CN102960823A - Compound sweetener suitable for sour drinks and preparation method of sweetener - Google Patents
Compound sweetener suitable for sour drinks and preparation method of sweetener Download PDFInfo
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- CN102960823A CN102960823A CN2012105007737A CN201210500773A CN102960823A CN 102960823 A CN102960823 A CN 102960823A CN 2012105007737 A CN2012105007737 A CN 2012105007737A CN 201210500773 A CN201210500773 A CN 201210500773A CN 102960823 A CN102960823 A CN 102960823A
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Abstract
The invention relates to a compound sweetener suitable for sour drinks and a preparation method of the sweetener. The compound sweetener is prepared from the following components: 3.33-8.33% of sucralose, 87.82-95.1% of glucose, 1.5-3.5% of maltodextrin, 0.01-0.05% of sclareolide, 0.01-0.05% of 2-acetylpyrrole and 0.05-0.25% of emulsifier; and the preparation method comprises the following process of: putting glucose and sucralose accounting for 40-60% of the total quantity into a multidimensional mixer for premixing at first; forming stable emulsion by the residual sucralose with other auxiliary sweeteners through emulsification; feeding the premixed mixture into a fluidized bed from the bottom of the spray fluidized bed under positive pressure so that the mixture flows in an accelerated manner from bottom to top; applying negative pressure to the upper part of the spray fluidized bed for vibration from top to bottom so that the mixture is boiled up and down in the fluidized bed to form fine sugar particles; and continuously spraying and dispersing the emulsion onto fine sugar particles in the fluidized bed by means of multi-point spray guns arranged on the sidewalls of the fluidized bed, thereby obtaining the compound sweetener.
Description
Technical field
The present invention relates to a kind of food additives, be specifically related to applicable composite sweetener of a kind of acidic beverages and preparation method thereof.
Background technology
In the last few years, raising along with expanding economy and people's lives wealth, obesity, hypertension, diabetes, carious tooth etc. become the height morbidity among the crowd, and the generation of these high morbidities is considered to especially with the sucrose Excessive Intake substantial connection is arranged with eating habit and diet structure.Therefore, as the sweetener of food additives, one of its development priority is exactly safe, without nutritive value, empty calory or functional high sweetener extremely low in calories.The characteristics of functional high sweetener are use safe, and consumption is few, and sugariness is high, and use cost is generally all far below sucrose, and this also is the power place that Food Science man continually develops novel high-intensity sweetener.At present, about 20 kinds of the granted high sweetener in countries in the world obtains that kind that the majority state approval allows to use mainly contains that saccharin sodium, honey element, 3,4-Dihydro-6-methyl-1,2,3-oxathiazin-4-one 2,2-dioxide potassium salt, Aspartame, Sucralose, alitame, knob are sweet, glycyrrhizin, stevioside, Momordica grosvenori is sweet and Talin etc.These high sweeteners have plenty of artificial synthetic, and are sweet etc. such as Aspartame, Sucralose, knob; What have then is natural extract, sweet etc. such as sky chrysanthemum glycosides and arhat.No matter be artificial synthesis edulcorant or natural extraction sweetener, at sugariness, sweet taste, stable aspects its pluses and minuses arranged respectively all, therefore, want to give full play to the optimal efficacy of these sweeteners, reduce cost, the most frequently used means are exactly compound at present.By carrying out various sweeteners or sweet substance compound, bring into play may exist between the various sweeteners synergistic function, in the hope of as far as possible approaching or satisfy the requirement of desirable sweetener: safety non-toxic, sweet taste is pure similar to sucrose (this is to be popular generally accepted sweet tastes), high sugariness, low heat value or without calorific value, stable height, unlikely dental caries, reduction cost.
In the prior art, the composite sweetener take Sucralose as main sweetening material is arranged, in the time of in being applied in the acidic beverages such as soda or fruit drink, it is that acidic beverages brings sugariness that these composite sweeteners can substitute white granulated sugar.But present Sucralose class composite sweetener also exist frontly sweetly come slowly, rear sweet and problem that pleasant impression is heavier, its sweet taste is compared with traditional white granulated sugar and is also had larger difference in the time of in being applied in acidic beverages, so that the mouthfeel of acidic beverages is not fine and do not liked by the consumer.
