CN106063583A - The preparation method of ree-oil additive and ree-oil - Google Patents
The preparation method of ree-oil additive and ree-oil Download PDFInfo
- Publication number
- CN106063583A CN106063583A CN201610556802.XA CN201610556802A CN106063583A CN 106063583 A CN106063583 A CN 106063583A CN 201610556802 A CN201610556802 A CN 201610556802A CN 106063583 A CN106063583 A CN 106063583A
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- Prior art keywords
- ree
- oil
- oil additive
- nicotine
- propylene glycol
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
-
- A24F47/008—
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The present invention discloses preparation method and the ree-oil of a kind of ree-oil additive, and wherein, the preparation method of described ree-oil additive comprises the following steps: is diluted by benzoic acid ethanol, obtains alcohol benzoate solution；Nicotine propylene glycol is diluted, obtains nicotine propylene glycol solution；Alcohol benzoate solution is mixed with nicotine propylene glycol solution, obtains ree-oil additive.Technical solution of the present invention can reduce the stimulation when being sucked to each sense organ of consumer of the ree-oil containing nicotine, improves ree-oil and sucks mouthfeel, increases and suck submissive sophistication.
Description
Technical field
The present invention relates to electronic cigarette oil tech field, particularly to preparation method and the ree-oil of a kind of ree-oil additive.
Background technology
It is known that traditional cigarette can produce the multiple harmful substances such as carbon monoxide and tar when burning, these are harmful to
Material major part all in the course of time, can be produced grievous injury to the health of consumer by consumer's suction body.In recent years, electricity
The appearance of sub-medicated cigarette alleviates this problem the most effectively with development.At present, the ree-oil of electronic cigarette all can mostly on the market
Adding liquid nicotine, to reduce the impression of sucking of traditional cigarette, but, the most directly it is added with the ree-oil meeting of liquid nicotine
When being sucked, each sense organ of consumer is produced and strongly stimulates, thus have a strong impact on consumer suck mouthfeel.
Summary of the invention
The main object of the present invention is to provide the preparation method of a kind of ree-oil additive, it is intended to reduce the cigarette containing nicotine
Oily stimulation when being sucked to each sense organ of consumer, improves ree-oil and sucks mouthfeel, increase and suck submissive sophistication.
For achieving the above object, the preparation method of the ree-oil additive that the present invention proposes comprises the following steps:
Benzoic acid ethanol is diluted, obtains alcohol benzoate solution；
Nicotine propylene glycol is diluted, obtains nicotine propylene glycol solution；
Alcohol benzoate solution is mixed with nicotine propylene glycol solution, obtains ree-oil additive.
Alternatively, in described alcohol benzoate solution, benzoic mass concentration scope is 10%～25%.
Alternatively, in described nicotine propylene glycol solution, the mass concentration scope of nicotine is 50%～70%.
Alternatively, described, alcohol benzoate solution is carried out in the step mixed with nicotine propylene glycol solution, benzene first
Acid ethanol solution is 1～6:1.3 with the mass ratio range of nicotine propylene glycol solution.
Alternatively, described alcohol benzoate solution is carried out, with nicotine propylene glycol solution, the step mixed after also wrap
Include:
Ree-oil additive is carried out water bath processing.
Alternatively, the temperature range of described water bath processing is 40 DEG C～60 DEG C, the time of described water bath processing be 0.5h～
2h。
Alternatively, described alcohol benzoate solution is carried out, with nicotine propylene glycol solution, the step mixed after also wrap
Include:
Ree-oil additive is carried out freezing processing.
Alternatively, the temperature range of described freezing processing is-3 DEG C～0 DEG C, the time of described freezing processing be 12h～
24h。
The present invention also proposes a kind of ree-oil, and described ree-oil includes basis ree-oil and ree-oil additive, described ree-oil additive
It it is the ree-oil additive prepared by the preparation method of above-mentioned ree-oil additive.
Alternatively, described ree-oil additive mass concentration in described ree-oil is less than 27%.
Technical scheme, benzoic acid dissolves in ethanol, nicotine dissolves in propylene glycol, then, by benzoic acid second
When alcoholic solution mixes with nicotine propylene glycol solution, the free group of partial nicotine and the benzoic free group of part
Between chemical combination can occur, generate corresponding crystallization mono-salt and/or the double salt of crystallization, thus strong at the physiology not affecting nicotine
Effectively reducing the nicotine zest to each sense organ of consumer in the case of degree, improve ree-oil and suck mouthfeel, increase is sucked soft
Along sophistication.
