CN105145580A - Anti-mite composition - Google Patents
Anti-mite composition Download PDFInfo
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- CN105145580A CN105145580A CN201510463927.3A CN201510463927A CN105145580A CN 105145580 A CN105145580 A CN 105145580A CN 201510463927 A CN201510463927 A CN 201510463927A CN 105145580 A CN105145580 A CN 105145580A
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Abstract
The invention belongs to the technical field of compounded pesticides, and concretely relates to an anti-mite composition. The anti-mite composition comprises the following raw materials in percent by weight: 0.1-20% of spirodiclofen, 0.1-60% of fluazinam, and the balance an auxiliary agent. The composition, which is formed by combining the two main ingredients according to the above ratio, is applicable to control multiple pest mites at the same time, and is applicable to kill multiple pest mites. Compared with a conventional manner of using multiple drugs to kill mite, the employed drug kind is reduced, drug usage cost is reduced, environment pollution is reduced, and the disclosed anti-mite composition possesses extremely good persistent period. Harmful mites are prevented from generating drug resistance by mixing the above pesticides, and the service life of different kinds of pesticides is prolonged.
Description
Technical field
The invention belongs to technical field of compounded pesticide, be specifically related to a kind of miticide composition.
Background technology
Evil mite occurs from generation to generation many, and fertility is strong, and under suitable temperature and humidity conditions, the evil mite quantity energy within a short period of time of growth at double rapidly, thus easily develops immunity to drugs to miticide, causes serious harm to the crops such as fruit tree, cotton, vegetables simultaneously.At present, in control of pest mite, great majority or the mode adopting multi-medicament to prevent and treat in batches, but the mode that this multi-medicament is prevented and treated in batches considerably increases cost and the difficulty of control.In order to prevent and treat day by day serious various harmful mite, countries in the world are all at the miticide of continuous development of new, in acaricidal development and application process, delay evil mite pesticide resistance or cross resistance is the key factor extending product service life, reasonable employment miticide, control access times and dosage, the miticide of different mechanism of action is used alternatingly or uses with and just seems particularly important.
Summary of the invention
For the problems referred to above, the invention provides a kind of miticide composition, can be used for killing multiple harmful mite, the mode that more traditional use multi-medicament kills mite is respectively compared, and decreases types of medicines, reduces drug cost, decrease environmental pollution.
A kind of miticide composition of the present invention, by weight percentage, the raw material of described miticide composition consists of: spiral shell mite ester 0.1-20%, fluazinam 0.1-60%, adjuncts Balance.
Described spiral shell mite ester is a kind of efficient, unique worm's ovum double play miticide, there is the brand-new mechanism of action, tool action of contace poison, there is no interior absorption, the Fatty synthesis of main suppression mite, block the energy metabolism of mite, if there is good fragmentation effect to the ovum of evil mite, young mite mite, there is the effect suppressing female mite spawning and hatching rate.
Described fluazinam belongs to 2,6-dinitroanilines, is generally used as protective fungicide, but inventor finds that fluazinam has certain acaricidal action and has synergistic effect to part miticide in the process of experiment.Fluazinam belongs to contact killing type, resistance of rainwater washing against, and lasting effect is stronger.After both are mixed, have complementary advantages, and without cross resistance in ratio range, there is certain synergistic function.
Preferably, the weight ratio of spiral shell mite ester and fluazinam is 1:60-20:1.
The formulation of described miticide composition is suspending agent or aqueous emulsion or water dispersible granules or microemulsion or wetting powder or missible oil formulation, and different dosage form can select different auxiliary agents according to the common practise of this area.Described auxiliary agent be selected from dispersant, emulsifier, antifreezing agent, thickener, defoamer, solvent, wetting agent, disintegrant, filler one or more.
