easily cause people's skin allergy, and human organ and function are caused to damage.It is opened from the last century 80's
Begin, skin expert finds that, various natural materials are added in skin care item, there is good nourishing effect, and nontoxic pair to skin
Effect, effective component extracting, which is added in skin care item, particularly from plant has more remarkable effect.
It but can be by extraction position, season, extraction and the guarantor of harvesting plus the effect of plant extract in skin care item
The factors such as method, the product content deposited influence, therefore the plant extract in actual product does not often play it really and should have
Effect.
Peony seed oil is the vegetable oil extracted by peony seeds, VA, VE, niacin, carrotene, unsaturation in peony seed oil
Content of fatty acid enriches, and has fabulous Nutritional Nursing Care effect to skin, can obviously improve skin epidermal cells circulatory function, promotees
Into the microcirculation of capillary of skin, the progress of anti-lipid peroxidation effect improves metabolism, delay skin aging
Process has crease-resistant, moisturizing whitening effect, light using rear skin smooth, hard to chloasma, skin aging wrinkle, skin keratin
Change decortication, wrinkled skin, dry skin have certain therapeutic effect.
Invention content
Technical problems based on background technology, the present invention propose a kind of containing the lotion of peony seed oil and its preparation side
Method, the lotion provided by the invention containing peony seed oil enough rapidly permeate into human skin, have tender white, crease-resistant, anti-aging, desalination color
The effects that spot, enhancing elasticity of skin, the peony seed oil quality contained is good, and unsaturated fatty acid content is high.
The present invention provides a kind of lotion containing peony seed oil, raw material includes by weight：It is 10-15 parts of glycerine, transparent
8-12 parts of matter acid, 5-8 parts of peony seed oil, 4-6 parts of grape pip essential oil, -2 parts of vitamin e1,6-9 parts of Aloe.arborescens, people
Join 2-3 parts of powder, 2-3 parts of astragalus membranaceus powder, 4-6 parts of matrimony vine, 20-25 parts of water.
Preferably, the granularity of ginseng pulverate is 200-300 mesh, and the granularity of astragalus membranaceus powder is 200-300 mesh.
Preferably, the preparation method of peony seed oil includes the following steps：
S1, the peony seeds after cleaning that will shell are immersed in 15-20 DEG C of water 8-10 hours, and taking-up drains away the water, Cord blood
After be crushed to 130-150 mesh, obtain peony seeds powder；
S2, the peony seeds powder obtained in S1 is subjected to low temperature drying, after water content reaches 8%-10%, is impregnated in absolute ethyl alcohol
4-5 hours, supercritical carbon dioxide extracting is carried out, obtains peony seeds crude oil；
S3, the peony seeds crude oil obtained in S2 is heated to 50-60 DEG C, it is molten adds in the sodium hydroxide that mass fraction is 9%-11%
Liquid after being stirred 15-20 minutes with the revolution of 60-70 r/min, is warming up to 70-80 DEG C, aluminium oxide is added in, with 18-25 r/min
Revolution stir 20-30 minute, keep the temperature 8-10 hours static, separate except water layer and precipitation, it is oily to obtain depickling；
The depickling oil obtained in S4, S3 obtains bleached oil by activated decoloration, and bleached oil is using vacuumizing deodorization
Obtain peony seed oil.
Preferably, the method for Cord blood is in subzero 40 DEG C-subzero 60 DEG C of environment in peony seed oil preparation method S1
It preserves 3-5 hours or is preserved 4-6 minutes in liquid nitrogen.
Preferably, the temperature of low temperature drying is 40-50 DEG C in peony seed oil preparation method S2.
Preferably, the usage amount of absolute ethyl alcohol is 0.8-1.2 times of peony seeds powder weight in peony seed oil preparation method S2.
Preferably, peony seed oil preparation method S2, which surpasses, closes in carbon dioxide abstraction, and the pressure of extraction is 23-35Mpa, is extracted
It is 35-45 DEG C to take temperature, and extraction time is 50-90 minutes, carbon dioxide flow 15-18L/h.
