WO2024256880A1 - System for agricultural sample slurry analysis and related methods - Google Patents
System for agricultural sample slurry analysis and related methods Download PDFInfo
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- WO2024256880A1 WO2024256880A1 PCT/IB2024/051820 IB2024051820W WO2024256880A1 WO 2024256880 A1 WO2024256880 A1 WO 2024256880A1 IB 2024051820 W IB2024051820 W IB 2024051820W WO 2024256880 A1 WO2024256880 A1 WO 2024256880A1
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- slurry
- stir chamber
- stirring device
- controller
- housing section
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Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/38—Diluting, dispersing or mixing samples
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
- B01F27/85—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with two or more stirrers on separate shafts
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/20—Measuring; Control or regulation
- B01F35/22—Control or regulation
- B01F35/2201—Control or regulation characterised by the type of control technique used
- B01F35/2209—Controlling the mixing process as a whole, i.e. involving a complete monitoring and controlling of the mixing process during the whole mixing cycle
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/286—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q involving mechanical work, e.g. chopping, disintegrating, compacting, homogenising
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/286—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q involving mechanical work, e.g. chopping, disintegrating, compacting, homogenising
- G01N2001/2866—Grinding or homogeneising
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N35/00—Automatic analysis not limited to methods or materials provided for in any single one of groups G01N1/00 - G01N33/00; Handling materials therefor
- G01N2035/00465—Separating and mixing arrangements
- G01N2035/00534—Mixing by a special element, e.g. stirrer
Definitions
- Test results provide valuable information on the chemical makeup of the soil such as plant-available nutrients and other important properties (e.g., levels of nitrogen, magnesium, phosphorous, potassium, pH, etc.) so that various amendments may be added to the soil to maximize the quality and quantity of crop production.
- the raw or bulk agricultural material samples such as soil (or other agricultural materials) extracted from the field may be prepared for analysis.
- the sample may be measured for various properties. Measurements may be performed to determine the chemical makeup or may be performed to ensure adequate sample size, density, or other parameters that may affect the quality of other measurements. In still other processes, measurements may be made and corrective actions taken to ensure the quality of the measurements.
- Improvements in agricultural sample preparation and analysis are desired.
- a stir chamber has a housing, a first sensor, a second sensor, and a third sensor.
- the housing defines an internal cavity configured to receive an agricultural sample.
- the internal cavity extends along a longitudinal axis from a bottom end to a top end.
- the first sensor is fluidly coupled to the internal cavity of the housing at a first location with respect to the longitudinal axis.
- the second sensor is fluidly coupled to the internal cavity of the housing at a second location with respect to the longitudinal axis.
- the third sensor is fluidly coupled to the internal cavity of the housing at a third location with respect to the longitudinal axis. The second location is located between the first and third locations.
- the first, second, and third sensors are configured to monitor one of a fluid level or a density of the sample.
- a system for analyzing an agricultural sample has a stir chamber and a controller.
- the stir chamber has a housing, a first sensor, and a second sensor.
- the housing defines an internal cavity configured to receive an agricultural sample.
- the internal cavity extends along a longitudinal axis from a bottom end to a top end.
- the first sensor is fluidly coupled to the internal cavity of the housing at a first location with respect to the longitudinal axis.
- the second sensor is fluidly coupled to the internal cavity of the housing at a second location with respect to the longitudinal axis.
- the controller is configured to receive a plurality of signals from the first and second sensors. At least one of the plurality of signals is used to compute a density of a first region of the internal cavity located between the first and second sensors.
- a method for analyzing a sample has a first step of providing a chamber having an internal cavity, the internal cavity extending along a longitudinal axis from a bottom end to a top end.
- the first sensor is fluidly coupled to the internal cavity at a first location with respect to the longitudinal axis and a second sensor is fluidly coupled to the internal cavity at a second location with respect to the longitudinal axis.
- a sample is added to the internal cavity.
- a plurality of signals from the first and second sensors are read.
- a density or a fluid level is computed using the plurality of signals from the first and second sensors.
- FIG. 1 is a schematic of an exemplary system for analyzing an agricultural sample
- FIG. 2 is a perspective view of a stir chamber as may be used in the exemplary system for analyzing an agricultural sample as shown in FIG. 1;
- FIG. 3 is a cross sectional view of the stir chamber of FIG. 2, taken along line 3-3;
- FIG. 4 is a cross sectional view of the stir chamber of FIG. 3, taken along line 4-4;
- FIG. 5 is a cross sectional view of the stir chamber of FIG. 2, taken along line 5-5;
- FIG. 6 is a cross sectional view of the stir chamber of FIG. 2, taken along line 6-6;
- FIG.7 is a schematic view of an alternate embodiment of a stir chamber as may be used in the system of FIG. 1; [0019] FIG.
- FIG. 8 is a flow chart illustrating a method for analyzing a sample
- FIG. 9 is a schematic system block diagram of an alternative system for processing analyzing an agricultural sample
- FIG. 10 is a first top perspective view of a stirring device of the system of FIG. 9 comprising a stir chamber for processing and analyzing an agricultural sample slurry
- FIG. 11 is a second top perspective view thereof
- FIG. 12 is a first bottom perspective view thereof
- FIG. 13 is a second bottom perspective view thereof
- FIG. 14 is a first side view thereof
- FIG. 15 is a second side view thereof
- FIG. 16 is a third side view thereof
- FIG. 10 is a schematic system block diagram of an alternative system for processing analyzing an agricultural sample
- FIG. 10 is a first top perspective view of a stirring device of the system of FIG. 9 comprising a stir chamber for processing and analyzing an agricultural sample slurry
- FIG. 11 is a second top perspective view thereof
- FIG. 12 is a first bottom perspective view thereof
- FIG. 13 is
- any reference to direction or orientation is merely intended for convenience of description and is not intended in any way to limit the scope of the present disclosure.
- Relative terms such as “lower,” “upper,” “horizontal,” “vertical,”, “above,” “below,” “up,” “down,” “top” and “bottom” as well as derivative thereof (e.g., “horizontally,” “downwardly,” “upwardly,” etc.) should be construed to refer to the orientation as then described or as shown in the drawing under discussion. These relative terms are for convenience of description only and do not require that the apparatus be constructed or operated in a particular orientation.