Detailed description of the invention
Technical scheme in the embodiment of the present invention will be clearly and completely described below, it is clear that described enforcement
Example is only a part of embodiment of the present invention rather than whole embodiments.Based on the embodiment in the present invention, this area
The every other embodiment that those of ordinary skill is obtained under not making creative work premise, broadly falls into present invention protection
Scope.
It addition, the technical scheme between each embodiment can be combined with each other, but must be with ordinary skill
Based on personnel are capable of, when technical scheme combination occur conflicting maybe cannot realize time will be understood that this technical side
The combination of case does not exists, the most not within the protection domain of application claims.
The present invention proposes the preparation method of a kind of ree-oil additive, is used for acquiring a kind of ree-oil additive, to reduce
It is added with the stimulation when being sucked to each sense organ of consumer of the ree-oil of this ree-oil additive, improves ree-oil and suck mouthfeel, increase
Add and suck submissive sophistication.
The preparation method of this ree-oil additive comprises the following steps:
Benzoic acid ethanol is diluted, obtains alcohol benzoate solution；Wherein, benzoic acid in alcohol benzoate solution
Preferred mass concentration range be 10%～25%.
Nicotine propylene glycol is diluted, obtains nicotine propylene glycol solution；Wherein, described nicotine propylene glycol is molten
In liquid, the preferred mass concentration range of nicotine is 50%～70%.
Alcohol benzoate solution is mixed with nicotine propylene glycol solution, and mixed solution is stirred until homogeneous surely
Fixed, obtain ree-oil additive；Wherein the preferred mass proportion of alcohol benzoate solution and nicotine propylene glycol solution be 1～
6:1.3。
Ree-oil additive is carried out water bath processing；Wherein, the preferred range of water bath processing is 40 DEG C～60 DEG C, water-bath
The preferred time processed is 0.5h～2h.
Ree-oil additive is carried out freezing processing；Wherein, the preferred range of freezing processing is-3 DEG C～0 DEG C, freezing
The preferred time processed is 12h～24h.
Technical scheme, benzoic acid dissolves in ethanol, nicotine dissolves in propylene glycol, then, by benzoic acid second
When alcoholic solution mixes with nicotine propylene glycol solution, chemical combination can occur between partial nicotine and part benzoic acid,
Generate corresponding crystallization mono-salt and/or the double salt of crystallization, thus effectively reduce in the case of the physiological strength not affecting nicotine
The nicotine zest to each sense organ of consumer, improves ree-oil and sucks mouthfeel, increase and suck submissive sophistication.
Additionally, ree-oil additive of the present invention, nicotine in ree-oil also can be made more preferable with the compatibility of flavor matter, make ree-oil
Suck there is more graceful, more comfortable note, thus improve the reduction of fragrance impression during traditional flammable cigarette smoking
Degree, brings the suction closer to traditional flammable Medicated cigarette to experience for consumer, and then meets consumer to traditional cigarette taste
Demand.
In addition, it is necessary to explanation, the water bath processing that ree-oil additive is carried out and/or freezing processing, all can promote
The stability of ree-oil additive, sucks mouthfeel improving ree-oil further, increases and suck submissive sophistication.
Below in conjunction with specific embodiment, the preparation method of ree-oil additive of the present invention is illustrated.
Embodiment 1:
Benzoic acid ethanol is diluted, it is thus achieved that benzoic acid Mass concentration is the alcohol benzoate solution of 10%, and fills
It is loaded in Brown Glass Brown glass bottles and jars only sealing to preserve, with standby.
Nicotine propylene glycol is diluted, it is thus achieved that nicotine mass concentration is the nicotine propylene glycol solution of 60%,
And fill seals preservation, with standby in Brown Glass Brown glass bottles and jars only.
Above-mentioned alcohol benzoate solution and above-mentioned nicotine propylene glycol solution are mixed according to mass ratio 1:1.3, stirs
I.e. obtain ree-oil additive after mixing uniformly, and fill seals preservation, with standby in Brown Glass Brown glass bottles and jars only.
Above-mentioned ree-oil additive carries out water bath processing, and wherein, the temperature of water bath processing is 40 DEG C, the time of water bath processing
For 0.5h, naturally cool to room temperature afterwards.
The above-mentioned ree-oil having cooled to room temperature interpolates row freezing processing, and wherein, the temperature of freezing processing is 0 DEG C, freezing
The time processed is 24h, and clear-cutting forestland is to room temperature afterwards.
Embodiment 2:
Benzoic acid ethanol is diluted, it is thus achieved that benzoic acid Mass concentration is the alcohol benzoate solution of 14%, and fills
It is loaded in Brown Glass Brown glass bottles and jars only sealing to preserve, with standby.