Preferably, peony seed oil preparation method S2, which surpasses, closes in carbon dioxide abstraction, the supercritical carbon dioxide extraction used
Taking instrument, there are two separating stills, and the pressure of the first separating still is 8-10Mpa, and temperature is 40-45 DEG C, and the pressure of the second separating still is 3-
5Mpa, temperature are 30-35 DEG C.
Preferably, surpass in peony seed oil preparation method S2 and close on carbon dioxide abstraction and use cyclohexane as entrainer.
Preferably, surpass in peony seed oil preparation method S2 and close on carbon dioxide abstraction, the flow of entrainer cyclohexane is two
Aoxidize the 6%-8% of carbon flow.
Preferably, 65- of the usage amount of sodium hydroxide solution for peony seeds crude oil weight in peony seed oil preparation method S3
68 times.
Preferably, the usage amount of aluminium oxide is 1-2 times of peony seeds crude oil weight in peony seed oil preparation method S3.
Preferably, the method for activated decoloration is in peony seed oil preparation method S4：In the depickling oil obtained in S3
Atlapulgite is added in, the addition of atlapulgite is the 4-5% of depickling weight of oil, is stirred with the revolution of 50-70 r/min, in 95-
It decolourizes 40-60 minutes at a temperature of 110 DEG C, is cooled to 40-50 DEG C, bleached oil is obtained by filtration.
Preferably, the method for deodorization being vacuumized in peony seed oil preparation method S4 is：It is 0.04- in vacuum degree
Under the conditions of 0.06MPa, bleached oil is heated to 150-170 DEG C, is kept for 4-5 hour, stop heating, treat oil temperature be cooled to 45 DEG C with
Vacuum will be removed when lower, obtains peony seed oil.
The present invention also provides the preparation methods of lotion of this kind containing peony seed oil, comprise the steps of：
Step 1：Matrimony vine is immersed in 50-60 DEG C of water 4-5 hours, solution A is obtained by filtration；
Step 2：Aloe.arborescens are removed the peel, Aloe.arborescens meat is mixed with the solution A obtained in step 1,
It squeezes the juice, obtains solution B；
Step 3：Glycerine, hyaluronic acid, ginseng pulverate, astragalus membranaceus powder are added in the solution B obtained in step 2, at 70-80 DEG C
It stirs evenly, obtains water phase liquid；
Step 4：Peony seed oil, grape pip essential oil, vitamin E are mixed, is stirred evenly at 70-80 DEG C, obtains oil phase liquid；
Step 5：The oil phase liquid obtained in step 4 is added in the water phase liquid obtained in step 3, homogeneous 15-20 minutes,
Obtain the lotion containing peony seed oil.
Preferably, the agitation revolution of homogeneous is 2800-3200rpm in step 5.
In lotion provided by the invention containing peony seed oil containing peony seed oil, ginseng pulverate, astragalus membranaceus powder, grape pip essential oil,
The natural components such as Aloe.arborescens, the lotion of the compositions such as cooperation glycerine, hyaluronic acid can rapidly permeate into human skin, have
The effects that having tender white, crease-resistant, anti-aging, lighten the stain, enhancing elasticity of skin.