Composite sweetener take Sucralose as main sweetening material in the prior art, can process by method or the spray-dired method of substep of simple blend, the composite sweetener that the simple blend method makes is with low cost, but be difficult to guarantee that main sweetening material Sucralose can be uniformly dispersed, and this point can affect the quality of composite sweetener product to a great extent.The spray-dired method of substep is that substep is dissolved in main sweetening material and each auxiliary sweetening material in the deionized water in batches, then the method by the wet spray drying is coated on each composition material on the granular sweetener by spraying respectively, the composite sweetener product sweetness that this method makes is uniformly dispersed, instant capacity is good, quality is better than the composite sweetener product that additive method makes, but its shortcoming is: material loss, the loss of especially main sweetening material is larger, machinery equipment power consumption is too high, the cost of product is significantly increased, and therefore this method also has been subject to certain restriction in implementation process.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, provide that a kind of cost is cheaper, the sugariness uniformity better and be particularly suitable for being applied to composite sweetener in the acidic beverages and preparation method thereof.
Purpose of the present invention is achieved through the following technical solutions:
The composite sweetener that a kind of acidic beverages is applicable comprises following percentage by weight composition: Sucralose 3.33～8.33%, glucose 87.82 ~ 95.1%, maltodextrin 1.5 ~ 3.5%, Clary sage lactone 0.01～0.05%, 2-acetyl pyrrole 0.01～0.05%, emulsifying agent 0.05～0.25%; Its preparation method comprises following processing step:
1. glucose and the Sucralose that accounts for total amount 40 ~ 60% are dropped in the Multidimensionblender, mixed 20 ~ 30 minutes with the progression of 800 ~ 1000rpm, obtain the mixed material of Sucralose and glucose;
2. maltodextrin, Clary sage lactone, 2-acetyl pyrrole, emulsifying agent, remaining Sucralose are mixed with water, obtain stable emulsion;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny Icing Sugar grain; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared emulsion continuously spraying be distributed on the Icing Sugar grain in the fluid bed, by heated-air drying, obtain described composite sweetener again.
According to the present invention, described emulsifying agent can be selected from sapn, tween or sucrose ester.
The preparation method of the composite sweetener that a kind of acidic beverages of the present invention is applicable comprises following processing step:
1. glucose and the Sucralose that accounts for total amount 40 ~ 60% are dropped in the Multidimensionblender, mixed 20 ~ 30 minutes with the progression of 800 ~ 1000rpm, obtain the mixed material of Sucralose and glucose;
2. maltodextrin, Clary sage lactone, 2-acetyl pyrrole, emulsifying agent, remaining Sucralose are mixed with water, obtain stable emulsion;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny Icing Sugar grain; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared emulsion continuously spraying be distributed on the Icing Sugar grain in the fluid bed, by heated-air drying, obtain described composite sweetener again.
Further, the preparation method of the composite sweetener that above-mentioned a kind of acidic beverages is applicable, step 3. in, the EAT of fluid bed is controlled at 40 ~ 90 ℃.
Again further, the preparation method of the composite sweetener that above-mentioned a kind of acidic beverages is applicable, step 3. in, when the emulsion spraying disperseed, the EAT of control fluid bed was between 40 ~ 70 ℃, the EAT of control fluid bed is at 70 ~ 90 ℃ during heated-air drying.
The substantive distinguishing features that technical solution of the present invention is outstanding and significant progressive being mainly reflected in:
The composition of raw materials of composite sweetener of the present invention cooperates by Clary sage lactone and 2-acetyl pyrrole to be modified the front sweet and pleasant impression of Sucralose; can effectively the front sweet of composite sweetener be shifted to an earlier date; cover the rear sweet and pleasant impression of Sucralose; make the mouthfeel of composite sweetener more near sucrose; in the time of in being applied to the acidic beverages such as soda, fruit juice, make the taste of drink more meet consumer's taste demand.
