WO2022036093A1 - Porous lost circulation material for reservoir section - Google Patents
Porous lost circulation material for reservoir section Download PDFInfo
- Publication number
- WO2022036093A1 WO2022036093A1 PCT/US2021/045740 US2021045740W WO2022036093A1 WO 2022036093 A1 WO2022036093 A1 WO 2022036093A1 US 2021045740 W US2021045740 W US 2021045740W WO 2022036093 A1 WO2022036093 A1 WO 2022036093A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- lcm
- wellbore
- objects
- subterranean formation
- pores
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K8/00—Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
- C09K8/50—Compositions for plastering borehole walls, i.e. compositions for temporary consolidation of borehole walls
- C09K8/516—Compositions for plastering borehole walls, i.e. compositions for temporary consolidation of borehole walls characterised by their form or by the form of their components, e.g. encapsulated material
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K8/00—Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
- C09K8/50—Compositions for plastering borehole walls, i.e. compositions for temporary consolidation of borehole walls
- C09K8/504—Compositions based on water or polar solvents
- C09K8/5045—Compositions based on water or polar solvents containing inorganic compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K8/00—Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
- C09K8/50—Compositions for plastering borehole walls, i.e. compositions for temporary consolidation of borehole walls
- C09K8/504—Compositions based on water or polar solvents
- C09K8/506—Compositions based on water or polar solvents containing organic compounds
- C09K8/508—Compositions based on water or polar solvents containing organic compounds macromolecular compounds
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH OR ROCK DRILLING; MINING
- E21B—EARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B21/00—Methods or apparatus for flushing boreholes, e.g. by use of exhaust air from motor
- E21B21/003—Means for stopping loss of drilling fluid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B33—ADDITIVE MANUFACTURING TECHNOLOGY
- B33Y—ADDITIVE MANUFACTURING, i.e. MANUFACTURING OF THREE-DIMENSIONAL [3D] OBJECTS BY ADDITIVE DEPOSITION, ADDITIVE AGGLOMERATION OR ADDITIVE LAYERING, e.g. BY 3D PRINTING, STEREOLITHOGRAPHY OR SELECTIVE LASER SINTERING
- B33Y80/00—Products made by additive manufacturing
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K2208/00—Aspects relating to compositions of drilling or well treatment fluids
- C09K2208/18—Bridging agents, i.e. particles for temporarily filling the pores of a formation; Graded salts
Definitions
- This disclosure relates to lost circulation material (LCM) for curing loss circulation in a wellbore in a subterranean formation.
- LCM lost circulation material
- Loss circulation occurs when drilling fluid (mud) or cement slurry flows into the subterranean formation instead of flowing up the annulus between the formation and the casing or work string.
- Loss circulation is the partial or complete loss of drilling fluid or cement slurry to the formation during drilling or cementing operations.
- Loss circulation can be brought on by natural or induced causes. Natural causes include naturally fractured formations or unconsolidated zones. Induced losses occur when the hydrostatic fluid column pressure exceeds the fracture gradient of the formation and the formation pores break down adequately to receive rather than resist the fluid.
- a loss circulation zone may be the result of fractures in the geological formation at the borehole or wellbore.
- Loss circulation material is a name for substances added to drilling fluids when drilling fluids are being loss downhole to the subterranean formation.
- the LCM may be fibrous (e.g., tree bark, shredded cane stalks, mineral fibers, and animal hair), flaky (e.g., mica flakes and pieces of plastic or cellophane sheeting), or granular (e.g., ground and sized limestone, carbonates or marble, wood, nut hulls, Formica, corncobs, or cotton hulls).
- LCM may be introduced into a mud system to reduce or prevent the flow of drilling fluid into a permeable formation.
- An aspect relates to a method of treating loss circulation in a wellbore in a subterranean formation.
- the method placing loss circulation material (LCM) having pores into the wellbore, and flowing the LCM to dispose the LCM against the subterranean formation at a loss circulation zone in the wellbore.
- the method includes flowing wellbore fluid from the wellbore through the pores into the subterranean formation.
- the method includes collecting solids onto the LCM from the wellbore fluid flowed through the pores to form a barrier to treat the loss circulation at the loss circulation zone.
- LCM loss circulation material
- Another aspect relates to a method of treating loss circulation in a wellbore in a subterranean formation.
- the method positioning LCM objects at a loss circulation zone in the wellbore at a hydrocarbon reservoir section of the subterranean formation, wherein the LCM objects have permeable portions.
- the method includes flowing wellbore fluid from the wellbore through the permeable portions into the subterranean formation, and collecting solids from the wellbore fluid onto the LCM objects to stop or reduce flow of the wellbore fluid through permeable portions into the subterranean formation.
- LCM that is a plurality of LCM objects, each LCM object of the plurality having a solid body with permeable sections including pores, wherein the plurality to arrange at a loss circulation zone in a wellbore in a subterranean formation to allow wellbore fluid to flow through the pores into the subterranean formation, and the plurality to collect solids from the wellbore fluid to form a flow barrier.
- FIGS. 1-3 are diagrams of loss circulation material (LCM) objects.
- FIG. 4 are diagrams of LCM objects as arranged.
- FIG. 5 is a diagram of a well site.
- FIG. 6 is a block flow diagram of a method of treating loss circulation in a wellbore in a subterranean formation.
- FIG. 7 is a block flow diagram of a method of treating loss circulation in a wellbore in a subterranean formation.
- FIG. 8 is a method of applying LCM to a wellbore in a subterranean formation.
- Some aspects of the present disclosure are directed to loss circulation material (LCM) having sections that are porous and permeable.
- the sections may be part of a solid body and formed in grooves of the solid body.
- the LCM may be flaky LCM.
- the LCM may be applied to treating loss control (loss circulation) in a pay zone (hydrocarbon reservoir section). Therefore, as discussed below, the LCM may be characterized as reservoir friendly.
- the LCM may be applied to loss circulation zones having permeable features of the subterranean formation in a hydrocarbon reservoir section of the subterranean formation.
- the permeable features in the subterranean formation may be highly permeable.
- the highly permeable features may be labeled as a super-k zone capable of producing at least 500 barrels per day per foot of thickness.
- the present flaky LCM are applicable to permeable zones in the formation that cause loss circulation, such as during drilling, but where the permeable zones would provide for hydrocarbon production during the subsequent production phase.
- drilling fluid employed in a hydrocarbon reservoir portion of the subterranean formation may be labeled as drill-in fluid.
- Drill-in fluid can be drilling fluid configured for drilling a borehole in a reservoir section, e.g., with intent to reduce damage to the formation and increase subsequent production of hydrocarbon.
- drill-in fluid can resemble a completion fluid.
- a drill-in fluid may include additives beneficial for filtration control and also carrying of rock cuttings, and the so forth.
- Some embodiments relate to a flaky LCM having porous sections that may be part of a solid body, residing or formed in grooves or channels of the solid body.
- the flaky LCM is permeable to hydrocarbon flow from the subterranean formation into the wellbore through the porous sections.
- the flaky LCM can have a cube shape or other shapes and be made of polymer such as via additive manufacturing or three dimensional (3D) printing.
- the flaky LCM are provided to the loss circulation zone in the wellbore (e.g., at a hydrocarbon reservoir section of the subterranean formation). Initially, drilling fluid flows through the flaky LCM porous portions into the subterranean formation. However, the pores are generally smaller than at least some of the solids in the drilling fluid.
- solids e.g., filler material, other LCMs, etc.
- solids in the drilling fluid form a filter cake on the flaky LCM on the wellbore side and thus stop flow of drilling fluid through the flaky LCM porous sections into the formation.
- the wellbore pressure is lower than the formation pressure. Therefore, produced hydrocarbon flows from the subterranean formation through the flaky LCM porous sections displacing the filter cake (on the wellbore side). Production from the subterranean formation may continue through the flaky LCM into the wellbore.
- Conventional flaky LCMs are generally non-porous and impermeable. Hence, the mat or barrier formed by the flakes (conventional flaky LCM) in the loss zone of a reservoir section will generally permanently seal and block the highly-conductive fluid channels of the loss zones that would be beneficial to enhance well productivity.
- Conventional flaky LCM can have a significant detrimental impact on productivity of a well because the LCM obstructs permeable features (e.g., fractures, super-k channels, etc.) of the subterranean formation at the reservoir section.
- embodiments of the present flaky LCMs having porous and permeable channels that are smaller than the drill solid particles of the mud system may generally prevent or reduce the loss of whole mud while drilling but allow the production of hydrocarbon after completing a well.
- Embodiments of the present techniques include reservoir-friendly flaky LCMs containing porous and permeable channels that are small enough to prevent the loss of whole mud while drilling but large enough to allow the production of hydrocarbon after completion of a well.
- Embodiments of the present flaky LCM may be manufactured by additive manufacturing via a 3D printer. Other applicable manufacturing techniques may include, for example, casting (cast molding), injection molding, or compression molding. The manufacturing technique selected for implementation may be in response to LCM technical specifications for particular applications of the LCM.
- FIGS. 1-3 are examples of the present LCM, which may be flaky LCM or flake LCM.
- Flaky or flake LCM can be LCM objects having a relatively large ratio of surface area to volume.
- Flaky LCM can generally be insoluble to the mud system (drilling fluid or carrier fluid) in which the flaky LCM is employed.
- Flaky LCM can be utilized to seal fluid loss zones (loss circulation zones) in a well (wellbore) to aid in stopping or reducing lost circulation.
- Flake LCM can be applied in an LCM pill and pumped into the wellbore section where loss circulation is occurring.
- Other LCM types e.g., granular, fiber, etc.
- FIGS. 1-3 each give a perspective view and approximate orthographic views of an LCM object of the present LCM. These examples of the present LCM objects depicted may be utilized in a plurality of the same or similar present LCM objects to give the LCM to treat loss circulation.
- the solid body 110, 210, 310 of the LCM object 100, 200, 300 in FIGS. 1-3, respectively, is a rectangular cuboid shape.
- Other embodiments of the LCM object have a solid body with a shape different than rectangular cuboid.
- the solid body can be a sphere, spheroid, ovoid, cuboid, rectangular cuboid, hyperrectangle, a pentahedron, or an irregular shape, and so on.
- the permeable sections 112, 212, 312 are elongated having a length substantially greater than their width.