The effects that peony seed oil has anti-oxidant, delay skin aging, inhibits color spot, prevents acne, bright and clean skin quality；Grape
There are two types of very important element, linolenic acid and proanthocyanidins for seed oil, and linolenic acid can resist free radical, anti-aging, side
It helps and absorbs vitamin C and E, strengthen the elasticity of the circulatory system, reduce the injury of ultraviolet light, protect the collagen in skin, change
Kind venous engorgement and oedema prevent melanin deposition, and proanthocyanidin has protection blood vessel elasticity, and protection skin is from the bitter edible plant of ultraviolet light
Poison prevents the destruction of collagenous fibres and elastomer, and skin is made to keep due elasticity and tension, avoids skin sagging and wrinkle
It generates；Aloe.arborescens aloe polysaccharide and vitamin have the skin of human body good nutrition, moisten, whitening effect, and
Blandness, it is comfortable after, there is certain curative effect to pachylosis, facial wrinkles, scar, freckle, acne etc.；The master of ginseng pulverate
Ingredient is wanted as ginseng soap, prostisol, a small amount of volatile oil, various amino acid and peptides, glucose, fructose, pectin and dimension life
Plain B1, B2, niacin, pantothenic acid etc., the nutritional ingredient of ginseng can not have skin any bad thorn by skin slow-absorbing
Swash, the capillary of skin can be expanded, promote skin blood cycle, enhance skin-nourishing, prevent skin dehydration, harden, corrugation,
So as to enhance the elasticity of skin, cell is made to obtain new life, it is bright and clean and moist to protection skin, presenility was prevented, plays U.S.
Appearance acts on；Radix Astragali is famous tonifying Qi good medicine, containing a kind of 20 amino acid and trace element, as beauty composition, has and promotes
Cell viability, delay skin aging enhance cutaneous immunisation power, the effect of anti-inflammation and sterilization.
The preparation method oil yield of peony seed oil provided by the invention is high, obtained peony seed oil remain natural activity into
Part, unsaturated fatty acid content is high, and anti-oxidant, delay skin aging inhibits color spot, prevents acne, bright and clean skin quality and other effects
It is good.
The methods of preparation method of peony seed oil provided by the invention is using water swelling, freezen protective, low-temperature grinding, solution
Peony seeds kind skin of having determined is hard, crushes the problem of difficulty is larger, and the granularity of peony seeds powder can reach 130-150 mesh, improve
Extraction efficiency.Low-temperature grinding reduce unrighted acid in crushing process because crush environment temperature rise due to caused by break
It is bad, reduce the loss of active constituent, and then improve the quality of peony seed oil.The present invention first impregnates peony seeds powder with ethyl alcohol,
Supercritical carbon dioxide extracting is carried out again, and cyclohexane is passed through in supercritical carbon dioxide extracting, and the use of entrainer makes male
The extraction efficiency of red seed oil is substantially improved, and the oil yield of peony seed oil improves more than 20-25%.
In peony seeds crude oil refines engineering, two steps of degumming and depickling are combined into one by the present invention, using excess
Sodium hydroxide solution and aluminium oxide match, and sodium hydroxide solution is added in peony seeds crude oil, can neutralize the trip in crude oil
From aliphatic acid, excessive sodium hydroxide makes solution alkaline, after adding in aluminium oxide, phosphatide, protein etc. is made to precipitate, and realizes
One step removal colloid and free fatty reduce technological process, and with certain decolorizing effect.Prepared by the method for the present invention
Peony seed oil reaches edible oil standard, for skin care item safe and non-toxic.
Specific embodiment
In the following, technical scheme of the present invention is described in detail by specific embodiment.
Embodiment 1
The present invention provides a kind of lotions containing peony seed oil, which is characterized in that its raw material includes by weight：12 parts of glycerine,
11 parts of hyaluronic acid, 6.7 parts of peony seed oil, 4.8 parts of grape pip essential oil, 1.4 parts of vitamin E, 7.8 parts of Aloe.arborescens,
200 2.6 parts of mesh ginseng pulverates, 2.4 parts of 300 mesh astragalus membranaceus powder, 5.2 parts of matrimony vine, 23 parts of water.
Embodiment 2
The present invention provides a kind of lotions containing peony seed oil, which is characterized in that its raw material includes by weight：13 parts of glycerine,
9 parts of hyaluronic acid, 7.8 parts of peony seed oil, 5.4 parts of grape pip essential oil, 1.2 parts of vitamin E, 8.6 parts of Aloe.arborescens,
300 2.2 parts of mesh ginseng pulverates, 2.7 parts of 250 mesh astragalus membranaceus powder, 4.3 parts of matrimony vine, 22 parts of water.
