WO2020215407A1 - 一种多功能提取设备 - Google Patents
一种多功能提取设备 Download PDFInfo
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- WO2020215407A1 WO2020215407A1 PCT/CN2019/087195 CN2019087195W WO2020215407A1 WO 2020215407 A1 WO2020215407 A1 WO 2020215407A1 CN 2019087195 W CN2019087195 W CN 2019087195W WO 2020215407 A1 WO2020215407 A1 WO 2020215407A1
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- WIPO (PCT)
- Prior art keywords
- extraction
- tank
- liquid
- condenser
- extraction device
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61J—CONTAINERS SPECIALLY ADAPTED FOR MEDICAL OR PHARMACEUTICAL PURPOSES; DEVICES OR METHODS SPECIALLY ADAPTED FOR BRINGING PHARMACEUTICAL PRODUCTS INTO PARTICULAR PHYSICAL OR ADMINISTERING FORMS; DEVICES FOR ADMINISTERING FOOD OR MEDICINES ORALLY; BABY COMFORTERS; DEVICES FOR RECEIVING SPITTLE
- A61J3/00—Devices or methods specially adapted for bringing pharmaceutical products into particular physical or administering forms
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/028—Flow sheets
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
Definitions
- the invention relates to the technical field of Chinese herbal medicine extraction, in particular to an extraction device.
- the extraction function of the above-mentioned traditional extraction tank is relatively simple, and there are certain restrictions on the types of materials to be extracted, and there are fewer types of materials that can be extracted.
- the present invention provides an extraction device to solve the above problems.
- an extraction equipment including: an extraction tank, including a tank body, the wall of the tank body is provided with a jacket; the tank body is suitable for filling the material mixed with the solvent The tank is also suitable for introducing air pressure gas to agitate the material liquid; the jacket is suitable for heating the material liquid to the extraction temperature. After the temperature is reached, circulating hot water is passed in to maintain the material liquid at the extraction temperature; and the first condenser, which is connected to the tank body, is suitable for condensing the solvent vapor entrained when the air pressure gas is discharged, so as to recover the solvent.
- the top and bottom of the tank are respectively provided with a first air duct and a second air duct, so as to introduce steam and/or air pressure gas into the tank.
- the extraction device further includes: a liquid collector which is respectively connected to the first condenser and the tank; the solvent vapor flows into the liquid collector after being condensed in the first condenser, And return to the tank from the liquid collector.
- the extraction device further includes: a water tank connected to the liquid collector; the compressed air flowing into the liquid collector is suitable for flowing through the water tank to be discharged after washing.
- an exhaust port is provided on the top of the tank; an exhaust pipe is connected between the exhaust port and the first condenser, and the exhaust pipe A water inlet pipe is connected to the upper part; an end of the exhaust pipe close to the exhaust port is provided with a filter screen device.
- the extraction tank further includes: a sieve plate, which is detachably installed in the tank body, the sieve plate is suitable for placing plant spices; the bottom of the tank body is suitable for The steam is introduced to distill the plant flavor to form a distilled gas, and the distilled gas is suitable for being condensed by the first condenser to form a distillate.
- a sieve plate which is detachably installed in the tank body, the sieve plate is suitable for placing plant spices
- the bottom of the tank body is suitable for The steam is introduced to distill the plant flavor to form a distilled gas
- the distilled gas is suitable for being condensed by the first condenser to form a distillate.
- the extraction device further includes: an oil-water separator connected to the first condenser and adapted to separate the distillate from oil and water to extract sesame oil.
- the jacket is provided with a water inlet and a water outlet
- the extraction device further includes: a water circulation temperature controller, which is connected to the jacket through a hot water pipe.
- the water outlet is connected with the water outlet so as to pass circulating hot water into the jacket.
- the extraction device further includes: a steam heater, which is respectively connected with the first air duct and the second air duct through a steam pipe, so as to introduce steam into the tank.
- a steam heater which is respectively connected with the first air duct and the second air duct through a steam pipe, so as to introduce steam into the tank.
- the extraction device further includes: an air storage tank, which is respectively connected with the first air duct and the second air duct, so as to pass air pressure gas into the tank body; and air pressure
- the air compressor is connected to the air storage tank, and the air compressor is suitable for compressing gas so as to form an air pressure gas and pass into the air storage tank.