Nicotine propylene glycol is diluted, it is thus achieved that nicotine mass concentration is the nicotine propylene glycol solution of 50%,
And fill seals preservation, with standby in Brown Glass Brown glass bottles and jars only.
Above-mentioned alcohol benzoate solution and above-mentioned nicotine propylene glycol solution are mixed according to mass ratio 2:1, stirring
I.e. obtain ree-oil additive after Jun Yun, and fill seals preservation, with standby in Brown Glass Brown glass bottles and jars only.
Above-mentioned ree-oil additive carries out water bath processing, and wherein, the temperature of water bath processing is 60 DEG C, the time of water bath processing
For 1h, naturally cool to room temperature afterwards.
The above-mentioned ree-oil having cooled to room temperature interpolates row freezing processing, and wherein, the temperature of freezing processing is 0 DEG C, freezing
The time processed is 12h, and clear-cutting forestland is to room temperature afterwards.
Embodiment 3:
Benzoic acid ethanol is diluted, it is thus achieved that benzoic acid Mass concentration is the alcohol benzoate solution of 18%, and fills
It is loaded in Brown Glass Brown glass bottles and jars only sealing to preserve, with standby.
Nicotine propylene glycol is diluted, it is thus achieved that nicotine mass concentration is the nicotine propylene glycol solution of 70%,
And fill seals preservation, with standby in Brown Glass Brown glass bottles and jars only.
Above-mentioned alcohol benzoate solution and above-mentioned nicotine propylene glycol solution are mixed according to mass ratio 3:1, stirring
I.e. obtain ree-oil additive after Jun Yun, and fill seals preservation, with standby in Brown Glass Brown glass bottles and jars only.
Above-mentioned ree-oil additive carries out water bath processing, and wherein, the temperature of water bath processing is 45 DEG C, the time of water bath processing
For 1.5h, naturally cool to room temperature afterwards.
The above-mentioned ree-oil having cooled to room temperature interpolates row freezing processing, and wherein, the temperature of freezing processing is-1 DEG C, freezing
The time processed is 18h, and clear-cutting forestland is to room temperature afterwards.
Embodiment 4:
Benzoic acid ethanol is diluted, it is thus achieved that benzoic acid Mass concentration is the alcohol benzoate solution of 21%, and fills
It is loaded in Brown Glass Brown glass bottles and jars only sealing to preserve, with standby.
Nicotine propylene glycol is diluted, it is thus achieved that nicotine mass concentration is the nicotine propylene glycol solution of 55%,
And fill seals preservation, with standby in Brown Glass Brown glass bottles and jars only.
Above-mentioned alcohol benzoate solution and above-mentioned nicotine propylene glycol solution are mixed according to mass ratio 4:1, stirring
I.e. obtain ree-oil additive after Jun Yun, and fill seals preservation, with standby in Brown Glass Brown glass bottles and jars only.
Above-mentioned ree-oil additive carries out water bath processing, and wherein, the temperature of water bath processing is 55 DEG C, the time of water bath processing
For 2h, naturally cool to room temperature afterwards.
The above-mentioned ree-oil having cooled to room temperature interpolates row freezing processing, and wherein, the temperature of freezing processing is-2 DEG C, freezing
The time processed is 20h, and clear-cutting forestland is to room temperature afterwards.
Embodiment 5:
Benzoic acid ethanol is diluted, it is thus achieved that benzoic acid Mass concentration is the alcohol benzoate solution of 25%, and fills
It is loaded in Brown Glass Brown glass bottles and jars only sealing to preserve, with standby.
Nicotine propylene glycol is diluted, it is thus achieved that nicotine mass concentration is the nicotine propylene glycol solution of 65%,
And fill seals preservation, with standby in Brown Glass Brown glass bottles and jars only.
Above-mentioned alcohol benzoate solution and above-mentioned nicotine propylene glycol solution are mixed according to mass ratio 6:1.3, stirs
I.e. obtain ree-oil additive after mixing uniformly, and fill seals preservation, with standby in Brown Glass Brown glass bottles and jars only.
Above-mentioned ree-oil additive carries out water bath processing, and wherein, the temperature of water bath processing is 50 DEG C, the time of water bath processing
For 2h, naturally cool to room temperature afterwards.
The above-mentioned ree-oil having cooled to room temperature interpolates row freezing processing, and wherein, the temperature of freezing processing is-3 DEG C, freezing
The time processed is 16h, and clear-cutting forestland is to room temperature afterwards.
