CN106190565A - Add the liquid detergent essence of left-handed 3,7-Dimethyl-6-octenenitrile - Google Patents

Add the liquid detergent essence of left-handed 3,7-Dimethyl-6-octenenitrile Download PDF

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Publication number
CN106190565A
CN106190565A CN201610730664.2A CN201610730664A CN106190565A CN 106190565 A CN106190565 A CN 106190565A CN 201610730664 A CN201610730664 A CN 201610730664A CN 106190565 A CN106190565 A CN 106190565A
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CN
China
Prior art keywords
octenenitrile
handed
dimethyl
acetate
liquid detergent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610730664.2A
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Chinese (zh)
Inventor
梁超
冯志洁
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Tianjin Double Horse Flavor & Fragrance New Technology Co Ltd
Original Assignee
Tianjin Double Horse Flavor & Fragrance New Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tianjin Double Horse Flavor & Fragrance New Technology Co Ltd filed Critical Tianjin Double Horse Flavor & Fragrance New Technology Co Ltd
Priority to CN201610730664.2A priority Critical patent/CN106190565A/en
Publication of CN106190565A publication Critical patent/CN106190565A/en
Pending legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/0007—Aliphatic compounds
    • C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/0007—Aliphatic compounds
    • C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
    • C11B9/0019—Aliphatic compounds containing oxygen as the only heteroatom carbocylic acids; Salts or esters thereof
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/50—Perfumes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Detergent Compositions (AREA)
  • Fats And Perfumes (AREA)

Abstract

The invention discloses a kind of liquid detergent essence adding left-handed 3,7-Dimethyl-6-octenenitrile.The present invention is made up of by described mass percent following components: ten aldehyde 0.1%, methyl nonyl acetaldehyde 0.15%, allyl hexanoate 0.05%, allyl cyclohexyl propionate 0.5%, jasminal 1%, mugwort oil 0.5%, benzyl acetate 1.5%, salicylic acid benzyl ester 8%, citronellol 4%, galaxolid 4%, geraniol 2%, geranyl acetate 0.5%, MDJ 11.2%, first position hexyl cinnamic aldehyde 8%, compounding acetic isoborneol ester 1.5%, lilestralis 2.5%, linalool 8%, linalyl acetate 8%, methyl ionone 1%, oleum Citri sinensis 7%, phenethanol 3%, left-handed 3,7-Dimethyl-6-octenenitrile 1%, dipropylene glycol 23.75% etc..Adding the liquid detergent essence of left-handed 3,7-Dimethyl-6-octenenitrile, general layout is stable, fragrance answers rhythm, put perfume (or spice) layer by layer, fragrance is novel, lasting is lasting.

