WO2024000915A1 - Porous ceramic atomizing core and preparation method therefor, and aerosol generating device - Google Patents

Porous ceramic atomizing core and preparation method therefor, and aerosol generating device Download PDF

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WO2024000915A1
WO2024000915A1 PCT/CN2022/124315 CN2022124315W WO2024000915A1 WO 2024000915 A1 WO2024000915 A1 WO 2024000915A1 CN 2022124315 W CN2022124315 W CN 2022124315W WO 2024000915 A1 WO2024000915 A1 WO 2024000915A1
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ceramic
powder
atomizing core
mesh
binder
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PCT/CN2022/124315
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French (fr)
Chinese (zh)
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宋文正
吴凤霞
李俊辉
胡勇齐
齐会龙
聂革
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深圳市吉迩科技有限公司
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    • C04B38/00Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
    • C04B38/06Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof by burning-out added substances by burning natural expanding materials or by sublimating or melting out added substances
    • C04B38/063Preparing or treating the raw materials individually or as batches
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    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
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    • C04B35/01Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
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Definitions

  • the present application relates to an aerosol generating device, and more specifically to a porous ceramic atomizing core and its preparation method and aerosol generating device.
  • the purpose of this application is to overcome the shortcomings of the existing technology and provide a porous ceramic atomizing core, its preparation method and an aerosol generating device, which have the advantages of low sintering temperature, small shrinkage, high strength, high porosity and uniform pore size.
  • ceramic powder includes wollastonite, diatomite and glass powder
  • the ceramic composite powder and the binder are subjected to an internal mixing process to obtain a ceramic block;
  • the ceramic particles and metal felt are inlaid and injection molded to obtain a ceramic body with a heating film;
  • the ceramic body is sintered to obtain a porous ceramic atomizing core.
  • the further technical solution is: the conditions for the mixture grinding treatment are: adding zirconia balls and grinding for 1-3 hours.
  • the further technical solution is to carry out the internal mixing process of the ceramic composite powder and the binder to obtain the ceramic block, which includes the following processing steps:
  • a further technical solution is that the binder is two or more of paraffin, beeswax, polyethylene and stearic acid.
  • the ceramic particles are uniform particles of 2-3 microns.
  • the conditions for the sintering treatment are: heating to 80°C at a heating rate of 60-100°C/h, holding for 0.5-1h, and then heating to 130°C at a heating rate of 30-60°C/h. Keep it warm for 1-3h, then raise it to 240°C at a heating rate of 10-50°C/h, keep it warm for 2-4h, then raise it to 310°C at a heating rate of 10-30°C/h, keep it warm for 1-2 hours, and then keep it warm for 1-2 hours.
  • the further technical solution is to mix and grind ceramic powder, sintering aid and pore-forming agent to obtain ceramic composite powder, wherein the ceramic powder includes wollastonite, diatomite and glass.
  • the ceramic powder includes wollastonite, diatomite and glass.
  • the wollastonite is 5%-20%
  • the diatomite is 10%-40%
  • the glass powder is 10%-25%
  • the sintering aid The content of the pore-forming agent is 3%-15%
  • the pore-forming agent is 10%-30%.
  • the particle size of the glass powder is one or two of 325 mesh and 600 mesh
  • the sintering aid is kaolin, white clay, titanium oxide, cordierite, potassium feldspar, perlite, One or more bauxite
  • the pore-forming agent is one or two of starch, polystyrene microspheres, and polymethylmethacrylate.
  • this application uses metal felt as the heating film of the atomization core.
  • the resistance of the metal felt is controllable, and the sintering shrinkage of the metal felt is small, thereby improving the atomization effect and yield rate.
  • wollastonite and diatomite are used as base materials. Since wollastonite has good thermal expansion, the drying shrinkage and firing shrinkage of the ceramic material are very small.
  • Glass powder, titanium oxide, boron nitride, Kaolin, feldspar, cordierite, etc. are used as sintering aids, which can increase strength and reduce sintering temperature.
  • Polymethyl methacrylate, polystyrene microspheres, starch, etc. are used as pore-forming agents. The selected pore-forming agents The agent particles are uniform and the porosity and pore size can be well controlled. Detailed description is as follows.
  • Figure 1 is an experimental data table of the embodiment of the present application.
  • the embodiment of the present application discloses a method for preparing a porous ceramic atomizing core, which includes the following steps: step 1 to step 4.
  • Step 1 Mix and grind ceramic powder, sintering aid and pore-forming agent to obtain ceramic composite powder, where the ceramic powder includes wollastonite, diatomite and glass powder.
  • wollastonite and diatomite as base materials, wollastonite has good thermal expansion, which makes the drying shrinkage and firing shrinkage of the ceramic material very small, thus making the ceramic atomizer core produced with a small shrinkage rate.
  • step 1 in terms of mass percentage, wollastonite is 5%-20%, diatomite is 10%-40%, glass powder is 10%-25%, and sintering aid is 3% -15%, pore-forming agent is 10%-30%.
  • the particle size of wollastonite is one or more of 325 mesh, 600 mesh, and 900 mesh
  • the particle size of diatomite is 200 mesh, 500 mesh, or 700 mesh.
  • the particle size of the glass powder is one or two of 325 mesh and 600 mesh
  • the sintering aid is kaolin, white clay, titanium oxide, cordierite, potassium feldspar, perlite, bauxite
  • the pore-forming agent is one or two of starch, polystyrene microspheres, and polymethylmethacrylate.
  • Using glass powder, titanium oxide, boron nitride, kaolin, feldspar, cordierite, etc. as sintering aids can increase strength and reduce sintering temperature.
  • Polymethyl methacrylate, polystyrene microspheres, starch, etc. are used as pore-forming agents.
  • the selected pore-forming agent particles are uniform and can well control the porosity and pore size.
  • Step 2 Mix the ceramic composite powder and the binder to obtain a ceramic block.
  • step 2 specifically includes the following sub-steps: step 21 and step 22.
  • Step 21 Stir the adhesive for half an hour until it is completely melted.
  • Step 22 Add the ceramic composite powder into the completely melted binder in multiple batches, stir for 6-8 hours, and collect for later use.
  • steps 21 and 22 weigh the adhesive in a certain proportion and put it into the internal mixer, set the appropriate temperature and rotation speed, and stir for half an hour until it is completely melted and turned into a clear liquid. Add the mixed ceramic composite powder to the internal mixer in multiple batches, stir for 6-8 hours and then collect it for later use to obtain a stable ceramic mass.
  • the binder is two or more of paraffin, beeswax, polyethylene, and stearic acid.
  • the binder is composed of 30%-70% paraffin, 15%-40% beeswax, 0-7% polyethylene, and 0-10% stearic acid in terms of mass percentage.
  • Step 3 Granulate the ceramic blocks.
  • the ceramic particles are uniform particles of 2-3 microns.
  • Step 4 The ceramic particles and metal felt are inlaid and injection molded to obtain a ceramic body with a heating film.
  • the metal felt into the mold, and obtain a regular-shaped ceramic body with a heating film through the inlay process and injection molding process. Since metal felt is used as the heating film of the atomizing core, the resistance of the metal felt is controllable, and the sintering shrinkage of the metal felt is small, thus improving the atomization effect and yield rate.
  • Step 5 Sintering the ceramic body to obtain a porous ceramic atomizing core.
  • the ceramic body is placed in a sintering furnace and cooled to obtain a porous ceramic atomizing core.