It should be noted that in other embodiments, in alcohol benzoate solution, benzoic mass concentration may select
Any value between 10%～25%, such as: 10%, 10.5%, 11%, 12%, 13%, 14%, 15%, 20%, 25%.
In nicotine propylene glycol solution, the mass concentration of nicotine may select any value between 50%～70%, such as:
50%, 50.5%, 51%, 52%, 53%, 54%, 55%, 60%, 70%.
Mass ratio when alcohol benzoate solution mixes with nicotine propylene glycol solution may select appointing between 1～6:1.3
One value, such as: 1:1.3,1:1,1.5:1,2:1,3:1,4:1,6:1.3.
The temperature of water bath processing may select any value between 40 DEG C～60 DEG C, such as: 40 DEG C, 40.5 DEG C, 41 DEG C, 42
℃、43℃、44℃、45℃、50℃、55℃、60℃。
The time of water bath processing may select any value between 0.5h～2h, such as: 0.5h, 0.6h, 0.7h, 0.8h,
0.9h、1h、1.5h、2h。
Any value between optional-3 DEG C～0 DEG C of the temperature of freezing processing, such as :-3 DEG C ,-2.5 DEG C ,-2 DEG C ,-1.5
℃、-1℃、-0.5℃、0℃。
The time of freezing processing may select any value between 12h～24h, such as: 12h, 12.5h, 13h, 14h, 15h,
17h、19h、22h、24h。
The present invention also proposes a kind of ree-oil, and this ree-oil includes basis ree-oil and ree-oil additive, and described ree-oil additive is
The ree-oil additive prepared by the preparation method of aforesaid ree-oil additive, described basis ree-oil includes propylene glycol, vegetable
Glycerol, flavoring agent and essence.
It should be understood that ree-oil additive is added to the ree-oil of basis according to nicotine equivalent, can configure and obtain difference
The ree-oil of nicotine content.It should be noted that the unit of nicotine content is mg/g in ree-oil.
Such as, if ree-oil additive is dense by the alcohol benzoate solution that benzoic acid Mass concentration is 25% and nicotine quality
Degree is the nicotine propylene glycol solution of 50%, prepares according to mass ratio 2:1, then:
As configured the ree-oil that nicotine content is 6mg/g, in this ree-oil, the mass concentration of above-mentioned ree-oil additive should configure
It is 3.6%.
As configured the ree-oil that nicotine content is 12mg/g, in this ree-oil, the mass concentration of above-mentioned ree-oil additive should configure
It is 7.2%.
As configured the ree-oil that nicotine content is 18mg/g, in this ree-oil, the mass concentration of above-mentioned ree-oil additive should configure
It is 10.8%.
As configured the ree-oil that nicotine content is 24mg/g, in this ree-oil, the mass concentration of above-mentioned ree-oil additive should configure
It is 14.4%.
The ree-oil of above-mentioned different nicotine contents is aspirated with traditional ree-oil with identical nicotine content respectively
Contrast, can obtain through great many of experiments: for being added with the more traditional ree-oil of ree-oil of ree-oil additive of the present invention, to consumer when sucking
The zest of each sense organ the most effectively reduces, and sucks mouthfeel and is all improved, and sucks submissive sophistication and is all increased.
Therefore, ree-oil Additive Properties of the present invention is excellent, and can be accustomed to being added ratio according to the suction of consumer
Reasonable adjustment, the use demand of most consumer can be met.
Preferably, described ree-oil additive mass concentration in described ree-oil is less than 27%, with beneficially consumer
Healthy.
The foregoing is only the preferred embodiments of the present invention, not thereby limit the scope of the claims of the present invention, every at this
Under the inventive concept of invention, utilize the equivalent structure transformation that description of the invention content is made, or directly/indirectly it is used in other
Relevant technical field is included in the scope of patent protection of the present invention.
Claims (10)
1. the preparation method of a ree-oil additive, it is characterised in that comprise the following steps:
Benzoic acid ethanol is diluted, obtains alcohol benzoate solution；
Nicotine propylene glycol is diluted, obtains nicotine propylene glycol solution；
Alcohol benzoate solution is mixed with nicotine propylene glycol solution, obtains ree-oil additive.
2. the preparation method of ree-oil additive as claimed in claim 1, it is characterised in that benzene in described alcohol benzoate solution
The mass concentration scope of formic acid is 10%～25%.
3. the preparation method of ree-oil additive as claimed in claim 1, it is characterised in that in described nicotine propylene glycol solution
The mass concentration scope of nicotine is 50%～70%.
