CN103205355B - Strong acoustic loading wine aging method and apparatus for the method - Google Patents
Strong acoustic loading wine aging method and apparatus for the method Download PDFInfo
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- CN103205355B CN103205355B CN201310103037.2A CN201310103037A CN103205355B CN 103205355 B CN103205355 B CN 103205355B CN 201310103037 A CN201310103037 A CN 201310103037A CN 103205355 B CN103205355 B CN 103205355B
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- 235000014101 wine Nutrition 0.000 title claims abstract description 54
- 238000000034 method Methods 0.000 title claims abstract description 51
- 230000032683 aging Effects 0.000 title claims abstract description 47
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims abstract description 114
- 239000007788 liquid Substances 0.000 claims description 19
- 238000005259 measurement Methods 0.000 claims description 14
- 230000006835 compression Effects 0.000 claims description 9
- 238000007906 compression Methods 0.000 claims description 9
- 230000001737 promoting effect Effects 0.000 claims description 6
- 230000029087 digestion Effects 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 6
- 238000005886 esterification reaction Methods 0.000 abstract description 6
- 235000019640 taste Nutrition 0.000 abstract description 6
- 230000032050 esterification Effects 0.000 abstract description 5
- 238000009835 boiling Methods 0.000 abstract description 4
- 235000009508 confectionery Nutrition 0.000 abstract description 4
- 230000004913 activation Effects 0.000 abstract description 3
- 125000003118 aryl group Chemical group 0.000 abstract description 3
- 230000003647 oxidation Effects 0.000 abstract description 3
- 238000007254 oxidation reaction Methods 0.000 abstract description 3
- 150000001299 aldehydes Chemical class 0.000 abstract 2
- 150000001735 carboxylic acids Chemical class 0.000 abstract 2
- 150000001298 alcohols Chemical class 0.000 abstract 1
- 238000001704 evaporation Methods 0.000 abstract 1
- 230000008020 evaporation Effects 0.000 abstract 1
- 238000012544 monitoring process Methods 0.000 description 10
- 125000002485 formyl group Chemical class [H]C(*)=O 0.000 description 5
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 230000005855 radiation Effects 0.000 description 4
- 239000000654 additive Substances 0.000 description 3
- 230000000996 additive effect Effects 0.000 description 3
- 230000003679 aging effect Effects 0.000 description 3
- 239000003205 fragrance Substances 0.000 description 3
- 238000006555 catalytic reaction Methods 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000007689 inspection Methods 0.000 description 2
- 230000001133 acceleration Effects 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000019658 bitter taste Nutrition 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 230000035622 drinking Effects 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 235000019990 fruit wine Nutrition 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
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- Non-Alcoholic Beverages (AREA)
- Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
Abstract
The present invention relates to a wine aging method and an apparatus for the method. Said method includes the steps of applying a strong sound wave produced from a strong acoustic wave generating unit into the wine for resonance of wine molecules, so as to enhance the molecule activation energy of various alcohols, aldehydes and other organics in the wine, increase the intermolecular effective collision rate, and accelerate rapid evaporation of low boiling components, oxidation and esterification. The aldehydes in the wine are constantly oxidized into carboxylic acids, and ethyl acetate with aromatic odor is produced through the esterification reaction of the carboxylic acids and alcohol , and thus making the wine taste mellow, sweet and soft. The strong acoustic loading wine aging method and the apparatus for the method improve the aging speed and the taste of the wine, and reduce the production costs.
Description
Technical field
The present invention relates to drinks production field, be specifically related to the equipment that a kind of drinks is urged aging method and realized the method.
Background technology
As everyone knows, existing drinks urges ageing to adopt often physics, chemistry and additive method, and wine is applied to certain effect, makes the composition element of wine that certain chemical reaction occur, with reach with standing storage after the suitable ageing level of the quality of wine.Traditional liquor ageing method has electromagnetic method, radiation method, additive method, supersonic method etc.Electromagnetic method utilizes cylindrical solenoid coil to produce the ageing that high frequency magnetic field takes catalysis wine, and radiation method utilizes the commercially available bulk wine of ^60Co-gamma-ray irradiation, but this kind of method may cause later stage radiation problem, thereby unhealthful.Supersonic method utilizes 20kHz sound wave to make " cavitation " effect in wine liquid, or utilizes hyperacoustic atomizing to realize promoting ageing, and generally speaking supersonic method can make digestion time shorten to 1/3.Although supersonic method does not increase radiation and does not increase other materials yet, utilizing sound wave to make the composition of wine collide to promote ageing reaction, is a kind of aging method without harm, but because hyperacoustic intensity is generally no more than 140dB, therefore urge ageing effect slower, can not enhance productivity.And the method for adding chemical reagent catalysis may cause additive that people is drunk and exerted an influence.