- the length of the permeable sections 112, 212, 312 may depend on the size (e.g., distance or area) of the sides of the solid body 110, 210, 310.
- the permeable sections 112, 212, 312 may generally run across the respective side.
- the width of the permeable sections 112, 212, 312 may be, for example, less than 1 mm or less than 0.5 mm.
- the permeable sections 112, 212, 312 have a depth into the solid body 110, 210, 310, such as less than 4 mm, less than 3 mm, or less than 2 mm.
- a difference generally between the respective LCM object 100, 200, 300 of FIGS. 1-3 is orientation of the permeable sections with regard to the solid body 110, 210, 310.
- FIG. 1 is the LCM object 100. Depicted are a perspective view 102, top view 104, front view 106, and side view 108.
- the LCM object 100 includes a solid body 110 having permeable sections 112 that include pores 114.
- the permeable sections 112 on four sides may be characterized as having a vertical orientation with respect to a given top and bottom (the remaining two sides).
- the solid body 110 is a rectangular cuboid in the illustrated embodiment.
- the length is in the range of 5 mm to 20 mm, or less than 30 mm, and the height and width are each in the range of 3 mm to 10 mm, or less than 10 mm.
- the L x H x W of the solid body 110 is 12 mm x 5 mm x 5 mm.
- the illustrated example of the solid body 110 has two sides designated as top 116 (top view 104) and bottom 118, respectively, for reference (given or assigned) so to label the orientation (vertical in this example) of the permeable sections on the four remaining sides.
- orientation of the permeable sections 112 on the four remaining sides may be characterized as vertical from top to bottom.
- the four remaining sides include the front 120 (front view 106), the back (not shown), and the two sides 122, 124 (side view 108) not the front or back.
- the back may generally be similar or identical to the front 120.
- the two sides 122, 124 may be the same or similar.
- the orientation or arrangement of the permeable sections 112 on the top 116 and bottom 118 may be as depicted or as otherwise specified.
- the number of permeable sections 112 at each of the top 116, bottom 118, front 102, and back may be at least 2, at least 3, at least 4, at least 5, or at least 6. In the illustrated embodiment, this number is 5.
- the number of permeable sections 112 for each of the two sides 122, 124 may be at least 1 , at least 2, at least 3, or at least 4. In the illustrated embodiment, this number is 3.
- the spacing between permeable sections 112 on a given side may be, for example, less than 2.5 mm, less than 2 mm, less than 1 .5 mm, less than 1 mm, or less than 0.5 mm. In the illustrated embodiment, this spacing is 1 .5 mm on the top 116, bottom 118, front 120, and back, and is 0.75 mm on the two sides 122, 124.
- the permeable sections 112 of the solid body 110 may be permeable portions of the solid body 110, porous sections of the solid body 110, porous portions of the solid body 110, permeable structures of or within the solid body 110, porous structures of or within the solid body 110, and the like.
- the permeable sections 112 may be generally part of the solid body 110 at or near the external surface of the solid body 110 and exposed to outside (external) of the solid body 110.
- the external surface of the permeable sections 112 may be an external surface of the solid body 110.
- the permeable sections 112 may be formed in recessed volumes such as grooves or channels.
- the exterior surface of the permeable sections 112 with respect to the exterior surface of the remaining part (portion) of the solid body 110 may be recessed, flushed (even), or protruding.
- the permeable sections 112 are elongated having a length substantially greater than their width.
- the width of the permeable sections 112 may be, for example, less than 1 mm or less than 0.5 mm.
- the permeable sections 112 have a depth into the solid body 110. The depth may be, for example, less than 4 mm, less than 3 mm, or less than 2 mm.
- the depth for the permeable sections 112 on the side 124 is indicated by reference numeral 126.
- the permeable sections 112 on one side may meet (interface and overlap) with permeable sections 112 on another side at where the two sides meet (at the edge between the two sides).
- the permeable sections 112 on the front 120 meet the permeable sections 112 on the bottom 118 at the edge where the front 120 and bottom 118 meet.
- Such interface or overlap of permeable sections 112 between sides may advance fluid flow through the LCM as arranged at a loss circulation zone.
- the width of the permeable sections 112 is 0.5 mm and the depth of the permeable sections 112 is 2 mm.
- the number of permeable sections 112 on each of the top 116, bottom 118, front 120, and back is 5 with a spacing of 1 .5 mm
- the number of permeable sections 112 on each side 122, 124 is 3 with a spacing of 0.75 mm.
- the pore size (e.g., width or diameter) of the pores 114 of the permeable sections 112 may be less than 100 microns, less than 50 microns, or less than 10 microns.
- the pore size may be specified to be less than the particle size of at least some of the solids in the wellbore fluid in the wellbore having the loss circulation zone being treated.
- FIG. 2 is an LCM object 200 similar to the LCM object 100 of FIG. 1 , but with a different orientation of permeable sections.
- FIG. 2 gives a perspective view 202, top view 204, front view 206, and side view 208 of the LCM object 200.
- the LCM object 200 includes a solid body 210 having permeable sections 212 including pores 214.
- the permeable sections 212 on four sides may be characterized as having a horizontal orientation with respect to a given top and bottom (remaining two sides).
- the solid body 210 is a rectangular cuboid in the illustrated embodiment. In implementations, the solid body 210 may have the same or similar values for L x W x H dimensions as the solid body 110 of FIG.
- the illustrated example of the solid body 210 has two sides assigned as top 216 and bottom 218, respectively, for reference (given) for labeling the orientation (horizontal in this example) of the permeable sections 212 on the four remaining sides.
- orientation of the permeable sections 212 on these four remaining sides may be characterized as horizontal with respect to the top 216 and bottom 218.
- the four remaining sides include the front 220, the back (not shown), and the two sides 222, 224 not the front or back.
- the back may generally be similar or identical to the front 220.
- the two sides 222, 224 may be the same or similar.
- the orientation or arrangement of the permeable sections 212 on the top 216 and bottom 218 may be as depicted or as otherwise specified.
- the number of permeable sections 212 at each of the front 220, back, and two sides 222, 224 may be at least 2, at least 3, at least 4, at least 5, or at least 6. In the illustrated embodiment, this number is 5.
- the number of permeable sections 212 for each of top 216 and bottom 218 may be at least 1 , at least 2, at least 3, or at least 4. In the illustrated embodiment, this number is 3.
- the spacing between permeable sections 212 on a given side may be, for example, less than 2.5 mm, less than 2 mm, less than 1 .5 mm, less than 1 mm, or less than 0.5 mm. In the illustrated embodiment, this spacing is 1 .5 mm on the front 220, back, and two sides 222, 224, and is 0.75 mm on the top 216 and the bottom 218.
- the permeable sections 212 of the solid body 210 may be permeable portions, porous sections, porous portions, permeable structures, porous structures, and the like.
- the width or diameter of the pores 214 (e.g., same or similar to pores 114) may be, for example, less than 100 microns, less than 50 microns, or less than 10 microns.
- the permeable sections 212 may be generally part of the solid body 210 at or near the external surface of the solid body 210 and exposed to the outside (external) of the solid body 210 exterior.
- the permeable sections 212 may be part of the solid body 210, the permeable sections 212 may be formed or reside in grooves or channels of the solid body 210.
- the exterior surface of the permeable sections 212 may be recessed, flushed (even), or protruding with respect to the exterior surface of the remaining part (portion) of the solid body 210.
- the elongated permeable sections 212 may have the same or similar dimensional (width, depth) values as the permeable sections 112 of FIG. 1.
- the depth for the permeable sections 212 on the bottom 218 is indicated by reference numeral 226.
- the solid body 210 has L x W x H of 12 mm x 5 mm x 5 mm, and in which the width of the permeable sections 212 is 0.5 mm and the depth of the permeable sections 212 is 2 mm.
- a combination or mixture of multiple LCM objects 100 and multiple LCM objects 200 may be utilize together collectively as LCM to treat loss circulation.
- the LCM with LCM objects having differing respective orientations of the permeable sections may advance the intercoupling of the permeable sections for fluid flow there through with the LCM as arranged at the loss circulation zone.
- the LCM may include a first set (group) of the flaky LCMs and second set (group) of the flaky LCMs with the first set having the same top designation as the second set, and wherein orientation of permeable sections in the first set is vertical from top to bottom, and orientation of permeable sections in the second set is horizontal with respect to top and bottom.
- orientation of permeable sections in the first group is 90° different than the orientation of permeable sections in the second group.
- LCM having a collection or plurality of LCM objects including LCM objects 100 and LCM objects 200 embodiments can be characterized without specifying a top or bottom in particular for reference but instead noting a given side.
- LCM objects 100 and LCM objects 200 the orientation of the permeable sections 112 in the first group is substantially perpendicular to the orientation of the permeable sections 212 in the second group.
- FIG. 3 is an LCM object 300. Depicted are a perspective view 302, top view 304, front view 306, and side view 308.
- the solid body 310 is a rectangular cuboid.
- the LCM object 300 includes the solid body 310 having permeable sections 312 including pores 314.
- the permeable sections 312 on four sides may be characterized as having a slanted orientation (not horizontal and not vertical) with respect to a given top and bottom (remaining two sides).
- the permeable sections 312 on all six sides may be characterized as having an orientation that is parallel with a diagonal on the respective side.
- the solid body 310 may have the same or similar values for L x W x H dimensions as the solid body 110 of FIG.
- the illustrated example of the solid body 310 has two sides assigned as top 316 and bottom 318, respectively.
- the four remaining sides include the front 320, the back (not shown), and the two sides 322, 324 not the front or back.
- the back side may generally be similar or identical to the front 320.
- the two sides 322, 324 may be the same or similar.
- the number of permeable sections 312 at each of the front 320 and the back may be, for example at least 4, at least 5, at least 6, at least 7, or at least 8. In the illustrated embodiment, this number is 7.
- the number of permeable sections 312 for each of top 316, bottom 318, and the two sides 322, 324 may be, for example, at least 3, at least 4, at least 5, or at least 6. In the illustrated embodiment, this number is 5.
- the spacing between permeable sections 312 on a given side may be, for example, less than 2.5 mm, less than 2 mm, less than 1 .5 mm, less than 1 mm, or less than 0.5 mm. In the illustrated embodiment, this spacing is about 1 mm.
- the permeable sections 312 of the solid body 310 may be permeable portions, porous sections, porous portions, permeable structures, porous structures, and the like.