Embodiment 3
The present invention provides a kind of lotions containing peony seed oil, which is characterized in that its raw material includes by weight：14 parts of glycerine,
10 parts of hyaluronic acid, 5.3 parts of peony seed oil, 5.7 parts of grape pip essential oil, 1.6 parts of vitamin E, 6.4 parts of Aloe.arborescens,
250 2.4 parts of mesh ginseng pulverates, 2.9 parts of 200 mesh astragalus membranaceus powder, 4.8 parts of matrimony vine, 24 parts of water.
Embodiment 4
The present invention provides a kind of lotions containing peony seed oil, which is characterized in that its raw material includes by weight：11 parts of glycerine,
12 parts of hyaluronic acid, 6.1 parts of peony seed oil, 4.3 parts of grape pip essential oil, 1.8 parts of vitamin E, 7.2 parts of Aloe.arborescens,
260 2.8 parts of mesh ginseng pulverates, 2.2 parts of 240 mesh astragalus membranaceus powder, 5.7 parts of matrimony vine, 21 parts of water.
Wherein, peony seed oil is prepared using following methods：
S1, the peony seeds after cleaning that will shell are immersed in 16 DEG C of water 9 hours, and taking-up drains away the water, and is crushed after Cord blood
To 140 mesh, peony seeds powder is obtained, the method for Cord blood is preserves 4.8 hours in subzero 47 DEG C of environment；
S2, the peony seeds powder obtained in S1 is subjected to low temperature drying at 44 DEG C, after water content reaches 8.9%, in peony seeds powder weight
It is impregnated 4.6 hours in 1 times of absolute ethyl alcohol of amount, carries out supercritical carbon dioxide extracting, it is super to close in carbon dioxide abstraction, extract
The pressure taken is 27Mpa, and extraction temperature is 42 DEG C, and extraction time is 71 minutes, carbon dioxide flow 16.8L/h；It uses
There are two separating stills for supercritical carbon dioxide extracting instrument, and the pressure of the first separating still is 8.9Mpa, and temperature is 42 DEG C, the second separation
The pressure of kettle is 3.6Mpa, and temperature is 33 DEG C；It is super to close on carbon dioxide abstraction and use cyclohexane as entrainer, the flow of cyclohexane
For 1.13L/h, the extract of the first separating still and the second separating still is merged, obtains peony seeds crude oil；
S3, the peony seeds crude oil obtained in S2 is heated to 57 DEG C, 66 times of mass fraction for adding in peony seeds crude oil weight is
9.8% sodium hydroxide solution after being stirred 17 minutes with the revolution of 68 r/min, is warming up to 73 DEG C, adds in peony seeds crude oil weight
1.5 times of aluminium oxide, after being stirred 24 minutes with the revolution of 21 r/min, keep the temperature static 9.1 hours, separate except water layer and heavy
It forms sediment, obtains depickling oil；
Atlapulgite is added in S4, the depickling oil obtained in S3, the addition of atlapulgite is the 4.3% of depickling weight of oil, with
The revolution stirring of 57 r/min, after decolourizing 48 minutes at a temperature of 104 DEG C, is cooled to 46 DEG C, bleached oil is obtained by filtration；In vacuum
It spends under the conditions of 0.05MPa, bleached oil to be heated to 162 DEG C, is kept for 4.4 hours, stops heating, when oil temperature is cooled to 40 DEG C
Vacuum is removed, obtains peony seed oil.
