CN104975523B - Preparation method of quick-dry wear-resisting textile fabric printing coating - Google Patents
Preparation method of quick-dry wear-resisting textile fabric printing coating Download PDFInfo
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- CN104975523B CN104975523B CN201510455298.XA CN201510455298A CN104975523B CN 104975523 B CN104975523 B CN 104975523B CN 201510455298 A CN201510455298 A CN 201510455298A CN 104975523 B CN104975523 B CN 104975523B
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- 239000011248 coating agent Substances 0.000 title claims abstract description 25
- 238000000576 coating method Methods 0.000 title claims abstract description 25
- 238000007639 printing Methods 0.000 title claims abstract description 15
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- 239000004744 fabric Substances 0.000 title claims abstract description 8
- 239000004753 textile Substances 0.000 title claims abstract description 7
- 239000004925 Acrylic resin Substances 0.000 claims abstract description 10
- 229920000178 Acrylic resin Polymers 0.000 claims abstract description 10
- 238000000034 method Methods 0.000 claims abstract description 10
- 229920000180 alkyd Polymers 0.000 claims abstract description 7
- 239000000203 mixture Substances 0.000 claims description 15
- 239000000843 powder Substances 0.000 claims description 11
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 10
- 239000003795 chemical substances by application Substances 0.000 claims description 9
- 239000000049 pigment Substances 0.000 claims description 9
- 238000003756 stirring Methods 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- LELOWRISYMNNSU-UHFFFAOYSA-N hydrogen cyanide Chemical compound N#C LELOWRISYMNNSU-UHFFFAOYSA-N 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 5
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 claims description 5
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 5
- 239000000440 bentonite Substances 0.000 claims description 5
- 229910000278 bentonite Inorganic materials 0.000 claims description 5
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims description 5
- 239000008199 coating composition Substances 0.000 claims description 5
- 239000003085 diluting agent Substances 0.000 claims description 5
- 239000012153 distilled water Substances 0.000 claims description 5
- 229920005610 lignin Polymers 0.000 claims description 5
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 5
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 5
- 239000000377 silicon dioxide Substances 0.000 claims description 5
- 235000012239 silicon dioxide Nutrition 0.000 claims description 5
- 239000002562 thickening agent Substances 0.000 claims description 5
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 4
- 238000005303 weighing Methods 0.000 claims description 4
- OMIGHNLMNHATMP-UHFFFAOYSA-N 2-hydroxyethyl prop-2-enoate Chemical class OCCOC(=O)C=C OMIGHNLMNHATMP-UHFFFAOYSA-N 0.000 claims description 3
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims description 3
- JIGUQPWFLRLWPJ-UHFFFAOYSA-N Ethyl acrylate Chemical compound CCOC(=O)C=C JIGUQPWFLRLWPJ-UHFFFAOYSA-N 0.000 claims description 3
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 3
- -1 diacetone acrylamides Chemical class 0.000 claims description 3
- 235000019441 ethanol Nutrition 0.000 claims description 3
- JMMWKPVZQRWMSS-UHFFFAOYSA-N isopropyl acetate Chemical class CC(C)OC(C)=O JMMWKPVZQRWMSS-UHFFFAOYSA-N 0.000 claims description 3
- PNJWIWWMYCMZRO-UHFFFAOYSA-N pent‐4‐en‐2‐one Natural products CC(=O)CC=C PNJWIWWMYCMZRO-UHFFFAOYSA-N 0.000 claims description 3
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims description 3
- 229920002472 Starch Polymers 0.000 claims description 2
- 238000006266 etherification reaction Methods 0.000 claims description 2
- 235000019698 starch Nutrition 0.000 claims description 2
- 239000008107 starch Substances 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims 1
- 238000001035 drying Methods 0.000 abstract description 7
- 230000002349 favourable effect Effects 0.000 abstract 1
- OMNKZBIFPJNNIO-UHFFFAOYSA-N n-(2-methyl-4-oxopentan-2-yl)prop-2-enamide Chemical compound CC(=O)CC(C)(C)NC(=O)C=C OMNKZBIFPJNNIO-UHFFFAOYSA-N 0.000 abstract 1
- 239000000975 dye Substances 0.000 description 4
- 238000012546 transfer Methods 0.000 description 4
- 238000011156 evaluation Methods 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000010017 direct printing Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 238000004806 packaging method and process Methods 0.000 description 2
- 239000003973 paint Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 1
- 238000012858 packaging process Methods 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
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Abstract
The invention relates to a preparation method of a quick-dry wear-resisting textile fabric printing coating. For the coating disclosed by the invention, acrylic resin favorable for increasing coating drying rate and prepared by adopting a special process is adopted, and diacetone-acrylamide and alkyd resin are added, so that the drying rate of the coating is further increased.