Summary of the invention
The present invention, in order to overcome the deficiency of above technology, provides a kind of method of strong sound wave acceleration liquor ageing and equipment of realizing the method for utilizing.
The present invention overcomes the technical scheme that its technical problem adopts:
This strong sound wave loads drinks and urges aging method, comprises the steps:
A) strong sound wave generating unit is connected in a sealed chamber;
B) wine newly distilling is inserted in sealed chamber;
C) open strong sound wave generating unit and make it to produce strong sound wave;
D) strong sound wave being entered in annular seal space makes drinks liquid produce cavitation phenomenon;
E) through certain promoting ageing, after the time, close strong sound wave generating unit.
The above-mentioned strong sound wave sound pressure of stating the generation of strong sound wave phonation unit is 140dB-180dB, and its frequency is 500Hz-1500Hz, and described digestion time is 5-20 minute.
In order to raise the efficiency and to reduce operation easier, sound pressure is 165dB, adjusts the frequency of strong sound wave, until the drinks liquid in sealed chamber produces vibrations uniformly.
In order to improve the quality of production, be also included in strong sound wave and make drinks liquid produce the process of measuring in real time ethyl acetate concentration in drinks liquid in cavitation processes.
In order to improve the quality of production, be also included in strong sound wave and make drinks liquid produce the process of measuring in real time strong sound wave sound pressure in cavitation processes.
Implement above-mentioned strong sound wave and load the equipment that drinks is urged aging method, comprise there is the strong sound pressurized compartment of sealed cavity, the sourdine that is connected in the strong sound wave generating unit of strong sound pressurized compartment front end and is connected in strong sound pressurized compartment rear end.
Above-mentioned strong sound wave generating unit comprises compressed-air loudspeaker, sound-source signal producer, computer and the compression gas tank for storing compressed air that is connected in compressed-air loudspeaker by tracheae, and the output terminal of described sound-source signal producer is electrically connected on compressed-air loudspeaker by signal wire; Its input terminus is electrically connected on computer by signal wire, and described compression gas tank is connected with air compressor by tracheae.
For the concentration of Real-Time Monitoring ethyl acetate, also bag is arranged at the ethyl acetate sensor in strong sound pressurized compartment, and described ethyl acetate sensor electrical is connected in ethyl acetate survey meter, and described ethyl acetate survey meter is electrically connected on computer.
In order to learn sound pressure and the frequency values in strong sound pressurized compartment, also comprise the sound transducer being arranged in strong sound pressurized compartment, described sound transducer is electrically connected on acoustic measurement instrument, and described acoustic measurement instrument is electrically connected on computer.
Operate above-mentioned strong sound wave and load the method that drinks is urged the equipment of ageing, comprise the steps:
(1) open computer, open acoustic measurement instrument, check the data acquisition and monitoring circuit being connected between acoustic measurement instrument and computer, by acoustic measurement instrument, check that whether sound transducer is working properly, and carry out sound pressure level calibration;
(2) open ethyl acetate survey meter, check the data acquisition and monitoring circuit being connected between ethyl acetate survey meter and computer, by ethyl acetate survey meter, check that whether ethyl acetate sensor is working properly;
(3) wine for the treatment of ageing is positioned in strong sound pressurized compartment;
(4) open sound-source signal producer, check the signal line between sound-source signal producer and computer; By computer control sound-source signal producer, produce pink noise afterwards;
(5) open air compressor, compressed air produces strong sound wave by compressed-air loudspeaker at a high speed, and strong sound wave enters strong sound pressurized compartment and carries out wine ageing;
(6) sound transducer Real-Time Monitoring sound pressure level feeding back on computer shows, it is 165dB that computer control sound-source signal producer regulates sound pressure level;
(7) computer control sound-source signal producer regulates the frequency of strong sound wave, until the drinks liquid in sealed chamber produces vibrations uniformly;
(8) work is after 15 minutes, and closing device takes out wine from strong sound pressurized compartment.
The invention has the beneficial effects as follows: the strong sound wave that strong sound wave phonation unit produces puts in wine, molecule in wine is resonated, strengthen multiple alcohol, aldehyde and other organic molecule activation energy in wine, improved its intermolecular effective collision rate, accelerated that low boiling point component volatilizees fast, oxidation, esterification.Make in wine aldehyde be constantly oxidized to carboxylic acid, and carboxylic acid again with alcohol generation esterification, generate and to there is the ethyl acetate of aromatic odour, thereby make vinosity sweet-smelling, sweet, soft.The aging speed that has improved wine, has reduced production cost, has improved the mouthfeel of wine.
