CN104432492A - Application of Pulullan or compound of Pulullan in cigarette - Google Patents
Application of Pulullan or compound of Pulullan in cigarette Download PDFInfo
- Publication number
- CN104432492A CN104432492A CN201410610021.5A CN201410610021A CN104432492A CN 104432492 A CN104432492 A CN 104432492A CN 201410610021 A CN201410610021 A CN 201410610021A CN 104432492 A CN104432492 A CN 104432492A
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- Prior art keywords
- pulullan
- pulullan polysaccharide
- cigarette
- compound
- application
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
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- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
The invention discloses application of Pulullan or a compound of the Pulullan in a cigarette. The Pulullan or the compound of the Pulullan is added in the cigarette cut tobacco processing process in a material adding mode, and the adding proportion is 2 g to 100 g per single box. The compound of the Pulullan is preferably formed by the following raw materials, by weight, 10 percent of the Pulullan, two percent of apple extracts, 20 percent of propylene glycol, 20 percent of glycerinum, 13 percent of sorbitol, and the balance deionized water. The Pulullan or the compound of the Pulullan is adopted as humectant for the cigarette, and due to the fact that the Pulullan has special fragrance, moisture maintenance is achieved, and meanwhile the fragrance of the cigarette can be increased.
Description
Technical field
The invention belongs to cigarette additive technical field, specifically relate to pulullan polysaccharide or the application of compound in cigarette containing pulullan polysaccharide.
Background technology
In production of cigarettes process, in order to improve the physical property of tobacco, often need add certain humectant.The humectant mainly polyol such as glycerine, propane diols, sorbierite of these chemical classes.This compounds only has single moistening effect, and can affect flue gas mass after burning.In production of cigarettes, researcher is exploring one always can moistureproof in high humidity environment, again can humectation in low moisture environments, can also promote the active material of fragrance component content and comfortable taste degree after cigarette burning, as volume humectant for smoke simultaneously.
Pulullan polysaccharide, has another name called Pul, pullulan, is a kind of fungi polysaccharide, is a kind of extracellular water-soluble macromolecule neutral polysaccharide synthesized by Aureobasidium pullulans (Aureobasidium pullulans).Dry pulullan polysaccharide powder is white, and no hygroscopicity, be readily dissolved in cold water and hot water, its molecular weight is generally 4.8 × 10
3~ 2.2 × 10
6between, pulullan polysaccharide now realizes commercialization, and commercialization pulullan polysaccharide mean molecule quantity is 2 × 10
5.
Pulullan polysaccharide or its associated extraction thing, in food service industry, Chang Zuowei antistaling agent and quality improver use, be applied in drug capsules as antioxidant in medical industry, in packaging industry, also can make thickness after drying or hot pressing is that the film of 0.01mm uses as packaging material.Along with the further expansion of research, its application is also in continuous extension.
Pulullan polysaccharide or its compound are used as humectant, be especially applied in cigarette by bidirectional modulation cigarette moisture content with improve cigarette physics humid keeping performance, humidity resistance and suction comfort level technology then there is not been reported.
Summary of the invention
The object of the invention is to improve unconspicuous present situation for existing humectant for smoke to cigarette moisture content bidirectional modulation poor effect, suction comfort level, by pulullan polysaccharide or pulullan polysaccharide is applied in cigarette as natural humectant after composite, ability is maintained to improve cigarette moisture content, strengthen humectation effect, and effectively improve cigarette smoking comfort level.
Object of the present invention is achieved by following scheme:
Except as otherwise noted, percentage of the present invention is percetage by weight.
I. the application of pulullan polysaccharide in production of cigarettes.
The application of described pulullan polysaccharide in production of cigarettes, is characterized in that: added in reinforced mode in cigarette shreds process by pulullan polysaccharide, adding proportion is the every single case of 2g ~ 100g/.This interpolation can at leaves storage, get damp again, mix and carry out with addition of process sections such as material.
Described pulullan polysaccharide is the outer water-soluble cement polysaccharide of born of the same parents of produced similar glucan, xanthans of being fermented by Aureobasidium pullulans, and its molecular size range scope is at 5kD ~ 150kD.The film forming of this polysaccharide, gas barrier property, plasticity, viscosity are all comparatively strong, and have the good characteristics such as soluble in water, nontoxic, colorless and odorless.
II. the application of pulullan polysaccharide compound in production of cigarettes.
In described pulullan polysaccharide compound, pulullan polysaccharide content is preferably 0.5% ~ 20% (weight ratio).