Described emulsifier is one or more in calcium dodecyl benzene sulfonate, alkylphenol polyoxyethylene, styrylphenol polyoxyethylene ether, polyoxyethylene nonylphenol ether, thermally coupled distillation columns, aliphatic acid polyethenoxy base ester, polyoxyethylene aliphatic alcohol ether, alkyl polyoxyethylene sulfate salt, phenethyl phenol polyethenoxy ether;
Described solvent be in dimethylbenzene, diesel oil, toluene, cyclohexanol, methyl alcohol, vegetable oil, turpentine oil, solvent naphtha, dimethyl formamide, ethanol, N-pyrrolidones, ethyl acetate, water equal solvent one or more;
Described wetting agent is lauryl sodium sulfate, calcium dodecyl benzene sulfonate, methyl naphthalene sulfonate formaldehyde condensate, pull open in powder, alkylnaphthalene sulfonate, spaonin powder etc. one or more;
Described dispersant is one or more in sodium lignin sulfonate, calcium lignosulfonate, alkylphenol polyoxyethylene formaldehyde condensation products sulphate, alkyl benzene sulfonate calcium salt, alkylphenol polyoxyethylene, polycarboxylate, aliphatic amine polyoxyethylene ether, glycerine fatty acid fat acid ester polyoxyethylene ether;
Described antifreezing agent is one or more in ethylene glycol, propane diols, glycerine, urea;
Described thickener is one or more in xanthans, Magnesiumaluminumsilicate, CMC, polyvinyl alcohol;
Described defoamer be silicone oil, C8-10 aliphatic alcohols compound, C10-20 saturated fat acid compounds one or more;
Described disintegrant is one or more in bentonite, ammonium sulfate, succinic acid, sodium bicarbonate, aluminium chloride, succinic acid;
Described filler is one or more in white carbon, kaolin, diatomite, precipitated calcium carbonate, starch.
Preferably, when the formulation of described composition is suspending agent, the material component of miticide composition is counted by weight: fluazinam 0.1-50 part, spiral shell mite ester 0.1-10 part, dispersant 0.1-10 part, emulsifier 0.1-10 part, antifreezing agent 0.1-4 part, thickener 0.1-4 part, defoamer 0.1-2 part, solvent 10-99.3 part.
Preferably, when the formulation of described miticide composition is aqueous emulsion, the material component of miticide composition is counted by weight: fluazinam 0.1-50 part, spiral shell mite ester 0.1-5 part, dispersant 0.1-10 part, emulsifier 0.1-10 part, antifreezing agent 0.1-4 part, solvent 21-99.5 part.
Preferably, when the formulation of described miticide composition is microemulsion, the material component of miticide composition is counted by weight: fluazinam 0.1-30 part, spiral shell mite ester 0.1-5 part, dispersant 0.1-15 part, wetting agent 0.1-15 part, antifreezing agent 0.1-4 part, solvent 31-99.5 part.
Preferably, when the formulation of described miticide composition is emulsifiable concentrate, the material component of miticide composition is counted by weight: fluazinam 0.1-40 part, spiral shell mite ester 0.1-10 part, emulsifier 0.1-12 part, solvent 38-99.7 part;
Preferably, when the formulation of described miticide composition is wetting powder, the material component of miticide composition is counted by weight: fluazinam 0.1-50 part, spiral shell mite ester 0.1-10 part, dispersant 0.1-10 part, wetting agent 0.1-10 part, filler 20-99.6 part.
Preferably, when the formulation of described miticide composition is water dispersible granules, the material component of miticide composition is counted by weight: fluazinam 0.1-50 part, spiral shell mite ester 0.1-5 part, dispersant 0.1-10 part, emulsifier 0.1-10 part, wetting agent 0.1-10 part, disintegrant 0.1-6 part, thickener 0.1-4 part, defoamer 0.1-2 part, filler 3-92 part.
The various formulation weight marks of miticide composition described above are all in 100 parts.The preparation method of various formulation is all prepared by the common process of this area different dosage form.
After above-mentioned two kinds of medicines pass through the binary built of aforementioned proportion, to multiple harmful mite, there is obvious Synergistic mite killing effect, may be used for control citrus red mite, panonychus citri, oranges and tangerines Schizotetranychus, Tetranychus urticae, Tetranychus cinnabarinus, and preventive effect is high, especially can more than 95% be reached to citrus red mite preventive effect.
Adopt composition of the present invention to the Toxicity Determination of citrus red mite:
The slide infusion process that test adopts FAO (Food and Agriculture Organization of the United Nation) (FAO) to recommend.The female one-tenth mite of 20 work inoculated by every block slide, and the basis of 3 preliminary experimenies is established series concentration value, and clear water contrasts, and often processes 3 times and repeats (totally 60 female one-tenth mites).Leaching medicine 5 blots with blotting paper after second immediately, then puts into 24-26 DEG C of insulating box, within after medicine 48 hours, checks lethality, calculates corrected mortality.
