CN105815571A - Feeding composition and application thereof to animal feed additive preparation - Google Patents
Feeding composition and application thereof to animal feed additive preparation Download PDFInfo
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- CN105815571A CN105815571A CN201610178864.1A CN201610178864A CN105815571A CN 105815571 A CN105815571 A CN 105815571A CN 201610178864 A CN201610178864 A CN 201610178864A CN 105815571 A CN105815571 A CN 105815571A
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Abstract
The invention provides a feeding composition and application thereof to animal feed additive preparation. The feeding composition contains a benzoic acid derivative and a myristic acid derivative. The benzoic acid derivative is selected from benzoate or benzoate ester, the myristic acid derivative is selected from myristate or myristate ester, and the optimal mass ratio of the benzoic acid derivative to the myristic acid derivative in the feeding composition is 6:1-1:1. The feeding composition can serve as an animal growth promoter, and particularly substitute feeding antibiotics or high-dosage zinc preparations or copper preparations and other traditional animal growth promoters for the animal breeding industry. The feeding composition is a novel and safe animal feed additive and suitable for animals including livestock, poultry and aquaculture animals and has wide market prospects.
Description
Technical field:
The invention belongs to animal feed additive field, relate to a kind of containing benzoic acid derivative and the feeding compositions of myristic acid derivant and the application in preparing animal feed additive.
Background technology:
The animal basal diet traditional original agricultural product of replacement that animal feed is the most required are applied in animal cultivation.People are often desirable to the animal growth at the minimum feedstuff efficient and healthful of the shortest time loss.In order to reach this purpose, the feed additive of various functions adds preparation in feedstuff in feed manufacturing process and becomes functional feed.Wherein, feeding antibiotic, zinc oxide or copper sulfate etc. are that the most conventional feed additive is for improving the production performance of animal and preventing and treating Animal diseases.But the life-time service of high dose inorganic zinc or Inorganic Copper class feed additive has metal toxicity to animal；And the abuse of feeding antibiotic also causes the generation of microorganism drug resistance, drug residue and drug resistance transmission to threaten human health.The appearance of these problems causes conventional feed additive to use in animal cultivation being restricted or disable.Therefore, animal farming industry is had great importance by the efficient feed additive developing novel safety.
Summary of the invention:
It is an object of the invention to provide a kind of containing benzoic acid derivative and the feeding compositions of myristic acid derivant and the application in the efficient animal feed additive preparing novel safety, for animal cultivation to maintain animal health and to improve the production performance of animal.
The benzoic acid derivative that the present invention relates to is that as shown in formula I or its structure is as shown in formula II for benzoate, its structure:
Wherein, M is selected from H, alkali metal；
Wherein, M is selected from alkaline-earth metal, Zn, Fe, Mn, Cu；
Its structure of described benzoate is as shown in formula III or formula IV:
Described R1Selected from C1-4Straight or branched alkyl；
Wherein, R2、R3And R4Selected from H andAnd R2、R3And R4The most all H；
Described alkali metal includes Na, K, Li etc..
Described alkaline-earth metal includes Ca, Mg, Be etc..
Monovalent metallic ion benzoate in above-mentioned benzoate can occur conventional acid-base neutralization to be dried preparation after reacting by benzoic acid with corresponding alkali.Bivalent metal ion benzoate in above-mentioned benzoate first passes through benzoic acid and sodium hydroxide generation routine neutralizes after reacting generation sodium benzoate, and further the chloride with bivalent metal ion is prepared through post processings such as precipitate and separate are dried after carrying out metathesis reaction.
Above-mentioned benzoate can be through benzylhydroperoxide and corresponding C1-4After straight or branched alkanol, glycerol become ester under enzymatic synthesis condition prepared by rectification.
The myristic acid derivant that the present invention relates to is that as shown in formula (V) or its structure is as shown in formula VI for myristinate or its structure:
Wherein, M is selected from H, alkali metal；
Wherein, M is selected from alkaline-earth metal, Zn, Fe, Mn, Cu；
Shown in its structure of described myristinate such as formula (VII) or formula (VIII):
Described R5Selected from C1-4Straight or branched alkyl；
Wherein, R6、R7And R8Selected from H and straight chain C13C (=O), and R6、R7And R8The most all H.