The preparation method of composite sweetener of the present invention carries out sweet the input in the Multidimensionblender with glucose of the part master of composite sweetener tentatively to mix first, then the sweet auxiliary sweetening material with other of remaining master is formed stable emulsion by emulsification, and disperse dry by the disposable spraying of advanced negative-pressure fluidized bed apparatus, make it to be coated on just mixed mixed material surface, obtain the Fluffy powder grain compound sweetener product.The present invention compares with the method for prior art simple blend, and the product instant capacity that obtains, sugariness dispersiveness etc. have significantly lifting, have good quality; And with prior art in batches spray-dired method compare, can greatly shorten the process-cycle again, the amount of saving energy has reduced production cost (about 60 ~ 75 minutes of product manufacturing cycle of the present invention, and in batches about 2 ~ 3 hours of the manufacturing cycle of spray drying process).
The specific embodiment
The composite sweetener that a kind of acidic beverages of the present invention is applicable, its composition is: Sucralose 3.33～8.33%, glucose 87.82 ~ 95.1%, maltodextrin 1.5 ~ 3.5%, Clary sage lactone 0.01～0.05%, 2-acetyl pyrrole 0.01～0.05%, emulsifying agent 0.05～0.25%.
Among the present invention, Clary sage lactone is mainly synthetic by sclareol, and it is a kind of good fragrance-enhancing tobacco flavouring.In blended type cigarette, can cover the thick assorted gas of tobacco, to improve and to improve flavor quality, give the characteristic perfume of tobacco happiness, make softer, the pure continuous entrance of cigarette.Clary sage lactone is mainly used among tobacco essence, tea, maple, pepper and the hot Flavor at present.The 2-acetyl pyrrole is a kind of water-soluble white, needle-shaped crystals body, and it has fragrance like walnut, Radix Glycyrrhizae, toast bread, the stir-fry fibert, can be used as the allotment of flavoring essence.
The preparation technology of this composite sweetener is as follows: first glucose and the Sucralose that accounts for total amount 40 ~ 60% are dropped in the Multidimensionblender, mixed 20 ~ 30 minutes with the progression of 800 ~ 1000rpm, obtain the mixed material of Sucralose and glucose; With maltodextrin, Clary sage lactone, 2-acetyl pyrrole, emulsifying agent, remaining Sucralose and deionized water mix and blend, obtain stable emulsion again; Then mixed material is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, the EAT of fluid bed is controlled at 40 ~ 90 ℃, forms tiny Icing Sugar grain; Multiple spot spray gun by the fluid bed sidepiece with prepared stable emulsion continuously spraying be distributed on the Icing Sugar grain in the fluid bed, when the emulsion spraying disperses, the EAT of control fluid bed is between 40 ~ 70 ℃, pass through again heated-air drying, the EAT of control fluid bed obtains described composite sweetener at 70 ~ 90 ℃ during heated-air drying.
Multidimensionblender used in the present invention adopts commercial 200 feather weight Multidimensionblenders, rotating speed level journey is 200 ~ 1800rpm, barrel is two taper, middle column, and during work, this Multidimensionblender can make the material in the barrel collide, pulverize and mix from a plurality of angles.