Concentration conversion is become natural logrithm value, corrected mortality is converted into arcsine transformation value, then with arcsine transformation value for dependent variable, with dosage natural logrithm value for independent variable, carry out linear regression analysis by DPS Biological Statistic Analysis Software, draw the toxicity regression linear equation of each medicament.Toxicity regression linear equation according to each medicament obtains corrected mortality arcsine transformation value (y), draws EC50 value by looking into antilogarithm table, then calculates toxicity index and the co-toxicity coefficient (CTC) of medicament according to the abundant method of Sun Yun.
Theoretical toxicity index × 100 of toxicity index/mixture of the theoretical toxicity index of the actual measurement toxicity index=standard agent EC50/ reagent agent EC50 × 100 single dose=theoretical toxicity index of the content mixture of single dose actual measurement toxicity index × single dose in mixture=each single dose theoretical toxicity index sum co-toxicity coefficient=mixture actual measurement
Evaluation criterion: CTC≤80 are antagonism, 80 < CTC < 120 are summation action, and CTC >=120 are synergistic effect, and experimental result please refer to table 1:
Table 1: the toxicity index of each medicament and the co-toxicity coefficient of spiral shell mite ester fluazinam
The experimental result of table 1 shows spiral shell mite ester and fluazinam, and 1:60 ~ 20:1 is composite in mass ratio, and all have synergistic effect to citrus red mite, when especially proportioning is between 1:50 ~ 15:1, synergy is more remarkable.
The miticide composition of the embodiment of the present invention, can be used for killing the multiple harmful mite causing citrus disease, the mode that more traditional use multi-medicament kills mite is respectively compared, and decreases types of medicines, reduces drug cost.
In sum, the present invention can simultaneously for preventing and treating multiple sick mite evil by the composition of the binary built of aforementioned proportion, can be used for killing multiple harmful mite, the mode that more traditional use multi-medicament kills mite is respectively compared, decrease types of medicines, reduce drug cost, decrease environmental pollution, and there is the good lasting period.Mixed Pharmacy can prevent and overcome pest mite class and develop immunity to drugs, and extends the service life of pesticide species.
Embodiment
Miticide composition provided by the invention is further illustrated, to understand the present invention better below by specific embodiment.
Embodiment 1
A kind of miticide composition, its material component is counted by weight: fluazinam 50 parts, spiral shell mite ester 10 parts, sodium lignin sulfonate 10 parts, calcium dodecyl benzene sulfonate 0.1 part, ethylene glycol 4 parts, xanthans 0.1 part, silicone oil 2 parts, dimethylbenzene supply 100 parts, according to a conventional method obtained suspending agent.
By the Recompounded pesticide of above-mentioned preparation, for reaching 99.7% to citrus red mite preventive effect.
Embodiment 2
A kind of miticide composition, its material component is counted by weight: fluazinam 0.1 part, spiral shell mite ester 0.5 part, calcium lignosulfonate 30 parts, alkylphenol polyoxyethylene 30 parts, glycerine 0.1 part, methyl alcohol supply 100 parts, according to a conventional method obtained aqueous emulsion.
By the agriculture chemical compounding of above-mentioned preparation, for reaching 99% to citrus red mite preventive effect.
Embodiment 3
A kind of miticide composition, its material component is counted by weight: fluazinam 40 parts, spiral shell mite ester 4 parts, polycarboxylate 8 parts, aliphatic acid polyethenoxy base ester 5 parts, lauryl sodium sulfate 10 parts, bentonite 6 parts, Magnesiumaluminumsilicate 4 parts, silicone oil 2 parts, white carbon supply 100 parts, according to a conventional method obtained water dispersible granules.
By the agriculture chemical compounding of above-mentioned preparation, for reaching 95.5% to oranges and tangerines Tetranychus cinnabarinus preventive effect.
Embodiment 4
A kind of miticide composition, its material component is counted by weight: fluazinam 50 parts, spiral shell mite ester 1 part, alkyl benzene sulfonate calcium salt 15 parts, calcium dodecyl benzene sulfonate 15 parts, glycerine 4 parts, vegetable oil supply 100 parts, according to a conventional method obtained microemulsion.