- the width or diameter of the pores 314 (e.g., same or similar to pores 114 and pores 214) may be, for example, less than 100 microns, less than 50 microns, or less than 10 microns.
- the permeable sections 312 may be part of the solid body 210 at or near the external surface of the solid body 310 and exposed to the outside (external) of the solid body 310 exterior.
- the permeable sections 312 may be part of the solid body 310, the permeable sections 312 may be formed or reside in grooves or channels of the solid body 310.
- the exterior surface of the permeable sections 312 may be recessed, flushed (even), or protruding with respect to the exterior surface of the remaining part (portion) of the solid body 310.
- the elongated permeable sections 312 may have the same or similar width and same or similar depth as the permeable sections 112 of FIG. 1 and permeable sections 212 of FIG. 2.
- the solid body 310 has L x Wx H of 12 mm x 5 mm x 5 mm, and in which the width of the permeable sections 312 is 0.5 mm and the depth of the permeable sections 312 is 2 mm.
- a combination or mixture of multiple LCM objects 100, multiple LCM objects 200, and multiple LCM objects 300 may be utilize together collectively as LCM to treat loss circulation.
- the LCM with LCM objects having differing respective orientations of the permeable sections may advance the intercoupling of the permeable sections for fluid flow there through within the LCM as arranged at the loss circulation zone.
- the LCM may include a first set (group) of the flaky LCMs, second set (group) of the flaky LCMs, and a third set (group) of the flaky LCMs with the first set, second set, and third set having the same top designation, and wherein orientation of permeable sections in the first set is vertical from top to bottom, orientation of permeable sections in the second set is horizontal with respect to top and bottom, and orientation of permeable sections in the second set is slanted (not horizontal and not vertical) with respect to top and bottom.
- the orientation of permeable sections on the four sides (not the top and bottom) for the LCM objects in the first group may be 90° different than the orientation of permeable sections on the respective four sides (not the top and bottom) for the LCM objects in the second group.
- the orientation of permeable sections for the LCM objects in the third group for a given (corresponding) side may be 45° different than the orientation of permeable sections in the first and second groups for that given (corresponding) side.
- LCM having a collection or plurality of LCM objects including LCM objects 100 (first group), LCM objects 200 (second group), and LCM objects 300 (third group) embodiments can be characterized without specifying a top or bottom in particular for reference but instead noting a given side.
- first group e.g., LCM objects 100
- second group e.g., LCM objects 200
- third group LCM objects 300
- embodiments can be characterized without specifying a top or bottom in particular for reference but instead noting a given side.
- the orientation of the permeable sections 112 in the first group is substantially perpendicular to the orientation of the permeable sections 212 in the second group.
- the orientation of the permeable sections 312 in the third group is 45° different than the first group and the second group.
- the orientation of the grooves is about 45° with respect to the orientation in the first and second groups.
- FIG. 4 is random arrangements 400 of flaky LCM objects 402.
- the flaky LCM objects 402 may be analogous to the LCM object 100, LCM object 200, or LCM object 300, or any combinations thereof.
- the flaky LCM objects 402 may randomly arrange at a loss circulation zone.
- the loss circulation zone may be in a hydrocarbon reservoir section of the subterranean formation.
- the flaky LCM objects 402 may randomly arrange at, in, or over features (e.g., permeable portions, fractures, etc.) of the subterranean formation that contribute to loss circulation.
- the LCM objects 402 as randomly arranged may allow wellbore fluid to flow through permeable sections (as intercoupled) of the LCM objects 402 into the subterranean formation.
- the pores of the permeable sections may be smaller than solids in the wellbore fluid. Therefore, the LCM objects 402 may collects solids from the wellbore fluid to form a flow barrier on the LCM objects 402 to stop or reduce flow of wellbore fluid (or drilling fluid) into the subterranean formation.
- a filter cake of the solids may form on the wellbore side of the LCM objects 402.
- the hydrocarbon may dislodge the collected solids or filter cake.
- the hydrocarbon may be produced through the permeable sections of the LCM objects 402 with the LCM object 402 remaining in place. In instances, some or majority of the LCM objects 402 may be displaced by the hydrocarbon.
- Loss circulation may occur in drilling or cementing operations.
- drilling fluid may be pumped via mud pumps into a wellbore through a drill string to a drill bit (at the bottom of the wellbore) that breaks rock to drill the borehole.
- the drilling fluid may discharge from nozzles on the drill bit and flow back up through an annulus to Earth surface.
- the annulus may be between the wellbore wall (formation surface) and the drill string, or between the wellbore wall (formation) and wellbore casing in which the drill string is inserted.
- the cement slurry may be pumped from the Earth surface into the wellbore down the interior of the casing and then upward from the bottom through the annulus between the casing and the formation.
- the cement does not adequately continue upward.
- the loss of cement slurries to such thief zones can cause problems during cementing including resulting in inadequate amounts of cement slurry in the annulus between the casing and the subterranean formation.
- the inadequate amounts of cement slurry could lead to poor zonal isolation during the subsequent production of hydrocarbon from the subterranean formation through the wellbore to the Earth surface.
- FIG. 5 is a well site 500 having a wellbore 502 through the Earth surface 504 into a subterranean formation 506 in the Earth crust.
- the subterranean 506 may also be labeled as a geological formation, hydrocarbon formation, reservoir, etc.
- Hydrocarbon may be produced from the subterranean formation 506 through the wellbore 502 to the surface 504.
- the hydrocarbon may be crude oil or natural gas, or both.
- a hole is drilled into the subterranean formation 506 to generate a drilled formation surface 508 as an interface for the wellbore 502 with the subterranean formation 506.
- the formation surface 508 may be characterized as the wellbore 502 wall.
- the wellbore 502 may have openhole portions but generally includes a cylindrical casing 510 as shown.
- the wellbore 502 in the depicted implementation of FIG. 5 is a cased wellbore 502.
- the wellbore 502 has a loss circulation zone 512 caused by loss-circulation features 514 of the subterranean formation 506 at that portion of the wellbore 502.
- the loss circulation zone 512 may be in a hydrocarbon reservoir section of the subterranean formation 506.
- the losscirculation features 514 along the wellbore 502 at the loss circulation zone 512 cause or contribute to the loss circulation.
- the loss-circulation features 514 are structural features or characteristics of the subterranean formation 506 at or near the wellbore 502.
- the features 514 may be fractures, voids, vugulars (vugs), gaps, permeable channels, cavities, cavernous openings, etc.
- a vugular may be a cavity in subterranean rock and can be lined with mineral precipitates.
- the features 514 or feature 514 generally may be a permeable zone or unconsolidated portion of the subterranean formation 506.
- the loss circulation zone 512 may be a super-k zone capable of producing at least 500 barrels hydrocarbon per day per foot of thickness.
- drilling fluid introduced from the surface 504 flowing downward through the casing 510 (and drill string) discharges from the drill bit (not shown) at the bottom of the wellbore 502, and flows upward through the annulus between the subterranean formation 506 and the casing 510 toward the surface 504 as return drilling fluid.
- Some or all of the drilling fluid flowing upward through the annulus may be lost through the features 514 (e.g., permeable zone or fractures) into the subterranean formation 506 at the loss circulation zone 512 in the wellbore 502.
- the cement slurry may be introduced from the surface 504 into the casing 510 in the wellbore 502 and discharges from the bottom of the casing 510.
- the cement slurry then flows up through the annulus between the formation 506 and the casing 510 toward the surface 504.
- the cement slurry flowing upward in the annulus may be lost through the features 514 into the subterranean formation 506 at the loss circulation zone 512.
- the present LCMs may be utilized to treat the loss circulation zone 512 to cure the loss circulation.
- This LCM (having permeable sections) as randomly arranged at the loss circulation zone 512 may initially allow wellbore fluid to flow into the subterranean formation 506 but collect solids from the wellbore fluid to form a flow barrier.
- the formed flow barrier may reduce or prevent flow of drilling fluid or cement slurry through the features 514 (e.g., super-k zone) into the subterranean formation 506.
- the solids may be added to the treatment fluid along with the present LCM objects or the solids may added to the wellbore 502 after application of the present LCM objects.
- a treatment fluid 516 having LCM that includes multiple LCM objects 100, 200, and/or 300 (FIGS. 1-3) or similar LCM objects may be introduced (e.g., pumped) into the wellbore 502.
- the treatment fluid 516 may be pumped by a surface pump (e.g., mud pump) of the surface equipment 518 at the surface 504.
- the pump may be associated with a drilling rig.
- the pump(s) can be skid-mounted in some instances.
- the pump may be a centrifugal pump, positive displacement (PD) pump, reciprocating PD pump such as a piston or plunger pump, and so on.
- the surface equipment 518 may include equipment (e.g., vessels, solid-handling equipment, piping, pumps etc.) to incorporate LCM objects, viscosifier, and solids (e.g., filler material, bridging material, other LCM products, etc.) into the treatment fluid 516.
- the solids are in addition to present LCM objects.
- the surface equipment 518 may include equipment to support other operations at the well site 500.
- the treatment fluid 516 may be, for example, drilling fluid (mud) or carrier fluid.
- the treatment fluid 516 may be oil-based or water-based.
- the treatment fluid 516 may include water, mineral oil, synthetic oil, a viscous additive (viscosifier), and so forth.
- the viscosifier may be, for example, bentonite, XC polymer, or starch for water-based treatment fluid 516.
- the viscosifier may be, for example, organophilic clay for oil-based treatment fluid 516.
- the treatment fluid 516 may be labeled as a treatment slurry in that the treatment fluid 516 includes the present LCM objects and optionally other solids.
- the treatment fluid 516 having the LCM objects 100 may be labeled or characterized as an LCM pill.
- a pill may be a relatively small quantity or volume (e.g., less than 500 barrels) of drilling fluid or carrier fluid as a specified blend utilized for a particular purpose in treating the wellbore 502 or subterranean formation 506.
- the size and geometry of the present LCM objects included in the treatment fluid 516 may be specified in response to (correlative with) size (e.g., cross-sectional area) or permeability of the features 514 (e.g., permeable portion, fractures, gaps, channels, cavities, openings, etc.) of the subterranean formation 506 at the loss circulation zone 512.