- the extraction device further includes: a liquid storage tank suitable for storing the extraction liquid; a filter, respectively connected to the tank body and the liquid storage tank, so that the extraction liquid flows from the tank body After being filtered by the filter, it enters the liquid storage tank.
- the extraction device further includes: a concentrator adapted to concentrate the extract, and the concentrator is a single-effect concentrator or a multi-effect concentrator.
- the concentrator includes: a heating chamber, which is suitable for introducing the extraction liquid to be concentrated and suitable for passing steam to heat the extraction liquid; an evaporation chamber, which circulates with the heating chamber The pipe is connected, so that the extraction liquid flows into the evaporation chamber after being heated by the heating chamber, and is separated into secondary steam and extraction liquid in the evaporation chamber, and the separated extraction liquid can flow back to the heating chamber through the circulation pipe;
- the evaporator is connected to the evaporation chamber so that the secondary vapor in the evaporator enters the second condenser for condensation; and the liquid collection tank is located below the second condenser and is connected to the second condenser through a conduit for The liquid condensed by the second condenser is introduced into the liquid collecting tank through the conduit.
- the liquid collection tank includes two upper and lower layers, and the upper and lower layers are connected by a catheter.
- the extraction device further includes: a vacuuming device connected to the second condenser so as to extract the gas flowing into the second condenser from the evaporation chamber.
- the vacuum pumping device includes: a vacuum pump; a third condenser connected to the second condenser and the vacuum pump through vacuum pipes; and a vacuum buffer tank located in the Below the third condenser and in communication with the third condenser; wherein, the vacuum pump is suitable for vacuuming the evaporation chamber, the second condenser and the third condenser; the liquid condensed by the third condenser Enter the vacuum buffer tank.
- the extraction device further includes: an extraction tank connected to the concentrator.
- an extraction equipment which first directly heats the material liquid directly by introducing steam into the extraction tank, and heats it to the extraction temperature, and then passes circulating hot water to the jacket of the extraction tank.
- the liquid undergoes auxiliary heating to keep the material liquid stable at the extraction temperature.
- compressed air is introduced to the top or bottom of the tank to agitate the material liquid, so that the material liquid is stirred more fully and higher extraction efficiency is obtained.
- the extraction equipment of the present invention By setting the first condenser connected with the tank, the solvent vapor entrained by the compressed air discharged during the extraction process can be condensed and recovered, and the solvent absorbed by the material residue can be condensed and recovered after the extraction is completed, thereby reducing the solvent To avoid the direct emission of solvent and pollute the environment.
- a detachable sieve is provided to place plant fragrances, and water vapor is introduced into the bottom of the tank, so that the plant fragrances can be distilled and extracted to obtain sesame oil.
- the extraction equipment of the present invention also includes a concentrator, so that the extraction liquid can be directly concentrated and separated after the extraction liquid is obtained, in one step.
- FIG. 1 shows a schematic structural diagram of an extraction device 300 according to an embodiment of the present invention
- FIG. 2 shows a partial diagram of the extraction module 100 according to an embodiment of the present invention
- Figure 3 shows a partial view of the extraction tank 110 according to an embodiment of the present invention
- Fig. 4 shows a partial view of a concentrator 200 according to an embodiment of the present invention.
- Fig. 1 shows a schematic structural diagram of an extraction device 300 of the present invention.
- the extraction device 300 includes an extraction module 100 suitable for extracting materials, and the extraction module 100 is suitable for extracting the material liquid after the material and the solvent are mixed to form an extraction liquid and store it.
- the material in the present invention can be, for example, Chinese herbal medicine, but is not limited thereto.
- the solvent used for extracting the material can be pure water or tap water, but also can be methanol solution or ethanol solution, but is not limited to this.
- the extraction module 100 includes an extraction tank 110 and a first condenser 120 communicating with the extraction tank 110.
- the extraction tank 110 includes a tank body 111, and the tank body 110 is suitable for containing the material liquid mixed with the material and the solvent.
- the wall of the tank body 111 is provided with a jacket 112.