By the agriculture chemical compounding of above-mentioned preparation, for reaching 95% to oranges and tangerines Tetranychus cinnabarinus preventive effect.
Embodiment 5
A kind of miticide composition, its material component is counted by weight: fluazinam 40 parts, spiral shell mite ester 10 parts, alkyl polyoxyethylene sulfate salt 12 parts, cyclohexanol supply 100 parts, according to a conventional method obtained emulsifiable concentrate.
By the agriculture chemical compounding of above-mentioned preparation, for reaching 95% to oranges and tangerines Tetranychus urticae preventive effect.
Embodiment 6
A kind of miticide composition, its material component is counted by weight: fluazinam 50 parts, spiral shell mite ester 10 parts, aliphatic amine polyoxyethylene ether 0.1 part, spaonin powder 10 parts, kaolin supply 100 parts, according to a conventional method obtained wetting powder.
By the agriculture chemical compounding of above-mentioned preparation, for reaching 95.5% to oranges and tangerines Tetranychus urticae preventive effect.
Embodiment 7
A kind of miticide composition, its material component is counted by weight: fluazinam 15 parts, spiral shell mite ester 1 part, lignin sulfonic acid sodium salt 2 parts, 4 parts, alkylphenol polyoxyethylene formaldehyde condensation products sulphate, Magnesiumaluminumsilicate 1 part, silicone oil 0.2 part, ethylene glycol 4 parts, water supplies 100 parts, according to a conventional method obtained suspending agent.
Above 1 part is 1g, by the agriculture chemical compounding of above-mentioned preparation, for reaching 99.7% to citrus red mite preventive effect.
Embodiment 8
A kind of miticide composition, its material component is counted by weight: fluazinam 60 parts, spiral shell mite ester 1 part, sodium lignin sulfonate 10 parts, calcium dodecyl benzene sulfonate 0.1 part, ethylene glycol 4 parts, xanthans 0.1 part, silicone oil 2 parts, dimethylbenzene supply 100 parts, according to a conventional method obtained suspending agent.
By the Recompounded pesticide of above-mentioned preparation, for reaching 99.3% to panonychus citri preventive effect.
Embodiment 9
A kind of miticide composition, its material component is counted by weight: fluazinam 1 part, spiral shell mite ester 20 parts, calcium lignosulfonate 10 parts, alkylphenol polyoxyethylene 10 parts, glycerine 0.1 part, methyl alcohol supply 100 parts, according to a conventional method obtained aqueous emulsion.
By the agriculture chemical compounding of above-mentioned preparation, for reaching 99.6% to oranges and tangerines Schizotetranychus preventive effect.
Embodiment 10
A kind of miticide composition, its material component is counted by weight: fluazinam 1 part, spiral shell mite ester 15 parts, polycarboxylate 8 parts, aliphatic acid polyethenoxy base ester 5 parts, lauryl sodium sulfate 10 parts, bentonite 6 parts, Magnesiumaluminumsilicate 4 parts, silicone oil 2 parts, white carbon supply 100 parts, according to a conventional method obtained water dispersible granules.
By the agriculture chemical compounding of above-mentioned preparation, for reaching 95.7% to oranges and tangerines Tetranychus cinnabarinus preventive effect.
Embodiment 11
A kind of miticide composition, its material component is counted by weight: fluazinam 2 parts, spiral shell mite ester 20 parts, alkyl benzene sulfonate calcium salt 15 parts, calcium dodecyl benzene sulfonate 15 parts, glycerine 4 parts, vegetable oil supply 100 parts, according to a conventional method obtained microemulsion.
By the agriculture chemical compounding of above-mentioned preparation, for reaching 97.2% to oranges and tangerines Tetranychus cinnabarinus preventive effect.
Embodiment 12
A kind of miticide composition, its material component is counted by weight: part supplied by fluazinam 3 parts, spiral shell mite ester 18 parts, alkyl polyoxyethylene sulfate salt 12 parts, cyclohexanol, according to a conventional method obtained emulsifiable concentrate.
By the agriculture chemical compounding of above-mentioned preparation, for reaching 95.8% to oranges and tangerines Tetranychus urticae preventive effect.