Described pulullan polysaccharide compound is preferably made up of following raw material: pulullan polysaccharide 10%, apple extract 2%, propane diols 20%, glycerine 20% and sorbierite 13%, and surplus is deionized water.
The described application of pulullan polysaccharide compound in production of cigarettes, is characterized in that: added in reinforced mode in cigarette shreds process by the pulullan polysaccharide compound prepared, adding proportion is the every single case of 2g ~ 100g/.Described interpolation can at leaves storage, get damp again, mix and carry out with addition of process sections such as material.
Relative to prior art, the present invention has the following advantages:
1, pulullan polysaccharide is secure as its security of edible natural prodcuts;
2, there is special aroma, can cigarette flavor be increased while humectation.
Accompanying drawing explanation
Fig. 1 is pipe tobacco moisturizing experiment water-cut variation figure;
Fig. 2 is pipe tobacco protection against the tide experiment water-cut variation figure.
Detailed description of the invention
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with drawings and Examples, the present invention is described in further detail.Described specific embodiment only in order to explain the present invention, the technical scheme be not intended to limit the present invention.
Embodiment 1
Get Aureobasidium pullulans zymotic fluid appropriate, put into extraction equipment, add 20 times of (w/w) water, after stirring under 75 DEG C of conditions lixiviate 2.5h, after filtration discards filter residue, concentrated leaching liquor, to appropriate, adds 95% ethanol of 8 times of volumes, alcohol filters after analysing 36h, gets filter residue and both obtained pulullan polysaccharide after vacuum drying.
Added in tobacco leaf leaves storage process with feed way by pulullan polysaccharide, addition is 20g/B.C (every single case).
Embodiment 2
Added in pipe tobacco resurgence process with feed way by pulullan polysaccharide, addition is 50g/B.C.
Embodiment 3
Pulullan polysaccharide compound is prepared by following formula table:
| Raw material | Percentage by weight |
| Pulullan polysaccharide | 10 |
| Apple extract | 2 |
| Propane diols | 20 |
| Glycerine | 20 |
| Sorbierite | 13 |
| Deionized water | Mend to 100 |
The pulullan polysaccharide compound prepared is added in pipe tobacco with reinforced form, addition 20g/B.C.
Embodiment 4
Pulullan polysaccharide compound is prepared by following formula table:
| Raw material | Percentage by weight |
| Pulullan polysaccharide | 15 |
| Fructus Jujubae extract | 2 |
| Propane diols | 20 |
| Sorbierite | 20 |
| Deionized water | Mend to 100 |
The pulullan polysaccharide compound prepared is added in pipe tobacco with reinforced form, addition 25g/B.C.
Embodiment 5
Pulullan polysaccharide compound is prepared by following formula table:
| Raw material | Percentage by weight |
| Pulullan polysaccharide | 10 |
| Tomato extract | 2 |
| Propane diols | 20 |
| Glycerine | 15 |
| Sorbierite | 25 |
| Deionized water | Mend to 100 |
The pulullan polysaccharide compound prepared is added in leaves storage process with reinforced form, addition 10g/B.C..
Embodiment 6
Pulullan polysaccharide compound is prepared by following formula table:
| Raw material | Percentage by weight |
| Pulullan polysaccharide | 10 |
| Tobacco extract | 2 |
| Propane diols | 20 |
| Glycerine | 20 |
| Sorbierite | 25 |
| Deionized water | Mend to 100 |
The pulullan polysaccharide compound prepared is added in leaves storage process with reinforced form, addition 15g/B.C..
Application experiment: the humid keeping performance confirmatory experiment that pulullan polysaccharide adds in cigarette
The humid keeping performance of tobacco humectant refers to the environment at low humidity or high humidity, makes cigarette at the regulating power preventing moisture loss or suppression moisture absorption.The quality evaluating humectant humid keeping performance mainly judges with the variable quantity of certain hour inner wrap strip moisture content.
Experimental example 1: pulullan polysaccharide pipe tobacco performance of keeping humidity is tested
One. experimental technique
According to completing pipe tobacco moisture regain described in embodiment 2, the pipe tobacco adding equivalent PG not add pulullan polysaccharide in contrast, detects moisture in cut tobacco content at following time point moisture teller.