- the system 100 comprises a grinder 110, a stir chamber 200, a pump 120, a filter 130, and an analysis unit 140.
- the grinder 110 receives an agricultural sample, such as soil, and grinds the sample to ensure that the maximum particle size of the agricultural sample is below that required for later analysis by the analysis unit 140. Examples of grinders which may be used can be found in commonly-owned U.S. Application Nos.
- the purpose of the stir chamber 200 is to ensure that the agriculture sample is homogeneous. This may be performed by a variety of methods, including mixing, stirring, shaking, vibrating, or any other means suitable to ensure thorough mixing of the sample. In addition, measurements may be performed on the sample to verify that adequate mixing has occurred. For instance the level of the sample within the stir chamber 200, the density, or the mass may be measured in an effort to determine adequate sample size and homogeneity.
- water may be added from a fluid source to achieve a target density, improve homogeneity, or other purposes. The fluid source may recycle water used elsewhere in the process or may add new water.
- the sample may be returned to the stir chamber from downstream components to perform additional processing as will be discussed in greater detail below.
- the sample passes to a pump 120.
- the pump 120 pressurizes the sample to ensure that it is effectively filtered by a filter 130.
- the pump 120 may be located downstream of the filter 130, such that the filter 130 is on the suction side of the pump 120.
- the pump 120 and filter 130 may be used to remove undesirably large components of the sample such as gravel that have passed through the grinder.
- the pump 120 and filter 130 may also be used to recirculate a portion of the sample along with additional water from a water source to enable additional treatment and adjustment of the sample slurry in the stir chamber 200. This may be done because only a portion of the sample is required for further testing.
- a controller 300 controls all functions of the stir chamber 300.
- the controller 300 comprises a memory 310, a processor 320, and a device interface 330.
- the controller 300 may be a central controller which controls functions for all components of the system. In other implementations 300, the controller 300 may be integrated into a single component such as the stir chamber 200. In this implementation, additional controllers 300 may be integrated into the other components and may communicate via a bus or other communications system. Alternately, the controller 300 may be integrated into a single component and may also connect to other components in the system. As can be seen, the arrangement of the controller 300 may be distributed or may be centralized as desired. [0045]
- the stir chamber 200 has a plurality of sensors 210. In the system 100, the sensors 210 are differential pressure sensors. The sensor 210 are coupled to the stir chamber 200 as illustrated, with each sensor 210 having a first side of the differential sensor coupled to the stir chamber 200.
- a second side of the sensor 210 may also be coupled to the stir chamber 200 or may be coupled to atmosphere as illustrated in Fig. 1. Any number of sensors 210 may be utilized as desired. [0046] In some embodiments, all of the second sides of the sensors 210 are coupled to atmosphere and in some other embodiments, all of the second sides of the sensors 210 are coupled to the stir chamber. As can be seen, all, some, or none of the second sides of the sensors 210 may be coupled to atmosphere and all, some, or none of the second sides may be coupled to the stir chamber 200. In yet further embodiments, the sensors 210 may be absolute, atmospheric, or gauge type sensors having only a single sensing input rather than the two sides or inputs of a differential sensor.
- the sensors 210 may not be pressure sensors, and may instead be optical, capacitive, ultrasonic, microwave, vibrating, ultrasonic, conductivity, laser, nuclear, or other types of sensors suitable for measuring density, fluid level, pressure, or other properties of a sample.
- Attorney Docket No.23075WO Multiple different types of sensors 210 may be utilized, and not all sensors 210 need be the same type.
- Figs. 2-6 an exemplary embodiment of a stir chamber 200 is illustrated.
- the stir chamber has a housing 220 formed of a gear head 221, an upper housing 222, a middle housing 223, and a lower housing 224.
- the gear head 221 receives a motor 225 and couples to the upper housing 222.
- the upper housing 222, middle housing 223, and lower housing 224 collectively form an internal cavity 230.
- the internal cavity 230 extends along a longitudinal axis A-A, the internal cavity 230 being elongate along the longitudinal axis A-A.
- the internal cavity 230 extends along the longitudinal axis A-A from a top end 231 to a bottom end 232.
- a plurality of ports 240 are formed into the housing 220 and are fluidly coupled to the internal cavity 230.
- the ports 240 may serve a variety of functions, including receiving a sample, outputting a sample, permitting sensors to measure the sample, allowing for injection of fluid such as water from a fluid source, or any other desired function.
- the plurality of ports 240 comprise a first sensing port 241, second sensing port 242, and third sensing port 243.
- the first, second, and third sensing ports 241, 242, 243 are arranged along the longitudinal axis A-A and fluidly coupled to the internal cavity 230.
- Each of the first, second, and third sensing ports 241, 242, 243 are configured to receive a sensor 210. More than three or less than three sensing ports may be utilized. One or two ports may provide adequate opportunities for sensing, while greater than three ports may provide additional granularity to the measured data.
- the housing 220 is generally arranged such that the longitudinal axis A-A is vertical with respect to gravity. This ensures that the sample settles at the bottom end 232 of the internal cavity 230. Thus, a level of the sample within the internal cavity 230 can be measured using the sensing ports 241, 242, 243, with the first sensing port 241 being submerged in the sample last as the sample is delivered to the internal cavity 230.
- the sensors 210 are installed into the first, second, and third sensing ports 241, 242, 243 as noted above.
- the sensors 210 may incorporate a fluid passage therethrough that allows clearing the first, second, and third sensing ports 241, 242, 243 in the event of clogs or to facilitate a complete rinse of the internal cavity 230.
- the sensors 210 are thus located at first, second, and third locations with respect to the longitudinal axis A-A.
- the first, second, and third locations each have a different position along the longitudinal axis A-A.
- a first region R1 is defined by the Attorney Docket No.23075WO first and second locations of the first and second sensing ports 241, 242.
- a second region R2 is defined by the second and third locations of the second and third sensing ports 242, 243.
- a third region R3 overlaps the first and second regions R1, R2 and is defined by the first and third locations of the first and third sensing ports 241, 243.
