CN107364029A - A kind of rubber vulcanization process - Google Patents
A kind of rubber vulcanization process Download PDFInfo
- Publication number
- CN107364029A CN107364029A CN201710620897.1A CN201710620897A CN107364029A CN 107364029 A CN107364029 A CN 107364029A CN 201710620897 A CN201710620897 A CN 201710620897A CN 107364029 A CN107364029 A CN 107364029A
- Authority
- CN
- China
- Prior art keywords
- rubber
- vulcanization
- parts
- cut
- kneaded
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B7/00—Mixing; Kneading
- B29B7/002—Methods
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C35/00—Heating, cooling or curing, e.g. crosslinking or vulcanising; Apparatus therefor
- B29C35/02—Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C43/00—Compression moulding, i.e. applying external pressure to flow the moulding material; Apparatus therefor
- B29C43/02—Compression moulding, i.e. applying external pressure to flow the moulding material; Apparatus therefor of articles of definite length, i.e. discrete articles
Abstract
The invention discloses a kind of rubber vulcanization process, first, prepare raw material:Design parameter in technological requirement, calculate raw material proportioning;Second, material is kneaded:By be placed in after rubber cut-parts butadiene-styrene rubber, cis-butadiene cement, zinc oxide, stearic acid, age resistor, accelerator mixture in be kneaded, melting temperature be 50 ~ 100 DEG C, mixing time is 15 ~ 25min;3rd, the vulcanization of rubber:Temperature, time and the pressure of adjustment vulcanization are tentatively vulcanized;4th, detection check:The rubber cut-parts tentatively vulcanizated carry out numerical value detection, and data test is carried out to low temperature resistant, wear-resisting, the resistance to drawing ability of rubber cut-parts;5th, sulfidization molding:The rubber cut-parts for detecting qualified are placed in mould, ensure that clamping pressure makes formed product after mould matched moulds.
Description
Technical field
The present invention relates to rubber product preparation field, particularly a kind of rubber vulcanization process.
Background technology
Vulcanization is that rubber is built bridge the general designation of crosslinking, and rubber is nugatory before no vulcanization, when rubber and other
By crosslinking agent in certain temperature and forming under the pressure, rubber mix after the auxiliary materials such as auxiliary material, such as filler, auxiliary agent are well mixed
Material is allowed to that cross-linked network occurs by crosslinking agent, and the valuable of various performances can be provided after being be combined with each other between molecule
Material.Rubber made from existing sulfurization technology, its usual pulling force and hardness are poor, it is impossible to meet that the needs of using waves.
The content of the invention
The present invention solves the technical problem of provide a kind of rubber vulcanization process, it is possible to increase the vulcanization matter of rubber
Amount, improve rubber quality.
In order to solve the above technical problems, one aspect of the present invention is:A kind of rubber vulcanization process is provided, its
Including:
First, prepare raw material:Design parameter in technological requirement, calculate raw material proportioning;
Second, material is kneaded:Butadiene-styrene rubber, cis-butadiene cement, zinc oxide, stearic acid, age resistor, accelerator will be placed in after rubber cut-parts
It is kneaded in mixture, melting temperature is 50 ~ 100 DEG C, and mixing time is 15 ~ 25min;
3rd, the vulcanization of rubber:Temperature, time and the pressure of adjustment vulcanization are tentatively vulcanized;
4th, detection check:The rubber cut-parts tentatively vulcanizated carry out numerical value detection, to the low temperature resistant, wear-resisting, resistance to of rubber cut-parts
Drawing ability carries out data test;
5th, sulfidization molding:The rubber cut-parts for detecting qualified are placed in mould, clamping pressure is ensured after mould matched moulds
Make formed product.
Preferably, in the 3rd step, the temperature of vulcanization is 150 ~ 180 DEG C, and the time of vulcanization is 10 ~ 15min, vulcanization
Pressure be 30Mpa.
Preferably, in the 4th step, the scope of low temperature resistant test is -50 ~ -35 DEG C;The wear-resisting grade of wear-resisting test
For 350;Scope >=20Mpa of resistance to tensile test.
The beneficial effects of the invention are as follows:A kind of rubber vulcanization process, the smooth heating of the curing temperature control used in the past
Vulcanization process is compared, and advantage and difference are being controlled in whole sulfidation to pressure, make production process more
Add easy operation.
Embodiment
Presently preferred embodiments of the present invention is described in detail below so that advantages and features of the invention can be easier to by
It will be appreciated by those skilled in the art that apparent clearly defined so as to be made to protection scope of the present invention.