- the concentration of the LCM objects 100 in the treatment fluid 216 may be, for example, in the range of 5 pounds per barrel (ppb) to 100 ppb, or at least 30 ppb. Additional solids (not the LCM objects 100) if included in the treatment fluid 216 may be, for example, as a concentration of less than 100 ppb in the treatment fluid 216.
- the present LCM product (e.g., LCM objects 100, 200, and/or 300) may randomly arrange at the features 514 to allow for flow of wellbore fluid through permeable sections of the LCM and thus collect solids from the wellbore fluid onto the LCM.
- the collection of solids may form a filter cake on the wellbore 502 side of the LCM to give a flow barrier in which flow may cease through the permeable sections from the wellbore 502 into the subterranean formation 506.
- the formed flow barrier may cure the loss circulation at the loss circulation zone.
- hydrocarbon production from the subterranean formation 506 into the wellbore (to the Earth surface 504) is initiated, the flow of the hydrocarbon displaces the collected solids (e.g., filter cake).
- hydrocarbon production may flow through the permeable sections of the LCM as applied and arranged at the features 514.
- the pressure of the subterranean formation 506 is greater than pressure in the wellbore 502. Such may provide motive force of flow of the hydrocarbon production and removal (via the hydrocarbon flow) of collected solids in or on the wellbore side of the LCM.
- additional solids may be added along with the present LCM objects (e.g., also less than 100 ppb) to the treatment fluid 516 at the surface 504.
- the combination of the present LCM objects and the additional solids may be less than 200 ppb in the treatment fluid 516.
- the added solids may include other LCM products as filler solids that can be collected by the present LCM (e.g., LCM objects 100, 200, and/or 300) to advance formation of the flow barrier.
- the added solids may generally include filler solids that may be labeled as filler material or bridging material.
- the filler solids as particles suspended in the treatment fluid 516 may be collected present LCM as random arranged at the lost circulation zone 512.
- the filler solids may include small particles having, for example, an effective diameter less than 2 mm in effective diameter down to micron scale (e.g., 100 microns).
- the filler solids may include volcanic ash (generally nonswelling), bentonite (generally swelling), Rev DustTM (generally non-reactive), ARC Plug or Nut plug (both known as bridging material), and the like.
- a blend design may be implemented in which two or more blends of the additives may be prepared in advanced, and then added to the treatment fluid 516 at the surface 504 at the time of application.
- a single sack for the LCM pill system may be implemented in which the present LCM objects and optionally other aforementioned additives are pre-mixed and added to the drilling mud (or carrier fluid) to give the treatment fluid 516. Such may save time, and accelerate the mixing process and improve the slurry quality.
- Single sack typically has all the components in one sack so that contents can be mixed at the same time at the same rate by pouring a single sack into, for example, the mud mixing hopper.
- Embodiments of the present flaky LCM may be manufactured by additive manufacturing via a 3D printer.
- the additive manufacturing may be, for example, fused deposition modeling (FDM) or other types of 3D printing.
- FDM fused deposition modeling
- the computer model driving the 3D printer may be configured or set (programmed) to form LCM having the solid body (specified size) with permeable sections. The number and placement of the permeable sections, as well as the pore sizes, are specified.
- the 3D material may be polymer or metal.
- the present LCM e.g., LCM objects 100, 200, 300
- Other applicable manufacturing techniques may include, for example, machining (subtractive manufacturing) or molding.
- Molding may include, for example, casting (cast molding), injection molding, or compression molding.
- the fabrication system may include, for example, an injection mold, to receive a material (for example, a polymer) to form the LCM objects 100, 200, 300.
- the mold may be shaped in the form of the solid body (specified size) having permeable sections (number and placement designated) with specified pore size.
- the manufacturing practice selected for implementation may be in response to LCM technical specifications for particular applications of the LCM.
- the present methods disclosed herein may include fabricating the LCM objects via 3D printing or other techniques.
- FIG. 6 is a method 600 of treating loss circulation in a wellbore in a subterranean formation.
- the method includes placing LCM (e.g., flaky LCM) having pores into the wellbore.
- LCM e.g., flaky LCM
- the LCM may have permeable sections having the pores.
- the placing of the LCM into the wellbore may involve pumping fluid having the LCM into the wellbore.
- the fluid may be, for example, drilling fluid (drilling mud) or carrier fluid.
- concentration of the LCM in the fluid is less than 100 ppb.
- the fluid pumped into the wellbore may include solids in addition to the LCM.
- the solids may include bridging material, filler material, or other LCM product not the LCM, or any combinations thereof.
- the method includes flowing the LCM to dispose the LCM against the subterranean formation at a loss circulation zone in the wellbore.
- the flowing of the LCM may involve flowing the LCM to dispose the LCM at features of the subterranean formation that contribute to loss circulation at the loss circulation zone.
- the LCM may randomly arrange at features of the loss circulation zone such that wellbore fluid can initially flow through the LCM pores into the subterranean formation.
- the loss circulation zone is at a hydrocarbon reservoir section of the subterranean formation.
- the method includes flowing wellbore fluid from the wellbore through the pores into the subterranean formation.
- the flowing of the wellbore fluid through the pores may involve allowing loss of wellbore fluid through the pores into the subterranean formation at the loss circulation zone.
- the wellbore pressure may generally be greater than the subterranean formation pressure.
- the wellbore pressure may be provided via a surface pump.
- the method includes collecting solids onto the LCM from the wellbore fluid flowed through the pores to form a barrier (e.g., flow barrier) to treat the loss circulation at the loss circulation zone.
- a barrier e.g., flow barrier
- To treat the loss circulation may involve to stop or reduce flow of the wellbore fluid into the subterranean formation at the loss circulation zone.
- the flow of the wellbore fluid through the pores into the subterranean formation may be stopped or reduced due to formation of the barrier.
- the pores may generally be smaller than the solids particles.
- the collecting of the solids may foul the pores.
- To form the barrier may involve the collecting of the solids fouling the pores.
- the collecting of the solids may form a filter cake of the solids on a wellbore side of the LCM.
- the collecting of the solids forms the barrier as a flow barrier across or over the pores.
- the solids may include, for example, bridging material, filler material, or other LCM product not the LCM
- the method includes producing hydrocarbon from the subterranean formation.
- the hydrocarbon may be, for example, crude oil or natural gas, or both.
- the production of the hydrocarbon may involve flowing the hydrocarbon from the subterranean formation through the LCM pores into the wellbore. The flowing of the hydrocarbon through the pores removes at least a portion of the solids collected on the LCM.
- FIG. 7 is a method 700 of treating loss circulation in a wellbore in a subterranean formation utilizing LCM that is multiple LCM objects (e.g., flaky LCM).
- the LCM objects have permeable portions (e.g., having pores).
- Each LCM object of the LCM objects may have a solid body having the permeable portions. In some examples, each solid body has at least five permeable portions.
- the LCM objects may be, for example, polymer or metal.
- the method may include fabricating the LCM objects by additive manufacturing (3D printing).
- the method includes positioning the LCM objects at a loss circulation zone in the wellbore at a hydrocarbon reservoir section of the subterranean formation.
- the positioning the LCM objects may involve placing the LCM objects from Earth surface into the wellbore and flowing the LCM objects in the wellbore to the loss circulation zone.
- the method includes flowing wellbore fluid from the wellbore through the permeable portions into the subterranean formation.
- the motive force for flow of the wellbore fluid may be pressure differential with wellbore pressure greater than pressure of the subterranean formation.
- the method includes collecting solids from the wellbore fluid onto the LCM objects to stop or reduce flow of the wellbore fluid through permeable portions into the subterranean formation.
- the solids may be smaller than the pores.
- the method may include producing hydrocarbon from the subterranean formation.
- the producing of the hydrocarbon may involve flowing the hydrocarbon from the subterranean formation through the permeable portions into the wellbore.
- the flowing of the hydrocarbon through the pores may dislodge the solids collected onto the permeable portions of the LCM objects.
- FIG. 8 is a method 800 of applying LCM to a wellbore in a subterranean formation.
- the LCM includes LCM objects that may be, for example, polymer or metal.
- the method includes pumping a slurry having base fluid, LCM objects, and solids into the wellbore to a loss circulation zone in the wellbore.
- the base fluid may be, for example, drilling fluid or a carrier fluid.
- the LCM objects each have a porous section(s).
- the LCM objects may each generally have multiple porous sections.
- Each LCM object of the LCM objects may have a solid body (e.g., cuboid shape) having the porous section(s) embedded therein. The porous section(s) may be exposed to external of the solid body.
- the method includes allowing the LCM objects to arrange (e.g., randomly) in the wellbore at the subterranean formation at the loss circulation zone.
- the porous section of each LCM object of the LCM objects may be multiple porous sections disposed in respective grooves of the LCM object. Some of the porous sections may intercouple in the arrangement for fluid flow there through.
- the method includes flowing the base fluid from the wellbore through the porous section(s) of at least some of the LCM objects into the subterranean zone.
- the porous section of each LCM object of the LCM objects have at least five porous sections spaced apart with respect to each other
- the method includes collecting the solids on the LCM objects to form a flow barrier to reduce or prevent loss circulation at the loss circulation zone.
- the porous sections may have pores, and wherein the pores are smaller than the solids.
- the method may include producing hydrocarbon from the subterranean formation, wherein producing the hydrocarbon involves flowing the hydrocarbon from the subterranean formation through porous section(s) of the LCM objects into the wellbore.
- the hydrocarbon flow through the porous section(s) may displace at least a portion of the solids collected on the LCM objects.
- An embodiment is a method of applying LCM to a wellbore in a subterranean formation, the method including: pumping a slurry comprising base fluid, LCM objects, and solids into the wellbore to a loss circulation zone in the wellbore, the LCM objects each comprising a porous section; allowing the LCM objects to arrange in the wellbore at the subterranean formation at the loss circulation zone; flowing the base fluid from the wellbore through the porous section of at least some of the LCM objects into the subterranean zone; and collecting the solids on the LCM objects to form a flow barrier to reduce or prevent loss circulation at the loss circulation zone.
- Each LCM object of the LCM objects may include a solid body having the porous section, wherein the solid body includes a cuboid shape having the porous section embedded therein, and wherein the porous section is exposed to external of the solid body.
- the porous section of each LCM object of the LCM objects may include multiple porous sections disposed in respective grooves of the LCM object, and wherein the LCM objects include polymer or metal.