Two. experimental result
Experimental result is as following table 1, Fig. 1:
Table 1 pipe tobacco moisturizing experiment moisturizing rate detects
From in upper table and Fig. 1, along with time lengthening, the cigarette humectation effect of adding two kinds of humectants declines all to some extent, the amplitude difference declined is little, but on every single time point, the pipe tobacco water content of adding pulullan polysaccharide is all a little more than the pipe tobacco adding PG, and show that pulullan polysaccharide is reinforced in pipe tobacco as humectant, its effect is better than the traditional humectant PG commonly used.
Experimental example 2: pulullan polysaccharide pipe tobacco humidity resistance is tested
One. experimental technique
Feed in raw material according to completing tobacco leaf leaves storage described in embodiment 1, the tobacco leaf adding equivalent PG not add pulullan polysaccharide in contrast, detects moisture content in leaves content at following time point moisture teller.
Two. experimental result
Experimental result is as following table 2, Fig. 2:
Table 2 protection against the tide experiment moisturizing rate detects
From upper table and Fig. 2, under humidity higher strip part (80%RH), when addition is 2g/B.C., the humidity resistance of pulullan polysaccharide humectant is better than contrasting PG, in whole testing time section, the pipe tobacco water content of adding pulullan polysaccharide, all lower than the water content of adding PG, shows that the humidity resistance of pulullan polysaccharide is better than PG.
Experimental example 3: the flavouring performance verification experiment that pulullan polysaccharide adds in cigarette
Experimental principle: with reference to the thinking about cigarette Style Evaluation in " Chinese-style cigarette style sensory evaluation method ", for fragrance surface, flue gas performance and mouthfeel aspect, sensory evaluation is carried out to the sample adding pulullan polysaccharide compound, participation is smoked panel test marking number 11 people, and design evaluatio marking form and fractional value are as following table 3:
Using embodiment 3 gained pulullan polysaccharide compound as laboratory sample.
Table 3 sense organ evaluating meter and marking numerical value
Experimental example 4: the flavouring experiment of pulullan polysaccharide
One. experimental technique
Feed in raw material according to completing purple cloud leaf group silk described in embodiment 3, with replace pulullan polysaccharide change and the purple cloud leaf group silk of the water gagings such as interpolation in contrast, carry out 11 people after by hand making cigarette and smoke panel test.
Two. experimental result
According to marking form designed in experimental principle, give a mark after cigarette after 11 people smoke panel test respectively, calculate average mark and obtain following result, in table 4:
Table 4 purple cloud leaf group control sample and sample contrast to smoke panel test and add up
From upper table statistics, add pulullan polysaccharide in the compound that purple cloud tobacco leaf formulation uses after, the suction sensory scores of cigarette obtains certain raising, certain lifting is had in fragrance performance and flue gas performance and mouthfeel, the compound showing the with the addition of pulullan polysaccharide compound not adding polysaccharide of comparing has certain flavouring effect, separately in the moist feeling and comfortableness of mouthfeel, also has certain effect.
Claims (6)
1. the application of pulullan polysaccharide in production of cigarettes.
2. the application of pulullan polysaccharide according to claim 1 in production of cigarettes, is characterized in that: added in reinforced mode in cigarette shreds process by pulullan polysaccharide, adding proportion is the every single case of 2g ~ 100g/.
3. the application of pulullan polysaccharide compound in production of cigarettes.
4. the application of pulullan polysaccharide compound according to claim 3 in production of cigarettes, it is characterized in that: added in reinforced mode in cigarette shreds process by the pulullan polysaccharide compound prepared, adding proportion is the every single case of 2g ~ 100g/.
5. the application of pulullan polysaccharide compound according to claim 4 in production of cigarettes, is characterized in that: in described pulullan polysaccharide compound, pulullan polysaccharide content is preferably 0.5% ~ 20% percetage by weight.