  • the conditions for sintering treatment are: heating to 80°C at a heating rate of 60-100°C/h, holding for 0.5-1h, then heating to 130°C at a heating rate of 30-60°C/h, holding for 1-3h, and then holding for 10 Heating to 240°C at a heating rate of -50°C/h, holding for 2-4h, then heating to 310°C at a heating rate of 10-30°C/h, holding for 1-2h, and then heating at a heating rate of 10-30°C/h
  • the temperature is increased to 390°C, maintained for 1-2h, then heated to 500°C at a heating rate of 30-50°C/h, kept for 1-2h, and then heated to 600-800°C at a heating rate of 60-100°C/h. °C, keep warm for 1-2h, and finally cool to room temperature.
  • the embodiment of the present application also discloses a porous ceramic atomizing core produced by the above preparation method.
  • the porous ceramic atomizing core has the advantages of low sintering temperature, small shrinkage, high strength, high porosity and uniform pore size.
  • the embodiment of the present application also discloses an aerosol generating device, which includes a host machine and the above-mentioned porous ceramic atomizing core.
  • the porous ceramic atomizing core is installed on the host machine, and the host machine provides power and atomization control for the atomizing core.
  • the preparation method of porous ceramic atomizing core includes the following steps:
  • the preparation method of porous ceramic atomizing core includes the following steps:
  • the preparation method of porous ceramic atomizing core includes the following steps:

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  • Compositions Of Oxide Ceramics (AREA)

Abstract

Embodiments of the present application disclose a porous ceramic atomizing core and a preparation method therefor, and an aerosol generating device. The method comprises: mixing and grinding ceramic powder, a sintering aid, and a pore forming agent to obtain ceramic composite powder, wherein the ceramic powder comprises wollastonite, diatomite, and glass powder; carrying out internal mixing on the ceramic composite powder and a binder to obtain a ceramic material block; granulating the ceramic material block to obtain ceramic particles; inlaying and injection molding the ceramic particles and a metal felt to obtain a ceramic body having a heating film; and sintering the ceramic body to obtain a porous ceramic atomizing core. The present application has the advantages of low sintering temperature, small shrinkage, high strength, high porosity, and uniform pore diameter.

Description

多孔陶瓷雾化芯及其制备方法和气溶胶产生装置Porous ceramic atomizing core and its preparation method and aerosol generating device 技术领域Technical field
本申请涉及气溶胶产生装置,更具体地说是多孔陶瓷雾化芯及其制备方法和气溶胶产生装置。The present application relates to an aerosol generating device, and more specifically to a porous ceramic atomizing core and its preparation method and aerosol generating device.
背景技术Background technique
目前常见的陶瓷雾化芯的发热膜通过厚膜印刷工艺制备,厚膜印刷工艺只能在平面上进行,但发热膜的阻值受到电子浆料、烧结温度等因素的影响,波动范围比较大,从而会影响产品的良品率与气溶胶产生基质的雾化效果,另外,常见的多孔陶瓷由高温烧结制备,对能源消耗大,而且收缩率大,产品尺寸不易控制,良品率低,从而造成成本增加。At present, the heating film of the common ceramic atomizing core is prepared through a thick film printing process. The thick film printing process can only be performed on a flat surface. However, the resistance of the heating film is affected by factors such as electronic paste and sintering temperature, and the fluctuation range is relatively large. , which will affect the product yield and the atomization effect of the aerosol-generating matrix. In addition, common porous ceramics are prepared by high-temperature sintering, which consumes a lot of energy and has a large shrinkage rate. The product size is difficult to control and the yield rate is low, resulting in Increased costs.
发明内容Contents of the invention
本申请的目的在于克服现有技术的不足,提供多孔陶瓷雾化芯及其制备方法和气溶胶产生装置,以具有烧结温度低、收缩率小、强度高、孔隙率高、孔径均匀的优点。The purpose of this application is to overcome the shortcomings of the existing technology and provide a porous ceramic atomizing core, its preparation method and an aerosol generating device, which have the advantages of low sintering temperature, small shrinkage, high strength, high porosity and uniform pore size.
为实现上述目的,本申请采用以下技术方案:In order to achieve the above purpose, this application adopts the following technical solutions:
上述说明仅是本申请技术方案的概述,为了能够更清楚了解本申请技术手段,可依照说明书的内容予以实施,并且为了让本申请的上述和其它目的、特征及优点能够更明显易懂,以下特举较佳实施例,详第一方面,多孔陶瓷雾化芯的制备方法,包括以下步骤:The above description is only an overview of the technical solutions of the present application. In order to have a clearer understanding of the technical solutions of the present application, they can be implemented in accordance with the contents of the description. In order to make the above and other purposes, features and advantages of the present application more obvious and easy to understand, the following A preferred embodiment is specifically cited to describe the first aspect, the preparation method of the porous ceramic atomizing core, including the following steps:
将陶瓷粉体、助烧剂和造孔剂进行混料研磨处理,以得到陶瓷复合粉体,其中,所述陶瓷粉体包括硅灰石、硅藻土和玻璃粉;Mixing and grinding ceramic powder, sintering aid and pore-forming agent to obtain ceramic composite powder, wherein the ceramic powder includes wollastonite, diatomite and glass powder;
将所述陶瓷复合粉体与粘结剂进行密炼处理,以得到陶瓷料块;The ceramic composite powder and the binder are subjected to an internal mixing process to obtain a ceramic block;
将陶瓷料块进行造粒处理,以得到陶瓷颗粒;Granulating the ceramic material blocks to obtain ceramic particles;
将陶瓷颗粒与金属毛毡经过镶嵌和注塑成型处理,以得到带发热膜的陶瓷坯体;The ceramic particles and metal felt are inlaid and injection molded to obtain a ceramic body with a heating film;
将陶瓷坯体进行烧结处理,以得到多孔陶瓷雾化芯。The ceramic body is sintered to obtain a porous ceramic atomizing core.
其进一步技术方案为:所述混料研磨处理的条件为:加入氧化锆球,且研磨1-3小时。The further technical solution is: the conditions for the mixture grinding treatment are: adding zirconia balls and grinding for 1-3 hours.
其进一步技术方案为:所述将所述陶瓷复合粉体与粘结剂进行密炼处理,以得到陶瓷料块,包括以下处理步骤:The further technical solution is to carry out the internal mixing process of the ceramic composite powder and the binder to obtain the ceramic block, which includes the following processing steps:
将粘结剂搅拌半个小时,使其完全融化;Stir the binder for half an hour until it is completely melted;
将陶瓷复合粉体分多次加入完全融化的粘结剂中,并搅拌6-8小时后收集备用。Add the ceramic composite powder to the completely melted binder in multiple batches, stir for 6-8 hours and then collect for later use.
其进一步技术方案为:所述粘结剂为石蜡、蜂蜡、聚乙烯、硬脂酸中的两种或多种。A further technical solution is that the binder is two or more of paraffin, beeswax, polyethylene and stearic acid.
其进一步技术方案为:所述陶瓷颗粒为2-3微米的均匀颗粒。A further technical solution is that the ceramic particles are uniform particles of 2-3 microns.