Description
Technical field
The present invention relates to the preparation method of the wear-resisting printing coating for textile fabrics of a kind of rapid-curing cutback.
Background of invention
Being coated with by color containing dyestuff or pigment and directly print to white or be infected with on the fabric of ground colour, on dyestuff or pigment, dye is solid
In place of stamp, thus obtain the printing method of various floral designs, be direct printing technique.Coating direct printing is at fibre
In dimension, the principle of coloring is different from general dyestuff, and its nationality binding agent is by insoluble granules of pigments set on the textile.Coating prints
Flower process environmental protection, it is not necessary to washing, the restriction to fabric is little, and technique is simple, and colorant match is convenient, and coloured light is prone to adjust and control, and prints
Pattern profile clear, well arranged, be rich in third dimension.Its printing quality directly shows very clear on printing machine, technique
Process is relatively brief, and printing quality is easily controlled, and is a kind of highly developed and most widely used technique.
Along with the rise of clothing personalized customization cybertimes and e-commerce field are provided and delivered requirement timely, personalized fixed
The rapid batch of uniform dress produces and the requirement of packaging delivery is more and more higher.This just requires printing coating energy within the extremely short time
Enough rapid draing is firm, to avoid occurring that adhesion is stained when packaging.But current pigment printing its drying time, print after
Rub resistance in short time, resistance to washing by rubbing with the hands property, heat-resisting stability are poor, have impact on the development of clothing personalized customization.
Summary of the invention
For solving the problems referred to above of printing coating, present invention employs following technical scheme:
The preparation method of the wear-resisting printing coating for textile fabrics of a kind of rapid-curing cutback, comprises the steps:
A) in terms of parts by weight, following component is weighed: 10 parts of N-[2-(2-methyl-4-oxopentyl)s, 15 parts of alkyd resin, 20 parts of acrylic acid
Resin, 40 parts of distilled water, 1 part of levelling agent, 2 parts of thickening agents, 0.5 part of fatty alcohol-polyoxyethylene ether, 1.5 parts of diluent etc., add
In agitator, with the speed of 350 turns/min, it is sufficiently stirred for disperseing 30 minutes, treats each component mix homogeneously, prepare mixed liquor；
B) in terms of parts by weight, weigh 50 parts of pigment, 10 parts of silicon dioxide powders, 3 parts of bentonite, 10 parts of alumina powders, mix
Closing uniformly, then feed the mixture in the mixed liquor that step 1) prepares, add the lignin sulfonic acid of 3 weight portions, 4 parts of etherificates are formed sediment
Powder, blender stirs 1 hour with the speed of 400 turns/min, more ground machine is fully ground, and is filtrated to get coating composition；
Described acrylic resin is adopted and is prepared with the following method:
In terms of parts by weight, take 20 parts of ethanol, 20 parts of propanol, 15 parts of isopropyl acetates, after mix homogeneously, add reactor
In, with the ramp of about 5-10 DEG C/min to 80 DEG C, it is incubated 30min, is then sequentially added into 20 parts of ethyl acrylate, 10 parts of first
Base acrylic acid, 15 parts of 2-(Acryloyloxy)ethanols, 2 parts of diacetone acrylamides, 1 part of azo dicyclohexyl formonitrile HCN, stirring mixing is all
Even, isothermal reaction 5 hours, it is cooled to 30 DEG C, drips 1.5ml strong aqua ammonia, be stirred for 30min, obtain acrylic resin.
Described levelling agent is organosilicon levelling agent.
Beneficial effect:
1) containing water-dispersible acrylic's resin in the coating of the present invention, it has good adhesive force, rate of drying
Hurry up, as one of the film-forming components of coating, it is possible to significantly improve the dry rate of coating serous coat.
2) coating of the present invention also uses beneficially improve N-[2-(2-methyl-4-oxopentyl) and the alkyd resin of dry rate, its
Work in coordination with acrylic resin, further increase the dry rate of ink slurry.
3) rate of drying of present invention water paint faster, can significantly reduce what water paint rate of drying brought slowly
The pattern adhesion that produces in printing and packaging process, the quality problems such as being stained, reduce production cost, there is actual application value pole.
4) rub resistance in the short time and resistance to wash fastness by rubbing with the hands after the coating of the present invention has good printing.
5) present invention does not contains the harmful substances such as formaldehyde, heavy metal and organotin, environmental protection, health.
Detailed description of the invention
Below in conjunction with embodiment, the present invention will be further described, but the scope of protection of present invention is not limited to reality
Execute the scope that example is expressed.
