CN101836764B - Natural plant extract microcapsule and cigarette filter tip containing same - Google Patents
Natural plant extract microcapsule and cigarette filter tip containing same Download PDFInfo
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- CN101836764B CN101836764B CN2010101383934A CN201010138393A CN101836764B CN 101836764 B CN101836764 B CN 101836764B CN 2010101383934 A CN2010101383934 A CN 2010101383934A CN 201010138393 A CN201010138393 A CN 201010138393A CN 101836764 B CN101836764 B CN 101836764B
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Abstract
The invention discloses a natural plant extract microcapsule and a cigarette filter tip containing the same, which aims to solve the technical problem of reducing harmful components in cigarette smoke. The microcapsule of the invention consists of the following components in parts by weight: 1 to 1.5 parts of natural plant extract and 1 to 2 parts of a capsule material, wherein the natural plant is wintergreen, honeysuckle, mentha haplocalyx or miracle fruit. In the cigarette filter tip, the natural plant extract microcapsule is added in tows, and the tows and the microcapsule are in a mass ratio of 1-100:0.1-100. Compared with the prior art, active components extracted from the natural plant is made into the microcapsule, and the microcapsule is added into the tows of the cigarette filter tip to make the filter bar of the cigarette; in the smoking process, the smoke flavor is enriched, the quality and harmony of the cigarette smoke can be improved, and harmful components in the cigarette can be selectively reduced, body health of a smoker can be protected, and the cigarette level is increased.
Description
Technical field
The present invention relates to a kind of micro-capsule and the cigarette filter rod that contains this micro-capsule, particularly a kind of plant extracts micro-capsule and the cigaratte filter that contains this plant extracts micro-capsule.
Background technology
Various countries all take much count of the exploitation of filter tip at present, and tobacco company and cigarette all making great efforts exploitation composite cigarette filter tip capable rod, mainly are in filter rod, to add macromolecular material, activated carbon, nano material etc. with filter tip manufacturer both at home and abroad.The filter rod that adopts these materials to process can filter the gaseous component in the flue gas, but possibly cause inharmonious or because the safety problem that material itself brings of flue gas.Along with the contradiction between smoking and the health is constantly aggravated, a lot of cigarette function of use filter rods are wherein used maximum activated carbon filter rods, can bring uncomfortable carbon flavor, contaminated environment in making filter rod to flue gas.One Chinese patent application 200710053328.X disclose a kind of adopt synthetic macromolecule strand material dipping peppermint essence film forming as cigarette with the mouth rod, when suction, can effectively discharge peppermint, do not change the excellent performance of mouth.One Chinese patent application numbers 200410065070.1 discloses a kind of being employed in and has added active carbon, molecular sieve, nano silicon etc. in the cigarette acetate silk, thus the harmful substance in the selective clearing flue gas.However still can not satisfy the needs that filter pernicious gas in the flue gas.Microcapsule technology all has wide application prospects in many-sides such as biology, medicine, agriculturals.Microencapsulation is applied to pharmacy industry for some time, because its special preparation way only is applied to the intermediate manufacturing of medicine at present.
Summary of the invention
The purpose of this invention is to provide a kind of natural plant extracts micro-capsule and contain the cigaratte filter of natural plant extracts micro-capsule, the technical problem that solve is the harmful components that reduce in the cigarette smoke.
The present invention adopts following technical scheme: a kind of natural plant extracts micro-capsule; Said natural plant extracts micro-capsule is made up of following proportion of masses: natural plant extracts 1-1.5 part, capsule material 1-2 part; Said natural plants is wintergreen, honeysuckle, peppermint or miracle fruit; Said capsule material adopts more than one of Arabic gum, gelatin, agar, sodium alginate, acrylic resin, beta-schardinger dextrin-, maltodextrin, shitosan, cellulose, polyester and silicon rubber, and microcapsule diameter is 0.001-0.5cm.