- the top and bottom of the tank 111 are respectively provided with a first air duct 113 and a second air duct 114.
- the first air duct 113 and the second air duct 114 are respectively connected to the steam pipe and the air pressure pipe.
- the air pipes are respectively provided with valves, so that steam and air pressure gas are controlled to be introduced into the first air pipe 113 and the second air pipe 114 through the switch of the control valve, and the first air pipe 113 and the second air pipe 114 are directed to the tank 111 Introduce steam and/or compressed air.
- the first air duct 113 at the top of the tank body 111 is also provided with a jet tube 119, which extends downward from the first air guide tube 113 to the lower part of the tank body 111, so that the steam or air introduced by the first air guide tube 113 The pressurized gas can flow into the tank 111 from the lower part of the tank 111 through the jet pipe 119.
- the extraction solution is an extraction solution obtained by continuously agitating the material solution with compressed air at the extraction temperature to fully and uniformly mix the material and the solvent, and then the effective components in the material are extracted into the solvent.
- parameters such as extraction temperature and heating time can be set by those skilled in the art, and the present invention does not limit this.
- the introduction of steam is stopped, and hot water of a predetermined temperature is circulated into the jacket 112 of the extraction tank 110 to assist in heating the material liquid in the tank body 111 to make Maintain a stable extraction temperature.
- the jacket 112 of the extraction tank 110 is supplementarily heated by circulating hot water, which is beneficial to stably control the extraction temperature and save energy.
- compressed air is also introduced from the top of the tank 110 through the first air duct 113, or compressed air is introduced from the bottom of the tank 110 through the second air duct 114, and the compressed air
- the material liquid is agitated, so that the spatial temperature of the material liquid is uniform, and at the same time, the effective components in the extracted materials are fully entered into the extraction liquid, and higher extraction efficiency is obtained.
- the extraction device 300 includes a steam heater 160, which communicates with the first air duct 113 and the second air duct 114 through a steam pipe, so as to introduce steam into the tank 111 to provide heat for the material liquid.
- the steam heater 160 may be an electric furnace.
- the extraction device 300 also includes a water circulation temperature controller 170, and the jacket 112 is provided with a water inlet and a water outlet.
- the water circulation temperature controller 170 is respectively connected with the water inlet and the water outlet of the jacket 112 through the hot water pipe, thereby forming a sealed circulating heating system. Circulating hot water is introduced into the jacket 112 to assist the heating of the liquid in the tank. , Make the material liquid at a stable extraction temperature.
- the water circulation temperature controller 170 can be a micro-control numerical heating device, which can set the water temperature as required.
- the water circulation temperature controller 170 is equipped with digitally displayed inlet water temperature, outlet water temperature, current water temperature and set water temperature, so as to automatically Adjust the heating temperature or stop heating.
- the heating temperature control range of the water circulation temperature controller 170 is 25-98°C.
- the extraction device 300 also includes an air storage tank 140 and an air compressor 145.
- the air compressor 145 is connected to the air storage tank 145.
- the air compressor 145 is adapted to compress gas to form an air pressure gas and pass it into the air storage tank for storage.
- the air storage tank 140 is respectively communicated with the first air duct 113 and the second air duct 114 through the compressed air pipe, so that the compressed air output from the compressed air pipe can be introduced into the tank body through the first air duct 113 or the second air duct 114 Within 111.
- Air pressure gas may include air, nitrogen, inert gas, etc.
- the air storage tank 140 is also connected with an air oil-water separator 141. Since the compressed air of the air compressor 145 will produce oily wastewater, the air oil-water separator 141 can filter the oily wastewater entrained by the compressed air output from the air storage tank 140, thereby purifying the compressed air and improving the access to the tank 111 The purity of the compressed air.
- the extraction tank 110 further includes a pneumatic device 105, and is adapted to control the opening or closing of the slag outlet cover 102 through the pneumatic device 105, and the power source for opening the slag outlet cover 102 is air pressure gas.
- the top of the tank 111 is provided with an exhaust port 115, and the compressed air introduced into the tank 111 is discharged through the exhaust port 115.