Described alkali metal includes Na, K, Li etc..
Described alkaline-earth metal includes Ca, Mg, Be etc..
Monovalent metallic ion myristate in above-mentioned myristate can occur conventional acid-base neutralization to be dried preparation after reacting by myristic acid with corresponding alkali.Bivalent metal ion myristate in above-mentioned myristate first passes through myristic acid and sodium hydroxide generation routine neutralizes after reacting generation Sodium myristate, and the chloride with bivalent metal ion is dried preparation through precipitate and separate after carrying out metathesis reaction further.
Above-mentioned myristinate can be through myristic acid and corresponding C1-4After straight or branched alkanol, glycerol become ester under enzymatic synthesis condition prepared by rectification.Gained myristinate can be rendered as solid-liquid different conditions at different temperatures.
Chain saturated fatty acids salt or chain saturated fatty acids ester are only used as energy extender application using the addition higher than 2% as feed additive always, especially apply in ruminant is such as the daily ration of milch cow and goat etc., feed intake, the milk yield of animal is not affected and but can change the component content in milk and composition.Having document to report, fatty acid ester such as myristic acid triglyceride can cause the Hyperlipidemia of animal as energy matter, and some animal occurs that poor growth is the most dead.
By experimentation, the present invention proves that myristinate or myristate are applied to the cultivation of animal and can improve the production performance of animal, be mainly reflected in weightening finish and feed conversion rate aspect.
The present invention finds first also by experiment, myristinate or myristate are united and applied in the cultivation of animal with benzoate or benzoate according to the proper ratio feeding compositions of composition and occur the collaborative effect improving breeding performonce fo animals compared with the effect that benzoic acid derivative or myristic acid derivant are used alone, and show in poultry or the weightening finish of aquatic animal and price of deed rate.It addition, there is control action in terms of having the diarrhoea to animal during use in conjunction concurrently the most simultaneously, reach the level of the feed additive common dose of conventional feeding antibiotic.
The feeding compositions that the present invention relates to comprises benzoic acid derivative and myristic acid derivant, and both form according to any proportion.Described benzoic acid derivative and myristic acid derivant content in the composition are according to mass fraction meter, and benzoic acid derivative is 1-20 part, and myristic acid derivant is 1 part.
Described feeding compositions in addition to benzoic acid derivative and myristic acid derivant possibly together with acceptable carrier, excipient, adjuvant, solvent or combinations thereof on feed processing industry.
In some technical schemes, the benzoic acid derivative in feeding compositions is benzoate.
In other technical schemes, the benzoic acid derivative in feeding compositions is preferably calcium benzoate.
In other technical schemes, the benzoic acid derivative in feeding compositions is preferably sodium benzoate.
In other technical schemes, the myristic acid derivant in feeding compositions is preferably calcium myristate.
In other technical schemes, the myristic acid derivant in feeding compositions is preferably myristic acid triglyceride.
In a technical scheme, by myristic acid derivant and benzoic acid derivative, with mass ratio as 1:1～1:6 uses to the healthy small weaning pig spice with different tests group, with not give any feed additive test control group compared with, the diarrhea rate incidence rate of piglets substantially reduce while average daily gain be greatly improved and feedstuff conversion ratio tool be significantly improved effect.
In other technical schemes, myristic acid derivant and benzoic acid derivative are united and applied in the healthy domestic animal such as cattle in other cultivation stage, horse, sheep, donkey, Canis familiaris L., mink, Nyctereutes procyonoides, in the cultivation of rabbit etc., in compositions, the mass ratio of myristic acid derivant and benzoic acid derivative is 1:1～1:20, make an addition in the basal diet of cultivated animals in the way of companion's material, during testing, animal is free choice feeding drinking-water, result according to statistics shows, it is that feedstuff sample feces or situation about having loose bowels the most does not occurs in gastrointestinal function in process of the test that the animal of cultivation the most significantly shows, feces molding is good；It addition, the average daily gain of cultivated animals increases significantly, the rate of returns of feedstuff significantly improves 0.5-10%.