Embodiment 1
The preparation of acrylic resin:
In terms of parts by weight, take 20 parts of ethanol, 20 parts of propanol, 15 parts of isopropyl acetates, after mix homogeneously, add reactor
In, with the ramp of about 5-10 DEG C/min to 80 DEG C, it is incubated 30min, is then sequentially added into 20 parts of ethyl acrylate, 10 parts of first
Base acrylic acid, 15 parts of 2-(Acryloyloxy)ethanols, 2 parts of diacetone acrylamides, 1 part of azo dicyclohexyl formonitrile HCN, stirring mixing is all
Even, isothermal reaction 5 hours, it is cooled to 30 DEG C, drips 1.5ml strong aqua ammonia, be stirred for 30min, obtain acrylic resin.
The preparation of coating:
Following component is weighed: 10 parts of N-[2-(2-methyl-4-oxopentyl)s, 15 parts of alkyd resin, 20 parts of acrylic acid trees in terms of parts by weight
Fat, 40 parts of distilled water, 1 part of levelling agent, 2 parts of thickening agents, 0.5 part of fatty alcohol-polyoxyethylene ether, 1.5 parts of diluent etc., addition is stirred
Mix in device, with the speed of 350 turns/min, be sufficiently stirred for disperseing 30 minutes, treat each component mix homogeneously, prepare mixed liquor；
Weighing 50 parts of pigment, 10 parts of silicon dioxide powders, 3 parts of bentonite, 10 parts of alumina powders in terms of parts by weight, mixing is all
Even, then feed the mixture in the mixed liquor that step 1) prepares, add the lignin sulfonic acid of 3 weight portions, 4 parts of etherification starch,
Blender stirs 1 hour with the speed of 400 turns/min, more ground machine is fully ground, and is filtrated to get coating composition.
Comparative example 1
Following component is weighed: 25 parts of N-[2-(2-methyl-4-oxopentyl)s in terms of parts by weight, 20 parts of alkyd resin, 40 parts of distilled water, 1
Part levelling agent, 1 part of thickening agent, 0.5 part of fatty alcohol-polyoxyethylene ether, 1.3 parts of diluent, add in agitator, with 350 turns/min
Speed, be sufficiently stirred for disperseing 30 minutes, treat each component mix homogeneously, prepare mixed liquor；
Weighing 50 parts of pigment, 10 parts of silicon dioxide powders, 3 parts of bentonite, 10 parts of alumina powders in terms of parts by weight, mixing is all
Even, then feed the mixture in aforementioned prepared mixed liquor, add the lignin sulfonic acid of 3 weight portions, blender with 400 turns/
The speed of min stirs 1 hour, more ground machine is fully ground, and is filtrated to get coating composition.
Comparative example 2
Following component is weighed: 25 parts of alkyd resin in terms of parts by weight, the acrylic resins that 20 parts of embodiments 1 prepare, 40
Part distilled water, 1 part of levelling agent, 1 part of thickening agent, 0.5 part of fatty alcohol-polyoxyethylene ether, 1.3 parts of diluent, add in agitator,
With the speed of 350 turns/min, it is sufficiently stirred for disperseing 30 minutes, treats each component mix homogeneously, prepare mixed liquor.
Weighing 50 parts of pigment, 10 parts of silicon dioxide powders, 3 parts of bentonite, 10 parts of alumina powders in terms of parts by weight, mixing is all
Even, then feed the mixture in aforementioned prepared mixed liquor, add the lignin sulfonic acid of 3 weight portions, blender with 400 turns/
The speed of min stirs 1 hour, more ground machine is fully ground, and is filtrated to get coating composition.
Above-mentioned each coating is dried speed, tack evaluation, and result is as follows:
Drying property evaluation method: print each coating to place 1 hour after leaflet, then stick covering paper tape and execute
Pressure, opens paper tape, measures the coating transfer amount on paper tape, and evaluation is divided into 3 grades:
Good: to transfer on paper tape almost without coating；General: only local has a small amount of coating to transfer on paper tape；
Difference: have many places and substantial amounts of coating to transfer on paper tape.
Claims (2)
1. the preparation method of the wear-resisting printing coating for textile fabrics of rapid-curing cutback, it is characterised in that comprise the steps:
A) in terms of parts by weight, following component is weighed: 10 parts of N-[2-(2-methyl-4-oxopentyl)s, 15 parts of alkyd resin, 20 parts of acrylic acid trees
Fat, 40 parts of distilled water, 1 part of levelling agent, 2 parts of thickening agents, 0.5 part of fatty alcohol-polyoxyethylene ether, 1.5 parts of diluent, add stirring
In device, with the speed of 350 turns/min, it is sufficiently stirred for disperseing 30 minutes, treats each component mix homogeneously, prepare mixed liquor；
B) weighing 50 parts of pigment, 10 parts of silicon dioxide powders, 3 parts of bentonite, 10 parts of alumina powders in terms of parts by weight, mixing is all
Even, then feed the mixture in the prepared mixed liquor of step a), add the lignin sulfonic acid of 3 weight portions, 4 parts of etherification starch,
Blender stirs 1 hour with the speed of 400 turns/min, more ground machine is fully ground, and is filtrated to get coating composition；
Described acrylic resin is adopted and is prepared with the following method:
In terms of parts by weight, take 20 parts of ethanol, 20 parts of propanol, 15 parts of isopropyl acetates, add after mix homogeneously in reactor, with
The ramp of 5-10 DEG C/min, to 80 DEG C, is incubated 30min, is then sequentially added into 20 parts of ethyl acrylate, 10 parts of metering systems
Acid, 15 parts of 2-(Acryloyloxy)ethanols, 2 parts of diacetone acrylamides, 1 part of azo dicyclohexyl formonitrile HCN, be uniformly mixed, constant temperature
React 5 hours, be cooled to 30 DEG C, drip 1.5ml strong aqua ammonia, be stirred for 30min, obtain acrylic resin.
