CN103131303B - A kind of powder coating containing Vanay - Google Patents
A kind of powder coating containing Vanay Download PDFInfo
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- CN103131303B CN103131303B CN201310040649.1A CN201310040649A CN103131303B CN 103131303 B CN103131303 B CN 103131303B CN 201310040649 A CN201310040649 A CN 201310040649A CN 103131303 B CN103131303 B CN 103131303B
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- CN
- China
- Prior art keywords
- vanay
- powder
- powder coating
- coating containing
- raw material
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000000843 powder Substances 0.000 title claims abstract description 31
- 239000011248 coating agent Substances 0.000 title claims abstract description 21
- 238000000576 coating method Methods 0.000 title claims abstract description 21
- URAYPUMNDPQOKB-UHFFFAOYSA-N triacetin Chemical compound CC(=O)OCC(OC(C)=O)COC(C)=O URAYPUMNDPQOKB-UHFFFAOYSA-N 0.000 title claims abstract description 18
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 10
- 239000002994 raw material Substances 0.000 claims abstract description 10
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000012764 mineral filler Substances 0.000 claims abstract description 7
- 239000002518 antifoaming agent Substances 0.000 claims abstract description 6
- 229920001296 polysiloxane Polymers 0.000 claims abstract description 6
- XGQJGMGAMHFMAO-UHFFFAOYSA-N 1,3,4,6-tetrakis(methoxymethyl)-3a,6a-dihydroimidazo[4,5-d]imidazole-2,5-dione Chemical compound COCN1C(=O)N(COC)C2C1N(COC)C(=O)N2COC XGQJGMGAMHFMAO-UHFFFAOYSA-N 0.000 claims abstract description 4
- CMQUQOHNANGDOR-UHFFFAOYSA-N 2,3-dibromo-4-(2,4-dibromo-5-hydroxyphenyl)phenol Chemical compound BrC1=C(Br)C(O)=CC=C1C1=CC(O)=C(Br)C=C1Br CMQUQOHNANGDOR-UHFFFAOYSA-N 0.000 claims abstract description 4
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims abstract description 4
- 239000004925 Acrylic resin Substances 0.000 claims abstract description 4
- 229920000178 Acrylic resin Polymers 0.000 claims abstract description 4
- 235000002918 Fraxinus excelsior Nutrition 0.000 claims abstract description 4
- 235000007164 Oryza sativa Nutrition 0.000 claims abstract description 4
- 239000004372 Polyvinyl alcohol Substances 0.000 claims abstract description 4
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000002956 ash Substances 0.000 claims abstract description 4
- 239000003822 epoxy resin Substances 0.000 claims abstract description 4
- 239000010903 husk Substances 0.000 claims abstract description 4
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 claims abstract description 4
- 239000000347 magnesium hydroxide Substances 0.000 claims abstract description 4
- 229910001862 magnesium hydroxide Inorganic materials 0.000 claims abstract description 4
- SSDSCDGVMJFTEQ-UHFFFAOYSA-N octadecyl 3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoate Chemical compound CCCCCCCCCCCCCCCCCCOC(=O)CCC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 SSDSCDGVMJFTEQ-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229920000647 polyepoxide Polymers 0.000 claims abstract description 4
- 229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 4
- 235000009566 rice Nutrition 0.000 claims abstract description 4
- 240000007594 Oryza sativa Species 0.000 claims abstract 2
- WUKWITHWXAAZEY-UHFFFAOYSA-L calcium difluoride Chemical compound [F-].[F-].[Ca+2] WUKWITHWXAAZEY-UHFFFAOYSA-L 0.000 claims description 12
- 239000010436 fluorite Substances 0.000 claims description 12
- 239000002893 slag Substances 0.000 claims description 12
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 6
- 239000012467 final product Substances 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- 238000002360 preparation method Methods 0.000 claims description 6
- 239000007787 solid Substances 0.000 claims description 4
- 239000002253 acid Substances 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 239000007822 coupling agent Substances 0.000 claims description 3
- 239000008367 deionised water Substances 0.000 claims description 3
- 229910021641 deionized water Inorganic materials 0.000 claims description 3
- 150000002148 esters Chemical class 0.000 claims description 3
- 239000010433 feldspar Substances 0.000 claims description 3
- 238000013467 fragmentation Methods 0.000 claims description 3