In other technical schemes, myristic acid derivant and benzoic acid derivative are united and applied in poultry such as chicken, duck, goose, Columba livia, guinea fowl, the cultivation of Carnis Coturnicis japonicae etc., in compositions, the mass ratio of myristic acid derivant and benzoic acid derivative is 1:1～1:20, inventor by the way of gavaging and feedstuff companion clothes mode give and cultivated animals, during testing, survival rate and performance index to animal are added up, the result of experiment shows, feeding compositions is given with test group compared with the blank assay group not giving any feed additive, the survival rate of animal has promoted and the average daily gain of animal is also rising, the conversion ratio of feedstuff obtains the improvement effect of highly significant.
In another technical scheme, myristic acid derivant and benzoic acid derivative are combined in the culture experiment being applied to the aquatic animals such as shrimp, fish, Eriocheir sinensis or Chinese yellow eel in the way of spice, test the rate of body weight gain of aquatic animal, survival rate lifting it is obvious that the conversion ratio of feedstuff is also significantly improved.
Further, present invention also offers described in comprise benzoic acid derivative and myristic acid derivant the application in preparing additive for animal feed of the feeding compositions.
Described additive for animal feed is except described feeding compositions is possibly together with pharmaceutically acceptable excipient, carrier, antioxidant, diluent, anti-caking agent, solvent or combinations thereof.
Described feed additive can add in feed processing industry in feedstuff according to formula forage demand and is prepared as functional feed applications in the raising of cultivated animals.
On the one hand described functional feed can maintain the healthy production performance on the other hand improving animal of animal.
It addition, the invention still further relates to the described feeding compositions containing benzoic acid derivative and myristic acid derivant to prepare the purposes of animal growth promoting agent.
Animal growth promoting agent prepared by the described feeding compositions containing benzoic acid derivative and myristic acid derivant is applied to animal cultivation and has significant effect in terms of improving efficiency of feed utilization, improving the production performance of animal, stimulating animal growth.
Animal growth promoting agent prepared by the described feeding compositions containing benzoic acid derivative and myristic acid derivant can substitute the application of feeding antibiotic class animal growth promoting agent further.
Animal growth promoting agent prepared by the described feeding compositions containing benzoic acid derivative and myristic acid derivant also can substitute the application as animal growth promoting agent of Pharmacological Level of Zinc preparation or copper agent further.
In one embodiment, the feeding compositions containing benzoic acid derivative and myristic acid derivant that the present invention provides is added to independent form in every daily sustenance of animal and is used.
In another embodiment, the feeding compositions containing benzoic acid derivative and myristic acid derivant that the present invention provides is prepared as the Feed forms such as additive premix, concentrated feed, mixed feed, beneficiated burden material complemental feed according to a certain percentage for animal edible with feedstuff, feed additive, carrier or diluent etc..
The feedstuff that the present invention relates to refers to derive from animal, plant, microorganism or mineral, for processing and fabricating feedstuff but be not belonging to the feeding material of feed additive.
The feed additive that the present invention relates to refer to feed manufacturing, make, a small amount of or trace substance that use process is added, including nutritional feed additive and non-nutritional feed additive.Nutritional feed additive refers to a small amount of or trace substance mixing in feedstuff for supplement feed nutritional labeling, including feed grade aminoacid, vitamin, mineral trace element, enzyme preparation, non-protein nitrogen etc..Non-nutritional feed additive refers to a small amount of or trace substance for ensureing or improve feed quality, improve the effects such as efficiency of feed utilization and mixing in feedstuff.
The carrier that the present invention relates to refers to carry active component, improves its dispersibility, and have good chemical stability and an adsorptivity can feeding material.
The diluent that the present invention relates to refers to be uniformly distributed in material additive raw material, the additive raw material of high concentration is diluted to pre-mixing agent or the material of premix material of low concentration, micro constitutent can be separated from each other, reduce reacting to each other between active component, do not affect, to increase the stability of active component, the physico-chemical property having related substance.
The additive premix that the present invention relates to refers to that the nutritional feed additive more than by two kinds (classes) or two kinds (class) is main, the feedstuff prepared according to a certain percentage with carrier or diluent, including compound premixed feed, trace element premixing feed, vitamin premixed feed.