- the three different locations along the longitudinal axis allow measurements to be taken at different heights with respect to the bottom end 232 of the internal cavity 230.
- the controller 300 is operably coupled to the sensors 210. A plurality of signals from the sensors 210 may be received by the controller 300, allowing data collection from the sensors 210 as will be discussed in greater detail below.
- the stir chamber 200 further incorporates an agitator 250.
- the agitator 250 collectively comprises the motor 225, a gear train 251, and two agitator shafts 252. Each agitator shaft 252 comprises a blade 253 that agitates the sample when the agitator shafts 252 are rotated.
- the gear train 251 connects the motor 225 to the agitator shafts 252.
- more than one motor 225 may be utilized and the gear train 251 omitted.
- the gear train 251 may be formed as a belt or chain drive instead of a gear drive, but may still be referred to as a gear train 251.
- the gear train 251 may serve to reduce or increase the speed of the agitator shafts 252 with respect to the motor 225, or the gear train 251 may provide no reduction or multiplication of the speed of the motor 225.
- the stir chamber 200 may utilize the sensors 210 to compute the density of the sample within the internal cavity 230. More specifically, the density of the sample may be measured in different regions within the internal cavity 230.
- the internal cavity 230 is first emptied such that it is only filled with air. The signals from the sensors 210 are then zeroed such that the readings are corrected for any deviation.
- Air has negligible pressure differential over Attorney Docket No.23075WO the distances between the sensors 210, so it can be assumed that the pressure differential should be zero.
- the internal cavity is filled with a reference fluid such as water, with the fluid filling the internal cavity 230 such that it covers the first, second, and third sensing ports 241, 242, 243.
- the reference fluid must have a known reference density.
- the reference density of water may be arbitrarily assigned to be 1, or may be in any conventional unit system.
- a pressure differential between any two locations is measured.
- the pressure differential may be calculated by the controller 300 based on signals from sensors 210 in the first and second sensing ports 241, 242.
- the first and third sensing ports 241, 243 or the second and third sensing ports 242, 243 may be utilized.
- the pressure differential between the two locations is then used as a reference differential pressure.
- the signals from the sensors 210 are received by the controller 300.
- the signals from the sensors 210 may be in the form of an analog voltage or current, or may be a digital signal.
- the signals from the sensors 210 correspond to a parameter measured by the respective sensor 210.
- the signals may vary with respect to time, and may represent a parameter such as pressure or some other parameter which is continuously changing based on the measured condition at the respective sensing port.
- the internal cavity 230 is filled with a fluid of unknown density such as the agricultural sample.
- specimen density reference density * specimen differential pressure / reference differential pressure.
- reference density is arbitrarily assigned a value of 1
- specimen density can be determined with reference to the reference density.
- specimens having half the density of the reference fluid would have a specimen density of 0.5.
- the density may be defined in terms of any accepted unit system. For instance, density may be defined in terms of grams per cubic centimeter, kilograms per cubic meter, pounds per cubic foot, or any other recognized unit system.
- the internal volume and location of the sensing ports 241, 242, 243 can be utilized to calculate an expected pressure differential between two ports of a given reference fluid. This can, in turn, be used to compute a Attorney Docket No.23075WO theoretical reference differential pressure that may be utilized to calculate the specimen density using the same equation as is used when an actual reference fluid is used. However, this suffers from some potential loss of accuracy due to variations in internal volume of the internal cavity 230, variations in the location of the sensors 210, and other variables. [0059] Furthermore, a method of determining the mass of the sample can be performed.
- the sensors 210 can be utilized to determine a level of the sample within the internal cavity 230. By comparing the pressure measured by each sensor 210 against atmospheric pressure, the presence or absence of the sample can be determined for each location. In addition, it is possible to calculate a level between the sensors 210 by combining density measurements with pressure measurements.
- the sample must have a level below the location of the first sensing port 241 with respect to the longitudinal axis A-A. If the sensor 210 at the first sensing port 241 measures a pressure greater than atmospheric pressure, then the sample must have a level above the location of the first sensing port 241. In combination with the pressure and density information, a level between ports 240 can be extrapolated. If additional sensing accuracy is desired, additional sensing ports may be added or additional sensors 210 of different types may be utilized. [0061] In yet a further method, information regarding the density within regions of the internal cavity 230 may be used to measure the homogeneity of the sample.
- the density of the sample can be measured in the first region R1 between the sensor 210 at the first sensing port 241 and the sensor 210 at the second sensing port 242.
- the density may also be measured in the second region R2 between the sensor 210 at the second sensing port 242 and the sensor 210 at the third sensing port 243.
- the Attorney Docket No.23075WO density may be measured in the third region R3 between the sensor 210 at the first sensing port 241 and the sensor 210 at the third sensing port 243.
- the density can be measured for the first and second regions R1, R2 and the third region R3 that overlaps both the first and second regions R1, R2.
- Adding additional sensors 210 at additional sensing ports will allow measurements in additional regions, further increasing the information regarding the homogeneity of the sample.
- each of the first, second, and third regions R1, R2, R3 may have different densities. The difference between the densities of the first, second, and third regions R1, R2, R3, allows a quantitative analysis of the homogeneity of the sample within the internal cavity 230.
- the agitator 250 may be activated in response to detecting a difference in density between two regions that exceeds a predetermined threshold.
- the speed of the motor 225 may be reduced to allow particles or other components of the sample to settle toward the bottom end 232 of the internal cavity 230.
- the speed of the motor 225 may be increased to increase agitation and move particles from the second region R2 to the first region R1.
- the speed of the agitator shafts 252 may be controlled using proportional control or may be activated according to a series of predetermined thresholds, with each threshold corresponding to a difference in density. In other implementations, the speed may be controlled in any known means designed to improve homogeneity of the sample. Any number of regions may be created by any number of sensors 210 as desired. [0066] In other implementations, the sensors 210 need not be located in sensor ports as shown in the embodiment of Figs. 2-6. In other implementations such as that shown schematically in Fig. 7, the sensors 210 may measure pressure at different locations using tubes or probes.
- Each tube of the sensors 210 terminates at a different location with respect to the longitudinal axis A-A to permit measurement at different heights just as with the embodiment of Figs. 2-6. Otherwise stated, the tube of each sensor 210 terminates at a first, second, or third sensing port 241, 242, 243.