Accompanying drawing explanation
Fig. 1 is the structural representation of equipment of the present invention;
In figure, 1. compressed-air loudspeaker the last 2. sound pressurized compartment 3. sourdine 4. compression gas tank 5. sound-source signal producer 6. ethyl acetate survey meter 7. ethyl acetate sensor 8. computer 9. sound transducer 10. acoustic measurement instrument.
Embodiment
Below in conjunction with accompanying drawing 1, the present invention will be further described.
Strong sound wave of the present invention loads drinks and urges aging method, comprises the steps: that (1) is connected in strong sound wave generating unit in one sealed chamber; (2) wine newly distilling is inserted in sealed chamber; (3) open strong sound wave generating unit and make it to produce strong sound wave; (4) strong sound wave being entered in annular seal space makes drinks liquid produce cavitation phenomenon; (5) through certain promoting ageing, after the time, close strong sound wave generating unit.Because the wine newly distilling is owing to containing a small amount of lower boiling excitor substance, can cause wine body quick-fried peppery, also have mud taste, poor taste, bitter taste also can cause wine body not alcohol and, not soft.In the elimination of this pungent and wine, the generation of fragrance all will complete through decomposition reaction for a long time, no matter be fruit wine or wine, the person who has rendered outstanding service of energy expire fragrance smell is ethyl acetate.But in new wine, the content of ethyl acetate is very little.And aldehyde, acid in wine does not only have fragrance, stimulates in addition the effect of throat.So it is raw, bitter, puckery so disagreeable to the taste that the wine of newly brewageing drinks, need some months to several years naturally store sth. in a cellar traditional aging process and could eliminate the taste of mixing, distribute strong aroma.
The strong sound wave sound pressure that above-mentioned strong sound wave phonation unit produces is 140dB-180dB, its frequency is 500Hz-1500Hz, it puts in wine, produce cavitation phenomenon, molecule in wine is resonated, strengthen multiple alcohol, aldehyde and other organic molecule activation energy in wine, improved its intermolecular effective collision rate, accelerate that low boiling point component volatilizees fast, oxidation, esterification.Make in wine aldehyde be constantly oxidized to carboxylic acid, and carboxylic acid again with alcohol generation esterification, generate and to there is the ethyl acetate of aromatic odour, thereby make vinosity sweet-smelling, sweet, soft.The aging speed that has improved wine, has reduced production cost, has improved the mouthfeel of wine.
Table 1
By table 1, can learn that thereupon the raising ethyl acetate content of sound pressure reaches 100mg/ml required time shorter and shorter, but the amplitude step-down that the time declines when sound pressure surpasses 165dB, and because the sound pressure difficulty that more height adjustment frequency evenly shakes the generation of drinks liquid is larger, therefore preferably sound pressure is 165dB.When sound pressure is adjusted into after 165dB, adjust the frequency of strong sound wave, until the drinks liquid in sealed chamber produces vibrations uniformly, so that the ageing process of wine is even.
Above-mentioned strong sound wave loading drinks is urged aging method also can be included in strong sound wave and is made to measure in real time the process of ethyl acetate concentration in drinks liquid and the process of measuring in real time strong sound wave sound pressure in drinks liquid generation cavitation processes.By the ethyl acetate concentration in Real-Time Monitoring drinks liquid and strong sound wave sound pressure, can better control the quality of drinks when the ageing, if ethyl acetate concentration is too high too low and strong sound wave sound pressure is too high too low, can take in time technique means to guarantee the ageing effect of drinks.
The present invention has also designed and has a kind ofly implemented above-mentioned strong sound wave and load the equipment that drinks is urged aging method, comprise there is the strong sound pressurized compartment 2 of sealed cavity, the sourdine 3 that is connected in the strong sound wave generating unit of strong sound pressurized compartment 2 front ends and is connected in strong sound pressurized compartment 2 rear ends.During use, the wine of new brew is placed in to strong sound pressurized compartment 2, utilizes afterwards strong sound wave generating unit produce strong sound wave and enter into pressurized compartment 2, make strong sound wave and wine effect, accelerate the ageing of wine.There is resonance and consume after part in the energy of strong sound wave molecule in making wine, remaining energy is converted into heat energy consumption by sourdine 3, can reduce the noise of system, prevents sound pollution.