4. the preparation method of ree-oil additive as claimed in claim 1, it is characterised in that described by alcohol benzoate solution
Carry out with nicotine propylene glycol solution in the step mixed, alcohol benzoate solution and the mass ratio of nicotine propylene glycol solution
Scope is 1～6:1.3.
5. the preparation method of ree-oil additive as claimed in claim 1, it is characterised in that described by alcohol benzoate solution
Also include after carrying out, with nicotine propylene glycol solution, the step mixed:
Ree-oil additive is carried out water bath processing.
6. the preparation method of ree-oil additive as claimed in claim 5, it is characterised in that the temperature range of described water bath processing
Being 40 DEG C～60 DEG C, the time of described water bath processing is 0.5h～2h.
7. the preparation method of ree-oil additive as claimed in claim 1, it is characterised in that described by alcohol benzoate solution
Also include after carrying out, with nicotine propylene glycol solution, the step mixed:
Ree-oil additive is carried out freezing processing.
8. the preparation method of ree-oil additive as claimed in claim 7, it is characterised in that the temperature range of described freezing processing
Being-3 DEG C～0 DEG C, the time of described freezing processing is 12h～24h.
9. a ree-oil, it is characterised in that including basis ree-oil and ree-oil additive, described ree-oil additive is by claim
The ree-oil additive that the preparation method of the ree-oil additive described in any one of 1-8 prepares.
10. ree-oil as claimed in claim 9, it is characterised in that described ree-oil additive mass concentration in described ree-oil
Less than 27%.
Priority Applications (1)
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| CN201610556802.XA CN106063583A (en) | 2016-07-14 | 2016-07-14 | The preparation method of ree-oil additive and ree-oil |
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| CN201610556802.XA CN106063583A (en) | 2016-07-14 | 2016-07-14 | The preparation method of ree-oil additive and ree-oil |
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Family
ID=57206974
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108208915A (en) * | 2017-12-29 | 2018-06-29 | 深圳睿思奇科技开发有限公司 | A kind of preparation method of tobacco tar drop thorn softener and the tobacco tar drop thorn softener prepared with this method |
| CN109363255A (en) * | 2018-12-19 | 2019-02-22 | 深圳昱朋科技有限公司 | Method, electronic cigarette oil additive and the electronics tobacco tar of electronic cigarette oil additive are prepared using waste tobacco leaf |
| CN111296900A (en) * | 2020-01-21 | 2020-06-19 | 云南云烁科技有限公司 | Electronic cigarette smoking amount detection method and system, mobile terminal and cloud server |
| CN111938197A (en) * | 2020-07-16 | 2020-11-17 | 深圳雪雾科技有限公司 | Electronic cigarette tobacco tar |
| CN113880802A (en) * | 2021-11-09 | 2022-01-04 | 深圳萨特瓦生物科技有限公司 | Tartaric acid-nicotine salt, preparation method and application thereof, and preparation method of anhydrous tartaric acid crystal |
| CN113912585A (en) * | 2021-11-09 | 2022-01-11 | 深圳萨特瓦生物科技有限公司 | Composite nicotine salt, preparation method and application thereof, electronic cigarette oil and electronic cigarette |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108208915A (en) * | 2017-12-29 | 2018-06-29 | 深圳睿思奇科技开发有限公司 | A kind of preparation method of tobacco tar drop thorn softener and the tobacco tar drop thorn softener prepared with this method |
| CN108208915B (en) * | 2017-12-29 | 2021-06-08 | 深圳睿思奇科技开发有限公司 | Preparation method of tobacco tar thorn-reducing softener and tobacco tar thorn-reducing softener prepared by same |
| CN109363255A (en) * | 2018-12-19 | 2019-02-22 | 深圳昱朋科技有限公司 | Method, electronic cigarette oil additive and the electronics tobacco tar of electronic cigarette oil additive are prepared using waste tobacco leaf |
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| CN113880802A (en) * | 2021-11-09 | 2022-01-04 | 深圳萨特瓦生物科技有限公司 | Tartaric acid-nicotine salt, preparation method and application thereof, and preparation method of anhydrous tartaric acid crystal |
| CN113912585A (en) * | 2021-11-09 | 2022-01-11 | 深圳萨特瓦生物科技有限公司 | Composite nicotine salt, preparation method and application thereof, electronic cigarette oil and electronic cigarette |
| CN113912585B (en) * | 2021-11-09 | 2023-02-24 | 深圳萨特瓦生物科技有限公司 | Composite nicotine salt, preparation method and application thereof, electronic cigarette oil and electronic cigarette |
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Application publication date: 20161102 |