- a particle distribution within the sample is illustrated as having a different distribution with respect to position along the longitudinal axis A-A.
- the use of an agitator 250 is optional. In some implementations, the agitator 250 may be omitted and density or fluid level measurements may be made without use of the agitator 250.
- a method for analyzing a sample 400 starts with step 410, providing a chamber 200 having an internal cavity 230.
- the internal cavity 230 extends along a longitudinal axis from a bottom end 232 to a top end 231.
- a first sensor 210 is fluidly coupled to the internal cavity 230 at a first location with respect to the longitudinal axis A-A.
- a second sensor 210 is fluidly coupled to the internal cavity 230 at a second location with respect to the longitudinal axis A-A.
- a third sensor 210 is fluidly coupled to the internal cavity 230 at a third location with respect to the longitudinal axis A-A.
- Each of the first, second, and third locations are different, and may be spaced from one another along the longitudinal axis A-A.
- a sample is added to the internal cavity 230.
- a plurality of signals from the sensors 210 are read by the controller 300.
- a density or fluid level of the sample is determined via the plurality of signals from the sensors 210.
- the sensors 210 may be pressure sensors 210.
- more than one density may be determined for different regions located between any two sensors as discussed above.
- FIGS.9-24 show an alternative embodiment of a slurry density measurement system.
- the system generally includes a stirring device 500 generally similar to the stirring device with stir chamber 200 and agitator 250 operable to stir the slurry, as previously described herein. Reference is made to the prior description for details which is not repeated here in full for the sake of brevity. The following description of the present stirring device will focus on the differences in the two designs which are pertinent.
- the stir chamber 502 of present stirring device 500 is configured differently in part for determining the density of the agricultural sample slurry in a different manner without use of pressure sensing ports 240 and related pressure sensing equipment.
- the present stirring device comprises a mechanically isolated stir chamber 502 configured to receive the agricultural sample slurry from grinder 110 and gently Attorney Docket No.23075WO agitate the slurry to keep the majority of agricultural solids (i.e. particles) in suspension for purposes of obtaining slurry density and other related measurements.
- the sample slurry may be a soil slurry in one non-limiting embodiment.
- the present mechanically isolated stir chamber 502 is formed by a section of the stirring device housing that is mechanically isolated from other portions of the stirring device and related appurtenances interfaced with the stir chamber such as the slurry inlet and outlet. Accordingly, the weight of the stir chamber is solely supported independently of other portions of the stirring device and related system by a load cell, such as without limitation a strain gauge 504 in one embodiment which is rigidly mounted to an available support structure. As further described herein, this allows an accurate weight of the stir chamber 502 to be measured empty and when filled with slurry; the difference representing the weight of the volume of slurry in the chamber. This information is used in conjunction with other measurements described below to determine the overall density of the slurry and water/solids ratio of the slurry.
- present stirring device 500 generally comprises a vertically elongated partially hollow housing 510 which may include an upper housing section 511 and lower housing section 512.
- Upper housing section 511 mounts and supports the agitator mechanism including agitator 250 driven by motor 225 and gear train 251, as previously described herein.
- the agitator may include only a single rotatable agitator shaft 252 and blade 253 assembly which is supported from above by upper housing section 511 in an overhead suspended manner as shown. It bears noting that two shaft and blade assemblies may be used in alternative embodiments if necessary for adequate agitation of the slurry to keep solid in suspension depending on the nature of the slurry.
- the agitator shaft is supported by the upper housing section of the stirring device independently of the stir chamber.
- the agitator shaft 252 and blade 253 may be directly driven by the motor such that the gear train may be omitted.
- the mode of agitation disclosed uses a single agitator shaft and blade assembly hanging down into the stir chamber 502 from upper housing section 511, other modes of agitating the slurry may be used in other embodiments, including for example but not limited to pneumatic agitation (bubbling air up into the internal cavity 530 of the stir chamber through the slurry), and recirculating the sample slurry through a separate pumped slurry flow loop.
- Lower housing section 512 defines the stir chamber 502 which includes internal cavity 530 configured for holding a volume of coarsely filtered slurry (or filtrate) received from grinder 110.
- Agitator shaft 252 and blade 253 assembly is positioned inside internal cavity 530, but not supported in any manner by the lower housing section 512.
- Upper housing section 511 provides sole support for the agitator shaft and blade assembly which enters the open top end 531 of the stir chamber internal cavity.
- Stir chamber 502 further includes a slurry inlet port 540 proximate to the top end of internal chamber 530 and a waste port 543 at the bottom or floor 530a of internal cavity 530.
- the stir chamber 502 defined by lower housing section 512 may be mechanically isolated from the upper housing section 511 in one embodiment via an isolation air gap 506 formed therebetween.
- An annular isolation air gap 508 may also be provided to also mechanically isolate the slurry inlet conduit 541 (e.g., section of piping or tubing) from the slurry inlet port 540 of the stir chamber. This prevents any support of the stir chamber by the slurry inlet conduit.
- the inlet conduit may be rigid in construction and could otherwise adversely affect obtaining an accurate stir chamber weight measurement by strain gauge 504.
- a slip joint may be used for the slurry inlet connection which incorporates the annular isolation air gap 508 as shown.
- Lower housing section 512 includes a support bracket 505 configured to fixedly couple the lower housing section (i.e. stir chamber) to one end 504a of the strain gauge 504 in a cantilevered manner as shown.
- Support bracket 505 may be mounted to one lateral side of the lower housing section.
- the opposite end 504b of the strain gauge is fixedly coupled to an available support structure, which in one embodiment may be provided by a portion of bracket 507 rigidly coupled to upper housing section 511.
- Other available support structures may be used to coupled end 504b of strain gauge configured 504 thereto which are not connected to the upper housing section.
- the strain gauge 504 may have a horizontally elongated structure as shown in one embodiment.
- Mechanical fasteners such as threaded fasteners in one non-limiting embodiment may be used to couple the strain gauge to bracket 507 and lower housing section 512 (i.e. stir chamber).
- Other types of mechanism fasteners such as rivets, clamps, etc. may be used.