Embodiment 5
The lotion containing peony seed oil in embodiment 4, the wherein preparation method of peony seed oil can also include the following steps：
S1, the peony seeds after cleaning that will shell are immersed in 18 DEG C of water 8.3 hours, and taking-up drains away the water, powder after Cord blood
135 mesh are broken to, obtain peony seeds powder, the method for Cord blood is preserves 4.2 hours in subzero 53 DEG C of environment；
S2, the peony seeds powder obtained in S1 is subjected to low temperature drying at 48 DEG C, after water content reaches 9.3%, in peony seeds powder weight
It is impregnated 4.2 hours in 0.9 times of absolute ethyl alcohol of amount, carries out supercritical carbon dioxide extracting, it is super to close in carbon dioxide abstraction,
The pressure of extraction is 33Mpa, and extraction temperature is 37 DEG C, and extraction time is 86 minutes, carbon dioxide flow 15.4L/h；It uses
Supercritical carbon dioxide extracting instrument there are two separating still, the pressure of the first separating still is 8.3Mpa, and temperature is 43 DEG C, second point
Pressure from kettle is 4.2Mpa, and temperature is 31 DEG C；It is super to close on carbon dioxide abstraction and use cyclohexane as entrainer, the stream of cyclohexane
It measures as 1.20 L/h.The extract of first separating still and the second separating still is merged, obtains peony seeds crude oil；
S3, the peony seeds crude oil obtained in S2 is heated to 52 DEG C, adds in 65.4 times of mass fraction of peony seeds crude oil weight
For 10.3% sodium hydroxide solution, after being stirred 18 minutes with the revolution of 64 r/min, 76 DEG C are warming up to, adds in peony seeds crude oil
1.7 times of aluminium oxide of weight after being stirred 28 minutes with the revolution of 19 r/min, is kept the temperature static 9.7 hours, separated except water layer
And precipitation, obtain depickling oil；
Atlapulgite is added in S4, the depickling oil obtained in S3, the addition of atlapulgite is the 4.8% of depickling weight of oil, with
The revolution stirring of 63 r/min, after decolourizing 52 minutes at a temperature of 97 DEG C, is cooled to 42 DEG C, bleached oil is obtained by filtration；In vacuum
It spends under the conditions of 0.044MPa, bleached oil to be heated to 158 DEG C, is kept for 4.6 hours, stops heating, treats that oil temperature is cooled to 43 DEG C
When remove vacuum, obtain peony seed oil.
Embodiment 6
The lotion containing peony seed oil in embodiment 4, the wherein preparation method of peony seed oil can also include the following steps：
S1, the peony seeds after cleaning that will shell are immersed in 19 DEG C of water 8.7 hours, and taking-up drains away the water, powder after Cord blood
150 mesh are broken to, obtain peony seeds powder, the method for Cord blood is preserves 3.3 hours in subzero 58 DEG C of environment；
S2, the peony seeds powder obtained in S1 is subjected to low temperature drying at 42 DEG C, after water content reaches 9.6%, in peony seeds powder weight
It is impregnated 4.8 hours in 1.1 times of absolute ethyl alcohols of amount, carries out supercritical carbon dioxide extracting, it is super to close in carbon dioxide abstraction, extract
The pressure taken is 24Mpa, and extraction temperature is 44 DEG C, and extraction time is 54 minutes, carbon dioxide flow 16.1L/h；It uses
There are two separating stills for supercritical carbon dioxide extracting instrument, and the pressure of the first separating still is 9.7Mpa, and temperature is 41 DEG C, the second separation
The pressure of kettle is 4.8Mpa, and temperature is 34 DEG C；It is super to close on carbon dioxide abstraction and use cyclohexane as entrainer, the flow of cyclohexane
For 1.01L/h.The extract of first separating still and the second separating still is merged, obtains peony seeds crude oil；
S3, the peony seeds crude oil obtained in S2 is heated to 59 DEG C, adds in 66.9 times of mass fraction of peony seeds crude oil weight
For 9.3% sodium hydroxide solution, after being stirred 19 minutes with the revolution of 62r/min, 72 DEG C are warming up to, adds in peony seeds crude oil weight
1.3 times of aluminium oxide of amount after being stirred 22 minutes with the revolution of 24 r/min, keeps the temperature static 8.3 hours, separate except water layer and
Precipitation obtains depickling oil；
Atlapulgite is added in S4, the depickling oil obtained in S3, the addition of atlapulgite is the 4.1% of depickling weight of oil, with
The revolution stirring of 68 r/min, after decolourizing 43 minutes at a temperature of 108 DEG C, is cooled to 48 DEG C, bleached oil is obtained by filtration；In vacuum
It spends under the conditions of 0.056MPa, bleached oil to be heated to 167 DEG C, is kept for 4.2 hours, stops heating, treats that oil temperature is cooled to 42 DEG C
When remove vacuum, obtain peony seed oil.