6. the application of pulullan polysaccharide compound according to claim 4 in production of cigarettes, it is characterized in that: described pulullan polysaccharide compound is preferably made up of the raw material of following weight percentage: pulullan polysaccharide 10%, apple extract 2%, propane diols 20%, glycerine 20% and sorbierite 13%, surplus is deionized water.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410610021.5A CN104432492A (en) | 2014-11-03 | 2014-11-03 | Application of Pulullan or compound of Pulullan in cigarette |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410610021.5A CN104432492A (en) | 2014-11-03 | 2014-11-03 | Application of Pulullan or compound of Pulullan in cigarette |
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| Publication Number | Publication Date |
|---|---|
| CN104432492A true CN104432492A (en) | 2015-03-25 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410610021.5A Pending CN104432492A (en) | 2014-11-03 | 2014-11-03 | Application of Pulullan or compound of Pulullan in cigarette |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107411163A (en) * | 2017-06-28 | 2017-12-01 | 常州万博金属构件厂 | One grows tobacco with anti-caking moisture regain agent and preparation method thereof |
| CN109984365A (en) * | 2019-05-13 | 2019-07-09 | 云南中烟工业有限责任公司 | A kind of biotinylation pulullan polysaccharide derivative is used to improve the purposes of the cigarette shreds biotin rate of transform |
| CN110051034A (en) * | 2019-05-13 | 2019-07-26 | 云南中烟工业有限责任公司 | A method of improving humidity preservation property of cigarette and humidity resistance |
| CN110522072A (en) * | 2019-07-23 | 2019-12-03 | 江苏鑫源烟草薄片有限公司 | A kind of preparation method heating the cigarette recombination stem core material that do not burn |
| CN113040410A (en) * | 2019-12-26 | 2021-06-29 | 中国科学院青岛生物能源与过程研究所 | Method for moisturizing cigar wrapper tobacco leaves |
| CN113974202A (en) * | 2021-10-25 | 2022-01-28 | 深圳市真味生物科技有限公司 | Environment-friendly electronic atomized liquid thickener and preparation method thereof |
| US11319566B2 (en) | 2017-04-14 | 2022-05-03 | Capsugel Belgium Nv | Process for making pullulan |
| US11576870B2 (en) | 2017-04-14 | 2023-02-14 | Capsugel Belgium Nv | Pullulan capsules |
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| US5518902A (en) * | 1992-08-20 | 1996-05-21 | Kabushiki Kaisha Hayashibara Seibutsu Kagaku Kenkyujo | High pullulan content product, and its preparation and uses |
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Patent Citations (5)
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Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US11878079B2 (en) | 2017-04-14 | 2024-01-23 | Capsugel Belgium Nv | Pullulan capsules |
| US11576870B2 (en) | 2017-04-14 | 2023-02-14 | Capsugel Belgium Nv | Pullulan capsules |
| US11319566B2 (en) | 2017-04-14 | 2022-05-03 | Capsugel Belgium Nv | Process for making pullulan |
| CN107411163A (en) * | 2017-06-28 | 2017-12-01 | 常州万博金属构件厂 | One grows tobacco with anti-caking moisture regain agent and preparation method thereof |
| CN109984365B (en) * | 2019-05-13 | 2021-07-09 | 云南中烟工业有限责任公司 | Application of biotinylation pullulan polysaccharide derivative in improving biotin transfer rate of cigarette cut tobacco |
| CN110051034B (en) * | 2019-05-13 | 2021-05-07 | 云南中烟工业有限责任公司 | Method for improving moisture retention and moisture resistance of cigarette cut tobacco |
| CN110051034A (en) * | 2019-05-13 | 2019-07-26 | 云南中烟工业有限责任公司 | A method of improving humidity preservation property of cigarette and humidity resistance |
| CN109984365A (en) * | 2019-05-13 | 2019-07-09 | 云南中烟工业有限责任公司 | A kind of biotinylation pulullan polysaccharide derivative is used to improve the purposes of the cigarette shreds biotin rate of transform |
| CN110522072B (en) * | 2019-07-23 | 2021-11-19 | 江苏鑫源烟草薄片有限公司 | Preparation method of recombined stem shred core material for cigarette by heating and non-combustion |
| CN110522072A (en) * | 2019-07-23 | 2019-12-03 | 江苏鑫源烟草薄片有限公司 | A kind of preparation method heating the cigarette recombination stem core material that do not burn |
| CN113040410A (en) * | 2019-12-26 | 2021-06-29 | 中国科学院青岛生物能源与过程研究所 | Method for moisturizing cigar wrapper tobacco leaves |
| CN113040410B (en) * | 2019-12-26 | 2022-11-18 | 中国烟草总公司海南省公司 | Method for moisturizing cigar wrapper tobacco leaves |
| CN113974202A (en) * | 2021-10-25 | 2022-01-28 | 深圳市真味生物科技有限公司 | Environment-friendly electronic atomized liquid thickener and preparation method thereof |
| CN113974202B (en) * | 2021-10-25 | 2023-09-01 | 深圳市真味生物科技有限公司 | Environment-friendly electronic atomized liquid thickener and preparation method thereof |
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Application publication date: 20150325 |