其进一步技术方案为:所述烧结处理的条件为:以60-100℃/h的升温速率升温到80℃,保温0.5-1h,接着以30-60℃/h的升温速率升温到130℃,保温1-3h,再以10-50℃/h的升温速率升温到240℃,保温2-4h,然后以10-30℃/h的升温速率升温到310℃,保温1-2h,再然后以10-30℃/h的升温速率升温到390℃,保温1-2h,再然后以30-50℃/h的升温速率升温到500℃,保温1-2h,再然后以60-100℃/h的升温速率升温到600-800℃,保温1-2h,最后冷却至室温。The further technical solution is: the conditions for the sintering treatment are: heating to 80°C at a heating rate of 60-100°C/h, holding for 0.5-1h, and then heating to 130°C at a heating rate of 30-60°C/h. Keep it warm for 1-3h, then raise it to 240°C at a heating rate of 10-50°C/h, keep it warm for 2-4h, then raise it to 310°C at a heating rate of 10-30°C/h, keep it warm for 1-2 hours, and then keep it warm for 1-2 hours. Raise the temperature to 390℃ at a heating rate of 10-30℃/h, keep it warm for 1-2h, and then raise it to 500℃ at a heating rate of 30-50℃/h, keep it warm for 1-2h, and then heat it up at a temperature of 60-100℃/h. Raise the temperature to 600-800℃ at a high heating rate, keep it warm for 1-2h, and finally cool to room temperature.
其进一步技术方案为:所述将陶瓷粉体、助烧剂和造孔剂进行混料研磨处理,以得到陶瓷复合粉体,其中,所述陶瓷粉体包括硅灰石、硅藻土和玻璃粉的步骤中,按质量百分比计算,所述硅灰石为5%-20%,所述硅藻土为10%-40%,所述玻璃粉为10%-25%,所述助烧剂为3%-15%,所述造孔剂为10%-30%。The further technical solution is to mix and grind ceramic powder, sintering aid and pore-forming agent to obtain ceramic composite powder, wherein the ceramic powder includes wollastonite, diatomite and glass. In the step of adding powder, in terms of mass percentage, the wollastonite is 5%-20%, the diatomite is 10%-40%, the glass powder is 10%-25%, and the sintering aid The content of the pore-forming agent is 3%-15%, and the pore-forming agent is 10%-30%.
其进一步技术方案为:所述将陶瓷粉体、助烧剂和造孔剂进行混料研 磨处理,以得到陶瓷复合粉体,其中,所述陶瓷粉体包括硅灰石、硅藻土和玻璃粉的步骤中,所述硅灰石的粒径为325目、600目、900目中的一种或多种,所述硅藻土的粒径为200目、500目、700目中的一种或两种,所述玻璃粉的粒径为325目、600目中的一种或两种,所述助烧剂为高岭土、白粘土、氧化钛、堇青石、钾长石、珍珠岩、铝矾土中的一种或多种,所述造孔剂为淀粉、聚苯乙烯微球、聚甲基丙烯酸甲酯中的一种或两种。The further technical solution is to mix and grind ceramic powder, sintering aid and pore-forming agent to obtain ceramic composite powder, wherein the ceramic powder includes wollastonite, diatomite and glass. In the step of powdering, the particle size of the wollastonite is one or more of 325 mesh, 600 mesh, and 900 mesh, and the particle size of the diatomite is one of 200 mesh, 500 mesh, and 700 mesh. One or two types, the particle size of the glass powder is one or two of 325 mesh and 600 mesh, the sintering aid is kaolin, white clay, titanium oxide, cordierite, potassium feldspar, perlite, One or more bauxite, and the pore-forming agent is one or two of starch, polystyrene microspheres, and polymethylmethacrylate.
第二方面,一种多孔陶瓷雾化芯,采用上述的制备方法制得。In the second aspect, a porous ceramic atomizing core is prepared using the above preparation method.
第三方面,一种气溶胶产生装置,包括主机以及上述的多孔陶瓷雾化芯;所述多孔陶瓷雾化芯安装于所述主机上。In a third aspect, an aerosol generating device includes a main machine and the above-mentioned porous ceramic atomizing core; the porous ceramic atomizing core is installed on the main machine.
本申请与现有技术相比的有益效果是:本申请采用金属毛毡作为雾化芯的发热膜,金属毛毡的阻值可控,而且金属毛毡烧结收缩小,从而提升了雾化效果和良品率,另外,以硅灰石与硅藻土为基体材料,由于硅灰石具有良好的热膨胀性,使陶瓷料的干燥收缩与烧成收缩都很小,以玻璃粉、氧化钛、氮化硼、高岭土、长石、堇青石等为助烧剂,能起到增加强度,降低烧结温度的作用,以聚甲基丙烯酸甲酯、聚苯乙烯微球、淀粉等为造孔剂,选用的造孔剂颗粒均匀,可以很好的控制孔隙率与孔径大小。细说明如下。The beneficial effects of this application compared with the existing technology are: this application uses metal felt as the heating film of the atomization core. The resistance of the metal felt is controllable, and the sintering shrinkage of the metal felt is small, thereby improving the atomization effect and yield rate. , In addition, wollastonite and diatomite are used as base materials. Since wollastonite has good thermal expansion, the drying shrinkage and firing shrinkage of the ceramic material are very small. Glass powder, titanium oxide, boron nitride, Kaolin, feldspar, cordierite, etc. are used as sintering aids, which can increase strength and reduce sintering temperature. Polymethyl methacrylate, polystyrene microspheres, starch, etc. are used as pore-forming agents. The selected pore-forming agents The agent particles are uniform and the porosity and pore size can be well controlled. Detailed description is as follows.
附图说明Description of drawings
为了更清楚地说明本申请实施例技术方案,下面将对实施例描述中所需要使用的附图作简单地介绍,显而易见地,下面描述中的附图是本申请的一些实施例,对于本领域普通技术人员来讲,在不付出创造性劳动的前提下,还可以根据这些附图获得其他的附图。In order to more clearly illustrate the technical solutions of the embodiments of the present application, the drawings needed to be used in the description of the embodiments will be briefly introduced below. Obviously, the drawings in the following description are some embodiments of the present application, which are of great significance to this field. Ordinary technicians can also obtain other drawings based on these drawings without exerting creative work.
图1为本申请实施例的实验数据表格。Figure 1 is an experimental data table of the embodiment of the present application.
具体实施方式Detailed ways
下面将结合本申请具体实施例,对本申请的技术方案进行清楚、完整 地描述,显然,所描述的实施例是本申请一部分实施例,而不是全部的实施例。基于本申请中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本申请保护的范围。The technical solution of the present application will be clearly and completely described below with reference to specific embodiments of the present application. Obviously, the described embodiments are part of the embodiments of the present application, rather than all of the embodiments. Based on the embodiments in this application, all other embodiments obtained by those of ordinary skill in the art without creative efforts fall within the scope of protection of this application.
应当理解,当在本说明书和权利要求书中使用时,术语“包括”和“包含”指示所描述特征、整体、步骤、操作、元素和/或组件的存在,但并不排除一个或多个其它特征、整体、步骤、操作、元素、组件和/或其集合的存在或添加。It should be understood that, when used in this specification and claims, the terms "comprising" and "comprising" indicate the presence of described features, integers, steps, operations, elements and/or components but do not exclude the presence of one or more The presence or addition of other features, integers, steps, operations, elements, components and/or collections thereof.
还应当理解,在本申请说明书中所使用的术语仅仅是出于描述特定实施例的目的而并不意在限制本申请。如在本申请说明书和所附权利要求书中所使用的那样,除非上下文清楚地指明其它情况,否则单数形式的“一”、“一个”及“该”意在包括复数形式。It should also be understood that the terminology used in the specification of the present application is for the purpose of describing particular embodiments only and is not intended to be limiting of the application. As used in this specification and the appended claims, the singular forms "a", "an" and "the" are intended to include the plural forms unless the context clearly dictates otherwise.