- An exhaust pipe 117 is connected between the exhaust port 115 and the first condenser 120, so that the first condenser 120 and the tank 111 are in communication through the exhaust pipe 117. Since the air pressure gas will entrain solvent vapor when discharged, the first condenser 120 connected with the tank 111 is arranged so that the air pressure gas and the entrained solvent vapor enter the first condenser 120 through the exhaust pipe 117 and pass through The first condenser 120 condenses and recovers the solvent vapor, thereby preventing the solvent loss in the extraction tank 110.
- a liquid collector 125 is provided below the first condenser 120.
- the top (liquid inlet) of the liquid collector 125 communicates with the condenser tube, and the bottom (liquid outlet) of the liquid collector 125 communicates with the tank 111.
- the solvent vapor entrained by the compressed air is condensed in the first condenser 120, and then flows into the liquid collector 125 for recovery, and can flow back from the liquid outlet of the liquid collector 125 to the tank 111 to extract materials. In this way, the solvent discharged with the compressed air can be reused. On the one hand, the loss of the solvent is reduced, and on the other hand, the solvent is prevented from being discharged into the atmosphere to pollute the environment.
- the extraction module 100 further includes a water tank 130, and the water tank 130 is in communication with a liquid collector 125.
- the compressed air gas that has not been condensed by the first condenser 120 and a small amount of uncondensed solvent vapor, after entering the liquid collector 125, will continue to flow through the water tank 130 and be washed out, further preventing the solvent vapor from being directly discharged into the atmosphere and polluting the environment .
- the exhaust pipe 117 is also connected with a water inlet pipe, and the water inlet pipe is provided with a manual valve so that after the manual valve controls the opening of the water inlet pipe, water flow can be introduced into the exhaust pipe 117, thereby Clean the material residue in the exhaust pipe 117.
- the end of the exhaust pipe 117 close to the exhaust port 115 is also provided with a filter device 116.
- the filter device 116 can intercept the material particles entrained when the air pressure gas is discharged, and prevent the material particles from entering the first condenser with the air pressure gas.
- air pressure gas and water vapor can be continuously introduced into the tank 111.
- the air pressure gas and water vapor can form a resultant force and carry away the solvent adsorbed by the material residue from the exhaust gas.
- the port 115 is discharged and enters the first condenser 120 for condensation, the condensed solvent enters the liquid collector 125, and the uncondensed gas flows through the water tank 130 and is discharged after washing. In this way, the solvent absorbed by the material residue can be recovered, the loss of the solvent can be reduced, and the direct discharge of the solvent and environmental pollution can be avoided.
- the extraction device 300 of the present invention can also extract sesame oil from plant flavors by distillation.
- Plant fragrances can be, for example, plant petals, plant branches and leaves, root bark, etc., but are not limited thereto.
- the extraction tank 110 further includes a sieve plate 118, and the sieve plate 118 is detachably installed in the tank body 111.
- the sieve plate 118 is installed in the tank 111, and the plant spices to be extracted are placed on the sieve plate 118.
- Steam is introduced from the bottom of the tank 111 through the second air duct 114, so that the effective components in the plant flavors are distilled with the steam to form distilled gas, so that the effective components in the plant flavors can be distilled and extracted.
- the extraction module 100 further includes an oil-water separator 160, and the oil-water separator 160 is in communication with the first condenser 120.
- the distilled gas formed by steam distillation of the active ingredients in the plant flavor flows into the first condenser 120 through the exhaust pipe 117, and is condensed by the first condenser 120 to form a distillate.
- the distillate flows into the oil-water separator 160 and is The oil and water are separated in the separator 160 to extract sesame oil.
- the oil-water separator 160 is also provided with an oil outlet 161 so as to lead the extracted sesame oil from the oil outlet 161.
- air pressure gas can also be introduced into the tank 111 through the first air duct 113 or the second air duct 114, so that the air pressure gas and water vapor can be formed Together, it helps to distill and extract the effective ingredients in plant spices more quickly and fully.
- the extraction module 100 further includes a liquid storage tank 150 and a filter 155, and the liquid storage tank 150 is suitable for storing the extracted liquid after extraction.
- an extraction liquid pipe 151 is connected to the bottom of the tank body 111, and the extraction liquid pipe 151 communicates with the liquid inlet of the filter 155, and the liquid outlet of the filter 155 communicates with the liquid storage tank 150.