The concentrated feed that the present invention relates to refers to the feedstuff mainly having protein, mineral and feed additive to prepare according to a certain percentage.
The mixed feed that the present invention relates to refers to according to cultivated animals nutritional need, the feedstuff multiple feedstuff and feed additive prepared according to a certain percentage.
The concentrate supplement that the present invention relates to refers to the nutrition into supplementary plant-eating animal, the feedstuff multiple feedstuff and feed additive prepared according to a certain percentage.
Additionally, the cultivated animals being suitable for containing benzoic acid derivative and the feeding compositions of myristic acid derivant or additive agent for feeding prepared therefrom or animal growth promoting agent that the present invention provides includes domestic animal, poultry and aquatic animal etc., and the especially control effect in the diarrhea of poultry and dyspepsia etc. is the most notable.
In another embodiment, the present invention provide containing benzoic acid derivative and the feeding compositions of myristic acid derivant or additive agent for feeding prepared therefrom or animal growth promoting agent etc. for the broiler of each growth stage, laying hen, hen, meat-type duck, laying ducks, goose, turkey, guinea fowl, Columba livia, Carnis Coturnicis japonicae and other can the raising of birds of artificial breeding.
In another embodiment, the present invention provide containing benzoic acid derivative and the feeding compositions of myristic acid derivant or additive agent for feeding prepared therefrom or animal growth promoting agent etc. for the beef cattle of each growth stage, milch cow, pig, support, horse, rabbit, Canis familiaris L., the raising of the domestic animal such as cat and donkey.
In another embodiment, the present invention provide containing benzoic acid derivative and the feeding compositions of myristic acid derivant or additive agent for feeding prepared therefrom or animal growth promoting agent etc. for the raising of the aquatic animal such as fish, shrimp, Chinese yellow eel, Eriocheir sinensis or Misgurni anguillicaudati of each growth stage.
In sum, the feeding compositions containing benzoic acid derivative and myristic acid derivant that the present invention provides is a kind of novel, safe animal feed additive, substitute feeding antibiotic class animal growth promoting agent and Pharmacological Level of Zinc preparation or the application of copper agent, the impact overcoming other toxic and side effects such as drug resistance, drug resistance transmission that feeding antibiotic causes in animal farming industry and heavy metal preparation prolonged application to cause animal health and human food safely, has large market prospect in animal farming industry.
Detailed description of the invention:
In order to describe the present invention, it is listed below embodiment.But it is to be understood that the invention is not restricted to these embodiments, only it is to provide the method putting into practice the present invention.
Benzoic acid derivative that following example of the present invention are used and myristic acid derivant are provided by the research and development centre of Guangzhou Insighter Biotechnology Co., Ltd., sample purity >=99%；Virginiamycin preparation used is import pre-mixing agent, factory of Belgium of Hui Bao company limited of the U.S. produce；Colistine sulfate used is produced by Shandong, Shandong drug resistance industry.
Embodiment 1: benzoic acid derivative and myristic acid derivant application effect in wean pig feed
The wean pig of 180 28 age in days average weights 7.61kg, DLY ternary miscellaneous lean meat species piglets such as 1 point 9 groups of table that body weight is close, often organize 20.After each group is added difference test additive in conventional creep feed (without any medicated feed additive, zinc oxide and high copper agent), free choice feeding and drinking-water, the average daily ingestion amount (ADF) of each test group test pig, average daily gain (ADG), the price of deed and diarrhea rate in adding up 10 days.Result is as shown in table 1, as it can be seen from table 1 just can reach the action effect of feeding antibiotic colistine sulfate 20ppm during additive capacity 2000ppm that benzoic acid derivative is in feedstuff；During the additive capacity 500ppm of myristic acid derivant, action effect is substantially better than the action effect of the permission using dosage 20ppm of virginiamycin.