Embodiment 7
The lotion containing peony seed oil in embodiment 4, the wherein preparation method of peony seed oil can also include the following steps：
S1, the peony seeds after cleaning that will shell are immersed in 17 DEG C of water 9.6 hours, and taking-up drains away the water, powder after Cord blood
145 mesh are broken to, obtain peony seeds powder, the method for Cord blood is preserves 3.6 hours in subzero 42 DEG C of environment；
S2, the peony seeds powder obtained in S1 is subjected to low temperature drying at 46 DEG C, after water content reaches 8.4%, in peony seeds powder weight
It is impregnated 4.4 hours in 1.2 times of absolute ethyl alcohol of amount, carries out supercritical carbon dioxide extracting, it is super to close in carbon dioxide abstraction,
The pressure of extraction is 31Mpa, and extraction temperature is 39 DEG C, and extraction time is 62 minutes, carbon dioxide flow 17.7L/h；It uses
Supercritical carbon dioxide extracting instrument there are two separating still, the pressure of the first separating still is 9.4Mpa, and temperature is 44 DEG C, second point
Pressure from kettle is 3.2Mpa, and temperature is 32 DEG C, and the extract of the first separating still and the second separating still is merged, obtains peony seeds
Crude oil；
S3, the peony seeds crude oil obtained in S2 is heated to 54 DEG C, adds in 67.8 times of mass fraction of peony seeds crude oil weight
For 10.7% sodium hydroxide solution, after being stirred 16 minutes with the revolution of 66 r/min, 78 DEG C are warming up to, adds in peony seeds crude oil
1.9 times of aluminium oxide of weight after being stirred 26 minutes with the revolution of 22r/min, is kept the temperature static 8.6 hours, separated except water layer
And precipitation, obtain depickling oil；
Atlapulgite is added in S4, the depickling oil obtained in S3, the addition of atlapulgite is the 4.6% of depickling weight of oil, with
The revolution stirring of 52 r/min, after decolourizing 57 minutes at a temperature of 101 DEG C, is cooled to 44 DEG C, bleached oil is obtained by filtration；In vacuum
It spends under the conditions of 0.058MPa, bleached oil to be heated to 153 DEG C, is kept for 4.8 hours, stops heating, treats that oil temperature is cooled to 41 DEG C
When remove vacuum, obtain peony seed oil.
Embodiment 8
Peony seeds low temperature is protected after being impregnated in the preparation method S1 of the lotion containing peony seed oil in embodiment 4, wherein peony seed oil
The method deposited can also be to be preserved 4.6 minutes in liquid nitrogen.
Embodiment 9
Peony seeds low temperature is protected after being impregnated in the preparation method S1 of the lotion containing peony seed oil in embodiment 4, wherein peony seed oil
The method deposited can also be to be preserved 4.2 minutes in liquid nitrogen.
Embodiment 10
Peony seeds low temperature is protected after being impregnated in the preparation method S1 of the lotion containing peony seed oil in embodiment 4, wherein peony seed oil
The method deposited can also be to be preserved 5.3 minutes in liquid nitrogen.
Embodiment 11
Peony seeds low temperature is protected after being impregnated in the preparation method S1 of the lotion containing peony seed oil in embodiment 4, wherein peony seed oil
The method deposited can also be to be preserved 5.7 minutes in liquid nitrogen.