Embodiment 1:
(1) get in 95.04 kilograms of glucose, 1.7 kilograms of inputs of the Sucralose Multidimensionblender, the progression of control Multidimensionblender is 1000rpm, mixes 25 minutes, obtains the mixed material of Sucralose and glucose;
(2) 1.63 kilograms of 1.5 kilograms of maltodextrins, 0.02 kilogram of Clary sage lactone, 0.01 kilogram of 2-acetyl pyrrole, 0.1 kilogram of emulsifier span, remaining Sucralose are mixed with deionized water, the intensification stirring and dissolving obtains stable emulsion;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny Icing Sugar grain; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared stable emulsion of step (2) on the interior Icing Sugar grain of fluid bed, the EAT of control fluid bed is between 40 ~ 70 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 70 ~ 90 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
Embodiment 2:
(1) get in 92.79 kilograms of glucose, 5 kilograms of inputs of the Sucralose Multidimensionblender, the progression of control Multidimensionblender is 1000rpm, mixes 25 minutes, obtains the mixed material of Sucralose and glucose;
(2) 2.8 kilograms of 2 kilograms of maltodextrins, 0.03 kilogram of Clary sage lactone, 0.03 kilogram of 2-acetyl pyrrole, 0.15 kilogram of emulsifier span, remaining Sucralose are mixed with deionized water, the intensification stirring and dissolving obtains stable emulsion;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny Icing Sugar grain; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared stable emulsion of step (2) on the interior Icing Sugar grain of fluid bed, the EAT of control fluid bed is between 40 ~ 70 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 70 ~ 90 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
Embodiment 3:
(1) get in 90.55 kilograms of glucose, 3 kilograms of inputs of the Sucralose Multidimensionblender, the progression of control Multidimensionblender is 1000rpm, mixes 20 minutes, obtains the mixed material of Sucralose and glucose;
(2) 3.67 kilograms of 2.5 kilograms of maltodextrins, 0.04 kilogram of Clary sage lactone, 0.04 kilogram of 2-acetyl pyrrole, 0.2 kilogram of emulsifier span, remaining Sucralose are mixed with deionized water, the intensification stirring and dissolving obtains stable emulsion;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny Icing Sugar grain; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared stable emulsion of step (2) on the interior Icing Sugar grain of fluid bed, the EAT of control fluid bed is between 40 ~ 70 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 70 ~ 90 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
Embodiment 4:
(1) get in 88.32 kilograms of glucose, 4.33 kilograms of inputs of the Sucralose Multidimensionblender, the progression of control Multidimensionblender is 1000rpm, mixes 20 minutes, obtains the mixed material of Sucralose and glucose;
(2) 4 kilograms of 3 kilograms of maltodextrins, 0.05 kilogram of Clary sage lactone, 0.05 kilogram of 2-acetyl pyrrole, 0.25 kilogram of emulsifier span, remaining Sucralose are mixed with deionized water, the intensification stirring and dissolving obtains stable emulsion;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny Icing Sugar grain; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared stable emulsion of step (2) on the interior Icing Sugar grain of fluid bed, the EAT of control fluid bed is between 40 ~ 70 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 70 ~ 90 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
The composite sweetener that adopts technical solution of the present invention to obtain, its main performance index sees Table 1.
Table 1
The composition of raw materials of composite sweetener of the present invention cooperates by Clary sage lactone and 2-acetyl pyrrole to be modified the front sweet and pleasant impression of Sucralose; can effectively the front sweet of composite sweetener be shifted to an earlier date; cover the rear sweet and pleasant impression of Sucralose, make the mouthfeel of composite sweetener more near sucrose.Composition collocation in the composition of raw materials of the present invention is scientific and reasonable, the pro rate of each composition is at optimum range, be particularly suitable in the acidic beverages such as soda, fruit juice, using, partly or entirely replace white granulated sugar or HFCS, produce the low-sugar-content and low-calorie drink that meets concept of modern health.
The present invention drops into the main sweetening material of the part of composite sweetener in the Multidimensionblender with glucose first and carries out tentatively mixing, then remaining main sweetening material and other auxiliary sweetening materials are formed stable emulsion by emulsification, and disperse dry by the disposable spraying of advanced negative-pressure fluidized bed apparatus, make it to be coated on just mixed mixed material surface, obtain the Fluffy powder grain compound sweetener product.The present invention compares with the method for prior art simple blend, and the product instant capacity that obtains, sugariness dispersiveness etc. have significantly lifting, have good quality; And with prior art in batches spray-dired method compare, can greatly shorten the process-cycle again, the amount of saving energy, reduced production cost (about 60 ~ 75 minutes of product manufacturing cycle of the present invention, and about 2 ~ 3 hours of the manufacturing cycle of spray drying process in batches, and the present invention just the mixed power consumption that uses Multidimensionblender be approximately fluidized bed with spraying electricity consumption of equipment amount 1/24).
The sugariness degree of modification of composite sweetener of the present invention can be adjusted by the consumption of Sucralose according to actual needs, and the present invention is fit to the composite sweetener of 20 ~ 50 times of sucrose sweetness of preparation usually.