Natural plant extracts micro-capsule of the present invention adopts following method to prepare: one, extract natural plants wintergreen, honeysuckle or miracle fruit extract; Two, natural plant extracts and capsule material are pressed mass ratio 1-1.5: 1-2, mix; Three, adopt the moulding of the dry parcel of spray drying process, feeding temperature is that 50 ℃, EAT are that 150-220 ℃, leaving air temp are 60-110 ℃, obtains the natural plant extracts micro-capsule.
Natural plant extracts of the present invention is paste, crystalloid or Powdered.
The extract of wintergreen of the present invention, honeysuckle or peppermint; Adopt following method to obtain: with wintergreen, honeysuckle or peppermint; 95% alcohol reflux with 4 times of wintergreen, honeysuckle or peppermint quality extracts each 2 hours of refluxing extraction, 30-65 ℃ of filtration 2 times; Filtrating decompression recycling ethanol under 0.05Mpa, 80 ℃, 2 hours conditions obtains paste extract to there not being the alcohol flavor.
The extract of miracle fruit of the present invention; Adopt following method to obtain: to adopt freeze-drying miracle fruit pulp, smash, the back centrifugation of blunging; Slag was with the absolute ethyl alcohol 10-30 ℃ cold soaking of 6 times of quality 12 hours; Filter, filtrating decompression recycling ethanol under 0.05Mpa, 80 ℃, 2 hours conditions obtains paste extract to there not being the alcohol flavor.
A kind of cigaratte filter that contains the natural plant extracts micro-capsule; Contain tow in the filter rod; Be added with the natural plant extracts micro-capsule in the said tow; The mass ratio of tow and micro-capsule is 1-100: 0.1-100, and said natural plant extracts micro-capsule is made up of following proportion of masses: natural plant extracts 1-1.5 part, capsule material 1-2 part, and said natural plants is wintergreen, honeysuckle, peppermint or miracle fruit; Said capsule material adopts more than one of Arabic gum, gelatin, agar, sodium alginate, acrylic resin, beta-schardinger dextrin-, maltodextrin, shitosan, cellulose, polyester and silicon rubber, and microcapsule diameter is 0.001-0.5cm.
Cigaratte filter natural plant extracts micro-capsule of the present invention adopts following method to prepare: one, extract natural plants wintergreen, honeysuckle or miracle fruit extract; Two, natural plant extracts and capsule material are pressed mass ratio 1-1.5: 1-2, mix; Three, adopt the moulding of the dry parcel of spray drying process, feeding temperature is that 50 ℃, EAT are that 150-220 ℃, leaving air temp are 60-110 ℃, obtains the natural plant extracts micro-capsule.
The extract of cigaratte filter wintergreen of the present invention, honeysuckle or peppermint; Adopt following method to obtain: with wintergreen, honeysuckle or peppermint; 95% alcohol reflux with 4 times of wintergreen, honeysuckle or peppermint quality extracts each 2 hours of refluxing extraction, 30-65 ℃ of filtration 2 times; Filtrating decompression recycling ethanol under 0.05Mpa, 80 ℃, 2 hours conditions obtains paste extract to there not being the alcohol flavor.
The extract of cigaratte filter miracle fruit of the present invention; Adopt following method to obtain: to adopt freeze-drying miracle fruit pulp, smash, the back centrifugation of blunging; Slag was with the absolute ethyl alcohol 10-30 ℃ cold soaking of 6 times of quality 12 hours; Filter, filtrating decompression recycling ethanol under 0.05Mpa, 80 ℃, 2 hours conditions obtains paste extract to there not being the alcohol flavor.
The present invention compared with prior art extracts active component and makes micro-capsule from natural plants, this micro-capsule is joined the filter rod of processing cigarette in the cigarette filter tow; In smoking process; Cigarette perfume (or spice) be can enrich, cigarette smoke quality and harmony increased, the harmful components in the selective reduction cigarette; The protection smoker's is healthy, thereby improves the cigarette class.