Embodiment 12
Surpass in the preparation method S2 of the lotion containing peony seed oil in embodiment 4, wherein peony seed oil and close on carbon dioxide abstraction
The flow of entrainer cyclohexane can also be 1.21L/h.
Embodiment 13
The present invention also provides the preparation methods of lotion of this kind containing peony seed oil, comprise the steps of：
Step 1：Matrimony vine is immersed in 54 DEG C of water 4.4 hours, solution A is obtained by filtration；
Step 2：Aloe.arborescens are removed the peel, Aloe.arborescens meat is mixed with the solution A obtained in step 1,
It squeezes the juice, obtains solution B；
Step 3：Glycerine, hyaluronic acid, ginseng pulverate, astragalus membranaceus powder are added in the solution B obtained in step 2, stirred at 77 DEG C
It mixes uniformly, obtains water phase liquid；
Step 4：Peony seed oil, grape pip essential oil, vitamin E are mixed, is stirred evenly at 73 DEG C, obtains oil phase liquid；
Step 5：The oil phase liquid obtained in step 4 is added in the water phase liquid obtained in step 3, is in agitation revolution
Homogeneous 18 minutes under 3000rpm, obtain the lotion containing peony seed oil.
Embodiment 14
The present invention also provides the preparation methods of lotion of this kind containing peony seed oil, comprise the steps of：
Step 1：Matrimony vine is immersed in 52 DEG C of water 4.8 hours, solution A is obtained by filtration；
Step 2：Aloe.arborescens are removed the peel, Aloe.arborescens meat is mixed with the solution A obtained in step 1,
It squeezes the juice, obtains solution B；
Step 3：Glycerine, hyaluronic acid, ginseng pulverate, astragalus membranaceus powder are added in the solution B obtained in step 2, stirred at 74 DEG C
It mixes uniformly, obtains water phase liquid；
Step 4：Peony seed oil, grape pip essential oil, vitamin E are mixed, is stirred evenly at 76 DEG C, obtains oil phase liquid；
Step 5：The oil phase liquid obtained in step 4 is added in the water phase liquid obtained in step 3, is in agitation revolution
Homogeneous 17 minutes under 2900rpm, obtain the lotion containing peony seed oil.
Embodiment 14
The present invention also provides the preparation methods of lotion of this kind containing peony seed oil, comprise the steps of：
Step 1：Matrimony vine is immersed in 58 DEG C of water 4.2 hours, solution A is obtained by filtration；
Step 2：Aloe.arborescens are removed the peel, Aloe.arborescens meat is mixed with the solution A obtained in step 1,
It squeezes the juice, obtains solution B；
Step 3：Glycerine, hyaluronic acid, ginseng pulverate, astragalus membranaceus powder are added in the solution B obtained in step 2, stirred at 72 DEG C
It mixes uniformly, obtains water phase liquid；
Step 4：Peony seed oil, grape pip essential oil, vitamin E are mixed, is stirred evenly at 79 DEG C, obtains oil phase liquid；
Step 5：The oil phase liquid obtained in step 4 is added in the water phase liquid obtained in step 3, is in agitation revolution
Homogeneous 16 minutes under 3100rpm, obtain the lotion containing peony seed oil.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto,
Any one skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (10)
1. a kind of lotion containing peony seed oil, which is characterized in that its raw material includes by weight：10-15 parts of glycerine, hyaluronic acid
8-12 parts, 5-8 parts of peony seed oil, 4-6 parts of grape pip essential oil, -2 parts of vitamin e1,6-9 parts of Aloe.arborescens, ginseng pulverate
2-3 parts, 2-3 parts of astragalus membranaceus powder, 4-6 parts of matrimony vine, 20-25 parts of water.