Above-mentioned strong sound wave generating unit comprises compressed-air loudspeaker 1, sound-source signal producer 5, computer 8 and the compression gas tank 4 for storing compressed air that is connected in compressed-air loudspeaker 1 by tracheae, and the output terminal of described sound-source signal producer 5 is electrically connected on compressed-air loudspeaker 1 by signal wire; Its input terminus is electrically connected on computer 8 by signal wire, and described compression gas tank 4 is connected with air compressor by tracheae.Air compressor is input to pressurized air in compression gas tank 4 and stores, computer 8 is controlled sound-source signal producer 5 and is produced audio control signal, and the audio control signal that the compressed air in compression gas tank 4 produces sound-source signal producer 5 by compressed-air loudspeaker fast changes the strong sound wave of myriawatt level into.
Also bag is arranged at the ethyl acetate sensor 7 in strong sound pressurized compartment 2, and described ethyl acetate sensor 7 is electrically connected on ethyl acetate survey meter 6, and described ethyl acetate survey meter 6 is electrically connected on computer 8.Ethyl acetate sensor 7 can carry out on-line monitoring to the wine in strong sound pressurized compartment, and monitoring numerical value is fed back to computer 8 by ethyl acetate survey meter 6, and its concentration numerical value shows in real time on computer 8.If ethyl acetate concentration exceeds standard in ageing process, computer 8 can be controlled sound-source signal producer 5 and quit work, and to avoid continuing ageing, causes the too high situation of ethyl acetate concentration, has guaranteed the quality of production, has realized the online detection of producing.
Also comprise the sound transducer 9 being arranged in strong sound pressurized compartment 2, described sound transducer 9 is electrically connected on acoustic measurement instrument 10, and described acoustic measurement instrument 10 is electrically connected on computer 8.Sound transducer 9 is for measuring sound pressure and the frequency values of the strong sound wave of strong sound pressurized compartment, and feed back on computer 8 and show by acoustic measurement instrument 10, accuracy when controlling sound-source signal producers 5 and adjust strong sound wave sound pressure level in strong sound pressurized compartment and frequency values by computer 8 to facilitate, the accuracy that has improved wine ageing with this, has guaranteed the quality of production.
Operating above-mentioned strong sound wave loading drinks urges the device, method of ageing as follows:
(1). open computer 8, open acoustic measurement instrument 10, check the data acquisition and monitoring circuit being connected between acoustic measurement instrument 10 and computer 8, whether working properly by acoustic measurement instrument 10 inspection sound transducers 9, and carry out sound pressure level calibration;
(2). open ethyl acetate survey meter 6, check the data acquisition and monitoring circuit being connected between ethyl acetate survey meter 6 and computer 8, whether working properly by ethyl acetate survey meter 6 inspection ethyl acetate sensors 7;
(3). the wine for the treatment of ageing is positioned in strong sound pressurized compartment 2;
(4). open sound-source signal producer 5, check the signal line between sound-source signal producer 5 and computer 8; By computer 8, control sound-source signal producer 5 afterwards and produce pink noise;
(5). open air compressor, compressed air produces strong sound wave by compressed-air loudspeaker 1 at a high speed, and strong sound wave enters strong sound pressurized compartment and carries out wine ageing;
(6). sound transducer 9 Real-Time Monitoring sound pressure levels also feed back to demonstration on computer 8, and it is 165dB that computer 8 is controlled sound-source signal producers 5 adjusting sound pressure levels;
(7). computer 8 is controlled the frequency that sound-source signal producer 5 regulates strong sound wave, until the drinks liquid in sealed chamber produces vibrations uniformly;
(8). work after 15 minutes, closing device takes out wine from strong sound pressurized compartment.
Table 2
Known by table 2, every hundred people of its ageing effect of 15 minutes of ageing that accelerate wine under the acoustic pressure condition of 165dB have 89 people to think that it is identical with the mouthfeel of the wine of natural ageing in 20 years, and promoting ageing in the time of 20 minutes the promoting ageing with respect to 15 minutes only increased by 2 percentage points, therefore learn by experiment, the digestion time of 15 minutes is optimal selection, can guarantee that drinking utensils after ageing has sweet-smelling, sweet, soft characteristic, can save the production time again, enhance productivity.