- 238000006062 fragmentation reaction Methods 0.000 claims description 3
- 239000010445 mica Substances 0.000 claims description 3
- 229910052618 mica group Inorganic materials 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 230000007935 neutral effect Effects 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 238000005303 weighing Methods 0.000 claims description 3
- 238000010298 pulverizing process Methods 0.000 claims description 2
- 230000007613 environmental effect Effects 0.000 abstract description 3
- 239000003063 flame retardant Substances 0.000 abstract description 2
- 231100000252 nontoxic Toxicity 0.000 abstract description 2
- 230000003000 nontoxic effect Effects 0.000 abstract description 2
- 241000209094 Oryza Species 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 230000032683 aging Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 238000010422 painting Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
Landscapes
- Paints Or Removers (AREA)
Abstract
The invention discloses a kind of powder coating containing Vanay, obtained by the raw material of following weight parts: bisphenol A type epoxy resin 98-105, acrylic resin 60-75, polyvinyl alcohol 10-20, Natvosol 1.5-3, mineral filler 110-115, tetramethoxymethylglycoluril 10-12, acrylate flow agent 0.5-1.3, silicone antifoam agent 1-2, st-yrax 0.7-1.2, nanometer rice husk ashes 1-2, tetrabromo-bisphenol? 0.3-0.6, magnesium hydroxide 0.8-1.2, anatase thpe white powder 3-5, Vanay 1-2, antioxidant 1076? 1-2.Environmental protection of the present invention, physical strength is high; Both easy to use, nontoxic fire-retardant again, weathering resistance is strong.
Description
Technical field
The present invention relates to paint field, is exactly a kind of powder coating containing Vanay.
Background technology
Powder coating is a kind of novel not containing solvent 100% solid powdery coating.There is solvent-free, pollution-free, recyclable, environmental protection, the saving energy and resource, reduce labor intensity and film physical strength high.Powder coating is form diverse with general coating, and it exists with the state of fines.Owing to not using solvent, so be called powder coating.The principal feature of powder coating has: have nuisanceless, high-level efficiency, saving resource feature.
Summary of the invention
The object of the present invention is to provide a kind of powder coating containing Vanay.
Above-mentioned purpose is realized by following scheme:
A kind of powder coating containing Vanay, it is characterized in that, obtained by the raw material of following weight parts: bisphenol A type epoxy resin 98-105, acrylic resin 60-75, polyvinyl alcohol 10-20, Natvosol 1.5-3, mineral filler 110-115, tetramethoxymethylglycoluril 10-12, acrylate flow agent 0.5-1.3, silicone antifoam agent 1-2, st-yrax 0.7-1.2, nanometer rice husk ashes 1-2, tetrabromo-bisphenol 0.3-0.6, magnesium hydroxide 0.8-1.2, anatase thpe white powder 3-5, Vanay 1-2, antioxidant 1076 1-2.
Described a kind of powder coating containing Vanay, is characterized in that: described mineral filler is made up of the raw material of following weight parts: feldspar in powder 30-32, modified Nano Fluorite slag 10-12, mica powder 10-15;
The preparation method of described modified Nano Fluorite slag is: after Fluorite slag is soaked 5-7 hour in the hydrochloric acid soln of 10-12%, take out, deionized water wash to neutral, after at 500-600 DEG C, calcine 3-5 hour, after cooling, fragmentation, crosses 100-200 mesh sieve, then adds the acid esters coupling agent dl-411 being equivalent to Fluorite slag weight 1.5-3%, after mixing, dry, grind to form nanometer powder, to obtain final product.
Described a kind of powder coating containing Vanay, is characterized in that:
Preparation method comprises the following steps:
(1), by each raw material of described weight part accurate weighing, under 500-600 rev/min, be uniformly mixed 3-4 minute, under 3800-4500 rev/min, be uniformly mixed 8-10 minute, after under 400-500 rev/min, be uniformly mixed 1-2 minute, stop stir, obtain mixture;
(2), by mixture forcing machine extrude at the temperature of 100-115 DEG C, obtain extruded stock;
(3), extruded stock crosses 100-200 mesh sieve after pulverizing, and to obtain final product.