A kind of 2. lotion containing peony seed oil according to claim 1, which is characterized in that the preparation side of the peony seed oil
Method includes the following steps：
S1, the peony seeds after cleaning that will shell are immersed in 15-20 DEG C of water 8-10 hours, and taking-up drains away the water, Cord blood
After be crushed to 130-150 mesh, obtain peony seeds powder；
S2, the peony seeds powder obtained in S1 is subjected to low temperature drying, after water content reaches 8%-10%, is impregnated in absolute ethyl alcohol
4-5 hours, supercritical carbon dioxide extracting is carried out, obtains peony seeds crude oil；
S3, the peony seeds crude oil obtained in S2 is heated to 50-60 DEG C, it is molten adds in the sodium hydroxide that mass fraction is 9%-11%
Liquid after being stirred 15-20 minutes with the revolution of 60-70 r/min, is warming up to 70-80 DEG C, aluminium oxide is added in, with 18-25 r/min
Revolution stir 20-30 minute, keep the temperature 8-10 hours static, separate except water layer and precipitation, it is oily to obtain depickling；
The depickling oil obtained in S4, S3 obtains bleached oil by activated decoloration, and bleached oil is using vacuumizing deodorization
Obtain peony seed oil.
A kind of 3. lotion containing peony seed oil according to claim 2, which is characterized in that the peony seed oil preparation method
The method of Cord blood is is preserved 3-5 hour in subzero 40 DEG C-subzero 60 DEG C of environment or preservation 4-6 divides in liquid nitrogen in S1
Clock.
A kind of 4. lotion containing peony seed oil according to claim 2, which is characterized in that the peony seed oil preparation method
The temperature of low temperature drying is 40-50 DEG C in S2.
A kind of 5. lotion containing peony seed oil according to claim 2, which is characterized in that the peony seed oil preparation method
The usage amount of absolute ethyl alcohol is 0.8-1.2 times of peony seeds powder weight in S2.
A kind of 6. lotion containing peony seed oil according to claim 2, which is characterized in that the peony seed oil preparation method
S2, which surpasses, to be closed in carbon dioxide abstraction, and the pressure of extraction is 23-35Mpa, and extraction temperature is 35-45 DEG C, extraction time 50-90
Minute, carbon dioxide flow 15-18L/h.
A kind of 7. lotion containing peony seed oil according to claim 2, which is characterized in that the peony seed oil preparation method
Surpass in S2 and close on carbon dioxide abstraction and use cyclohexane as entrainer.
A kind of 8. lotion containing peony seed oil according to claim 7, which is characterized in that the peony seed oil preparation method
Surpass in S2 and close on carbon dioxide abstraction, the flow of entrainer cyclohexane is the 6%-8% of carbon dioxide flow.
A kind of 9. lotion containing peony seed oil according to claim 2, which is characterized in that the peony seed oil preparation method
The usage amount of sodium hydroxide solution is 65-68 times of peony seeds crude oil weight in S3, and the usage amount of aluminium oxide is peony seeds crude oil
1-2 times of weight.
10. a kind of preparation method of the lotion containing peony seed oil, which is characterized in that comprise the steps of：
Step 1：Matrimony vine is immersed in 50-60 DEG C of water 4-5 hours, solution A is obtained by filtration；
Step 2：Aloe.arborescens are removed the peel, Aloe.arborescens meat is mixed with the solution A obtained in step 1,
It squeezes the juice, obtains solution B；
Step 3：Glycerine, hyaluronic acid, ginseng pulverate, astragalus membranaceus powder are added in the solution B obtained in step 2, at 70-80 DEG C
It stirs evenly, obtains water phase liquid；
Step 4：Peony seed oil, grape pip essential oil, vitamin E are mixed, is stirred evenly at 70-80 DEG C, obtains oil phase liquid；
Step 5：The oil phase liquid obtained in step 4 is added in the water phase liquid obtained in step 3, homogeneous 15-20 minutes,
Obtain the lotion containing peony seed oil.
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Application publication date: 20180612 |