- Other types of load sensors operable to measure the weight (mass) of the stir chamber and able to structurally support the stir Attorney Docket No.23075WO chamber independently of the stirring device upper housing section in the manner described herein may be used. [0079] It bears noting that the strain gauge readings are sensitive to forces and vibration coming from outside the sample slurry stir chamber 502.
- any wires, flow conduits (tubing, piping, etc.) or other appurtenances that must still be connected to the sample chamber are preferably strain relieved nearby (i.e. self supported without reliance on the stir chamber for support) so that they cannot support or “push” or “pull” on the stir chamber system in any manner which could adversely affect accurate slurry weight/mass measurements by strain gauge 504.
- strain gauge 504. An example of this is slurry inlet mounting bracket 541a previously described herein.
- the load cell (e.g., strain gauge 504) is used to measure the weight (mass) of the slurry inside the stir chamber by determining the differential weight between an empty stir chamber and then again when filled with slurry; the difference representing the weight of the slurry alone.
- the volume of slurry must also be determined (density being a measure of the mass per unit volume of material).
- a level sensor 515 may be provided to determine the volume of slurry in stir chamber 502.
- Level sensor 515 may be a non-contact type level sensor in one embodiment such as a ultrasonic transducer or similar; however, other type level sensors including contact level sensors could be used if appropriate.
- Sensor 515 may be mounted to upper housing section 511 and has a line of sight directly into internal cavity 530 of the stir chamber 502 through the open top end to of the chamber in order to detect a surface level of the slurry, which is correlated to the height of the column of slurry in the stir chamber via controller 300. Since the dimensions of the stir chamber internal cavity 530 are precisely known, the volume of slurry held therein at any given time can be readily determined as a function of the height of the column of slurry present. This information can be preprogrammed into controller 300 for use in determining the volume of slurry based on the slurry level detection (height of slurry column). [0082] The accuracy and repeatability of the volume measurements via level sensor 5151 is dependent on the cleanliness of the sensor.
- the sensor in one embodiment is preferably mounted in upper housing section 511 of stirring device 500 as far removed from the surface of the liquid Attorney Docket No.23075WO slurry in the stir chamber 502 as possible to avoid being splashed when the slurry is agitated.
- a downwardly open sensor cavity 515a recessed into the bottom of upper housing section 511 may be provided to maximize the distance of the sensor from the surface level of the sample slurry.
- the density of the slurry can be determined by dividing the total mass of slurry (weight) measured via strain gauge 504 by the volume of slurry determined via level sensor 515. In one embodiment, the density can be calculated automatically by programmable controller 300 shown in the modified system block diagram of FIG. 9.
- Strain gauge 504 and level sensor 515 are operably and communicably linked to controller 300, which is programmed with the appropriate program instructions (e.g., control logic) to calculate the density of the slurry based on the measured weight (mass) and calculated volume of the slurry based on slurry level measurement.
- a method for automatically determining density of the agricultural sample slurry via controller 300 may comprise the following steps implemented by the controller. [0085] First, the controller 300 measures the weight of the stir chamber 502 in an empty condition any time before the start of a sample slurry processing run without slurry present in the chamber. This provides a first empty stir chamber weight.
- an amount (volume) of slurry is added to the stir chamber (e.g., internal cavity 530) via slurry inlet port 540, such as from the grinder 110 as shown in FIG. 9.
- The may be done via controller opening isolation valve 525 (or manually) in the flow conduit between grinder 110 and stir chamber 502 (represented by the solid flow arrows).
- Valve 525 is then closed to fluidly isolate the grinder from the stir chamber and controller 300.
- the controller measures the weight of stir chamber 502 with slurry filled in the internal cavity 530. This provides a second filled stir chamber weight.
- the slurry may be agitated via agitator 250 before or after the measurements is taken, but preferably not during slurry weight and level measurements.
- the controller next calculates/determines the actual weight of the slurry by comparing and subtracting the empty stir chamber weight from the filled stir chamber weight. This represents the mass of slurry present in the stir chamber. It bears noting that the mass of slurry added to the stir chamber 502 may initially be unknown.
- the weight of the slurry is determined by controller 300 based on the actual volume of slurry present in the stir chamber 502.
- Controller 300 also automatically determines the volume of sample slurry present in stir chamber 502 via level sensor 515, either before, after, or simultaneously with the step of Attorney Docket No.23075WO determining the mass (weight) of the slurry.
- Level sensor 515 is activated by the controller to measure the level of the slurry in stir chamber 502.
- Controller 300 has been preprogrammed with data related to the volume of slurry present in stir chamber internal cavity 530 as a function of the height of the slurry column represented by the slurry level measurement, such as via a lookup table or appropriate equation.
- the controller executes a routine to readily correlate the level of the slurry measured in real-time (via detecting the top surface of the slurry) to a corresponding representative volume of slurry present based on the height of the slurry column detected. It is well within the ambit of those skilled in the art to program the controller with the appropriate data and software instructions to make the correlation between measured slurry surface level and volume.
- controller 300 calculates the overall density of the slurry based on the slurry weight/mass and slurry level measurements obtained by the strain gauge and level of the entire slurry sample in stir chamber 502. This recognizes that the slurry is not an ideally homogenous mixture, so that measuring the entire slurry sample averages out areas of lower or higher density in the slurry mass. It bears noting that the slurry weight and level measurements are preferably performed when the agitator 250 is not in operation so that the slurry is in a still and stable condition. This is desirable to ensure that accuracy for the slurry level detection and the weight/mass measurements.
- stirring device 500 further includes a spectrometer 550 to determine the water/solids ratio of the agricultural sample slurry.
- Spectrometer 550 is operably coupled to programmable controller 300 as shown in FIG. 9.
- the spectrometer may be mounted proximate to the bottom end of stir chamber 502, and in one non-limiting embodiment as illustrated may be mounted on the underside the chamber to maximize the spectrometer’s exposure to heavier-than-water particles in the sample slurry, which tend to settle to the bottom of the chamber.
- Spectrometer 550 comprises a lens 551 fluidly sealed to stir chamber 502 to give the spectrometer a line of sight directed upwards into internal cavity 530 of the stir chamber.