The specific embodiment
Below in conjunction with embodiment the present invention is done further explain.Natural plant extracts micro-capsule of the present invention; Form by following proportion of masses: natural plant extracts 1-1.5, capsule material 1-2; Natural plants is wintergreen, honeysuckle, peppermint or miracle fruit; The capsule material adopts more than one of Arabic gum, gelatin, agar, sodium alginate, acrylic resin, beta-schardinger dextrin-, maltodextrin, shitosan, cellulose, polyester and silicon rubber, is arbitrary proportion when two or more, and microcapsule diameter is 0.001-0.5cm.Adopt following method to prepare: one, extract natural plants wintergreen, honeysuckle or miracle fruit extract, natural plant extracts is paste, crystalloid or Powdered; Two, natural plant extracts and capsule material are pressed mass ratio 1-1.5: 1-2, mix; Three, adopt the moulding of the dry parcel of spray drying process, feeding temperature is that 50 ℃, EAT are that 150-220 ℃, leaving air temp are 60-110 ℃, obtains the natural plant extracts micro-capsule, and its particle diameter is 0.001-0.5cm.
Extract the extract of natural plants wintergreen, honeysuckle or peppermint; Can adopt following method to obtain: with wintergreen, honeysuckle or peppermint, to extract 2 times, adopt the hengyang, hunan province city to create the multi-function extractor refluxing extraction device of triumphant pharmaceutical equipment Co., Ltd, model TQ-Z with 95% alcohol reflux of 4 times of wintergreen, honeysuckle or peppermint quality; Each 2 hours; 30-65 ℃ of filtration, filtrating decompression recycling ethanol under 0.05Mpa, 80 ℃, 2 hours conditions obtains paste extract to there not being the alcohol flavor.
Extract the extract of natural plants miracle fruit; Can adopt following method to obtain: to adopt freeze-drying miracle fruit pulp, smash, the back centrifugation of blunging; Slag was with the absolute ethyl alcohol 10-30 ℃ cold soaking of 6 times of quality 12 hours; Filter, filtrating decompression recycling ethanol under 0.05Mpa, 80 ℃, 2 hours conditions obtains paste extract to there not being the alcohol flavor.
The natural plant extracts that the present invention adopts contains active component: the main active ingredient of wintergreen is homoarbutin (homoarbutin
), Hyperoside (hyperin
), and cardiac stimulant step-down, anti-inflammatory analgesic, antibacterial, sedation are arranged; Honeysuckle contains chlorogenic acid (ChlorogenicAcid
); Be the main antibiotic effective ingredient of honeysuckle, antibacterial, antiviral, analgesic, antiinflammatory action are arranged; The main active ingredient of peppermint is menthol (Menthol
), excitor nerve is arranged, separates thermal sweating, anti-bacterial, anti-itching, antivirus action; The main active ingredient of miracle fruit is miracle fruit plain (miraculin), has the effect of adjustment hyperglycaemia, hypertension, high fat of blood, gout, uric acid, headache.Volatile ingredient in the active component is a menthol, and water soluble ingredient is chlorogenic acid, Hyperoside, and the vegetable butter soluble components is complicated ingredients such as miracle fruit element, and stability is lower.Adopt micro-capsule,,, the stability of plant liquid fat is strengthened the solidification of liquid oily active component the microencapsulation of vegetable butter soluble components.
The cigaratte filter that contains the natural plant extracts micro-capsule of the present invention is added with the natural plant extracts micro-capsule in the tow of filter rod, the mass ratio of tow and micro-capsule is 1-100: 0.1-100.Adopt following method preparation: in tow, evenly add the natural plant extracts micro-capsule,, obtain containing the cigaratte filter of natural plant extracts micro-capsule then by prior art moulding filter rod.