- the filter 155 is respectively connected to the tank 111 and the liquid storage tank 150.
- the extraction liquid pipe 151 is opened to lead the extracted liquid from the tank 111 and enter the filter 155. It is filtered, and further, the filtered extract is introduced into the liquid storage tank 150 again.
- the extraction device 300 further includes a concentrator 200, which is adapted to concentrate the extraction liquid.
- the concentrator 200 is a single-effect concentrator or a multi-effect concentrator.
- the concentrator 200 is a single-effect concentrator, which includes a heating chamber 210, an evaporation chamber 220, a second condenser 230 and a liquid collecting tank 240.
- the heating chamber 210 can be connected to the liquid storage tank 150, so that the extracted liquid in the liquid storage tank 150 can be introduced into the heating chamber 210, and the heating chamber 210 is connected to the steam heater 160 through a steam pipe, so that the heating chamber 210 can pass into The steam heats the extract.
- the heating chamber 210 and the liquid storage tank 150 may also be in an independent state without communication.
- the extraction liquid in the liquid storage tank 150 can be pumped into the heating chamber 210 by a liquid medicine pump and placed in the heating chamber 210. Heating by steam.
- the upper and lower parts of the heating chamber 210 are respectively connected to the evaporation chamber 220 through a circulation pipe, and the top of the evaporation chamber 220 is in communication with the second condenser 230.
- the liquid collection tank 240 is located below the second condenser 230 and is connected to the second condenser 230. Connected by conduit. In this way, the extraction liquid is heated by the heating chamber 210 and flows into the evaporation chamber 220 from the upper circulation pipe by means of a vacuum external force, and is separated into the secondary steam and the extraction liquid in the evaporation chamber 220.
- the extraction liquid separated by the evaporation chamber 220 can flow back into the heating chamber 210 through the lower circulation pipe, and then flow into the evaporation chamber 220 after being heated by the heating chamber 210 to form the circulating heating and evaporation of the extraction liquid to realize the concentration of the extraction liquid.
- the secondary vapor separated by the evaporation chamber 220 enters the second condenser 230 to be condensed into liquid, and is introduced into the liquid collecting tank 240 through the pipe.
- the liquid collecting tank 240 has a double-layer structure, including upper and lower layers, and the upper and lower layers are connected by a catheter 245.
- the liquid in the upper layer of the liquid collecting tank 240 can pass through the catheter 245.
- the catheter 245 is provided with a valve.
- the valve of the catheter 245 can be closed to drain the liquid in the lower layer, and then the valve can be opened to connect the upper and lower layers of the liquid collecting tank 240, and the upper layer of liquid can pass through the catheter 245. Import to the lower layer.
- the concentrator 200 in the present invention can continuously evaporate and condense the solvent in the extract to be recovered in the liquid collecting tank 240, thereby realizing continuous concentration of the extract.
- the wall of the evaporation chamber 220 is also provided with an evaporation chamber jacket 222.
- the evaporation chamber jacket 222 and the water circulation temperature controller 170 are also communicated through a hot water pipe, so as to pass into the evaporation chamber jacket 222.
- the circulating hot water provides heat for the separated extraction liquid in the evaporation chamber 220, ensuring that the extraction liquid circulating into the heating chamber 210 has a higher temperature, and the concentration efficiency is improved.
- the extraction device 300 further includes a vacuuming device 250, and the vacuuming device 250 is connected to the second condenser 230 and can extract the vaporized gas in the evaporation chamber 220.
- the vacuum device 250 includes a third condenser 251, a vacuum buffer tank 252, and a vacuum pump 253.
- the vacuum pump 253 may be a water ring vacuum pump, but is not limited thereto.
- the third condenser 251 is connected to the second condenser 230 and the vacuum pump 253 through an evacuated tube, respectively.
- the vacuum buffer tank 252 is located below the third condenser 251 and communicates with the third condenser 251. In this way, the vaporized gas in the evaporation chamber 220 (passing through the second condenser 230) can be extracted into the third condenser 251 by the vacuum pump 253 to be further condensed, and the uncondensed gas in the third condenser 251 can be pumped away; The liquid condensed by the triple condenser 251 enters the vacuum buffer tank 252.