还应当进一步理解,在本申请说明书和所附权利要求书中使用的术语“和/或”是指相关联列出的项中的一个或多个的任何组合以及所有可能组合,并且包括这些组合。It will be further understood that the term "and/or" as used in this specification and the appended claims refers to and includes any and all possible combinations of one or more of the associated listed items. .
本申请实施例公开了一种多孔陶瓷雾化芯的制备方法,包括以下步骤:步骤1-步骤4。The embodiment of the present application discloses a method for preparing a porous ceramic atomizing core, which includes the following steps: step 1 to step 4.
步骤1:将陶瓷粉体、助烧剂和造孔剂进行混料研磨处理,以得到陶瓷复合粉体,其中,陶瓷粉体包括硅灰石、硅藻土和玻璃粉。Step 1: Mix and grind ceramic powder, sintering aid and pore-forming agent to obtain ceramic composite powder, where the ceramic powder includes wollastonite, diatomite and glass powder.
按一比例将硅灰石、硅藻土、玻璃粉助烧剂和造孔剂放入球磨机中,加入质量比为1:2的氧化锆球,球磨1-3小时后收集备用。Put wollastonite, diatomaceous earth, glass powder sintering aid and pore-forming agent into a ball mill in a proportion, add zirconia balls with a mass ratio of 1:2, and collect after ball milling for 1-3 hours for later use.
通过以硅灰石与硅藻土为基体材料,由于硅灰石具有良好的热膨胀性,使陶瓷料的干燥收缩与烧成收缩都很小,进而使得制作出的陶瓷雾化芯,收缩率小。By using wollastonite and diatomite as base materials, wollastonite has good thermal expansion, which makes the drying shrinkage and firing shrinkage of the ceramic material very small, thus making the ceramic atomizer core produced with a small shrinkage rate. .
在一实施例中,步骤1中,按质量百分比计算,硅灰石为5%-20%,硅藻土为10%-40%,玻璃粉为10%-25%,助烧剂为3%-15%,造孔剂为10%-30%。In one embodiment, in step 1, in terms of mass percentage, wollastonite is 5%-20%, diatomite is 10%-40%, glass powder is 10%-25%, and sintering aid is 3% -15%, pore-forming agent is 10%-30%.
在一实施例中,步骤1中,硅灰石的粒径为325目、600目、900目中的一 种或多种,硅藻土的粒径为200目、500目、700目中的一种或两种,玻璃粉的粒径为325目、600目中的一种或两种,助烧剂为高岭土、白粘土、氧化钛、堇青石、钾长石、珍珠岩、铝矾土中的一种或多种,造孔剂为淀粉、聚苯乙烯微球、聚甲基丙烯酸甲酯中的一种或两种。In one embodiment, in step 1, the particle size of wollastonite is one or more of 325 mesh, 600 mesh, and 900 mesh, and the particle size of diatomite is 200 mesh, 500 mesh, or 700 mesh. One or two types, the particle size of the glass powder is one or two of 325 mesh and 600 mesh, and the sintering aid is kaolin, white clay, titanium oxide, cordierite, potassium feldspar, perlite, bauxite One or more of them, the pore-forming agent is one or two of starch, polystyrene microspheres, and polymethylmethacrylate.
以玻璃粉、氧化钛、氮化硼、高岭土、长石、堇青石等为助烧剂,能起到增加强度,降低烧结温度的作用。Using glass powder, titanium oxide, boron nitride, kaolin, feldspar, cordierite, etc. as sintering aids can increase strength and reduce sintering temperature.
以聚甲基丙烯酸甲酯、聚苯乙烯微球、淀粉等为造孔剂,选用的造孔剂颗粒均匀,可以很好的控制孔隙率与孔径大小。Polymethyl methacrylate, polystyrene microspheres, starch, etc. are used as pore-forming agents. The selected pore-forming agent particles are uniform and can well control the porosity and pore size.
步骤2:将陶瓷复合粉体与粘结剂进行密炼处理,以得到陶瓷料块。Step 2: Mix the ceramic composite powder and the binder to obtain a ceramic block.
在一实施例中,步骤2具体包括以下子步骤:步骤21、步骤22。In one embodiment, step 2 specifically includes the following sub-steps: step 21 and step 22.
步骤21、将粘结剂搅拌半个小时,使其完全融化。Step 21: Stir the adhesive for half an hour until it is completely melted.
步骤22、将陶瓷复合粉体分多次加入完全融化的粘结剂中,并搅拌6-8小时后收集备用。Step 22: Add the ceramic composite powder into the completely melted binder in multiple batches, stir for 6-8 hours, and collect for later use.
对于步骤21、步骤22,以一定的比例称量粘接剂放入密炼机,设置合适的温度与转速,搅拌半个小时,将其完全融化,状态为清澈的液体。将混合后的陶瓷复合粉体分多次加入密炼机,搅拌6-8小时后收集备用,得到稳定的陶瓷料块。For steps 21 and 22, weigh the adhesive in a certain proportion and put it into the internal mixer, set the appropriate temperature and rotation speed, and stir for half an hour until it is completely melted and turned into a clear liquid. Add the mixed ceramic composite powder to the internal mixer in multiple batches, stir for 6-8 hours and then collect it for later use to obtain a stable ceramic mass.
在一实施例中,粘结剂为石蜡、蜂蜡、聚乙烯、硬脂酸中的两种或多种。In one embodiment, the binder is two or more of paraffin, beeswax, polyethylene, and stearic acid.
在一实施例中,按质量百分比计算,由石蜡为30%-70%,蜂蜡为15%-40%,聚乙烯为0-7%,硬脂酸为0-10%构成粘结剂。In one embodiment, the binder is composed of 30%-70% paraffin, 15%-40% beeswax, 0-7% polyethylene, and 0-10% stearic acid in terms of mass percentage.
步骤3:将陶瓷料块进行造粒处理。优选地,陶瓷颗粒为2-3微米的均匀颗粒。Step 3: Granulate the ceramic blocks. Preferably, the ceramic particles are uniform particles of 2-3 microns.
步骤4:将陶瓷颗粒与金属毛毡经过镶嵌和注塑成型处理,以得到带发热膜的陶瓷坯体。Step 4: The ceramic particles and metal felt are inlaid and injection molded to obtain a ceramic body with a heating film.
将造粒料放入注塑机的料筒,将金属毛毡放入模具,经过镶嵌工艺与注塑成型工艺得到形状规则的带发热膜的陶瓷坯体。由于采用金属毛毡作为雾化芯 的发热膜,金属毛毡的阻值可控,而且金属毛毡烧结收缩小,从而提升了雾化效果和良品率,Put the granulated material into the barrel of the injection molding machine, put the metal felt into the mold, and obtain a regular-shaped ceramic body with a heating film through the inlay process and injection molding process. Since metal felt is used as the heating film of the atomizing core, the resistance of the metal felt is controllable, and the sintering shrinkage of the metal felt is small, thus improving the atomization effect and yield rate.
步骤5:将陶瓷坯体进行烧结处理,以得到多孔陶瓷雾化芯。Step 5: Sintering the ceramic body to obtain a porous ceramic atomizing core.
将陶瓷坯体放入烧结炉处理,冷却后得到多孔陶瓷雾化芯。The ceramic body is placed in a sintering furnace and cooled to obtain a porous ceramic atomizing core.