- the spectrometer 550 is configured and operable to measure reflectivity of the sample slurry in the stir chamber. More particularly, spectrometer 550 in one aspect is operable for measuring particle density (grams per milliliter) of the solids in the slurry. Based on the reflectivity Attorney Docket No.23075WO measurement of the sample solids in stir chamber 502, physical properties of the sample material can be determined, including the density of the solids (particles) in suspension in the sample slurry.
- controller 300 may be programmed to automatically calculate the water/solids ratio.
- the soil particle density can be predicted and correlated to the reflectivity measurements of the sample via experimental methods, which is well within the ambit of those skilled in the art. This information can form the basis for programming controller 300 to make the correlation between reflectivity and particle density automatically.
- the current actual ratio of water mass to sample solids (particles) mass in the sample slurry can further be determined by controller 300 based on the reflectivity readings. Based on the real-time or actual current ratio, the controller 300 will automatically adjust the sample slurry in stir chamber 502 as needed until the desired target water/solids ratio has been reached which is optimized for analysis of the sample in the chemical/property analysis unit 140 of the system (see, e.g., FIG. 9).
- One non-limiting embodiment of the process implemented by controller 300 to achieve the desired target water/solids ratio (i.e. mass ratio) based on reflectivity measurements collected by spectrometer 550 may include but is not limited to the following control steps. Step (1): Determining a real-time or actual current water/solids ratio based on reflectivity measurements of the sample recorded by spectrometer 550. Step (2) Comparing the actual water/solids ratio to a preprogrammed target water/solids ratio for the sample slurry.
- Step (3) Adjusting the actual water/solids ratio to meet the target water/solids ratio. For example, if the actual water/solids ratio is less than the target water/solids ratio, controller 300 adds water to the stir chamber 502 (via slurry inlet port 540, a separate water inlet port, or a slurry recirculation inlet port) and repeating steps (1) and (2) one or more times until the controller 300 determines that the target water/solids ratio in the sample slurry is met. For example, the controller will initiate a process to add water to stir chamber 502 if the actual current water/solids ratio is less than the target ratio (i.e. more Attorney Docket No.23075WO dilution water is needed in the slurry).
- the target ratio i.e. more Attorney Docket No.23075WO dilution water is needed in the slurry.
- controller 300 may briefly open isolation valve 525 to add an additional amount of slurry from grinder 110 into stir chamber 502. Steps (1) and (2) are again repeated as needed until the target ratio is met.
- a predetermined +/- variance in the target water/solids ratio may be programmed into controller 300 in some embodiments when permissible so that a measured actual water/solids ratio may be considered to meet the target water/solids ratio for purposes of the sample analysis if not greater or less than a programmed tolerance percentage.
- an acceptable target range of water/solids ratio may be used by the controller in some embodiments in lieu of a single absolute value for the target ratio.
- the pump 120 which takes suction for stir chamber 502 to transfer slurry to the analysis unit 140 may also be used to recirculate a portion of the sample slurry via recirculation line 120a along with adding water to the recirculated slurry from an external water source (see, e.g., FIG. 9) as the means to adjust (i.e. decrease) the water/solids ratio of the sample slurry in stir chamber 502.
- the spectrometer 550 may also be used to identify other properties of the sample, including but not limited to soil structure (e.g., sand content), color profile, and organic matter content. By monitoring the reflectance of the sample at various levels of agitation, properties of fractions of the sample can also be measured (e.g., stop agitating the sample and let heavy particles settle downward onto the lens 551 of the spectrometer). [0097] Once the desired target mass ratio of water to solids for the slurry has been reached, the sample slurry is ready for chemical analysis.
- Stirring device 500 includes a vertically-extending filtrate suction tube 521 through which pump 120 (a slurry pump in one embodiment) can extract slurry from the internal cavity 530 of stir chamber 502 via one or more filtrate outlet ports 520.
- pump 120 a slurry pump in one embodiment
- plural outlet ports may be provided which are fluidly coupled to the vertical suction tube 521 via a branched flow manifold 521a as shown.
- the use of multiple smaller filtrate outlet ports allows several samples to be drawn simultaneously from stir chamber 502 for different portions of the analysis unit to test for different analytes at the same time in parallel.
- a single larger filtrate outlet port may be used instead.
- the filtrate outlet ports 520 may be disposed in the upper housing section 511 of the stirring device and may extend laterally Attorney Docket No.23075WO through the upper housing section (see, e.g., FIGS.22-23) as shown.
- the filtrate suction tube 521 is suspended from the upper housing section 511 such that the weight of the tube is preferably supported solely by the upper housing section alone. This support configuration does not add to weight of the stir chamber when weighting the slurry via strain gauge 504, as described elsewhere herein.
- the filtrate outlet ports 520 could instead be disposed in the sidewall of the lower housing section 512 (stir chamber 502) such that the filtrate suction tube 521 would then be supported by the stir chamber and its weight taken into account when weighing the slurry.
- the filtrate suction tube 521 would then be supported by the stir chamber and its weight taken into account when weighing the slurry.
- the filtration feature may comprise a slurry secondary filter 522 (grinder 110 acting as the primary filter for large particle separation).
- Filter 522 is disposed upstream of pump 120 in the slurry flow circuit shown in FIG. 9.
- the filter 522 may be disposed inside stir chamber 502, and may be coupled to the filtrate suction tube 521 inside the internal cavity 530 of the stir chamber.
- filter 522 may be coupled to the bottom inlet end of suction tube 521 which hangs down from above into stir chamber internal cavity 530 and is suspended above the bottom of the cavity (see, e.g., FIG. 22).
- filter 522 may be a mesh filter comprising a mesh screen having a plurality of mesh openings sized to prevent solid particles exceeding a predetermined maximum size from being drawn into the filtrate suction tube 521 and passing downstream. Accordingly, the size of the screen openings of such a filter are sized in proportion to the smallest flow passage of the analysis equipment of analysis unit 140 to not pass particles exceeding the smallest flow passage size (e.g., diameter).
- the separation feature comprises limiting the rotational speed of the agitator 250 so that the heaviest (largest) particles in the sample slurry are not lifted high enough in the slurry column to be drawn toward and onto the secondary filter 522, which is located and suspended by a vertical distance above the floor or bottom of the stir chamber in internal cavity 530.