Claims (6)
1. strong sound wave loads drinks and urges an aging method, it is characterized in that: comprise the steps:
A) strong sound wave generating unit is connected in a sealed chamber;
B) wine newly distilling is inserted in sealed chamber;
C) open strong sound wave generating unit and make it to produce strong sound wave;
D) strong sound wave being entered in annular seal space makes drinks liquid produce cavitation phenomenon;
E) through certain promoting ageing, after the time, close strong sound wave generating unit;
The strong sound wave sound pressure that described strong sound wave phonation unit produces is 140dB-180dB, and its frequency is 500Hz-1500Hz, and described digestion time is 5-20 minute.
2. strong sound wave according to claim 1 loads drinks and urges aging method, it is characterized in that: sound pressure is 165dB, adjusts the frequency of strong sound wave, until the drinks liquid in sealed chamber produces vibrations uniformly.
3. strong sound wave according to claim 1 and 2 loads drinks and urges aging method, it is characterized in that: strong sound wave make drinks liquid measure drinks liquid in real time in producing cavitation processes in ethyl acetate concentration.
4. strong sound wave according to claim 3 loads drinks and urges aging method, it is characterized in that: at strong sound wave, make to measure in real time strong sound wave sound pressure in drinks liquid generation cavitation processes.
5. one kind loads for strong sound wave claimed in claim 1 the equipment that drinks is urged aging method, it is characterized in that: comprise the strong sound pressurized compartment (2) with sealed cavity, the sourdine (3) that is connected in the strong sound wave generating unit of strong sound pressurized compartment (2) front end and is connected in strong sound pressurized compartment (2) rear end, described strong sound wave generating unit comprises compressed-air loudspeaker (1), sound-source signal producer (5), computer (8) and the compression gas tank for storing compressed air (4) that is connected in compressed-air loudspeaker (1) by tracheae, the output terminal of described sound-source signal producer (5) is electrically connected on compressed-air loudspeaker (1) by signal wire, its input terminus is electrically connected on computer (8) by signal wire, described compression gas tank (4) is connected with air compressor by tracheae, ethyl acetate sensor (7) is installed in described strong sound pressurized compartment (2), described ethyl acetate sensor (7) is electrically connected on ethyl acetate survey meter (6), described ethyl acetate survey meter (6) is electrically connected on computer (8).
6. equipment according to claim 5, it is characterized in that: sound transducer (9) is installed in described strong sound pressurized compartment (2), described sound transducer (9) is electrically connected on acoustic measurement instrument (10), and described acoustic measurement instrument (10) is electrically connected on computer (8).
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310103037.2A CN103205355B (en) | 2013-03-28 | 2013-03-28 | Strong acoustic loading wine aging method and apparatus for the method |
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| CN201310103037.2A CN103205355B (en) | 2013-03-28 | 2013-03-28 | Strong acoustic loading wine aging method and apparatus for the method |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105400677B (en) * | 2015-12-25 | 2018-09-04 | 宜宾金喜来酒业有限公司 | A kind of foraging white spirit system |
| US20200071645A1 (en) * | 2018-08-29 | 2020-03-05 | Meyer Sound Laboratories, Incorporated | Apparatus and method for modifying a responsive liquid held in a liquid container having resonant frequencies in the audio frequency range |
| CN109517712A (en) * | 2018-12-25 | 2019-03-26 | 周相真 | A kind of method and apparatus of new wine accelerated ageing |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2175231Y (en) * | 1993-12-24 | 1994-08-24 | 李全庆 | Equipment for ageing of alcoholic beverage |
| CN2428952Y (en) * | 2000-02-02 | 2001-05-09 | 王德全 | Multifunctional adjustable apparatus for establishing magnetic pulses, electric fields and acoustic fields |
| CN201753351U (en) * | 2010-07-27 | 2011-03-02 | 武汉嘉鹏电子有限公司 | Wine aging device |
| CN203128538U (en) * | 2013-03-28 | 2013-08-14 | 王勇 | Strong sound wave loading wine aging accelerating equipment |
-
2013
- 2013-03-28 CN CN201310103037.2A patent/CN103205355B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2175231Y (en) * | 1993-12-24 | 1994-08-24 | 李全庆 | Equipment for ageing of alcoholic beverage |
| CN2428952Y (en) * | 2000-02-02 | 2001-05-09 | 王德全 | Multifunctional adjustable apparatus for establishing magnetic pulses, electric fields and acoustic fields |
| CN201753351U (en) * | 2010-07-27 | 2011-03-02 | 武汉嘉鹏电子有限公司 | Wine aging device |
| CN203128538U (en) * | 2013-03-28 | 2013-08-14 | 王勇 | Strong sound wave loading wine aging accelerating equipment |
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