烧结处理的条件为:以60-100℃/h的升温速率升温到80℃,保温0.5-1h,接着以30-60℃/h的升温速率升温到130℃,保温1-3h,再以10-50℃/h的升温速率升温到240℃,保温2-4h,然后以10-30℃/h的升温速率升温到310℃,保温1-2h,再然后以10-30℃/h的升温速率升温到390℃,保温1-2h,再然后以30-50℃/h的升温速率升温到500℃,保温1-2h,再然后以60-100℃/h的升温速率升温到600-800℃,保温1-2h,最后冷却至室温。The conditions for sintering treatment are: heating to 80℃ at a heating rate of 60-100℃/h, holding for 0.5-1h, then heating to 130℃ at a heating rate of 30-60℃/h, holding for 1-3h, and then holding for 10 Heating to 240℃ at a heating rate of -50℃/h, holding for 2-4h, then heating to 310℃ at a heating rate of 10-30℃/h, holding for 1-2h, and then heating at a heating rate of 10-30℃/h The temperature is increased to 390℃, maintained for 1-2h, then heated to 500℃ at a heating rate of 30-50℃/h, kept for 1-2h, and then heated to 600-800℃ at a heating rate of 60-100℃/h. ℃, keep warm for 1-2h, and finally cool to room temperature.
本申请实施例还公开了一种上述制备方法制得的多孔陶瓷雾化芯,该多孔陶瓷雾化芯烧结温度低、收缩率小、强度高、孔隙率高、孔径均匀的优点。The embodiment of the present application also discloses a porous ceramic atomizing core produced by the above preparation method. The porous ceramic atomizing core has the advantages of low sintering temperature, small shrinkage, high strength, high porosity and uniform pore size.
本申请实施例还公开了一种气溶胶产生装置,包括主机以及上述的多孔陶瓷雾化芯,多孔陶瓷雾化芯安装于主机上,主机为雾化芯提供电源及雾化控制。The embodiment of the present application also discloses an aerosol generating device, which includes a host machine and the above-mentioned porous ceramic atomizing core. The porous ceramic atomizing core is installed on the host machine, and the host machine provides power and atomization control for the atomizing core.
为了使本技术领域的人员更好地理解本申请技术方案,下面将结合附图,对本申请实施例中的技术方案进行更清楚、完整地描述。In order to enable those skilled in the art to better understand the technical solutions of the present application, the technical solutions in the embodiments of the present application will be described more clearly and completely below in conjunction with the accompanying drawings.
实施例1Example 1
多孔陶瓷雾化芯的制备方法,包括以下步骤:The preparation method of porous ceramic atomizing core includes the following steps:
(1)按质量百分比计算,称量15%的325目的硅灰石,称量30%的500目的硅藻土,称量15%的玻璃粉,称量3%的高岭土,称量1%的氧化钛,称量3%的堇青石,称量3%的珍珠岩,称量30%的聚苯乙烯微球,放入球磨机中,加入质量比为1:2的氧化锆球,球磨3小时后收集备用。(1) Calculate based on mass percentage, weigh 15% of 325 mesh wollastonite, weigh 30% of 500 mesh diatomite, weigh 15% of glass powder, weigh 3% of kaolin, weigh 1% of For titanium oxide, weigh 3% cordierite, weigh 3% perlite, weigh 30% polystyrene microspheres, put them into a ball mill, add zirconia balls with a mass ratio of 1:2, and ball mill for 3 hours. Collect for later use.
(2)按质量百分比计算,称量70%的石蜡,称量30%的蜂蜡,将其放入密炼机,设置温度为90℃,转速为100r/min。半小时后,粘结剂已完全融化,此时加入称量好的陶瓷粉,继续密炼8个小时,然后收集备用。(2) Calculate based on mass percentage, weigh 70% of the paraffin wax, weigh 30% of the beeswax, put it into the internal mixer, set the temperature to 90°C, and the rotation speed to 100r/min. After half an hour, the binder has completely melted. At this time, add the weighed ceramic powder, continue to mix for 8 hours, and then collect it for later use.
(3)将密炼好的陶瓷块放入造粒机进行造粒,然后收集备用。(3) Put the internally mixed ceramic blocks into the granulator for granulation, and then collect them for later use.
(4)将造粒料放入注塑机的料筒,将金属毛毡放入模具,将镶嵌工艺与注塑成型结合起来,制备出陶瓷生坯。(4) Put the granulated material into the barrel of the injection molding machine, put the metal felt into the mold, and combine the inlay process with injection molding to prepare a ceramic green body.
(5)将陶瓷坯体放入烧结炉中,以60℃/h升温到80℃,保温1h,以30℃/h升温到130℃,保温3h,以25℃/h升温到240℃,保温4h,以20℃/h升温到310℃,保温2h,以10℃/h升温到390℃,保温1h,以30℃/h升温到500℃,保温2h,以60℃/h升温到720℃,保温2h,冷却至室温。即获得制备的多孔陶瓷雾化芯。(5) Put the ceramic body into the sintering furnace, raise the temperature to 80°C at 60°C/h, keep it warm for 1 hour, raise the temperature to 130°C at 30°C/h, keep it warm for 3 hours, raise the temperature to 240°C at 25°C/h, and keep it warm. 4h, heat up to 310℃ at 20℃/h, hold for 2h, heat up to 390℃ at 10℃/h, hold for 1h, heat up to 500℃ at 30℃/h, hold for 2h, heat up to 720℃ at 60℃/h , keep warm for 2h, and cool to room temperature. That is, the prepared porous ceramic atomizing core is obtained.
实施例2Example 2
多孔陶瓷雾化芯的制备方法,包括以下步骤:The preparation method of porous ceramic atomizing core includes the following steps:
(1)按质量百分比计算,称量5%的325目的硅灰石,称量10%的600目的硅灰石,称量30%的200目的硅藻土,称量20%的玻璃粉,称量2%的高岭土,称量1%的氧化钛,称量3%的堇青石,称量30%的聚苯乙烯微球,放入球磨机中,加入质量比为1:2的氧化锆球,球磨3小时后收集备用。(1) Calculate based on mass percentage, weigh 5% of 325 mesh wollastonite, weigh 10% of 600 mesh wollastonite, weigh 30% of 200 mesh diatomite, weigh 20% of glass powder, weigh Weigh 2% kaolin, 1% titanium oxide, 3% cordierite, 30% polystyrene microspheres, put them into a ball mill, and add zirconia balls with a mass ratio of 1:2. After ball milling for 3 hours, collect and set aside.
(2)按质量百分比计算,称量50%的石蜡,称量35%的蜂蜡,称量6%的聚乙烯,称量9%的聚乙烯,将其放入密炼机,设置温度为120℃,转速为150r/min,半小时后,粘结剂已完全融化。设置温度为90℃,转速为100r/min,温度达到设定温度时,加入称量好的陶瓷粉,继续密炼8个小时,然后收集备用。(2) Calculate based on mass percentage, weigh 50% paraffin, weigh 35% beeswax, weigh 6% polyethylene, weigh 9% polyethylene, put it into the internal mixer, and set the temperature to 120 ℃, the rotation speed is 150r/min, and after half an hour, the binder has completely melted. Set the temperature to 90°C and the rotation speed to 100r/min. When the temperature reaches the set temperature, add the weighed ceramic powder and continue mixing for 8 hours, then collect it for later use.
(3)将密炼好的陶瓷块放入造粒机进行造粒,然后收集备用。(3) Put the internally mixed ceramic blocks into the granulator for granulation, and then collect them for later use.