- agitator 250 has a maximum rotational speed selected to keep sample solids large particles at the bottom of the stir chamber 502, which prevents the large particles from being drawn to the secondary filter 522.
- the agitator is configured and operable to stir the slurry via the blade 253 at a maximum speed selected so that at least some larger particles drop out of suspension from the slurry and collect at a bottom of the internal cavity 530 of the stir chamber.
- the bottom or floor 530a of stir chamber internal cavity 530 may be sloped from side to side such that the portion of the floor beneath the filter may be lower than the portion of the floor beneath the agitator blade 253 (see, e.g., FIG. 21).
- This deeper portion of stir chamber internal cavity 530 beneath the filtrate suction tube 521 and filter 522 forms a recess or pocket in which larger particles can settle out of suspension and collect without being drawn upwards towards the filter 522.
- waste port 543 may be coupled to this deeper portion of the stir chamber internal cavity 530 beneath the filter 522 to more effectively flush residual solids out with water between slurry processing runs.
- a vacuum sensor 523 may be disposed upstream of pump 120 between secondary filter 522 and the pump to allow for the detection of a clogged secondary filter screen.
- vacuum sensor 523 may be fluidly coupled to and disposed on the filtrate suction tube 521 on the downstream filtrate side of secondary filter 522.
- the vacuum sensor may be operable coupled to programmable controller 300 to provide automatic detection of a plugged/clogged filter 522 by the controller. The controller may then terminate slurry extraction from stir chamber 502 by stopping operation of pump 120 until the clogged filter can be cleaned.
- vacuum sensor 523 may be fluidly coupled to the flow conduit 120b between pump 120 and stir chamber 502 (reference FIG. 9).
- pump 120 may be omitted altogether and the slurry filtrate may flow via gravity from stir chamber 502 to analysis unit 140 for processing and analysis for various analytes or other relevant properties of the agricultural sample.
- Attorney Docket No.23075WO [0104]
- the agricultural sample slurry preparation system including grinder-filter apparatus 110 and waste collection system including waste collection apparatus 160 disclosed herein is usable with and may form part of an overall agricultural sampling and analysis systems, such as but not limited to those described in U.S. Patent Application Publication No. 2018/0124992A1 and PCT Publication No.
- Example 1 a stirring device for processing an agricultural slurry comprising: a stir chamber comprising an upper housing section and a lower housing section defining an internal cavity configured to receive an agricultural sample slurry; a strain gauge structurally coupled to and independently supporting the stir chamber, the strain gauge configured and operable to Attorney Docket No.23075WO measure a weight of the stir chamber with and without slurry therein; wherein the stir chamber is mechanically isolated from other portions of the stirring device.
- Example 2 the stirring device according to Example 1, wherein the lower housing section is mechanically isolated from the upper housing section by an isolation air gap formed therebetween.
- Example 3 the stirring device according to Example 2, wherein the stir chamber is supported in a cantilevered manner by the strain gauge.
- Example 4 the stirring device according to any one of Examples 1-3, further comprising a level sensor disposed in the upper housing section, the level sensor being operable to measure a level of the slurry.
- Example 5 the stirring device according to Example 4, wherein the level sensor is a non- contact type level sensor having a line of sight into the stir chamber to detect the level of the slurry.
- Example 6 the stirring device according to Examples 4 or 5, further comprising a spectrometer mounted to the stir chamber, the spectrometer being operable to measure reflectivity of solids in the slurry in the stir chamber.
- Example 7 the stirring device according to Example 6, wherein the spectrometer is mounted proximate to a bottom end of the stir chamber and comprises a lens sealed to the stir chamber, the spectrometer having a line of sight into the stir chamber.
- Example 8 - the stirring device according to Example 6, further comprising a programmable controller operably coupled to the strain gauge, level sensor, and spectrometer, the controller being configured to determine a density of the sample slurry based on measurements obtained by the strain gauge and level sensor.
- Example 9 the stirring device according to Example 8, wherein the controller is configured to determine a water mass to solids mass ratio of the slurry via the reflectivity of the solids in the slurry measured by the spectrometer.
- Example 10 the stirring device according to any one of Examples 1-9, wherein the strain gauge is supported from the upper housing section via a bracket.
- Example 11 the stirring device according to Example 10, wherein the strain gauge comprises a first end coupled to the lower housing section and a second end coupled to the upper housing section by a bracket.
- Example 12 the stirring device according to Examples 2 or 3, wherein the stir chamber further comprises a slurry inlet port which is fluidly isolated from a slurry inlet conduit by an annular isolation air gap.
- Example 13 the stirring device according to Examples 2 or 3, wherein the stir chamber further comprising a vertically-extending filtrate suction tube configured to extract slurry from the internal cavity through one or more filtrate outlet ports of the stirring device.
- Example 14 the stirring device according to Example 13, wherein the one or more filtrate outlet ports are disposed in the upper housing section of the stirring device, and the filtrate suction tube is suspended in the internal cavity of the stir chamber from the upper housing section.
- Example 15 the stirring device according to Examples 13 or 14, wherein the filtrate suction tube extends vertically from at least a top end of the stir chamber down into a lower portion of the internal cavity of the stir chamber.
- Example 16 the stirring device according to any one of Examples 13-15, wherein the filtrate suction tube is fluidly coupled to a pump via the filtrate outlet ports, the pump operable to apply suction to the filtrate suction tube for extracting the slurry from the stir chamber.
- Example 17 the stirring device according to Example 16, further comprising a filter fluidly coupled to the filtrate suction tube inside the internal cavity of the stir chamber to filter the slurry.
- Example 18 the stirring device according to Example 17, wherein the filter comprises a mesh screen having openings sized to prevent solid particles exceeding a maximum size from being drawn into the filtrate suction tube.
- Example 19 the stirring device according to Examples 17 or 18, further comprising a vacuum sensor disposed upstream of the pump between the pump and the filter, the vacuum sensor operable to detect a vacuum condition which is indicative of a clogged condition of the filter.