The cigarette of containing the cigaratte filter of natural plant extracts micro-capsule; During smoking; Active component in the natural plant extracts is released under the flue gas higher temperature, and the harmful components in the cigarette are comprehensively fallen, and plays the evil effect of falling; Active component good for health to the smoker simultaneously or flavouring is inhaled in smoker's body with flue gas, and the cigarette smoke that makes is plentiful, free from extraneous odour, assorted gas.Compare with common filter tip, following advantage is arranged: 1, promote the cigarette smoke quality.2, the harmful components in the reduction cigarette mainstream flue gas.3, do not change the original processing technology of cigarette filter.4, increase cigarette perfume, reduce the flue gas spread effect.5, safety non-toxic.
The cigarette that the cigaratte filter that adopts the present invention to contain the natural plant extracts micro-capsule is made, by Guangdong provincial cigarette teacher of the smokeing panel test according to GB5606.4-2005 cigarette sense organ specification requirement smoke panel test, flue gas is full, pure and mild, free from extraneous odour, assorted gas are few.
Embodiment 1, makes the natural plant extracts micro-capsule, and plant extract logistics cream extracts: the wintergreen of choosing clean drying; 95% alcohol reflux that adds 4 times of its quality extracts 2 times, each 2 hours, filters; Filtrating decompression recycling ethanol under 0.05Mpa, 80 ℃, 2 hours conditions obtains wintergreen plant extract logistics cream to there not being the alcohol flavor, and the wall material adopts 1: 1 Arabic gum of mass ratio and maltodextrin; The mass ratio of plant extract logistics cream and wall material is 1: 2, and feeding temperature is 50 ℃, 220 ℃ of spray-drying condition EATs; 80 ℃ of leaving air temps make microcapsules, and microcapsules are pressed tow when the common filter stick wire-beam forming and the micro-capsule mass ratio evenly adds wherein at 100: 1; Obtain micro-capsule mouth rod, process cigarette by conventional cigarette process.When Guangdong provincial cigarette teacher of the smokeing panel test, cigarette smoke was pure and mild, comfortable, coordinate, and fragrant is arranged, the free from extraneous odour gas of mixing.
Embodiment 2, make the natural plant extracts micro-capsule, and plant extract logistics cream extracts: the honeysuckle of choosing clean drying; 95% alcohol reflux that adds 4 times of its quality extracts 2 times, each 2 hours, filters; Filtrating decompression recycling ethanol under 0.05Mpa, 80 ℃, 2 hours conditions obtains honeysuckle plant extract logistics cream to there not being the alcohol flavor, and it is the wall material that maltodextrin, beta-schardinger dextrin-and sodium alginate press mass ratio at 1: 1: 0.2; The mass ratio of plant extract logistics cream and wall material is 1: 2, and feeding temperature is 50 ℃, 150 ℃ of spray-drying EATs; 80 ℃ of leaving air temps make microcapsules, and microcapsules are pressed tow when the common filter stick wire-beam forming and the micro-capsule mass ratio evenly adds wherein at 100: 2; Obtain micro-capsule mouth rod, and process cigarette by conventional cigarette process.When Guangdong provincial cigarette teacher of the smokeing panel test, cigarette smoke was pure and mild, coordinate, the free from extraneous odour gas of mixing.
Embodiment 3, make the natural plant extracts micro-capsule, and plant extract logistics cream extracts: the peppermint herb of choosing clean drying; 95% alcohol reflux that adds 4 times of its quality extracts 2 times, each 2 hours, filters; Filtrating decompression recycling ethanol under 0.05Mpa, 80 ℃, 2 hours conditions obtains mint plants extract flow cream to there not being the alcohol flavor, and it is the wall material that Arabic gum, maltodextrin and gelatin press mass ratio at 1: 1: 0.5; The mass ratio of plant extract logistics cream and wall material is 1: 2, and feeding temperature is 50 ℃, 180 ℃ of spray-drying EATs, 60 ℃ of leaving air temps; Make microcapsules; Microcapsules are pressed tow when the common filter stick wire-beam forming and the micro-capsule mass ratio evenly adds wherein at 100: 0.1, obtain micro-capsule mouth rod, and process cigarette by conventional cigarette process.When Guangdong provincial cigarette teacher of the smokeing panel test, cigarette smoke was pure and mild, coordinate, and the peppermint distinctive smell is arranged, the free from extraneous odour gas of mixing.