(4)将造粒料放入注塑机的料筒,将金属毛毡放入模具,将镶嵌工艺与注塑成型结合起来,制备出陶瓷生坯。(4) Put the granulated material into the barrel of the injection molding machine, put the metal felt into the mold, and combine the inlay process with injection molding to prepare a ceramic green body.
(5)将陶瓷坯体放入烧结炉中,以80℃/h升温到80℃,保温1h,以40℃/h升温到130℃,保温3h,以30℃/h升温到240℃,保温4h,以20℃/h升温到310℃,保温2h,以13℃/h升温到390℃,保温1h,以30℃/h升温到500℃,保温2h,以60℃/h升温到670℃,保温2h,冷却至室温。即获得制备的多孔陶瓷雾化芯。(5) Put the ceramic body into the sintering furnace, raise the temperature to 80°C at 80°C/h, keep it warm for 1 hour, raise the temperature to 130°C at 40°C/h, keep it warm for 3 hours, raise the temperature to 240°C at 30°C/h, and keep it warm 4h, heat up to 310℃ at 20℃/h, hold for 2h, heat up to 390℃ at 13℃/h, hold for 1h, heat up to 500℃ at 30℃/h, hold for 2h, heat up to 670℃ at 60℃/h , keep warm for 2h, and cool to room temperature. That is, the prepared porous ceramic atomizing core is obtained.
实施例3Example 3
多孔陶瓷雾化芯的制备方法,包括以下步骤:The preparation method of porous ceramic atomizing core includes the following steps:
(1)按质量百分比计算,称量15%的325目的硅灰石,称量5%的600目 的硅灰石,称量15%的200目的硅藻土,称量10%的500目的硅藻土,称量17%的玻璃粉,称量5%的高岭土,称量1%的氧化钛,称量2%的白粘土,称量4%的堇青石,称量26%的聚苯乙烯微球,放入球磨机中,加入质量比为1:2的氧化锆球,球磨3小时后收集备用。(1) Calculate based on mass percentage, weigh 15% of 325 mesh wollastonite, weigh 5% of 600 mesh wollastonite, weigh 15% of 200 mesh diatomaceous earth, weigh 10% of 500 mesh diatomaceous earth Soil, weigh 17% glass powder, weigh 5% kaolin, weigh 1% titanium oxide, weigh 2% white clay, weigh 4% cordierite, weigh 26% polystyrene micro Put the balls into the ball mill, add zirconia balls with a mass ratio of 1:2, and collect them after ball milling for 3 hours.
(2)按质量百分比计算,称量50%的石蜡,称量35%的蜂蜡,称量6%的聚乙烯,称量9%的聚乙烯,将其放入密炼机,设置温度为120℃,转速为150r/min,半小时后,粘结剂已完全融化。设置温度为90℃,转速为100r/min,温度达到设定温度时,加入称量好的陶瓷粉,继续密炼8个小时,然后收集备用。(2) Calculate based on mass percentage, weigh 50% paraffin, weigh 35% beeswax, weigh 6% polyethylene, weigh 9% polyethylene, put it into the internal mixer, and set the temperature to 120 ℃, the rotation speed is 150r/min, and after half an hour, the binder has completely melted. Set the temperature to 90°C and the rotation speed to 100r/min. When the temperature reaches the set temperature, add the weighed ceramic powder and continue mixing for 8 hours, then collect it for later use.
(3)将密炼好的陶瓷块放入造粒机进行造粒,然后收集备用。(3) Put the internally mixed ceramic blocks into the granulator for granulation, and then collect them for later use.
(4)将造粒料放入注塑机的料筒,将金属毛毡放入模具,将镶嵌工艺与注塑成型结合起来,制备出陶瓷生坯。(4) Put the granulated material into the barrel of the injection molding machine, put the metal felt into the mold, and combine the inlay process with injection molding to prepare a ceramic green body.
(5)将陶瓷坯体放入烧结炉中,以70℃/h升温到80℃,保温1h,以30℃/h升温到130℃,保温3h,以10℃/h升温到240℃,保温4h,以20℃/h升温到310℃,保温2h,以15℃/h升温到390℃,保温1h,以30℃/h升温到500℃,保温2h,以60℃/h升温到750℃,保温2h,冷却至室温。即获得制备的多孔陶瓷雾化芯。(5) Put the ceramic body into the sintering furnace, raise the temperature to 80°C at 70°C/h, keep it warm for 1 hour, raise the temperature to 130°C at 30°C/h, keep it warm for 3 hours, raise the temperature to 240°C at 10°C/h, and keep it warm. 4h, heat up to 310℃ at 20℃/h, hold for 2h, heat up to 390℃ at 15℃/h, hold for 1h, heat up to 500℃ at 30℃/h, hold for 2h, heat up to 750℃ at 60℃/h , keep warm for 2h, and cool to room temperature. That is, the prepared porous ceramic atomizing core is obtained.
请参考图1,从图1的表格中给出的三个实施例的实验数据可知,在保持烧结温度较低的情况下,仍能保证制备出的多孔陶瓷雾化芯具有收缩率小、强度高、孔隙率高、孔径均匀的特点。Please refer to Figure 1. From the experimental data of the three examples given in the table of Figure 1, it can be seen that while the sintering temperature is kept low, the prepared porous ceramic atomizing core can still be guaranteed to have low shrinkage and high strength. It has the characteristics of high porosity and uniform pore size.
以上所述,仅为本申请的具体实施方式,但本申请的保护范围并不局限于此,任何熟悉本技术领域的技术人员在本申请揭露的技术范围内,可轻易想到各种等效的修改或替换,这些修改或替换都应涵盖在本申请的保护范围之内。因此,本申请的保护范围应以权利要求的保护范围为准。The above are only specific embodiments of the present application, but the protection scope of the present application is not limited thereto. Any person familiar with the technical field can easily think of various equivalent methods within the technical scope disclosed in the present application. Modification or replacement, these modifications or replacements shall be covered by the protection scope of this application. Therefore, the protection scope of this application should be subject to the protection scope of the claims.

Claims (20)

  1. 多孔陶瓷雾化芯的制备方法,其中,包括以下步骤:A method for preparing a porous ceramic atomizing core, which includes the following steps:
    将陶瓷粉体、助烧剂和造孔剂进行混料研磨处理,以得到陶瓷复合粉体,其中,所述陶瓷粉体包括硅灰石、硅藻土和玻璃粉;Mixing and grinding ceramic powder, sintering aid and pore-forming agent to obtain ceramic composite powder, wherein the ceramic powder includes wollastonite, diatomite and glass powder;
    将所述陶瓷复合粉体与粘结剂进行密炼处理,以得到陶瓷料块;The ceramic composite powder and the binder are subjected to an internal mixing process to obtain a ceramic block;
    将陶瓷料块进行造粒处理,以得到陶瓷颗粒;Granulating the ceramic material blocks to obtain ceramic particles;
    将陶瓷颗粒与金属毛毡经过镶嵌和注塑成型处理,以得到带发热膜的陶瓷坯体;The ceramic particles and metal felt are inlaid and injection molded to obtain a ceramic body with a heating film;
    将陶瓷坯体进行烧结处理,以得到多孔陶瓷雾化芯。The ceramic body is sintered to obtain a porous ceramic atomizing core.
  2. 根据权利要求1所述的多孔陶瓷雾化芯的制备方法,其中,所述混料研磨处理的条件为:加入氧化锆球,且研磨1-3小时。The method for preparing a porous ceramic atomizing core according to claim 1, wherein the conditions for the mixing and grinding treatment are: adding zirconia balls and grinding for 1-3 hours.