Impact and the health-care effect of the growth performance of wean pig are studied by table 1 benzoic acid derivative and myristic acid derivant
Embodiment 2: the calcium benzoate of various dose and calcium myristate application effect in wean pig feed
The wean pig of 140 28 age in days average weights 7.61kg, DLY ternary miscellaneous lean meat species piglets such as 2 points 7 groups of table that body weight is close, often organize 20.After each group is added the test additive of various dose in conventional creep feed (without any medicated feed additive, zinc oxide and high copper agent), free choice feeding and drinking-water, the average daily ingestion amount (ADF) of each test group test pig, average daily gain (ADG), the price of deed and diarrhea rate in adding up 10 days.Result is as shown in table 2, from table 2 it can be seen that calcium benzoate and calcium myristate present dosage effect to the control of animal diarrhea rate and the change of production performance；But, from the whole result of each test group contrast visible in terms of controlling animal diarrhea rate calcium benzoate there is obvious advantage, and calcium myristate relative efficacy in the improvement to breeding performonce fo animals is more notable.
Impact and the health-care effect of the growth performance of wean pig are studied by table 2 calcium benzoate and calcium myristate
Embodiment 3: the use in conjunction of calcium benzoate and calcium myristate action effect in wean pig feed
The DLY ternary miscellaneous lean meat species ablactational baby pig that 160 28 age in days body weight are close is divided into 8 groups, often group 20.Each group is added calcium myristate and/or the calcium benzoate of various dose in the creep feed without any feed additive, free choice feeding and drinking-water during test, average daily gain (ADG), the price of deed and the diarrhea rate of each test group test pig in adding up 10 days.Result shows (table 3), and calcium benzoate is significantly improved effect with calcium myristate use in conjunction to the production performance tool of the control effect test pig the most simultaneously of the diarrhea rate of test pig.
Table 3 calcium benzoate and the calcium myristate use in conjunction effect in weaning pigs
Embodiment 4: the use in conjunction of calcium benzoate and calcium myristate application effect in chicken material.
The 1400 plumage 1 the biggest yellow-feather broilers of age in days are randomly divided into 7 test group, and each test group comprises 4 parallel test groups, and each parallel test group is 50 plumages, and are often organizing interpolation calcium benzoate and/or the calcium myristate of various dose in feedstuff respectively.Experimental period, raises in cages, free choice feeding and freely drinking water, totally 28 days experimental period, the average daily gain (ADG) of each test group test chicken, average feedstuff-meat ratio (AFCR) and survival rate in adding up 28 days.Result of the test shows, the calcium butyrate of 1200ppm is higher than to the survival rate of blank group test chicken；To the test group with the forage feed of the calcium myristate of various dose while containing 1200ppm calcium benzoate, while the survival rate of test chicken raises, production performance promotes effect significantly (table 4).
Table 4 calcium benzoate and the calcium myristate use in conjunction effect in broiler material
Embodiment 5: calcium benzoate and the calcium myristate use in conjunction effect in Ctenopharyngodon idellua feed
Test fish used is Ctenopharyngodon idellus, Aquatic product field, English Saite test site, Guangzhou carry out.The Mylopharyngodon piceus kind that bouncing, specification are consistent raise in large cage 4 weeks after just for formal culture experiment, experimental system is buoyancy small-sized net cage.Small-sized net cage is placed in one, test site 3500m with the most foster net cage2Pond in, the pond depth of water～1.5m, pond water is water under abundant aeration.During test, Ctenopharyngodon idellus 200 tail of hungry 1d being randomly divided into 5 groups, often group sets 4 repetitions, and each repetition puts 10 tail fishes, and entirety is put in 16 net cages after weighing at random, feeds different test feeds respectively.Test feed formula is prepared voluntarily, and different tests group is by being separately added into different test additives in basestocks.Test uses artificial limit food to throw something and feed, and feeding amount adjusts weekly once, and two groups of levels of throwing something and feeding (by original body mass) are completely the same, and throw something and feed every day twice (7:30 and 15:00).Test 8 weeks by a definite date.
Calcium benzoate or calcium benzoate are shown in Table 5 with calcium myristate use in conjunction to the growth promotion result of the test of fish.Result display is added calcium benzoate or calcium benzoate and is superior to matched group with the united test group of calcium myristate in terms of weightening finish, feed coefficient and survival rate, has obvious growth enhancing effect.