Described a kind of powder coating containing Vanay, is characterized in that:
Described silicone antifoam agent solid content is 25%.
Beneficial effect of the present invention is: environmental protection of the present invention, and physical strength is high; Both easy to use, nontoxic fire-retardant again, weathering resistance is strong.
Embodiment
A powder coating containing Vanay is obtained by the raw material of following weight parts (kg): bisphenol A type epoxy resin 98, acrylic resin 72, polyvinyl alcohol 15, Natvosol 1.9, mineral filler 110, tetramethoxymethylglycoluril 12, acrylate flow agent 1.3, solid content is the silicone antifoam agent 1.4 of 25%, st-yrax 0.7, nanometer rice husk ashes 2, tetrabromo-bisphenol 0.6, magnesium hydroxide 1.2, anatase thpe white powder 5, Vanay 1, antioxidant 1076 1.2.
Described mineral filler is made up of the raw material of following weight parts: feldspar in powder 32, modified Nano Fluorite slag 12, mica powder 15;
The preparation method of described modified Nano Fluorite slag is: after Fluorite slag is soaked 7 hours in the hydrochloric acid soln of 12%, take out, deionized water wash to neutral, after calcine 5 hours at 600 DEG C, after cooling, fragmentation, crosses 200 mesh sieves, then adds the acid esters coupling agent dl-411 being equivalent to Fluorite slag weight 1.5%, after mixing, dry, grind to form nanometer powder, to obtain final product.
Described a kind of powder coating containing Vanay, preparation method comprises the following steps:
(1), by each raw material of described weight part accurate weighing, be uniformly mixed 3.5 minutes under prior to 500 revs/min, under 4200 revs/min, be uniformly mixed 10 minutes, after under 400 revs/min, be uniformly mixed 1 minute, stop stir, obtain mixture;
(2), by mixture forcing machine extrude at the temperature of 115 DEG C, obtain extruded stock;
(3), extruded stock pulverize after cross 140 mesh sieves, to obtain final product.
Adopt high pressure electrostatic painting on foundry goods the present embodiment gained coating, voltage is 60KV, and average film thickness is 65-75 micron, and condition of cure is 180 DEG C of bakings 20 minutes;
Performance index are as follows:
According to GB/T1732 test, shock resistance >=50kg.cm;
According to GB/T6739 test, pencil hardness >=H level;
480hQUV-B accelerated light ageing experimental test obtains, and protects light rate and reaches 87%.
Gained coatingsurface is smooth, bubble-free, particle, shrinkage cavity, pin hole.
Claims (3)
1. the powder coating containing Vanay, it is characterized in that, obtained by the raw material of following weight parts: bisphenol A type epoxy resin 98-105, acrylic resin 60-75, polyvinyl alcohol 10-20, Natvosol 1.5-3, mineral filler 110-115, tetramethoxymethylglycoluril 10-12, acrylate flow agent 0.5-1.3, silicone antifoam agent 1-2, st-yrax 0.7-1.2, nanometer rice husk ashes 1-2, tetrabromo-bisphenol 0.3-0.6, magnesium hydroxide 0.8-1.2, anatase thpe white powder 3-5, Vanay 1-2, antioxidant 1076 1-2;
Described mineral filler is made up of the raw material of following weight parts: feldspar in powder 30-32, modified Nano Fluorite slag 10-12, mica powder 10-15;
The preparation method of described modified Nano Fluorite slag is: after Fluorite slag is soaked 5-7 hour in the hydrochloric acid soln of 10-12%, take out, deionized water wash to neutral, after at 500-600 DEG C, calcine 3-5 hour, after cooling, fragmentation, crosses 100-200 mesh sieve, then adds the acid esters coupling agent dl-411 being equivalent to Fluorite slag weight 1.5-3%, after mixing, dry, grind to form nanometer powder, to obtain final product.