  3. 根据权利要求1所述的多孔陶瓷雾化芯的制备方法,其中,所述将所述陶瓷复合粉体与粘结剂进行密炼处理,以得到陶瓷料块,包括以下处理步骤:The method for preparing a porous ceramic atomizing core according to claim 1, wherein the internal mixing process of the ceramic composite powder and the binder to obtain the ceramic block includes the following processing steps:
    将粘结剂搅拌半个小时,使其完全融化;Stir the binder for half an hour until it is completely melted;
    将陶瓷复合粉体分多次加入完全融化的粘结剂中,并搅拌6-8小时后收集备用。Add the ceramic composite powder to the completely melted binder in multiple batches, stir for 6-8 hours and then collect for later use.
  4. 根据权利要求3所述的多孔陶瓷雾化芯的制备方法,其中,所述粘结剂为石蜡、蜂蜡、聚乙烯、硬脂酸中的两种或多种。The method for preparing a porous ceramic atomizing core according to claim 3, wherein the binder is two or more of paraffin, beeswax, polyethylene, and stearic acid.
  5. 根据权利要求1所述的多孔陶瓷雾化芯的制备方法,其中,所述陶瓷颗粒为2-3微米的均匀颗粒。The method for preparing a porous ceramic atomizing core according to claim 1, wherein the ceramic particles are uniform particles of 2-3 microns.
  6. 根据权利要求1所述的多孔陶瓷雾化芯的制备方法,其中,所述烧结处理的条件为:以60-100℃/h的升温速率升温到80℃,保温0.5-1h,接着以30-60℃/h的升温速率升温到130℃,保温1-3h,再以10-50℃/h的升温速率升温到240℃,保温2-4h,然后以10-30℃/h的升温速率升温到310℃,保温1-2h,再然后以10-30℃/h的升温速率升温到390℃,保 温1-2h,再然后以30-50℃/h的升温速率升温到500℃,保温1-2h,再然后以60-100℃/h的升温速率升温到600-800℃,保温1-2h,最后冷却至室温。The method for preparing a porous ceramic atomizing core according to claim 1, wherein the sintering treatment conditions are: heating to 80°C at a heating rate of 60-100°C/h, maintaining the temperature for 0.5-1h, and then proceeding to 30-100°C. Heating to 130℃ at a heating rate of 60℃/h, holding for 1-3h, then heating to 240℃ at a heating rate of 10-50℃/h, holding for 2-4h, and then heating at a heating rate of 10-30℃/h to 310℃, keep for 1-2h, then raise the temperature to 390℃ at a heating rate of 10-30℃/h, keep for 1-2h, then raise the temperature to 500℃ at a heating rate of 30-50℃/h, and keep for 1 -2h, then raise the temperature to 600-800℃ at a heating rate of 60-100℃/h, keep it warm for 1-2h, and finally cool to room temperature.
  7. 根据权利要求1所述的多孔陶瓷雾化芯的制备方法,其中,所述将陶瓷粉体、助烧剂和造孔剂进行混料研磨处理,以得到陶瓷复合粉体,其中,所述陶瓷粉体包括硅灰石、硅藻土和玻璃粉的步骤中,按质量百分比计算,所述硅灰石为5%-20%,所述硅藻土为10%-40%,所述玻璃粉为10%-25%,所述助烧剂为3%-15%,所述造孔剂为10%-30%。The method for preparing a porous ceramic atomizing core according to claim 1, wherein the ceramic powder, sintering aid and pore-forming agent are mixed and ground to obtain ceramic composite powder, wherein the ceramic In the step where the powder includes wollastonite, diatomite and glass powder, in terms of mass percentage, the wollastonite is 5%-20%, the diatomite is 10%-40%, and the glass powder is The content of the burning aid is 10%-25%, the burning aid is 3%-15%, and the pore-forming agent is 10%-30%.
  8. 根据权利要求1所述的多孔陶瓷雾化芯的制备方法,其中,所述将陶瓷粉体、助烧剂和造孔剂进行混料研磨处理,以得到陶瓷复合粉体,其中,所述陶瓷粉体包括硅灰石、硅藻土和玻璃粉的步骤中,所述硅灰石的粒径为325目、600目、900目中的一种或多种,所述硅藻土的粒径为200目、500目、700目中的一种或两种,所述玻璃粉的粒径为325目、600目中的一种或两种,所述助烧剂为高岭土、白粘土、氧化钛、堇青石、钾长石、珍珠岩、铝矾土中的一种或多种,所述造孔剂为淀粉、聚苯乙烯微球、聚甲基丙烯酸甲酯中的一种或两种。The method for preparing a porous ceramic atomizing core according to claim 1, wherein the ceramic powder, sintering aid and pore-forming agent are mixed and ground to obtain ceramic composite powder, wherein the ceramic In the step where the powder includes wollastonite, diatomite and glass powder, the particle size of the wollastonite is one or more of 325 mesh, 600 mesh, and 900 mesh, and the particle size of the diatomite is It is one or both of 200 mesh, 500 mesh, and 700 mesh. The particle size of the glass powder is one or two of 325 mesh and 600 mesh. The sintering aid is kaolin, white clay, oxidized clay, etc. One or more of titanium, cordierite, potassium feldspar, perlite, and bauxite, and the pore-forming agent is one or two of starch, polystyrene microspheres, and polymethyl methacrylate. .
  9. 一种多孔陶瓷雾化芯,其中,所述多孔陶瓷雾化芯的制备方法包括以下步骤:A porous ceramic atomizing core, wherein the preparation method of the porous ceramic atomizing core includes the following steps:
    将陶瓷粉体、助烧剂和造孔剂进行混料研磨处理,以得到陶瓷复合粉体,其中,所述陶瓷粉体包括硅灰石、硅藻土和玻璃粉;Mixing and grinding ceramic powder, sintering aid and pore-forming agent to obtain ceramic composite powder, wherein the ceramic powder includes wollastonite, diatomite and glass powder;
    将所述陶瓷复合粉体与粘结剂进行密炼处理,以得到陶瓷料块;The ceramic composite powder and the binder are subjected to an internal mixing process to obtain a ceramic block;
    将陶瓷料块进行造粒处理,以得到陶瓷颗粒;Granulating the ceramic material blocks to obtain ceramic particles;
    将陶瓷颗粒与金属毛毡经过镶嵌和注塑成型处理,以得到带发热膜的陶瓷坯体;The ceramic particles and metal felt are inlaid and injection molded to obtain a ceramic body with a heating film;
    将陶瓷坯体进行烧结处理,以得到多孔陶瓷雾化芯。The ceramic body is sintered to obtain a porous ceramic atomizing core.
  10. 根据权利要求9所述的多孔陶瓷雾化芯,其中,所述混料研磨处理的条件为:加入氧化锆球,且研磨1-3小时。The porous ceramic atomization core according to claim 9, wherein the conditions for the mixing and grinding treatment are: adding zirconia balls and grinding for 1-3 hours.
  11. 根据权利要求9所述的多孔陶瓷雾化芯,其中,所述将所述陶瓷复合粉体与粘结剂进行密炼处理,以得到陶瓷料块,包括以下处理步骤:The porous ceramic atomizing core according to claim 9, wherein the internal mixing process of the ceramic composite powder and the binder to obtain the ceramic block includes the following processing steps:
    将粘结剂搅拌半个小时,使其完全融化;Stir the binder for half an hour until it is completely melted;
    将陶瓷复合粉体分多次加入完全融化的粘结剂中,并搅拌6-8小时后收集备用。Add the ceramic composite powder to the completely melted binder in multiple batches, stir for 6-8 hours and then collect for later use.