Embodiment 13
A kind of miticide composition, its material component is counted by weight: fluazinam 1 part, spiral shell mite ester 15 parts, aliphatic amine polyoxyethylene ether 0.1 part, spaonin powder 10 parts, kaolin supply 100 parts, according to a conventional method obtained wetting powder.
By the agriculture chemical compounding of above-mentioned preparation, for reaching 96.5% to oranges and tangerines Tetranychus cinnabarinus preventive effect.
Embodiment 14
A kind of miticide composition, its material component is counted by weight: fluazinam 1 part, spiral shell mite ester 12 parts, lignin sulfonic acid sodium salt 2 parts, 4 parts, alkylphenol polyoxyethylene formaldehyde condensation products sulphate, Magnesiumaluminumsilicate 1 part, silicone oil 0.2 part, ethylene glycol 4 parts, water supplies 100 parts, according to a conventional method obtained suspending agent.
By the agriculture chemical compounding of above-mentioned preparation, for reaching 99.4% to citrus red mite preventive effect.
Comparative example
In order to detect the miticidal effect of composition of the present invention, now enumerate following contrast experiment's data:
16% fluazinam spiral shell mite ester suspending agent is made according to the proportioning described in embodiment 7.2500 times, 2000 times and 1500 times are diluted respectively by by the made product of above proportioning, 500 grams per liter fluazinam suspending agents, 24% spiral shell mite ester suspending agent control citrus red mite; Control panonychus citri, dilutes 3000 times, 2000 times and 2000 times respectively; Control oranges and tangerines Schizotetranychus, dilutes 6000 times, 3000 times and 4000 times respectively and carries out the test of pesticide effectiveness; Every test of pesticide effectiveness data are in Table 2-table 4.
Table 216% fluazinam spiral shell mite ester suspending agent control citrus red mite test of pesticide effectiveness result
Table 316% fluazinam spiral shell mite ester suspending agent control panonychus citri test of pesticide effectiveness result
Table 416% fluazinam spiral shell mite ester suspending agent control oranges and tangerines Schizotetranychus test of pesticide effectiveness knot
Can be found out by above-mentioned experiment, 16% fluazinam spiral shell mite ester suspending agent of the embodiment of the present invention 7 has good preventive effect to different types of oranges and tangerines evil mite at different growth periods.
Comprehensive Correlation, in table 1 data be each proportioning to the virulence coefficient of two spotted spider mite and co-toxicity coefficient, the virulence that both composite successful is used alone higher than two kinds of medicines, composite drug effect together obviously obtains gain; Spiral shell mite ester in example 7: fluazinam=1:15 proportioning describes spiral shell mite ester on application example: during fluazinam=1:15, effect for three kinds, oranges and tangerines field acarid (citrus red mite/panonychus citri/oranges and tangerines Schizotetranychus) all reaches obvious effect, comprehensively three kinds of acarid practical application effects are evaluated, spiral shell mite ester: during fluazinam=1:15, effect gain is obvious.
The foregoing is only the preferred embodiments of the present invention, be not limited to the present invention, for a person skilled in the art, the present invention can have various modifications and variations.Within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (6)
1. a miticide composition, is characterized in that: by weight percentage, and the raw material of described miticide composition consists of: spiral shell mite ester 0.1-20%, fluazinam 0.1-60%, adjuncts Balance.
2. a kind of miticide composition according to claim 1, is characterized in that: in described miticide composition, and the weight ratio of spiral shell mite ester and fluazinam is 1:60-20:1.
3. a kind of miticide composition according to claim 1, is characterized in that: the formulation of described miticide composition is suspending agent or aqueous emulsion or water dispersible granules or microemulsion or wetting powder or missible oil formulation.
4. a kind of miticide composition according to claim 1, is characterized in that: the auxiliary agent in described miticide composition be selected from dispersant, emulsifier, antifreezing agent, thickener, defoamer, solvent, wetting agent, disintegrant, filler one or more.