Embodiment 4, make the natural plant extracts micro-capsule, and plant extract logistics cream extracts: get freeze-drying miracle fruit Xishuangbanna Tropical Plant Garden, Chinese Academy of Sciences; Meng Lun town, Mengla County, Yunnan Province, the postal volume bought in November, 666303,2009; Pulp is smashed a little, stirs centrifugation after 3 hours with 20 times of quality water, and residue was with the absolute ethyl alcohol 10-30 ℃ cold soaking of 6 times of quality 12 hours; Filter, decompression recycling ethanol obtains miracle fruit plant extract logistics cream to there not being the alcohol flavor under 0.05Mpa, 80 ℃, the 2 hours conditions; Shitosan, Arabic gum are pressed mass ratio 1: 0.5 as the wall material, and the mass ratio of plant extract logistics cream and wall material is 1.5: 1, again through the spray drying method for preparation microcapsules; Feeding temperature is that 50 ℃, EAT are that 180 ℃, leaving air temp are 110 ℃, makes microcapsules, and microcapsules are pressed tow when the common filter stick wire-beam forming and the micro-capsule mass ratio evenly adds wherein at 100: 0.1; Obtain micro-capsule mouth rod, and process cigarette by conventional cigarette process.When Guangdong provincial cigarette teacher of the smokeing panel test, cigarette smoke pure and mild full, coordinate, fragrant and sweet flavor is arranged, the free from extraneous odour gas of mixing.
Wintergreen, honeysuckle and peppermint are medicinal herbs most in use.The freeze-drying miracle fruit originates from Xishuangbanna Tropical Plant Garden, Chinese Academy of Sciences.
Claims (7)
1. natural plant extracts micro-capsule; It is characterized in that: said natural plant extracts micro-capsule is made up of following proportion of masses: natural plant extracts 1-1.5 part, capsule material 1-2 part; Said natural plants is a miracle fruit; Said capsule material adopts more than one of Arabic gum, gelatin, agar, sodium alginate, acrylic resin, beta-schardinger dextrin-, maltodextrin, shitosan, cellulose, polyester and silicon rubber, and microcapsule diameter is 0.001-0.5cm.
2. natural plant extracts micro-capsule according to claim 1 is characterized in that: said natural plant extracts micro-capsule adopts following method to prepare: one, extract natural plants miracle fruit extract; Two, natural plant extracts and capsule material are pressed mass ratio 1-1.5: 1-2, mix; Three, adopt the moulding of the dry parcel of spray drying process, feeding temperature is that 50 ℃, EAT are that 150-220 ℃, leaving air temp are 60-110 ℃, obtains the natural plant extracts micro-capsule.
3. natural plant extracts micro-capsule according to claim 2 is characterized in that: said natural plant extracts is paste, crystalloid or Powdered.
4. natural plant extracts micro-capsule according to claim 2 is characterized in that: the extract of said miracle fruit, adopt following method to obtain: to adopt freeze-drying miracle fruit pulp; Smash; Blunge back centrifugation, slag is with the absolute ethyl alcohol 10-30 ℃ cold soaking of 6 times of quality 12 hours, filtration; Filtrating decompression recycling ethanol under 0.05Mpa, 80 ℃, 2 hours conditions obtains paste extract to there not being the alcohol flavor.