- the porous section of each LCM object of the LCM objects is at least five porous sections spaced apart with respect to each other, wherein the five porous sections have pores, and wherein the pores are smaller than the solids.
- the method may include producing hydrocarbon from the subterranean formation, wherein producing the hydrocarbon involves flowing the hydrocarbon from the subterranean formation through the porous section into the wellbore, and wherein flowing the hydrocarbon through the porous section displaces at least a portion of the solids collected on the LCM objects.
- Another embodiment is a plurality of LCM objects, each LCM object of the plurality having a solid body (e.g., cuboid shape) having permeable sections including pores, wherein the plurality of LCM objects to arrange at a loss circulation zone in a wellbore in a subterranean formation to initially allow wellbore fluid to flow through the pores into the subterranean formation, and the plurality of the LCM objects to collect solids from the wellbore fluid to form a flow barrier.
- the plurality of LCM objects as arranged to intercouple permeable sections among the plurality at the loss circulation zone, and wherein the pores are smaller than the solids.
- the plurality of LCM objects may be flaky LCM.
- Each LCM object of the plurality may be polymer or metal.
- each LCM object of the plurality has at least five permeable sections.
- the plurality of LCM objects may include a first set of the LCM objects having a first orientation of the permeable sections, and a second set of the LCM objects having a second orientation of the permeable sections different than the first orientation.
- the LCM permeable sections of the solid body of each LCM object of the plurality may be disposed at are near an external surface of the solid body.
- the permeable sections may be elongated and have depth into the solid body.
- the solid body has a length less than 30 mm, a height less than 10 mm, and a width less than 10 mm.
- the permeable sections of the solid body of each LCM object of the plurality may be spaced apart.
- the plurality of LCM objects may be fabricated by additive manufacturing (3D printing).
- Tables 1-4 below give Examples of treatment fluids that may deploy the present LCM (e.g., FIGS. 1-4).
- the present LCM can be shaped LCM having permeable sections.
- the treatment fluids (Tables 1-4) are indicated as drill-in fluids and may be altered at least with respect to incorporating the present LCM. While drill-in fluid is noted, treatment fluids as indicated in Tables 1-4 may be drilling fluid more generally or a carrier fluid.
- the treatment fluids may have an aqueous fluid phase or a non-aqueous fluid phase.
- the aqueous phase can be fresh water, monovalent salt water, or divalent salt water, and so forth.
- the non-aqueous phase can be, for example, mineral oil or synthetic oil, and the like.
- Examples of the treatment fluid can include a viscosifier, a fluid loss additive, and calcium carbonate (CaCO3).
- the CaCO3 can be granular as coarse particles (C), medium particles (M), or fine particles (F), or any combinations thereof.
- the viscosifier can be, for instance, a polysaccharide (e.g., xanthan gum or XC polymer), a carboxymethyl cellulose (CMC), or a cellulose derivative (e.g., polyanionic cellulose or PAC), or any combinations thereof.
- the fluid loss additive can be, for example, starch, psyllium husk powder, or a polyanionic cellulose polymer (e.g., PAC LVTM available from AMC Drilling Optimisation of Balcatta, Western Australia, Australia), or any combinations thereof.
- the present LCM e.g., shaped LCM with permeable sections
- the units in Tables 1-4 below are cubic centimeter (cc) or grams (g).
- the volumes of the water (fresh water or salt water) (Tables 1-3) are given as a reference basis with respect to the associated remaining components in the given Table.
- the volumes of the oil (mineral oil or synthetic) in Table 4 are given as a basis with respect to the associated remaining components in Table 4.
Landscapes
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Mining & Mineral Resources (AREA)
- Geology (AREA)
- Environmental & Geological Engineering (AREA)
- Fluid Mechanics (AREA)
- Physics & Mathematics (AREA)
- Mechanical Engineering (AREA)
- Geochemistry & Mineralogy (AREA)
- Inorganic Chemistry (AREA)
- Treatment Of Sludge (AREA)
- Processing Of Solid Wastes (AREA)
- Filtering Materials (AREA)
Abstract
Description
Claims
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US16/991,817 | 2020-08-12 | ||
| US16/991,817 US11352545B2 (en) | 2020-08-12 | 2020-08-12 | Lost circulation material for reservoir section |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| WO2022036093A1 true WO2022036093A1 (en) | 2022-02-17 |
Family
ID=77640768
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PCT/US2021/045740 Ceased WO2022036093A1 (en) | 2020-08-12 | 2021-08-12 | Porous lost circulation material for reservoir section |
Country Status (2)
| Country | Link |
|---|---|
| US (2) | US11352545B2 (en) |
| WO (1) | WO2022036093A1 (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US11352545B2 (en) | 2020-08-12 | 2022-06-07 | Saudi Arabian Oil Company | Lost circulation material for reservoir section |
| US20250243720A1 (en) * | 2024-01-25 | 2025-07-31 | Everpoint Services Inc. | Lost Circulation Material Comprising Reclaimed Fiberglass Wind Turbine Blades |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2626779A (en) * | 1949-12-16 | 1953-01-27 | Arthur L Armentrout | Method of recovering lost circulation occurring in production strata in wells |
| US2789948A (en) * | 1954-05-18 | 1957-04-23 | Texas Co | Lost circulation |
| US20100230164A1 (en) * | 2009-03-12 | 2010-09-16 | Daniel Guy Pomerleau | Compositions and methods for inhibiting lost circulation during well operation |
Family Cites Families (191)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2452724A (en) | 1945-06-05 | 1948-11-02 | George B Bradshaw | Soap-making process |
| US2943679A (en) | 1955-07-15 | 1960-07-05 | Pan American Petroleum Corp | Well-servicing compositions and methods |
| US2944018A (en) * | 1956-10-22 | 1960-07-05 | Borcherdt Bert | Composition and process for preventing or restoring lost circulation |
| US2933136A (en) * | 1957-04-04 | 1960-04-19 | Dow Chemical Co | Well treating method |
| US3042607A (en) | 1960-01-06 | 1962-07-03 | George R Morris | Drilling fluid |
| US3132693A (en) | 1961-12-26 | 1964-05-12 | Weisend Charles Frederick | Composition comprising hydroxyethyl cellulose, polyvinylpyrrolidone and organic sulfonate, cement slurry prepared therefrom and method of cementing wells therewith |
| US3410797A (en) | 1964-11-13 | 1968-11-12 | Exxon Research Engineering Co | Drilling muds |
| US3629102A (en) | 1967-06-29 | 1971-12-21 | Pan American Petroleum Corp | Preventing loss of drilling fluid to drilled formations |
| US3761410A (en) | 1971-03-22 | 1973-09-25 | Nl Industries Inc | Composition and process for increasing the lubricity of water base drilling fluids |
| US3966632A (en) | 1974-06-06 | 1976-06-29 | G. D. Searle & Co. | Vegetable oil emulsion |
| US4063603A (en) | 1976-09-02 | 1977-12-20 | Rayborn Jerry J | Drilling fluid lubricant |
| US4280915A (en) | 1977-06-23 | 1981-07-28 | Nl Industries, Inc. | Salt stable lubricant for water base drilling fluids |
| US4181617A (en) | 1978-02-13 | 1980-01-01 | Milchem Incorporated | Aqueous drilling fluid and lubricant composition |
| US4340858A (en) | 1979-08-13 | 1982-07-20 | Philip M. Hinderstein | Test fixture |
| SU1118663A1 (en) | 1980-03-14 | 1984-10-15 | Всесоюзный Научно-Исследовательский И Проектный Институт По Подготовке К. Транспортировке И Переработке Природного Газа | Lubrication additive for clay drilling muds |
| US4474665A (en) | 1981-09-28 | 1984-10-02 | W. R. Grace & Co. | Use of ground, sized cocoa bean shells as a lost circulation material in drilling mud |
| US4472882A (en) | 1982-09-13 | 1984-09-25 | Hutter Rudolf J | Squareness test fixture |
| US4458528A (en) | 1982-12-30 | 1984-07-10 | Mobil Oil Corporation | Stickometer |
| FI66899C (en) | 1983-02-11 | 1984-12-10 | Kasvisoeljy Vaextolje Ab Oy | SMOERJMEDEL MED TRIGLYCERIDER SOM HUVUDKONPONENT |
| US4491181A (en) | 1983-03-31 | 1985-01-01 | Gulf Research And Development Co. | Method of freeing stuck drill string using spotting fluid |
| DE3622826A1 (en) | 1986-07-08 | 1988-01-21 | Henkel Kgaa | POWDERED LUBRICANT ADDITIVES FOR WATER-BASED DRILL RINSING |
| US5294651A (en) | 1987-03-23 | 1994-03-15 | Phillips Petroleum Company | Fluid loss additives for well cementing compositions |
| US4770795A (en) | 1987-08-24 | 1988-09-13 | Nalco Chemical Company | Calcium tolerant deflocculant for drilling fluids |
| US4829816A (en) | 1987-11-06 | 1989-05-16 | Standard Oil Production Company | Method and apparatus for testing spotting fluids for releasing stuck drill pipe |
| DE3801476A1 (en) | 1988-01-20 | 1989-08-03 | Henkel Kgaa | COMPOSITIONS FOR THE EXEMPTION OF FIXED DRILLING RESTAURANTS |
| US5252554A (en) | 1988-12-19 | 1993-10-12 | Henkel Kommanditgesellschaft Auf Aktien | Drilling fluids and muds containing selected ester oils |