The embodiment of the present invention includes:A kind of rubber vulcanization process, its step include:
First, prepare raw material:Design parameter in technological requirement, calculate raw material proportioning;
Second, material is kneaded:Butadiene-styrene rubber, cis-butadiene cement, zinc oxide, stearic acid, age resistor, accelerator will be placed in after rubber cut-parts
It is kneaded in mixture, melting temperature is 50 ~ 100 DEG C, and mixing time is 15 ~ 25min;
3rd, the vulcanization of rubber:Temperature, time and the pressure of adjustment vulcanization are tentatively vulcanized;The temperature of vulcanization is 150 ~ 180
DEG C, the time of vulcanization is 10 ~ 15min, and the pressure of vulcanization is 30Mpa;
4th, detection check:The rubber cut-parts tentatively vulcanizated carry out numerical value detection, to the low temperature resistant, wear-resisting, resistance to of rubber cut-parts
Drawing ability carries out data test;The scope of low temperature resistant test is -50 ~ -35 DEG C;The wear-resisting grade of wear-resisting test is 350;Resistance to pulling force
Scope >=20Mpa of test;
5th, sulfidization molding:The rubber cut-parts for detecting qualified are placed in mould, clamping pressure is ensured after mould matched moulds
Make formed product.
According to above-mentioned processing step, the design parameter of its design of the other embodiment 1 ~ 6 of this programme use is as shown in the table:
This technique is heated up by graded, so as to control sulfidation.What is controlled with the curing temperature used in the past is flat
Sliding temperature vulcanization process is compared, and advantage and difference are being controlled in whole sulfidation to pressure, make production
Process is more prone to operate, and can reduce conversion error between temperature and pressure in process of production causes caused by insufficient pressure
Defect, it can more increase solubility of the sizing material to gas on microcosmic, in the generation for macroscopically showing as reducing bubble.By right
The tracking and testing repeatedly of sizing material, the physical and mechanical properties of sizing material have good guarantor after curing after this sulfur form vulcanization
Card.
The above embodiments merely illustrate the technical concept and features of the present invention, and its object is to allow person skilled in the art
Scholar can understand present disclosure and be carried out, and it is not intended to limit the scope of the present invention, all according to the present invention
The equivalent change or modification that Spirit Essence is made, it should all cover within the scope of the present invention.
Claims (3)
- A kind of 1. rubber vulcanization process, it is characterised in that:Its step includes:First, prepare raw material:Design parameter in technological requirement, calculate raw material proportioning;Second, material is kneaded:Butadiene-styrene rubber, cis-butadiene cement, zinc oxide, stearic acid, age resistor, accelerator will be placed in after rubber cut-parts It is kneaded in mixture, melting temperature is 50 ~ 100 DEG C, and mixing time is 15 ~ 25min;3rd, the vulcanization of rubber:Temperature, time and the pressure of adjustment vulcanization are tentatively vulcanized;4th, detection check:The rubber cut-parts tentatively vulcanizated carry out numerical value detection, to the low temperature resistant, wear-resisting, resistance to of rubber cut-parts Drawing ability carries out data test;5th, sulfidization molding:The rubber cut-parts for detecting qualified are placed in mould, clamping pressure is ensured after mould matched moulds Make formed product.
- A kind of 2. rubber vulcanization process according to claim 1, it is characterised in that:In 3rd step, the temperature of vulcanization For 150 ~ 180 DEG C, the time of vulcanization is 10 ~ 15min, and the pressure of vulcanization is 30Mpa.