  12. 根据权利要求11所述的多孔陶瓷雾化芯,其中,所述粘结剂为石蜡、蜂蜡、聚乙烯、硬脂酸中的两种或多种。The porous ceramic atomization core according to claim 11, wherein the binder is two or more of paraffin, beeswax, polyethylene, and stearic acid.
  13. 根据权利要求9所述的多孔陶瓷雾化芯,其中,所述陶瓷颗粒为2-3微米的均匀颗粒。The porous ceramic atomization core according to claim 9, wherein the ceramic particles are uniform particles of 2-3 microns.
  14. 根据权利要求9所述的多孔陶瓷雾化芯,其中,所述烧结处理的条件为:以60-100℃/h的升温速率升温到80℃,保温0.5-1h,接着以30-60℃/h的升温速率升温到130℃,保温1-3h,再以10-50℃/h的升温速率升温到240℃,保温2-4h,然后以10-30℃/h的升温速率升温到310℃,保温1-2h,再然后以10-30℃/h的升温速率升温到390℃,保温1-2h,再然后以30-50℃/h的升温速率升温到500℃,保温1-2h,再然后以60-100℃/h的升温速率升温到600-800℃,保温1-2h,最后冷却至室温。The porous ceramic atomization core according to claim 9, wherein the sintering treatment conditions are: heating to 80°C at a heating rate of 60-100°C/h, maintaining the temperature for 0.5-1h, and then heating to 30-60°C/h. The temperature is raised to 130℃ at a heating rate of h, maintained for 1-3h, then heated to 240℃ at a heating rate of 10-50℃/h, kept for 2-4h, and then heated to 310℃ at a heating rate of 10-30℃/h. , keep warm for 1-2h, then raise the temperature to 390℃ at a heating rate of 10-30℃/h, keep warm for 1-2h, then raise the temperature to 500℃ at a heating rate of 30-50℃/h, and keep warm for 1-2h. Then raise the temperature to 600-800°C at a heating rate of 60-100°C/h, keep it warm for 1-2 hours, and finally cool to room temperature.
  15. 根据权利要求9所述的多孔陶瓷雾化芯,其中,所述将陶瓷粉体、助烧剂和造孔剂进行混料研磨处理,以得到陶瓷复合粉体,其中,所述陶瓷粉体包括硅灰石、硅藻土和玻璃粉的步骤中,按质量百分比计算,所述硅灰石为5%-20%,所述硅藻土为10%-40%,所述玻璃粉为10%-25%,所述助烧剂为3%-15%,所述造孔剂为10%-30%。The porous ceramic atomizing core according to claim 9, wherein the ceramic powder, sintering aid and pore-forming agent are mixed and ground to obtain ceramic composite powder, wherein the ceramic powder includes In the steps of wollastonite, diatomite and glass powder, in terms of mass percentage, the wollastonite is 5%-20%, the diatomite is 10%-40%, and the glass powder is 10% -25%, the burning aid is 3%-15%, and the pore-forming agent is 10%-30%.
  16. 根据权利要求9所述的多孔陶瓷雾化芯,其中,所述将陶瓷粉体、助烧剂和造孔剂进行混料研磨处理,以得到陶瓷复合粉体,其中,所述陶瓷粉体包括硅灰石、硅藻土和玻璃粉的步骤中,所述硅灰石的粒径为325目、600目、900目中的一种或多种,所述硅藻土的粒径为200目、500目、700目中的一种或两种,所述玻璃粉的粒径为325目、600目中的一种或两种,所述助烧剂为高岭土、白粘土、氧化钛、堇青石、钾长石、珍珠岩、 铝矾土中的一种或多种,所述造孔剂为淀粉、聚苯乙烯微球、聚甲基丙烯酸甲酯中的一种或两种。The porous ceramic atomizing core according to claim 9, wherein the ceramic powder, sintering aid and pore-forming agent are mixed and ground to obtain ceramic composite powder, wherein the ceramic powder includes In the steps of wollastonite, diatomite and glass powder, the particle size of the wollastonite is one or more of 325 mesh, 600 mesh, and 900 mesh, and the particle size of the diatomite is 200 mesh. , one or both of 500 mesh and 700 mesh, the particle size of the glass powder is one or both of 325 mesh and 600 mesh, the sintering aid is kaolin, white clay, titanium oxide, cordyle One or more of bluestone, potassium feldspar, perlite, and bauxite, and the pore-forming agent is one or two of starch, polystyrene microspheres, and polymethylmethacrylate.
  17. 一种气溶胶产生装置,其中,包括主机以及多孔陶瓷雾化芯;所述多孔陶瓷雾化芯安装于所述主机上;所述多孔陶瓷雾化芯的制备方法包括以下步骤:An aerosol generating device, which includes a host and a porous ceramic atomizing core; the porous ceramic atomizing core is installed on the host; the preparation method of the porous ceramic atomizing core includes the following steps:
    将陶瓷粉体、助烧剂和造孔剂进行混料研磨处理,以得到陶瓷复合粉体,其中,所述陶瓷粉体包括硅灰石、硅藻土和玻璃粉;Mixing and grinding ceramic powder, sintering aid and pore-forming agent to obtain ceramic composite powder, wherein the ceramic powder includes wollastonite, diatomite and glass powder;
    将所述陶瓷复合粉体与粘结剂进行密炼处理,以得到陶瓷料块;The ceramic composite powder and the binder are subjected to an internal mixing process to obtain a ceramic block;
    将陶瓷料块进行造粒处理,以得到陶瓷颗粒;Granulating the ceramic material blocks to obtain ceramic particles;
    将陶瓷颗粒与金属毛毡经过镶嵌和注塑成型处理,以得到带发热膜的陶瓷坯体;The ceramic particles and metal felt are inlaid and injection molded to obtain a ceramic body with a heating film;
    将陶瓷坯体进行烧结处理,以得到多孔陶瓷雾化芯。The ceramic body is sintered to obtain a porous ceramic atomizing core.
  18. 根据权利要求17所述的气溶胶产生装置,其中,所述混料研磨处理的条件为:加入氧化锆球,且研磨1-3小时。The aerosol generating device according to claim 17, wherein the conditions for the mixing and grinding treatment are: adding zirconia balls and grinding for 1-3 hours.
  19. 根据权利要求17所述的气溶胶产生装置,其中,所述将所述陶瓷复合粉体与粘结剂进行密炼处理,以得到陶瓷料块,包括以下处理步骤:The aerosol generating device according to claim 17, wherein the internal mixing process of the ceramic composite powder and the binder to obtain the ceramic block includes the following processing steps:
    将粘结剂搅拌半个小时,使其完全融化;Stir the binder for half an hour until it is completely melted;
    将陶瓷复合粉体分多次加入完全融化的粘结剂中,并搅拌6-8小时后收集备用。Add the ceramic composite powder to the completely melted binder in multiple batches, stir for 6-8 hours and then collect for later use.
  20. 根据权利要求19所述的气溶胶产生装置,其中,所述粘结剂为石蜡、蜂蜡、聚乙烯、硬脂酸中的两种或多种。The aerosol generating device according to claim 19, wherein the binder is two or more of paraffin, beeswax, polyethylene, and stearic acid.
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