5. cigaratte filter that contains the natural plant extracts micro-capsule; Contain tow in the filter rod; It is characterized in that: be added with the natural plant extracts micro-capsule in the said tow; The mass ratio of tow and micro-capsule is 1-100: 0.1-100, and said natural plant extracts micro-capsule is made up of following proportion of masses: natural plant extracts 1-1.5 part, capsule material 1-2 part, and said natural plants is a miracle fruit; Said capsule material adopts more than one of Arabic gum, gelatin, agar, sodium alginate, acrylic resin, beta-schardinger dextrin-, maltodextrin, shitosan, cellulose, polyester and silicon rubber, and microcapsule diameter is 0.001-0.5cm.
6. the cigaratte filter that contains the natural plant extracts micro-capsule according to claim 5 is characterized in that: said natural plant extracts micro-capsule adopts following method to prepare: one, extract natural plants miracle fruit extract; Two, natural plant extracts and capsule material are pressed mass ratio 1-1.5: 1-2, mix; Three, adopt the moulding of the dry parcel of spray drying process, feeding temperature is that 50 ℃, EAT are that 150-220 ℃, leaving air temp are 60-110 ℃, obtains the natural plant extracts micro-capsule.
7. the cigaratte filter that contains the natural plant extracts micro-capsule according to claim 6 is characterized in that: the extract of said miracle fruit, adopt following method to obtain: to adopt freeze-drying miracle fruit pulp; Smash; Blunge back centrifugation, slag is with the absolute ethyl alcohol 10-30 ℃ cold soaking of 6 times of quality 12 hours, filtration; Filtrating decompression recycling ethanol under 0.05Mpa, 80 ℃, 2 hours conditions obtains paste extract to there not being the alcohol flavor.
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| CN101972038A (en) * | 2010-10-28 | 2011-02-16 | 上海理工大学 | Slowly-released filter stick essence microcapsule and preparation method thereof |
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| CN102068038A (en) * | 2010-12-31 | 2011-05-25 | 贵州中烟工业有限责任公司 | Method for preparing heat-sensitive moisture-retaining central line filter stick of cigarette |
| CN102551211A (en) * | 2011-12-25 | 2012-07-11 | 云南正邦生物技术有限公司 | Preparation method for instant release type cigarette mouth rod |
| CN104256892A (en) * | 2014-09-09 | 2015-01-07 | 云南中烟工业有限责任公司 | Method for extracting Pu-Er raw tea essential oil and purpose of Pu-Er raw tea essential oil in cigarette filter stick |
| CN104921289A (en) * | 2015-06-17 | 2015-09-23 | 云南中烟工业有限责任公司 | Honeysuckle glyceryl triacetate extract and application thereof in cigarette |
| CN105175796A (en) * | 2015-07-31 | 2015-12-23 | 云南中烟工业有限责任公司 | Preparation method for ternary blending polysaccharide of schizophyllan, arabinose and maltodextrin and applications |
| CN105249531A (en) * | 2015-08-06 | 2016-01-20 | 云南中烟工业有限责任公司 | Method for preparing phoebe zhennan extracts and application thereof |
| CN107034020A (en) * | 2017-04-27 | 2017-08-11 | 河南中烟工业有限责任公司 | A kind of quick-fried pearl honeysuckle compound of cigarette and its application in cigarette |
| CN108301060A (en) * | 2018-03-05 | 2018-07-20 | 厦门安踏体育用品有限公司 | Mint extract microcapsules, acrylic fiber, fabric and relevant preparation method |
| CN109673855A (en) * | 2019-01-29 | 2019-04-26 | 湖南江海环保实业有限公司 | For producing the composite flavor modifying agent of high palatability ammonium chloride, high palatability ammonium chloride and preparation method thereof |
| CN109793269A (en) * | 2019-01-30 | 2019-05-24 | 湖北中烟工业有限责任公司 | Preparation method and application for the floral type tow in Novel heating not burning tobacco |
| CN110859320A (en) * | 2019-10-11 | 2020-03-06 | 国药控股星鲨制药（厦门）有限公司 | Plant brittle capsule for cigarettes and preparation method thereof |
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