- Example 20 the device according to any one of Examples 1-19, further comprising an agitator including a rotatable agitator shaft with blade disposed in the internal cavity of the stir chamber and a motor operably coupled to the agitator shaft, the agitator shaft being supported by the upper housing section of the stirring device independently of the stir chamber.
- Example 21 the device according to Example 20, wherein the agitator is configured and operable to stir the slurry via the blade at a maximum speed selected so that at least some particles Attorney Docket No.23075WO drop out of suspension from the slurry and collect at a bottom of the internal cavity of the stir chamber.
- Example 22 an agricultural slurry analysis system comprising: a stirring device comprising an upper housing section and a lower housing section defining a stir chamber configured to receive an agricultural sample slurry; a strain gauge coupled to the stir chamber, the strain gauge configured and operable to measure a weight of the stir chamber with and without slurry therein; a level sensor disposed in the upper housing section, the level sensor operable to measure a level of the slurry in the stir chamber; a programmable controller operably coupled to the strain gauge and level sensor, the controller being configured to: receive an actual weight measurement of the stir chamber via the strain gauge; determine a weight of the slurry in the stir chamber based on the actual weight measurement; receive an actual slurry level measurement from the level sensor; and determine a density of the slurry based on the actual weight measurement and the actual slurry level measurement.
- Example 23 the system according to Example 22, wherein the controller is configured to determine the weight of the slurry by receiving a first weight measurement of the stir chamber without the slurry therein, and a second weight measurement of the stir chamber with the slurry therein, the controller being configured to determine the weight of the slurry by subtracting the first weight measurement from the second weight measurement.
- Example 24 - the system according to Example 23, wherein the controller is configured to correlate the actual slurry level measurement with a corresponding volume of slurry in the stir chamber.
- Example 25 the system according to Example 24, wherein the controller is operable to determine the density of the slurry by dividing the weight of the slurry by the volume of the slurry in the stir chamber.
- Example 26 the system according to any one of Examples 22-25, further comprising a spectrometer configured to measure a density of particles in suspension within the slurry, and the controller determining an actual water mass to soil mass ratio of the slurry based on the particle density measurement.
- Example 27 the system according to Example 26, wherein the spectrometer is configured to measure reflectivity of the particles to determine the density of the particles.
- Attorney Docket No.23075WO [0133]
- Example 28 - the system according to Examples 26 or 27, wherein the controller compares the actual water mass to soil mass ratio with a preprogrammed target water mass to soil mass ratio.
- Example 29 the system according to Example 28, wherein the controller is configured to initiate a process to add water to the stir chamber when the actual water mass to soil mass ratio is less than the target water mass to soil mass ratio.
- Example 30 the system according to any one of Examples 22-29, further comprising a pump configured to draw slurry from the stir chamber through a filter.
- Example 31 the system according to Example 30, further comprising a vacuum sensor operably coupled to the controller and disposed upstream of the pump in a slurry flow circuit, the vacuum sensor operable to detect a vacuum condition between the pump and filter which is indicative of a clogged filter.
- Example 32 the system according to Example 31, wherein the controller is operable to terminate operation of the pump upon detection of the vacuum condition.
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Abstract
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Priority Applications (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP24708888.3A EP4728259A1 (en) | 2023-06-15 | 2024-02-26 | System for agricultural sample slurry analysis and related methods |
| CN202480039776.6A CN121311752A (en) | 2023-06-15 | 2024-02-26 | Systems and related methods for analyzing agricultural sample slurries |
| AU2024305239A AU2024305239A1 (en) | 2023-06-15 | 2024-02-26 | System for agricultural sample slurry analysis and related methods |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US202363508341P | 2023-06-15 | 2023-06-15 | |
| US63/508,341 | 2023-06-15 |
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| Publication Number | Publication Date |
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| WO2024256880A1 true WO2024256880A1 (en) | 2024-12-19 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PCT/IB2024/051820 Ceased WO2024256880A1 (en) | 2023-06-15 | 2024-02-26 | System for agricultural sample slurry analysis and related methods |
Country Status (5)
| Country | Link |
|---|---|
| EP (1) | EP4728259A1 (en) |
| CN (1) | CN121311752A (en) |
| AR (1) | AR132119A1 (en) |
| AU (1) | AU2024305239A1 (en) |
| WO (1) | WO2024256880A1 (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6364062B1 (en) | 1999-11-08 | 2002-04-02 | Otis Elevator Company | Linear tracking mechanism for elevator rope |
| US20180124992A1 (en) | 2016-11-07 | 2018-05-10 | The Climate Corporation | Agricultural implements for soil and vegetation analysis |
| WO2020012369A2 (en) | 2018-07-10 | 2020-01-16 | Precision Planting Llc | Agricultural sampling system and related methods |
| US20210269331A1 (en) * | 2018-07-10 | 2021-09-02 | Vermeer Manufacturing Company | Systems and methods for dewatering slurries |
-
2024
- 2024-02-26 EP EP24708888.3A patent/EP4728259A1/en active Pending
- 2024-02-26 CN CN202480039776.6A patent/CN121311752A/en active Pending
- 2024-02-26 AU AU2024305239A patent/AU2024305239A1/en active Pending
- 2024-02-26 WO PCT/IB2024/051820 patent/WO2024256880A1/en not_active Ceased
- 2024-03-13 AR ARP240100615A patent/AR132119A1/en unknown
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6364062B1 (en) | 1999-11-08 | 2002-04-02 | Otis Elevator Company | Linear tracking mechanism for elevator rope |
| US20180124992A1 (en) | 2016-11-07 | 2018-05-10 | The Climate Corporation | Agricultural implements for soil and vegetation analysis |
| WO2020012369A2 (en) | 2018-07-10 | 2020-01-16 | Precision Planting Llc | Agricultural sampling system and related methods |
| US20210269331A1 (en) * | 2018-07-10 | 2021-09-02 | Vermeer Manufacturing Company | Systems and methods for dewatering slurries |
Also Published As
| Publication number | Publication date |
|---|---|
| CN121311752A (en) | 2026-01-09 |
| EP4728259A1 (en) | 2026-04-22 |
| AU2024305239A1 (en) | 2026-01-22 |
| AR132119A1 (en) | 2025-05-28 |
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