- A kind of 3. rubber vulcanization process according to claim 1, it is characterised in that:In 4th step, low temperature resistant test Scope be -50 ~ -35 DEG C;The wear-resisting grade of wear-resisting test is 350;Scope >=20Mpa of resistance to tensile test.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201710620897.1A CN107364029A (en) | 2017-07-27 | 2017-07-27 | A kind of rubber vulcanization process |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201710620897.1A CN107364029A (en) | 2017-07-27 | 2017-07-27 | A kind of rubber vulcanization process |
Publications (1)
Publication Number | Publication Date |
---|---|
CN107364029A true CN107364029A (en) | 2017-11-21 |
Family
ID=60307216
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201710620897.1A Pending CN107364029A (en) | 2017-07-27 | 2017-07-27 | A kind of rubber vulcanization process |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN107364029A (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107877883A (en) * | 2017-10-30 | 2018-04-06 | 青岛三祥科技股份有限公司 | The forming method of special-shaped rubber tube |
CN116903941A (en) * | 2023-07-14 | 2023-10-20 | 宁国中奕橡塑有限公司 | One-time molding vulcanization process for rubber products |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104669483A (en) * | 2013-11-29 | 2015-06-03 | 招远市东晟橡胶制品有限公司 | Rubber vulcanizing technology |
CN105985543A (en) * | 2015-01-30 | 2016-10-05 | 中国石油天然气股份有限公司 | Rubber composition and preparation method thereof |
CN106378893A (en) * | 2016-08-31 | 2017-02-08 | 柳州元吉兴工业技术有限公司 | Rubber vulcanization process |
-
2017
- 2017-07-27 CN CN201710620897.1A patent/CN107364029A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104669483A (en) * | 2013-11-29 | 2015-06-03 | 招远市东晟橡胶制品有限公司 | Rubber vulcanizing technology |
CN105985543A (en) * | 2015-01-30 | 2016-10-05 | 中国石油天然气股份有限公司 | Rubber composition and preparation method thereof |
CN106378893A (en) * | 2016-08-31 | 2017-02-08 | 柳州元吉兴工业技术有限公司 | Rubber vulcanization process |
Non-Patent Citations (2)
Title |
---|
工艺手册编写组: "《工艺手册》", 31 December 1979, 国营长风机器厂 * |
王忠: "《高分子材料与工程》", 30 September 2007, 陕西人民出版社 * |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107877883A (en) * | 2017-10-30 | 2018-04-06 | 青岛三祥科技股份有限公司 | The forming method of special-shaped rubber tube |
CN116903941A (en) * | 2023-07-14 | 2023-10-20 | 宁国中奕橡塑有限公司 | One-time molding vulcanization process for rubber products |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN102975303B (en) | Preparation method of rubber material for preparing temperature-resistant and oil-resistant rubber products for vehicle pipelines | |
CN107189236A (en) | Sulfur cross-linking EPT rubber composition, preparation method, purposes and its application product that a kind of heat-proof aging, low pressure become | |
CN103160129B (en) | Mold rubber and preparation method thereof | |
CN105848923B (en) | Tire production Rubber compound | |
CN106633216B (en) | A kind of wide temperature zone high damping blending type rubber material and preparation method thereof | |
CN103435917B (en) | Colored terpolymer EP rubber of high rigidity adapting to microwave vulcanization and preparation method thereof | |
CN104292535A (en) | NBR/PVC elastomer by taking LNBR as plasticizer and preparation method of elastomer | |
CN103772885A (en) | Flat PC/ABS (polycarbonate/acrylonitrile butadiene styrene) automobile dashboard material and preparation method thereof | |
CN107364029A (en) | A kind of rubber vulcanization process | |
CN108084504A (en) | A kind of method for synthesizing ageing-resistant natural rubber | |
CN101134825A (en) | Color-change resistant latch-locked valve cock rubber formula and method for making same | |
CN103497518A (en) | Novel mold rubber and preparation method thereof | |
Ren et al. | Reinforced mechanical properties of functionalized silica and eggshell filled guayule natural rubber composites | |
CN105400209B (en) | A kind of preparation method for the high-temperature silicon disulfide rubber that extrusion molding is enhanced with precipitated silica | |
CN107880560A (en) | Wear-resisting type transmission belt rubber cover and its preparation technology | |
CN102942716A (en) | Composite type heat conducting rubber and method for preparing same | |
CN103289411A (en) | Silicone rubber/ethylene-propylene-diene rubber binary blend closed-cell foamed material and preparation method thereof | |
CN111117050A (en) | PE blown film and preparation method thereof | |
CN108299708B (en) | Ultra-light and ultra-wear-resistant rubber and preparation method thereof | |
CN103275363A (en) | Anti-static flavorless disulfide sponge sizing material, and preparation method and application thereof | |
CN103254476A (en) | Rubber master batch and preparation method thereof | |
CN107266756A (en) | A kind of compounding rubber sulfuration process | |
CN107141532A (en) | Without asbestos seal gasket and preparation method thereof | |
CN105175903A (en) | Rubber modified addition auxiliary agent and preparation method therefor | |
CN114672172A (en) | Silicone rubber capable of being stored for long time by adding platinum vulcanizing agent and preparation method thereof |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
RJ01 | Rejection of invention patent application after publication |
Application publication date: 20171121 |
|
RJ01 | Rejection of invention patent application after publication |