| DE3842659A1 (en) | 1988-12-19 | 1990-06-28 | Henkel Kgaa | USE OF SELECTED ESTEROILS IN DRILLING RINSING, IN PARTICULAR FOR THE OFF-SHORE DEVELOPMENT OF PETROLEUM OR. NATURAL GAS DEPOSIT (I) |
| FR2642840B1 (en) | 1989-02-09 | 1993-06-25 | Total Petroles | METHOD AND CELL FOR MEASURING THE COEFFICIENTS OF ADHESION AND FRICTION OF A DRILLING FLUID |
| US5253709A (en) | 1990-01-29 | 1993-10-19 | Conoco Inc. | Method and apparatus for sealing pipe perforations |
| US5009269A (en) | 1990-07-31 | 1991-04-23 | Conoco Inc. | Well cement fluid loss additive and method |
| US5161407A (en) | 1990-10-16 | 1992-11-10 | Iowa State University Research Foundation, Inc. | Means and method of soil water desorption |
| US5118664A (en) | 1991-03-28 | 1992-06-02 | Bottom Line Industries, Inc. | Lost circulation material with rice fraction |
| US5260268A (en) | 1991-07-18 | 1993-11-09 | The Lubrizol Corporation | Methods of drilling well boreholes and compositions used therein |
| US5424284A (en) | 1991-10-28 | 1995-06-13 | M-I Drilling Fluids Company | Drilling fluid additive and method for inhibiting hydration |
| US5587354A (en) | 1992-09-25 | 1996-12-24 | Integrity Industries, Inc. | Drilling fluid and drilling fluid additive |
| GB2275342B (en) | 1993-02-19 | 1996-08-21 | Pumptech Nv | Apparatus and method for measuring the sticking tendency of drilling mud |
| US5380469A (en) | 1993-03-18 | 1995-01-10 | Calgene Chemical, Inc. | Polyglycerol esters as functional fluids and functional fluid modifiers |
| CA2497728C (en) | 1993-04-05 | 2008-02-19 | Roger J. Card | Control of particulate flowback in subterranean wells |
| RU2055089C1 (en) | 1993-07-21 | 1996-02-27 | Евгений Алексеевич Коновалов | Method for production of concentrate of drilling technological liquids |
| US5407879A (en) | 1993-09-29 | 1995-04-18 | American Colloid Company | Method of improving the contaminant resistance of a smectite clay by rewetting and impregnating the clay with a water-soluble polymer, and redrying the polymer-impregnated clay |
| US5338471A (en) | 1993-10-15 | 1994-08-16 | The Lubrizol Corporation | Pour point depressants for industrial lubricants containing mixtures of fatty acid esters and vegetable oils |
| FI95395C (en) | 1994-09-07 | 1996-01-25 | Raision Tehtaat Oy Ab | Enzymatic process for preparing a synthetic ester of vegetable oil |
| FI95367C (en) | 1994-09-07 | 1996-01-25 | Raision Tehtaat Oy Ab | Method for preparing a synthetic ester from vegetable oil |
| US5525126A (en) | 1994-10-31 | 1996-06-11 | Agricultural Utilization Research Institute | Process for production of esters for use as a diesel fuel substitute using a non-alkaline catalyst |
| RU2076132C1 (en) | 1995-06-01 | 1997-03-27 | Тюменский научно-исследовательский и проектный институт природного газа и газовых технологий | Lubrication agent for drilling muds |
| US5707940A (en) | 1995-06-07 | 1998-01-13 | The Lubrizol Corporation | Environmentally friendly water based drilling fluids |
| EP0770661A1 (en) | 1995-10-27 | 1997-05-02 | B W Mud Limited | Lubricant for drilling mud |
| US5637795A (en) | 1995-11-01 | 1997-06-10 | Shell Oil Company | Apparatus and test methodology for measurement of bit/stabilizer balling phenomenon in the laboratory |
| JPH09157570A (en) | 1995-12-05 | 1997-06-17 | Riso Kagaku Corp | Emulsion ink for stencil printing |
| US5789349A (en) | 1996-03-13 | 1998-08-04 | M-I Drilling Fluids, L.L.C. | Water-based drilling fluids with high temperature fluid loss control additive |
| US5676213A (en) | 1996-04-10 | 1997-10-14 | Schlumberger Technology Corporation | Method and apparatus for removing mudcake from borehole walls |
| US5713965A (en) | 1996-04-12 | 1998-02-03 | The United States Of America As Represented By The Secretary Of Agriculture | Production of biodiesel, lubricants and fuel and lubricant additives |
| US5602341A (en) | 1996-05-07 | 1997-02-11 | Chrysler Corporation | Test fixture for spot welds |
| US6589917B2 (en) | 1996-08-02 | 2003-07-08 | M-I Llc | Invert emulsion drilling fluids and muds having negative alkalinity and elastomer compatibility |
| US5698502A (en) | 1996-09-11 | 1997-12-16 | Exxon Chemical Patents Inc | Polyol ester compositions with unconverted hydroxyl groups for use as lubricant base stocks |
| DE19647598A1 (en) | 1996-11-18 | 1998-05-20 | Henkel Kgaa | Use of selected fatty alcohols and their mixtures with carboxylic acid esters as a lubricant component in water-based drilling fluid systems for excavating soil |
| US5703022A (en) | 1997-01-06 | 1997-12-30 | The Lubrizol Corporation | Sulfurized vegetable oils containing anti-oxidants for use as base fluids |
| FR2758185B1 (en) | 1997-01-09 | 1999-07-02 | Schlumberger Cie Dowell | DEVICE AND METHOD FOR MEASURING CHARACTERISTICS OF AN OIL FLUID OR THE LIKE |
| US6045070A (en) | 1997-02-19 | 2000-04-04 | Davenport; Ricky W. | Materials size reduction systems and process |
| AU8164898A (en) | 1997-06-27 | 1999-01-19 | Baker Hughes Incorporated | Drilling system with sensors for determining properties of drilling fluid downhole |
| US6055850A (en) | 1997-12-24 | 2000-05-02 | Turner; Daniel R. | Multi-directional permeameter |
| FR2781498B1 (en) | 1998-07-21 | 2002-06-28 | Elf Exploration Prod | METHOD OF USING BIODEGRADABLE DRILLING SLUDGE |
| US6887283B1 (en) | 1998-07-24 | 2005-05-03 | Bechtel Bwxt Idaho, Llc | Process for producing biodiesel, lubricants, and fuel and lubricant additives in a critical fluid medium |
| NO308138B1 (en) | 1998-10-06 | 2000-07-31 | Norske Stats Oljeselskap | H2S removal in drilling mud |
| FR2785991B1 (en) | 1998-11-12 | 2002-09-13 | Dowell Schlumberger Services | DEVICE AND METHOD FOR MEASURING CHARACTERISTICS OF A PETROLEUM FLUID OR THE LIKE |
| DE19852971A1 (en) | 1998-11-17 | 2000-05-18 | Cognis Deutschland Gmbh | Lubricants for drilling fluids |
| US6127560A (en) | 1998-12-29 | 2000-10-03 | West Central Cooperative | Method for preparing a lower alkyl ester product from vegetable oil |
| US6267186B1 (en) | 1999-06-14 | 2001-07-31 | Spectral, Inc. | Spotting fluid and method of treating a stuck pipe |
| CA2379897A1 (en) | 1999-07-29 | 2001-02-08 | Halliburton Energy Services, Inc. | Method and composition for scavenging sulphide in drilling fluids |
| WO2001012581A1 (en) | 1999-08-18 | 2001-02-22 | David Gavin Brooke Boocock | Single-phase process for production of fatty acid methyl esters from mixtures of triglycerides and fatty acids |
| US6465587B1 (en) | 2000-12-08 | 2002-10-15 | Hercules Incorporated | Polymeric fluid loss additives and method of use thereof |
| MXPA03005918A (en) | 2000-12-29 | 2005-02-14 | Halliburton Energy Serv Inc | Thinners for invert emulsions. |
| US6605570B2 (en) | 2001-03-01 | 2003-08-12 | Schlumberger Technology Corporation | Compositions and methods to control fluid loss in surfactant-based wellbore service fluids |
| CN1318427A (en) | 2001-05-18 | 2001-10-24 | 林建生 | Light diesel oil emulsifier produced with waste vegetable oil and animal fat and its application |
| DE10138686A1 (en) | 2001-08-07 | 2003-02-27 | Suedzucker Ag | Use of a polyester composition as hydraulic fluid |
| US20030130135A1 (en) | 2001-11-13 | 2003-07-10 | Crompton Corporation | Emulsifier for oil-based drilling fluids |
| US6508306B1 (en) | 2001-11-15 | 2003-01-21 | Halliburton Energy Services, Inc. | Compositions for solving lost circulation problems |
| US7066285B2 (en) | 2002-01-16 | 2006-06-27 | Halliburton Energy Services, Inc. | Method and composition for preventing or treating lost circulation |
| US6770602B2 (en) | 2002-01-31 | 2004-08-03 | M-I Llc | Oil based well fluids with high solids content |
| BR0202361B1 (en) | 2002-06-21 | 2010-11-03 | oil-based biodegradable drilling fluid compositions and oil and gas well drilling process. | |
| US20040129460A1 (en) | 2002-08-01 | 2004-07-08 | Macquoid Malcolm | Method for using coconut coir as a lost circulation material for well drilling |
| DE10243700A1 (en) | 2002-09-20 | 2004-04-01 | Oelmühle Leer Connemann Gmbh & Co. | Method and device for producing biodiesel |
| US7008474B2 (en) | 2003-01-31 | 2006-03-07 | Tohoku Ricoh Co., Ltd. | Water-in-oil type emulson ink for stencil printing |
| EP1651706A1 (en) | 2003-08-06 | 2006-05-03 | The Procter & Gamble Company | Coated water-swellable material |
| US20050113260A1 (en) | 2003-11-21 | 2005-05-26 | Wood Robert R. | Drilling fluids |
| CA2461524C (en) | 2004-03-18 | 2013-05-28 | Wayne L. Bennett | Method of sealing subterranean zones |
| US7493803B2 (en) | 2004-03-23 | 2009-02-24 | Benthic Geotech Pty Ltd. | Ball penetrometer for soft soils testing |
| US7226895B2 (en) | 2004-04-06 | 2007-06-05 | Baker Hughes Incorporated | Drilling fluid systems for reducing circulation losses |
| WO2006023172A2 (en) | 2004-08-16 | 2006-03-02 | Fairmount Minerals, Ltd. | Control of particulate flowback in subterranean formations using elastomeric resin coated proppants |
| US7264053B2 (en) | 2005-03-24 | 2007-09-04 | Halliburton Energy Services, Inc. | Methods of using wellbore servicing fluids comprising resilient material |
| RU2007145596A (en) | 2005-06-09 | 2009-07-20 | Биосфере Инвайроментал Энерджи Ллс (Us) | SYSTEMS AND METHODS FOR ESTHERIFICATION AND TRANSFER OF FATS AND OILS |
| US20090131711A1 (en) | 2005-07-29 | 2009-05-21 | Pos Pilot Plant Corp. | Single-stage esterification of oils and fats |