5. a kind of miticide composition according to claim 4, is characterized in that: described emulsifier is one or more in calcium dodecyl benzene sulfonate, alkylphenol polyoxyethylene, styrylphenol polyoxyethylene ether, polyoxyethylene nonylphenol ether, thermally coupled distillation columns, aliphatic acid polyethenoxy base ester, polyoxyethylene aliphatic alcohol ether, alkyl polyoxyethylene sulfate salt, phenethyl phenol polyethenoxy ether;
Described solvent be in dimethylbenzene, diesel oil, toluene, cyclohexanol, methyl alcohol, vegetable oil, turpentine oil, solvent naphtha, dimethyl formamide, ethanol, N-pyrrolidones, ethyl acetate, water equal solvent one or more;
Described wetting agent is lauryl sodium sulfate, calcium dodecyl benzene sulfonate, methyl naphthalene sulfonate formaldehyde condensate, pull open in powder, alkylnaphthalene sulfonate, spaonin powder etc. one or more;
Described dispersant is one or more in sodium lignin sulfonate, calcium lignosulfonate, alkylphenol polyoxyethylene formaldehyde condensation products sulphate, alkyl benzene sulfonate calcium salt, alkylphenol polyoxyethylene, polycarboxylate, aliphatic amine polyoxyethylene ether, glycerine fatty acid fat acid ester polyoxyethylene ether;
Described antifreezing agent is one or more in ethylene glycol, propane diols, glycerine, urea;
Described thickener is one or more in xanthans, Magnesiumaluminumsilicate, CMC, polyvinyl alcohol;
Described defoamer be silicone oil, C8-10 aliphatic alcohols compound, C10-20 saturated fat acid compounds one or more;
Described disintegrant is one or more in bentonite, ammonium sulfate, succinic acid, sodium bicarbonate, aluminium chloride, succinic acid;
Described filler is one or more in white carbon, kaolin, diatomite, precipitated calcium carbonate, starch.
6. a kind of miticide composition according to claim 1, is characterized in that: said composition is for preventing and treating citrus red mite, panonychus citri, oranges and tangerines Schizotetranychus, Tetranychus urticae, Tetranychus cinnabarinus.
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| CN107736385A (en) * | 2017-11-25 | 2018-02-27 | 惠州市无龄康态健康科技有限公司 | A kind of composition pesticide of extract containing Azalea pontica and fluazinam |
| CN109566628A (en) * | 2017-09-28 | 2019-04-05 | 沈阳中化农药化工研发有限公司 | A kind of miticide composition and its application |
| CN109744244A (en) * | 2018-12-28 | 2019-05-14 | 京博农化科技有限公司 | A kind of miticide composition of fluazinam and fenpyroximate |
| CN109757491A (en) * | 2018-12-28 | 2019-05-17 | 京博农化科技有限公司 | A kind of miticide composition of containing fluazinam and jervine |
| CN110278954A (en) * | 2018-03-19 | 2019-09-27 | 江苏扬农化工股份有限公司 | A kind of miticide composition of fluazinam and fenpyroximate compounding |
| CN110278951A (en) * | 2018-03-19 | 2019-09-27 | 江苏扬农化工股份有限公司 | A kind of miticide composition of fluazinam and propargite compounding |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109566628A (en) * | 2017-09-28 | 2019-04-05 | 沈阳中化农药化工研发有限公司 | A kind of miticide composition and its application |
| CN109566628B (en) * | 2017-09-28 | 2021-04-02 | 沈阳中化农药化工研发有限公司 | Acaricidal composition and application thereof |
| CN107736385A (en) * | 2017-11-25 | 2018-02-27 | 惠州市无龄康态健康科技有限公司 | A kind of composition pesticide of extract containing Azalea pontica and fluazinam |
| CN110278954A (en) * | 2018-03-19 | 2019-09-27 | 江苏扬农化工股份有限公司 | A kind of miticide composition of fluazinam and fenpyroximate compounding |
| CN110278951A (en) * | 2018-03-19 | 2019-09-27 | 江苏扬农化工股份有限公司 | A kind of miticide composition of fluazinam and propargite compounding |
| CN109744244A (en) * | 2018-12-28 | 2019-05-14 | 京博农化科技有限公司 | A kind of miticide composition of fluazinam and fenpyroximate |
| CN109757491A (en) * | 2018-12-28 | 2019-05-17 | 京博农化科技有限公司 | A kind of miticide composition of containing fluazinam and jervine |
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Application publication date: 20151216 |