2. a kind of powder coating containing Vanay according to claim 1, is characterized in that: preparation method comprises the following steps:
(1), by each raw material of described weight part accurate weighing, under 500-600 rev/min, be uniformly mixed 3-4 minute, under 3800-4500 rev/min, be uniformly mixed 8-10 minute, after under 400-500 rev/min, be uniformly mixed 1-2 minute, stop stir, obtain mixture;
(2), by mixture forcing machine extrude at the temperature of 100-115 DEG C, obtain extruded stock;
(3), extruded stock crosses 100-200 mesh sieve after pulverizing, and to obtain final product.
3. a kind of powder coating containing Vanay according to claim 1, is characterized in that: described silicone antifoam agent solid content is 25%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310040649.1A CN103131303B (en) | 2013-02-03 | 2013-02-03 | A kind of powder coating containing Vanay |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310040649.1A CN103131303B (en) | 2013-02-03 | 2013-02-03 | A kind of powder coating containing Vanay |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103131303A CN103131303A (en) | 2013-06-05 |
| CN103131303B true CN103131303B (en) | 2015-11-11 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310040649.1A Expired - Fee Related CN103131303B (en) | 2013-02-03 | 2013-02-03 | A kind of powder coating containing Vanay |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103131303B (en) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103483952B (en) * | 2013-09-03 | 2016-06-22 | 安徽精一机械设备有限公司 | A kind of Acrylic transparent powder paint |
| CN104387955A (en) * | 2014-12-07 | 2015-03-04 | 李永志 | Anti-mold automotive powder coating with good adhesive force |
| CN105623468A (en) * | 2016-01-19 | 2016-06-01 | 安徽华辉塑业科技股份有限公司 | Flame-retardant heat insulation coating and production method thereof |
| CN105524534A (en) * | 2016-01-19 | 2016-04-27 | 安徽华辉塑业科技股份有限公司 | Epoxy powder coating capable of purifying air and preparation method and application thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS49121830A (en) * | 1973-03-27 | 1974-11-21 | ||
| CN101001929A (en) * | 2004-08-10 | 2007-07-18 | 中国涂料株式会社 | High-solid anticorrosive coating composition, high-solid rapidly-curable anticorrosive coating composition, method of coating ship or the like, high-solid anticorrosive film and rapidly cured high-sol |
| CN101519544A (en) * | 2009-04-03 | 2009-09-02 | 丹阳市科瑞特粉末新材料有限公司 | Ultra-low temperature epoxy resin nylon hybrid thermosetting powder coating and method for preparing same |
-
2013
- 2013-02-03 CN CN201310040649.1A patent/CN103131303B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS49121830A (en) * | 1973-03-27 | 1974-11-21 | ||
| CN101001929A (en) * | 2004-08-10 | 2007-07-18 | 中国涂料株式会社 | High-solid anticorrosive coating composition, high-solid rapidly-curable anticorrosive coating composition, method of coating ship or the like, high-solid anticorrosive film and rapidly cured high-sol |
| CN101519544A (en) * | 2009-04-03 | 2009-09-02 | 丹阳市科瑞特粉末新材料有限公司 | Ultra-low temperature epoxy resin nylon hybrid thermosetting powder coating and method for preparing same |
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| Publication number | Publication date |
|---|---|
| CN103131303A (en) | 2013-06-05 |
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Legal Events
| Date | Code | Title | Description |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CB03 | Change of inventor or designer information |
Inventor after: Liao Dongdi Inventor before: Ni Jinpei |
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| CB03 | Change of inventor or designer information | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20171222 Address after: 528318 Guangdong Foshan city Shunde District Longjiang town Wan an industrial district Patentee after: Foshan City Shunde District Longjiang Town Wanan Paint Co., Ltd. Address before: The new town of Anhui province Wuhu City fan 241200 Fanchang County Economic Development Office Patentee before: Ni Jinpei |
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| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20201217 Address after: No.1 Zhenxing Road, Yandu District, Yancheng City, Jiangsu Province Patentee after: Yancheng high tech Zone Investment Group Co.,Ltd. Address before: 528318 Industrial Zone, Wan'an village, Longjiang Town, Shunde District, Foshan City, Guangdong Province Patentee before: Foshan City Shunde District Longjiang Town Wanan Paint Co.,Ltd. |
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| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20151111 Termination date: 20210203 |