| WO2007041785A1 (en) | 2005-10-11 | 2007-04-19 | Biolectric Pty Ltd | Low viscosity vegetable oil-based dielectric fluids |
| US7422061B2 (en) | 2005-11-07 | 2008-09-09 | Calfrac Well Services Ltd. | Fluid loss additives and methods |
| WO2007095009A2 (en) * | 2006-02-10 | 2007-08-23 | Nash, Kenneth, L. | Methods and compositions for sealing fractures, voids, and pores of subterranean rock formations |
| US20070287636A1 (en) | 2006-06-09 | 2007-12-13 | Sun Drilling Products Corporation | Drilling fluid additive and base fluid compositions of matter containing B100 biodiesels; and applications of such compositions of matter in well drilling, completion, and workover operations |
| CA2553872A1 (en) | 2006-07-27 | 2008-01-27 | Luc C. Duchesne | A device for the transesterification of animal and plant glycerides intofatty acid alkyd esters for small scale production of biodiesel and value added products |
| US7989402B2 (en) | 2006-09-14 | 2011-08-02 | Elementis Specialties, Inc. | Functionalized clay compositions for aqueous based drilling fluids |
| US7754661B2 (en) | 2006-11-28 | 2010-07-13 | Innovative Chemical Technologies Canada Ltd | Recycling of oil-based drilling muds |
| RU2336291C1 (en) | 2007-01-26 | 2008-10-20 | Общество с ограниченной ответственностью "ПермНИПИнефть" | Emulsifing and stabilising agent for invert emulsions and method of preparation of invert emulsion drill mud on its basis |
| US8307916B1 (en) * | 2007-02-27 | 2012-11-13 | Wald H Lester | Controlling fluid loss in oil and gas wells |
| WO2008144905A1 (en) | 2007-05-28 | 2008-12-04 | Engineered Drilling Solutions Inc. | Use of wax in oil-based drilling fluid |
| US8728989B2 (en) | 2007-06-19 | 2014-05-20 | Clearwater International | Oil based concentrated slurries and methods for making and using same |
| WO2009006731A1 (en) | 2007-07-06 | 2009-01-15 | Canadian Energy Services L.P. | Drilling fluid additive for reducing lost circulation in a drilling operation |
| WO2009014585A1 (en) | 2007-07-26 | 2009-01-29 | Exxonmobil Upstream Research Company | Method for controlling loss of drilling fluid |
| US7814782B2 (en) | 2007-08-13 | 2010-10-19 | Baker Hughes Incorporated | Downhole gas detection in drilling muds |
| EP2188489A1 (en) | 2007-08-24 | 2010-05-26 | M-I Llc | Method and apparatus for fluid loss measurements of wellbore fluids |
| CN101784643A (en) | 2007-08-24 | 2010-07-21 | 纳幕尔杜邦公司 | Lubrication oil compositions |
| US20090075847A1 (en) | 2007-09-14 | 2009-03-19 | Wawrzos Frank A | Drilling fluid lubricant and method of use |
| EP2036963A1 (en) | 2007-09-14 | 2009-03-18 | Cognis Oleochemicals GmbH | Lubricants for drilling fluids |
| CN100519687C (en) | 2007-11-20 | 2009-07-29 | 孝英 | Preparation of high temperature resistant lubricant for drilling liquid by animal plant oil |
| US7753128B2 (en) | 2007-11-21 | 2010-07-13 | Schlumberger Technology Corporation | Method and system for well production |
| EP2085447A1 (en) | 2007-12-26 | 2009-08-05 | Services Pétroliers Schlumberger | Method and composition for curing lost circulation |
| US8043997B2 (en) | 2008-02-29 | 2011-10-25 | Halliburton Energy Services Inc. | Lost circulation material formulation and method of use |
| TR200802665A2 (en) | 2008-04-17 | 2009-11-23 | Tübi̇tak- Türki̇ye Bi̇li̇msel Ve Teknoloji̇k Araştirma Kurumu | Batch production processes of fatty acid alkyl esters using homogeneous alkali polymeric gel catalyst (hapjek). |
| US8006758B2 (en) | 2008-04-28 | 2011-08-30 | Reynolds Thomas A | Waste material processing for oil recovery |
| US8141661B2 (en) | 2008-07-02 | 2012-03-27 | Clearwater International, Llc | Enhanced oil-based foam drilling fluid compositions and method for making and using same |
| EP2172533A1 (en) * | 2008-09-26 | 2010-04-07 | Services Pétroliers Schlumberger | Composition for borehole treatment |
| WO2010065634A2 (en) | 2008-12-04 | 2010-06-10 | M-I L.L.C. | Lubricant for water-based muds and methods of use thereof |
| US8151633B2 (en) | 2008-12-05 | 2012-04-10 | Halliburton Energy Services Inc. | Methods and systems for characterizing LCM particle plugging and rheology in real time |
| US20100230169A1 (en) | 2009-03-12 | 2010-09-16 | Daniel Guy Pomerleau | Compositions and methods for inhibiting lost circulation during well operations |
| US8101555B2 (en) | 2009-04-30 | 2012-01-24 | Rayborn Sr Jerry | Spotting fluids containing syrups |
| EP2261458A1 (en) | 2009-06-05 | 2010-12-15 | Services Pétroliers Schlumberger | Engineered fibres for well treatments |
| US20110009299A1 (en) | 2009-07-10 | 2011-01-13 | Van Zanten Ryan | Emulsion stabilizing agents for drilling and completion fluids |
| US8413745B2 (en) | 2009-08-11 | 2013-04-09 | Baker Hughes Incorporated | Water-based mud lubricant using fatty acid polyamine salts and fatty acid esters |
| US9896612B2 (en) | 2009-12-24 | 2018-02-20 | Schlumberger Technology Corporation | Methods for controlling lost circulation in a subterranean well and materials there for |
| US20130210630A1 (en) | 2010-07-02 | 2013-08-15 | Isp Investments Inc. | Self-emulsifying oil |
| US8563482B2 (en) | 2010-09-22 | 2013-10-22 | Saudi Arabian Oil Company | Environment friendly base fluid to replace the toxic mineral oil-based base fluids |
| WO2012061147A1 (en) | 2010-10-25 | 2012-05-10 | Isp Investments Inc. | Salt-tolerant, thermally-stable rheology modifiers |
| RO126123A0 (en) | 2010-11-01 | 2011-03-30 | Maria Fiti | Non-conventional process for preparing ecological lubricants for water-beased drilling fluids |
| US8563479B2 (en) | 2010-11-03 | 2013-10-22 | Saudi Arabian Oil Company | Volcanic ash-based drilling mud to overcome drilling challenges |
| US8623790B2 (en) | 2010-12-21 | 2014-01-07 | Newpark Drilling Fluids Llc | Method of drilling a subterranean well with crosslinked polyacrylic acid |
| WO2012106597A1 (en) | 2011-02-04 | 2012-08-09 | Lord Corporation | Polyols and their use in hydrocarbon lubricating and drilling fluids |
| CN102286273B (en) | 2011-09-05 | 2013-07-03 | 中国石油大学(华东) | Oil-in-water emulsifier as well as preparation and use methods thereof |
| US9006151B2 (en) | 2011-09-12 | 2015-04-14 | Saudi Arabian Oil Company | Water-based drilling fluid composition having a multifunctional mud additive for reducing fluid loss during drilling |
| EP2758624A2 (en) * | 2011-09-20 | 2014-07-30 | Saudi Arabian Oil Company | Permeable lost circulation drilling liner |
| US8726990B2 (en) | 2011-10-07 | 2014-05-20 | Halliburton Energy Services, Inc | Lost-circulation material made from a recycled ceramic |
| US8613319B2 (en) | 2011-10-07 | 2013-12-24 | Halliburton Energy Services, Inc. | Lost-circulation material made from a recycled material containing asphalt |
| US8887808B2 (en) | 2011-11-09 | 2014-11-18 | Halliburton Energy Services, Inc. | Engineered methods and materials for wellbore strengthening in subterranean operations |
| EP2782970A1 (en) | 2011-11-21 | 2014-10-01 | Tucc Technology LLC | Dissipative surfactant aqueous-based drilling system for use in hydrocarbon recovery operations from heavy oil and tar sands |
| US20130160998A1 (en) | 2011-12-23 | 2013-06-27 | Francois M. Auzerais | Lost Circulation Materials and Methods of Using Same |
| US9285355B2 (en) | 2012-01-30 | 2016-03-15 | Halliburton Energy Services, Inc. | Method and apparatus for testing lost circulation materials for subterranean formations |
| WO2013116072A1 (en) | 2012-02-02 | 2013-08-08 | Board Of Supervisors Of Louisiana State University And Agricultural And Mechanical College | Engineering plastic/ inorganic fiber blends as lost circulation materials |
| EP2814903A1 (en) | 2012-02-13 | 2014-12-24 | Basf Se | Use of terpolymers as fluid loss additives in well cementing |
| US8972235B2 (en) | 2012-02-21 | 2015-03-03 | Halliburton Energy Services, Inc. | Methods and systems for subterranean bore hole fracture simulation |
| US20130284518A1 (en) | 2012-04-27 | 2013-10-31 | 3M Innovative Properties Company | Method of using multi-component fibers as lost-circulation material |
| US9188522B2 (en) | 2012-05-10 | 2015-11-17 | Halliburton Energy Services, Inc. | Methods and systems for testing lost circulation materials |
| CN104870598A (en) | 2012-06-28 | 2015-08-26 | 罗地亚经营管理公司 | Environmentally Friendly Solvent System/Surfactant System for Drilling Fluids |
| GB2506603A (en) | 2012-10-02 | 2014-04-09 | Brendon Steven O'toole | Drilling fluids comprising ground grape seeds |
| US20140102188A1 (en) | 2012-10-15 | 2014-04-17 | Halliburton Energy Services, Inc, | Method and apparatus for testing lost circulation materials within a permeability plugging apparatus |
| US20140309146A1 (en) | 2013-04-15 | 2014-10-16 | Prime Eco Research And Development, Llc | Emulsions and methods usable within a wellbore |
| US9835608B2 (en) | 2012-12-20 | 2017-12-05 | Saudi Arabian Oil Company | Method for assessing ablation modulai of mudcakes to predict ease of mudcake removal or cleaning efficiency of cleaning/washing/spacer fluids |
| CN105051518B (en) | 2012-12-21 | 2018-11-27 | 蓝帜株式会社 | Viscosity measurement and viscosimeter |
| US9714565B2 (en) | 2012-12-31 | 2017-07-25 | M-I L.L.C. | Slot tester |
| US9206681B2 (en) | 2013-02-07 | 2015-12-08 | Superior Graphite Co. | Wellbore fluid testing assembly |