The use in conjunction test in Ctenopharyngodon idellua feed of table 5 calcium benzoate and calcium myristate is grouped and result
Above-described embodiment is the present invention preferably embodiment; but embodiments of the present invention are also not restricted to the described embodiments; the change made under other any spirit without departing from the present invention and principle, modify, substitute, combine, simplification etc. all should be the substitute mode of equivalence, within being included in protection scope of the present invention.
Claims (10)
1. a feeding compositions, it is characterised in that containing benzoic acid derivative and myristic acid derivant；
Described benzoic acid derivative is that as shown in formula I or its structure is as shown in formula II for benzoate or its structure:
Wherein, M is selected from H, alkali metal；
Wherein, M is selected from alkaline-earth metal, Zn, Fe, Mn, Cu；
Its structure of described benzoate is as shown in formula III or formula IV:
Described R1Selected from C1-4Straight or branched alkyl；
Wherein, R2、R3And R4Selected from H andAnd R2、R3And R4The most all H；
Described myristic acid derivant is that as shown in formula (V) or its structure is as shown in formula VI for myristinate or its structure:
Wherein, M is selected from H, alkali metal；
Wherein, M is selected from alkaline-earth metal, Zn, Fe, Mn, Cu；
Shown in its structure of described myristinate such as formula (VII) or formula (VIII):
Described R5Selected from C1-4Straight or branched alkyl；
Wherein, R6、R7And R8Selected from H and straight chain C13C (=O), and R6、R7And R8The most all H.
Feeding compositions the most according to claim 1, it is characterised in that according to the mass fraction, the described benzoic acid derivative contained be the number of 1-6 part and described myristic acid derivant be 1 part.
Feeding compositions the most according to claim 2, it is characterised in that according to the mass fraction, it is 1 part with myristic acid derivant that the number of the described benzoic acid derivative that described feeding compositions contains is 4 parts.
Feeding compositions the most according to claim 1, it is characterised in that described benzoic acid derivative is calcium benzoate, described myristic acid derivant is calcium myristate.
5. the application in preparing animal feed additive of the feeding compositions described in any one of claim 1-4.
Application the most according to claim 5, it is characterised in that described animal feed additive is animal growth promoter.
Application the most according to claim 5, it is characterised in that described animal is domestic animal, poultry or aquatic animal.
Application the most according to claim 7, it is characterised in that described domestic animal is the pig of each growth stage, cattle, sheep, horse, rabbit, Canis familiaris L., cat or donkey.
Application the most according to claim 7, it is characterised in that described poultry is the chicken of each growth stage, turkey, guinea fowl, duck, goose, Columba livia or Carnis Coturnicis japonicae.
Application the most according to claim 7, it is characterised in that described aquatic animal is the fish of each growth stage, shrimp, Eriocheir sinensis or Chinese yellow eel.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108617856A (en) * | 2018-03-14 | 2018-10-09 | 广州英赛特生物技术有限公司 | Application of the zinc benzoate in preparing animal feed additive |
| CN111011634A (en) * | 2019-12-31 | 2020-04-17 | 广东汇海农牧科技集团有限公司 | Pig feed additive for preventing diarrhea of weaned piglets and pig feed |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101331915A (en) * | 2007-06-29 | 2008-12-31 | 帝斯曼知识产权资产管理有限公司 | Animal feed composition |
| CN104186958A (en) * | 2014-05-23 | 2014-12-10 | 广州英赛特生物技术有限公司 | Applications of copper myristate as feed additive |
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2016
- 2016-03-25 CN CN201610178864.1A patent/CN105815571A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101331915A (en) * | 2007-06-29 | 2008-12-31 | 帝斯曼知识产权资产管理有限公司 | Animal feed composition |
| CN104186958A (en) * | 2014-05-23 | 2014-12-10 | 广州英赛特生物技术有限公司 | Applications of copper myristate as feed additive |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108617856A (en) * | 2018-03-14 | 2018-10-09 | 广州英赛特生物技术有限公司 | Application of the zinc benzoate in preparing animal feed additive |
| CN111011634A (en) * | 2019-12-31 | 2020-04-17 | 广东汇海农牧科技集团有限公司 | Pig feed additive for preventing diarrhea of weaned piglets and pig feed |
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