What need to understand is: the above only is preferred embodiment of the present invention; for those skilled in the art; under the prerequisite that does not break away from the principle of the invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (5)
1. the composite sweetener that acidic beverages is applicable is characterized in that comprising following percentage by weight composition: Sucralose 3.33～8.33%, glucose 87.82 ~ 95.1%, maltodextrin 1.5 ~ 3.5%, Clary sage lactone 0.01～0.05%, 2-acetyl pyrrole 0.01～0.05%, emulsifying agent 0.05～0.25%; Its preparation method comprises following processing step:
1. glucose and the Sucralose that accounts for total amount 40 ~ 60% are dropped in the Multidimensionblender, mixed 20 ~ 30 minutes with the progression of 800 ~ 1000rpm, obtain the mixed material of Sucralose and glucose;
2. maltodextrin, Clary sage lactone, 2-acetyl pyrrole, emulsifying agent, remaining Sucralose are mixed with water, obtain stable emulsion;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny Icing Sugar grain; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared emulsion continuously spraying be distributed on the Icing Sugar grain in the fluid bed, by heated-air drying, obtain described composite sweetener again.
2. the applicable composite sweetener of a kind of acidic beverages according to claim 1, it is characterized in that: described emulsifying agent is sapn, tween or sucrose ester.
3. the preparation method of the applicable composite sweetener of a kind of acidic beverages claimed in claim 1 is characterized in that comprising following processing step:
1. glucose and the Sucralose that accounts for total amount 40 ~ 60% are dropped in the Multidimensionblender, mixed 20 ~ 30 minutes with the progression of 800 ~ 1000rpm, obtain the mixed material of Sucralose and glucose;
2. maltodextrin, Clary sage lactone, 2-acetyl pyrrole, emulsifying agent, remaining Sucralose are mixed with water, obtain stable emulsion;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny Icing Sugar grain; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared emulsion continuously spraying be distributed on the Icing Sugar grain in the fluid bed, by heated-air drying, obtain described composite sweetener again.
4. the preparation method of the applicable composite sweetener of a kind of acidic beverages according to claim 3 is characterized in that: step 3. in, the EAT of fluid bed is controlled at 40 ~ 90 ℃.
5. the preparation method of the applicable composite sweetener of a kind of acidic beverages according to claim 4, it is characterized in that: step 3. in, when the emulsion spraying disperseed, the EAT of control fluid bed was between 40 ~ 70 ℃, and the EAT of control fluid bed is at 70 ~ 90 ℃ during heated-air drying.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| WO2015071663A1 (en) * | 2013-11-13 | 2015-05-21 | Tate & Lyle Technology Limited | High intensity sweetener composition |
| EP3528641A4 (en) * | 2016-10-18 | 2020-06-03 | Breslin, Paul | Glucose beverage comprising exogenous flavor source and color |
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| CN101810313A (en) * | 2009-12-07 | 2010-08-25 | 苏州工业园区尚融科技有限公司 | Dessert sweetener and production process |
| CN102396695A (en) * | 2010-09-15 | 2012-04-04 | 长沙市龙润食品添加剂有限公司 | Composite sweetening agent |
| CN102415547A (en) * | 2011-12-09 | 2012-04-18 | 苏州工业园区尚融科技有限公司 | Compound sweetener and preparation method thereof |
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| CN1527672A (en) * | 2001-07-19 | 2004-09-08 | �Դ���� | Flavor-improving compositions and application thereof |
| CN101810313A (en) * | 2009-12-07 | 2010-08-25 | 苏州工业园区尚融科技有限公司 | Dessert sweetener and production process |
| CN102396695A (en) * | 2010-09-15 | 2012-04-04 | 长沙市龙润食品添加剂有限公司 | Composite sweetening agent |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| WO2015071663A1 (en) * | 2013-11-13 | 2015-05-21 | Tate & Lyle Technology Limited | High intensity sweetener composition |
| GB2534782A (en) * | 2013-11-13 | 2016-08-03 | Tate & Lyle Tech Ltd | High intensity sweetener composition |
| EP3528641A4 (en) * | 2016-10-18 | 2020-06-03 | Breslin, Paul | Glucose beverage comprising exogenous flavor source and color |
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Application publication date: 20130313 |