Preparation method the most according to claim 1, it is characterised in that: described levelling agent is organosilicon levelling agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510455298.XA CN104975523B (en) | 2015-07-30 | 2015-07-30 | Preparation method of quick-dry wear-resisting textile fabric printing coating |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510455298.XA CN104975523B (en) | 2015-07-30 | 2015-07-30 | Preparation method of quick-dry wear-resisting textile fabric printing coating |
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| Publication Number | Publication Date |
|---|---|
| CN104975523A CN104975523A (en) | 2015-10-14 |
| CN104975523B true CN104975523B (en) | 2017-01-11 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201510455298.XA Active CN104975523B (en) | 2015-07-30 | 2015-07-30 | Preparation method of quick-dry wear-resisting textile fabric printing coating |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20100160496A1 (en) * | 2007-04-27 | 2010-06-24 | Jeong Woo Son | Acrylic acid ester copolymer composition and redispersible powders |
| CN102558989A (en) * | 2010-12-09 | 2012-07-11 | 海洋化工研究院 | Anti-fouling coating material with excellent compatibility and use thereof |
| CN103642305A (en) * | 2013-12-02 | 2014-03-19 | 安徽猛牛彩印包装有限公司 | High-bonding printing ink and preparation method thereof |
| CN104530872A (en) * | 2014-12-30 | 2015-04-22 | 佛山金智节能膜有限公司 | Intelligent temperature controlling coating with oriented structure and preparation method thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10328906A1 (en) * | 2003-06-26 | 2005-01-13 | Endress + Hauser Process Solutions Ag | field bus |
-
2015
- 2015-07-30 CN CN201510455298.XA patent/CN104975523B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20100160496A1 (en) * | 2007-04-27 | 2010-06-24 | Jeong Woo Son | Acrylic acid ester copolymer composition and redispersible powders |
| CN102558989A (en) * | 2010-12-09 | 2012-07-11 | 海洋化工研究院 | Anti-fouling coating material with excellent compatibility and use thereof |
| CN103642305A (en) * | 2013-12-02 | 2014-03-19 | 安徽猛牛彩印包装有限公司 | High-bonding printing ink and preparation method thereof |
| CN104530872A (en) * | 2014-12-30 | 2015-04-22 | 佛山金智节能膜有限公司 | Intelligent temperature controlling coating with oriented structure and preparation method thereof |
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| Publication number | Publication date |
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| CN104975523A (en) | 2015-10-14 |
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| C41 | Transfer of patent application or patent right or utility model | ||
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Inventor after: Wang Xiaoxia Inventor before: Jin Shuanglei |
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Effective date of registration: 20161018 Address after: Zhejiang province Jinhua City Xiguan Street 321000 Wucheng Dong Zhai community Dong Kang Lane 6, Room 203 Applicant after: JINHUA ZHICHAN WUYUAN INFORMATION TECHNOLOGY Co.,Ltd. Address before: 312000 Zhejiang city of Shaoxing province Zhuji city Jiyang street Jin Jin Road No. 9 Applicant before: Jin Shuanglei |
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Effective date of registration: 20190515 Address after: 432800 No. 86 Changzheng Road, Chengguan Town, Dawu County, Xiaogan City, Hubei Province Patentee after: DAWU GOLD SOURCE TEXTILES & GARMENTS CORP LTD. OF HUBEI Address before: 321000 Room 203, Dong Kang lane, Tung residence community, Xiguan Street, Wucheng District, Jinhua, Zhejiang, China. Patentee before: JINHUA ZHICHAN WUYUAN INFORMATION TECHNOLOGY Co.,Ltd. |
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Denomination of invention: A preparation method of fast drying and wear-resistant textile printing coating Effective date of registration: 20230824 Granted publication date: 20170111 Pledgee: Dawu sub branch of Bank of Hubei Co.,Ltd. Pledgor: DAWU GOLD SOURCE TEXTILES & GARMENTS CORP LTD. OF HUBEI Registration number: Y2023420000331 |
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