Description

Add the liquid detergent essence of left-handed 3,7-Dimethyl-6-octenenitrile
Technical field
The present invention relates to liquid detergent composition field, more specifically, relate to a kind of add washing of left-handed 3,7-Dimethyl-6-octenenitrile Clothing liquid essence.
Background technology
Due to era development, social progress.People are more and more higher to the requirement of fragrance, and the liquid detergent of a collection of fragrant atmosphere concept is fast Speed is fashionable.The most also have influence on daily use chemicals industry, daily use chemicals industry occurs much liquid detergent essence now, but all feels excessively to people Low grade, lacks the front perfumery rhythm of the outburst of high-grade fragrant atmosphere concept.Some front tune fragrance road of my company existing liquid detergent essence Single, new citrus raw material need to be introduced, left-handed 3,7-Dimethyl-6-octenenitrile can provide lifts one's head fragrant outburst and Citrus fragrance, soft aroma and, natural.
Summary of the invention
The technical problem to be solved is, overcomes the deficiencies in the prior art, it is provided that a kind of interpolation is left-handed The liquid detergent essence of 3,7-Dimethyl-6-octenenitrile.
The present invention adds the liquid detergent essence of left-handed 3,7-Dimethyl-6-octenenitrile, is made up of by described mass percent following components:
Ten aldehyde 0.1%
Methyl nonyl acetaldehyde 0.15%
Allyl hexanoate 0.05%
Allyl cyclohexyl propionate 0.5%
Jasminal 1%
Mugwort oil 0.5%
Benzyl acetate 1.5%
Salicylic acid benzyl ester 8%
Citronellol 4%
Flos Caryophylli oil 0.05%
P-cresyl phenylacetate 0.05%
Ethyl 2-methylbutyrate 0.3%
Galaxolid 4%
Geraniol 2%
Geranyl acetate 0.5%
MDJ 11.2%
Folic acetate 0.1%
First position hexyl cinnamic aldehyde 8%
B position violet ketone 0.1%
Compounding acetic isoborneol ester 1.5%
Lilestralis 2.5%
Linalool 8%
Linalyl acetate 8%
Menthone 0.1%
Methyl ionone 1%
Oleum Citri sinensis 7%
Phenethanol 3%
Rose oxide 10%(dipropylene glycol solvent) 0.05%
Terpineol 1%
Tonalid 0.5%
Ligustral 0.5%
Left-handed 3,7-Dimethyl-6-octenenitrile 1%
Dipropylene glycol 23.75%.
Compared with prior art, the invention has the beneficial effects as follows: adding the liquid detergent essence of left-handed 3,7-Dimethyl-6-octenenitrile, general layout is steady Determine, fragrance answers rhythm, put perfume (or spice) layer by layer, fragrance is novel, lasting is lasting.This essence design is front tune: have the lemon of tension force Road and rural scenery.Middle tune: unique Bulgarian Fructus Pruni salicinae style, is full of the sense of nature, allows people be in a cheerful frame of mind.Keynote: light The gracefulness of lavandula angustifolia, betray light taste.Left-handed 3,7-Dimethyl-6-octenenitrile serves in this formula to be formed a connecting link, and merges overall work With, both improve Citrus fragrant, and made again draft intensity increase, promote the stereovision of overall essence.
Detailed description of the invention
Below in conjunction with experimental example, the present invention is described in further detail.
The present invention adds the liquid detergent essence of left-handed 3,7-Dimethyl-6-octenenitrile, composed of the following components:
Ten aldehyde 0.1g
Methyl nonyl acetaldehyde 0.15g
Allyl hexanoate 0.05g
Allyl cyclohexyl propionate 0.5g
Jasminal 1g
Mugwort oil 0.5g
Benzyl acetate 1.5g
Salicylic acid benzyl ester 8g
Citronellol 4g
Flos Caryophylli oil 0.05g
P-cresyl phenylacetate 0.05g
Ethyl 2-methylbutyrate 0.3g
Galaxolid 4g
Geraniol 2g
Geranyl acetate 0.5g
MDJ 11.2g
Folic acetate 0.1g
First position hexyl cinnamic aldehyde 8g
B position violet ketone 0.1g
Compounding acetic isoborneol ester 1.5g
Lilestralis 2.5g
Linalool 8g
Linalyl acetate 8g
Menthone 0.1g
Methyl ionone 1g
Oleum Citri sinensis 7g
Phenethanol 3g
Rose oxide 10%(dipropylene glycol solvent) 0.05g
Terpineol 1g
Tonalid 0.5g
Ligustral 0.5g
Left-handed 3,7-Dimethyl-6-octenenitrile 1g
Dipropylene glycol 23.75g
Above component being put in reactor, stirring is until raw material is the most fused.
Left-handed 3,7-Dimethyl-6-octenenitrile molecular formula: C10H17N, fragrance Citrus perfume, QINGXIANG, fruital, the fragrance of a flower, fragrance remaining time reach 48h with On, can be widely used in daily chemical essence formula.This spice is used in liquid detergent composition, can strengthen the Citrus of essence itself Breath, improves hay-scented intensity, and slightly fruit is sweet, makes overall liquid detergent essence class have a certain upgrade.
Experimental verification: with liquid detergent essence for experiment, aromatic style change and effect before and after left-handed 3,7-Dimethyl-6-octenenitrile is added in contrast.
In table one, A sample is the liquid detergent essence adding left-handed 3,7-Dimethyl-6-octenenitrile；B sample is liquid detergent essence.
Experiment: carry out crowd's sampling, organize 10 Ren Pingxiang groups, contrasts before and after experiment liquid detergent essence is added new raw material The results are shown in Table one.
Adding the essence of the left-handed 3,7-Dimethyl-6-octenenitrile of new raw material as can be seen here, general layout is stable, the multiple rhythm of fragrance, to put perfume (or spice), fragrance layer by layer new Grain husk, lasting are lasting.
Table one
A sample B sample
No. 1 √
No. 2 √
No. 3 √
No. 4 √
No. 5 √
No. 6 √
No. 7 √
No. 8 √
No. 9 √
No. 10 √
Note: A sample is the sample adding the left-handed 3,7-Dimethyl-6-octenenitrile of new raw material,
Beat " √ " for thinking that essence fragrance is good, perfume breath is strong.
The above is only the preferred embodiment of the present invention, it is noted that for the common skill of the art For art personnel, under the premise without departing from the principles of the invention, it is also possible to make some improvements and modifications, these improvements and modifications Also should be regarded as protection scope of the present invention.