| US9175529B2 (en) * | 2013-02-19 | 2015-11-03 | Halliburton Energy Services, Inc. | Methods and compositions for treating subterranean formations with interlocking lost circulation materials |
| CA2995943A1 (en) | 2013-06-03 | 2014-12-11 | Saudi Arabian Oil Company | Method of conversion of a drilling mud to a gel-based lost circulation material to combat lost circulation during continuous drilling |
| CN104371674A (en) | 2013-07-03 | 2015-02-25 | 中国石油化工集团公司 | Drilling fluid lubricant prepared from waste plant oil and preparation method thereof |
| US9688901B2 (en) | 2013-07-05 | 2017-06-27 | James Blair Fontenot | Lost circulation drilling fluids comprising elastomeric rubber particles and a method for decreasing whole mud loss using such composition |
| AU2014309168B2 (en) | 2013-08-19 | 2018-11-08 | Ingevity South Carolina, Llc | Methods for producing emulsifiers for oil-based drilling fluids |
| GB201317626D0 (en) * | 2013-10-04 | 2013-11-20 | Schlumberger Holdings | Solids in borehole fluids |
| GB2518441A (en) * | 2013-09-23 | 2015-03-25 | Schlumberger Holdings | Solids in borehole fluids |
| CN105579660A (en) | 2013-09-23 | 2016-05-11 | 普拉德研究及开发股份有限公司 | Solids in Borehole Fluids |
| CA2924636C (en) | 2013-10-18 | 2018-05-29 | Halliburton Energy Services, Inc. | Surface treated lost circulation material |
| MX2016006784A (en) | 2013-11-26 | 2016-09-07 | Schlumberger Technology Bv | Methods for treating subterranean formations. |
| WO2015108501A1 (en) | 2014-01-14 | 2015-07-23 | Halliburton Energy Services, Inc. | Methods of enhancing fluid loss control using additives |
| US9797212B2 (en) | 2014-03-31 | 2017-10-24 | Schlumberger Technology Corporation | Method of treating subterranean formation using shrinkable fibers |
| US20150292278A1 (en) | 2014-04-09 | 2015-10-15 | Sharp-Rock Technologies, Inc. | Method of Stopping Lost Circulation |
| US9834718B2 (en) | 2014-05-06 | 2017-12-05 | Saudi Arabian Oil Company | Ecofriendly lubricating additives for water-based wellbore drilling fluids |
| US9932510B2 (en) | 2014-06-10 | 2018-04-03 | Halliburton Energy Services, Inc. | Lost-circulation materials of two different types of fibers |
| US9739694B2 (en) | 2014-08-28 | 2017-08-22 | Saudi Arabian Oil Company | Method and apparatus for testing gel-based lost circulation materials |
| GB2530495A (en) | 2014-09-23 | 2016-03-30 | Schlumberger Holdings | Solids in borehole fluids |
| RU2679196C2 (en) * | 2014-10-06 | 2019-02-06 | Шлюмбергер Текнолоджи Б.В. | Methods for zonal isolation and treatment diversion with shaped particles |
| US20160168443A1 (en) | 2014-12-16 | 2016-06-16 | Schlumberger Technology Corporation | Nanocellulose materials for oilfield applications |
| US10633400B2 (en) * | 2015-02-28 | 2020-04-28 | Melior Innovations, Inc. | Nanocomposite silicon oxygen carbon materials and uses |
| US20160266030A1 (en) | 2015-03-10 | 2016-09-15 | Saudi Arabian Oil Company | Determining Mudcake Properties |
| US20170058180A1 (en) | 2015-09-01 | 2017-03-02 | King Fahd University Of Petroleum And Minerals | Environmentally safe filtration control agents for drilling fluids |
| US9783727B2 (en) | 2015-10-22 | 2017-10-10 | Halliburton Energy Services, Inc. | Fluid loss control package for use in subterranean formation operations |
| WO2017079123A1 (en) | 2015-11-02 | 2017-05-11 | Lubrizol Oilfield Solutions, Inc. | Lubricant for water based drilling fluid |
| US10174238B2 (en) | 2015-11-18 | 2019-01-08 | Earth Lubricants, LLC | Environmentally friendly lubricant for drilling processes |
| GB2562683B (en) | 2016-04-04 | 2022-05-25 | Halliburton Energy Services Inc | Lubricant for drilling and drill-in fluids |
| US10800959B2 (en) | 2016-06-30 | 2020-10-13 | Saudi Arabian Oil Company | Date tree waste-based compound fibrous LCMs |
| CN106833556B (en) | 2016-12-08 | 2019-08-27 | 中石化石油工程技术服务有限公司 | A kind of reversible emulsifier, its preparation method and environment-friendly reversible emulsified drilling fluid and application |
| US11111742B2 (en) | 2017-03-16 | 2021-09-07 | Saudi Arabian Oil Company | Apparatus for loss circulation material performance evaluation |
| US10494884B2 (en) | 2017-07-14 | 2019-12-03 | Saudi Arabian Oil Company | Used automobile tires as loss circulation material |
| US10577527B2 (en) | 2017-11-14 | 2020-03-03 | Saudi Arabian Oil Company | Waste vegetable oil-based emulsifier for invert emulsion drilling fluid |
| RU2652378C1 (en) | 2017-11-27 | 2018-04-26 | федеральное государственное бюджетное образовательное учреждение высшего образования "Воронежский государственный университет" (ФГБОУ ВО "ВГУ") | Method for obtaining the ethers of polyglycerine from waste production of vegetable oil |
| US11078748B2 (en) * | 2019-02-05 | 2021-08-03 | Saudi Arabian Oil Company | Lost circulation shapes |
| US11105180B2 (en) * | 2019-08-19 | 2021-08-31 | Saudi Arabian Oil Company | Plugging formation fractures |
| US11434708B2 (en) * | 2020-06-10 | 2022-09-06 | Saudi Arabian Oil Company | Lost circulation fabric, method, and deployment systems |
| US11352545B2 (en) | 2020-08-12 | 2022-06-07 | Saudi Arabian Oil Company | Lost circulation material for reservoir section |
-
2020
- 2020-08-12 US US16/991,817 patent/US11352545B2/en active Active
-
2021
- 2021-08-12 WO PCT/US2021/045740 patent/WO2022036093A1/en not_active Ceased
-
2022
- 2022-03-15 US US17/695,228 patent/US11739249B2/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2626779A (en) * | 1949-12-16 | 1953-01-27 | Arthur L Armentrout | Method of recovering lost circulation occurring in production strata in wells |
| US2789948A (en) * | 1954-05-18 | 1957-04-23 | Texas Co | Lost circulation |
| US20100230164A1 (en) * | 2009-03-12 | 2010-09-16 | Daniel Guy Pomerleau | Compositions and methods for inhibiting lost circulation during well operation |
Also Published As
| Publication number | Publication date |
|---|---|
| US11352545B2 (en) | 2022-06-07 |
| US11739249B2 (en) | 2023-08-29 |
| US20220049147A1 (en) | 2022-02-17 |
| US20220204832A1 (en) | 2022-06-30 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US9783727B2 (en) | Fluid loss control package for use in subterranean formation operations | |
| US8916506B2 (en) | High solids content slurries, systems and methods | |
| US5325921A (en) | Method of propagating a hydraulic fracture using fluid loss control particulates | |
| RU2405920C2 (en) | Method for formation of packings in multiple perforation channels in casing string of well bore | |
| US8936082B2 (en) | High solids content slurry systems and methods | |
| CA2153183C (en) | Fluid system for controlling fluid losses during hydrocarbon recovery operations | |
| EA024051B1 (en) | High solids content slurries and method | |
| US10738584B2 (en) | Enhancing propped complex fracture networks | |
| WO2016019416A1 (en) | Drilling fluid additive | |
| WO1994001232A1 (en) | Waste disposal in hydraulically fractured earth formations | |
| US11739249B2 (en) | Lost circulation material for reservoir section | |
| NO20141396A1 (en) | METHODS OF MINIMIZING PROPPANT TRANSFER IN CRACKING TREATMENT | |
| CA3072133C (en) | Degradable diversion material having a urea compound | |
| CN107605425A (en) | Stratum raising formation strength method is cohered in closure in coal bed gas suede capsule drilling fluid | |
| WO2017123937A1 (en) | Compositions useful for diverting or stopping fluids in subterranean operations | |
| CN110700808A (en) | End sand-removing fracturing method | |
| US11753883B2 (en) | Lost circulation material having tentacles | |
| NO20240828A1 (en) | Open-cell, natural materials as lost-circulation material | |
| US11879089B1 (en) | Lost circulation material package with tailored particle size distribution | |
| AU2013403378B2 (en) | Wellbore fluids comprising hydrated inorganic oxide materials and associated methods | |
| RU2347900C1 (en) | Drilling-in method | |
| US12410666B2 (en) | Methods of using multi-particle lost circulation material in highly porous or fractured formations | |
| RU2478768C1 (en) | Method for well drilling | |
| Baret et al. | 6 Cement/Formation Interactions |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 121 | Ep: the epo has been informed by wipo that ep was designated in this application |
Ref document number: 21766060 Country of ref document: EP Kind code of ref document: A1 |
|
| NENP | Non-entry into the national phase |
Ref country code: DE |
|
| WWE | Wipo information: entry into national phase |
Ref document number: 523442498 Country of ref document: SA |
|
| 32PN | Ep: public notification in the ep bulletin as address of the adressee cannot be established |
Free format text: NOTING OF LOSS OF RIGHTS PURSUANT TO RULE 112(1) EPC (EPO FORM 1205A DATED 19/06/2023) |
|
| 122 | Ep: pct application non-entry in european phase |
Ref document number: 21766060 Country of ref document: EP Kind code of ref document: A1 |
|
| WWE | Wipo information: entry into national phase |
Ref document number: 523442498 Country of ref document: SA |
|
| WWE | Wipo information: entry into national phase |
Ref document number: 523442498 Country of ref document: SA |
|
| WWE | Wipo information: entry into national phase |
Ref document number: 523442498 Country of ref document: SA |