Claims (1)

1. add a liquid detergent essence for left-handed 3,7-Dimethyl-6-octenenitrile, it is characterized in that, by following components by described mass percent group Become:
Ten aldehyde 0.1%
Methyl nonyl acetaldehyde 0.15%
Allyl hexanoate 0.05%
Allyl cyclohexyl propionate 0.5%
Jasminal 1%
Mugwort oil 0.5%
Benzyl acetate 1.5%
Salicylic acid benzyl ester 8%
Citronellol 4%
Flos Caryophylli oil 0.05%
P-cresyl phenylacetate 0.05%
Ethyl 2-methylbutyrate 0.3%
Galaxolid 4%
Geraniol 2%
Geranyl acetate 0.5%
MDJ 11.2%
Folic acetate 0.1%
First position hexyl cinnamic aldehyde 8%
B position violet ketone 0.1%
Compounding acetic isoborneol ester 1.5%
Lilestralis 2.5%
Linalool 8%
Linalyl acetate 8%
Menthone 0.1%
Methyl ionone 1%
Oleum Citri sinensis 7%
Phenethanol 3%
Rose oxide 10%(dipropylene glycol solvent) 0.05%
Terpineol 1%
Tonalid 0.5%
Ligustral 0.5%
Left-handed 3,7-Dimethyl-6-octenenitrile 1%
Dipropylene glycol 23.75%.
CN201610730664.2A 2016-08-26 2016-08-26 Add the liquid detergent essence of left-handed 3,7-Dimethyl-6-octenenitrile Pending CN106190565A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610730664.2A CN106190565A (en) 2016-08-26 2016-08-26 Add the liquid detergent essence of left-handed 3,7-Dimethyl-6-octenenitrile

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610730664.2A CN106190565A (en) 2016-08-26 2016-08-26 Add the liquid detergent essence of left-handed 3,7-Dimethyl-6-octenenitrile

Publications (1)

Publication Number Publication Date
CN106190565A true CN106190565A (en) 2016-12-07

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107937132A (en) * 2017-11-17 2018-04-20 恩格乐香精香料（上海）有限公司 A kind of daily use chemicals lemon extract and preparation method
CN112266821A (en) * 2020-09-11 2021-01-26 厦门馨米兰香精香料有限公司 Essence for grain germ laundry detergent
CN112569393A (en) * 2019-09-27 2021-03-30 广州汽车集团股份有限公司 Vehicle fragrance and preparation method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103037907A (en) * 2010-03-31 2013-04-10 境味股份有限公司 Methods, compositions and articles for olfactory-active substances
CN103113990A (en) * 2013-03-14 2013-05-22 天津市双马香精香料新技术有限公司 Preparation method and application of citrus essential oil fumet
CN105132170A (en) * 2015-08-28 2015-12-09 上海应用技术学院 Lemon essence for water-based ink and preparation method of lemon essence
CN105255589A (en) * 2014-06-12 2016-01-20 天津市双马香精香料新技术有限公司 Detergent essence added with peonile
CN105316108A (en) * 2014-06-12 2016-02-10 天津市双马香精香料新技术有限公司 Laundry detergent essence added with tricyclodecenyl n-butyrate

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103037907A (en) * 2010-03-31 2013-04-10 境味股份有限公司 Methods, compositions and articles for olfactory-active substances
CN103113990A (en) * 2013-03-14 2013-05-22 天津市双马香精香料新技术有限公司 Preparation method and application of citrus essential oil fumet
CN105255589A (en) * 2014-06-12 2016-01-20 天津市双马香精香料新技术有限公司 Detergent essence added with peonile
CN105316108A (en) * 2014-06-12 2016-02-10 天津市双马香精香料新技术有限公司 Laundry detergent essence added with tricyclodecenyl n-butyrate
CN105132170A (en) * 2015-08-28 2015-12-09 上海应用技术学院 Lemon essence for water-based ink and preparation method of lemon essence

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
何洛强: ""日化香精调配技巧"", 《香料香精化妆品》 *
唐健: ""香茅腈的合成及其应用"", 《辽宁化工》 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107937132A (en) * 2017-11-17 2018-04-20 恩格乐香精香料（上海）有限公司 A kind of daily use chemicals lemon extract and preparation method
CN112569393A (en) * 2019-09-27 2021-03-30 广州汽车集团股份有限公司 Vehicle fragrance and preparation method thereof
CN112266821A (en) * 2020-09-11 2021-01-26 厦门馨米兰香精香料有限公司 Essence for grain germ laundry detergent

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Application publication date: 20161207