- the vacuum pump 253 can pump the evaporation chamber 220, the second condenser 230, and the third condenser 251 into a vacuum state.
- the vacuum device 250 extracts the vaporized gas in the evaporation chamber 220, so that the inside of the concentrator 200 can be in a negative pressure environment, so that the extraction liquid can reach the concentration requirement more quickly under the negative pressure environment.
- the third condenser 251 and the vacuum buffer tank 252 the uncondensed gas in the second condenser 230 is further condensed, so that a stable vacuum degree in the concentrator 200 can be achieved, and the pressure difference between the inside and outside of the concentration tank can be buffered. To prevent backflow.
- the extraction device 300 may also be provided with an extraction tank (not shown in the figure), by connecting the extraction tank with the concentrator 200, specifically with the outlet of the heating chamber 210, so that the extraction in the concentrator 200 After the liquid concentration is completed, by pressurizing the concentrator 200 or decompressing the extraction tank, the pressure difference between the concentrator 200 and the extraction tank is generated, so that the concentrated fluid in the concentrator 200 can be introduced into the extraction tank and in The concentrated liquid is extracted in the extraction tank.
- an extraction tank not shown in the figure
- the description of the terms “one embodiment”, “some embodiments”, “specific embodiments”, etc. means that specific features, structures, materials, or characteristics described in conjunction with the embodiment or example are included in the present invention In at least one embodiment or example.
- the schematic representation of the above-mentioned terms does not necessarily refer to the same embodiment or example.
- the described specific features, structures, materials or characteristics may be combined in any one or more embodiments or examples in a suitable manner.
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Abstract
一种提取设备(300),包括:提取罐(110),包括罐体(111),罐体(111)的壁部设有夹套(112);罐体(111)适于装入物料与溶剂混合后的料液,并适于导入蒸汽对料液加热,以使料液加热到提取温度;罐体(111)还适于导入空压气体对料液进行搅动;夹套(112)适于在料液加热到提取温度后通入循环热水,以使料液维持在提取温度;以及第一冷凝器(120),与罐体(111)连通,适于对空压气体排放时夹带的溶剂蒸汽进行冷凝,以便回收溶剂。提取设备(300)能充分提取物料的有效成分、提取效率高,并能回收溶剂,在获得提取液后能直接对提取液进行浓缩分离,一步到位,还可以对植物香料进行蒸馏提取而获得香油。
Description
本发明涉及中草药提取技术领域,尤其涉及一种提取设备。
目前,大多数中药制药厂或中草药制品厂家,提取中草药应用的仍是传统的提取罐,并采用提取罐夹套通蒸汽的方式对料液进行加热,这种加热方式会导致夹套温度波动较大,不稳定。而且,传统的提取罐,罐体的容体较大,多为2m
3~10m
3,因而在提取固体物料时,不适合机械搅动,通常是采取罐体外对流的方式使料液缓慢对流,很难获得搅动效果,而且耗时长,能耗大,提取效率低,热源消耗大,提取过程中逸出废气,污染环境。有些厂家对提取罐采用机械搅动料液,但在提取过程中,常发生搅动桨卡料,物液打旋现象,提取效果低。另外,传统的提取罐,在物料提取完毕后,不能有效回收物料吸附的有机溶剂,一方面造成溶剂的损耗较大,另一方面直接排放沾有有机溶剂的物料会造成环境污染。
此外,上述传统的提取罐的提取功能也比较单一,对提取的物料种类有一定限制,可提取的物料种类较少。
发明内容
为此,本发明提供了一种提取设备,以解决上面存在的问题。
根据本发明的一个方面,提供了一种提取设备,包括:提取罐,包括罐体,所述罐体的壁部设有夹套;所述罐体适于装入物料与溶剂混合后的料液,并适于导入蒸汽对料液加热,以使料液加热到提取温度;所述罐体还适于导入空压气体对料液进行搅动;所述夹套适于在料液加热到提取温度后通入循环热水,以使料液维持在提取温度;以及第一冷凝器,与所述罐体连通,适于对空压气体排放时夹带的溶剂蒸汽进行冷凝,以便回收溶剂。
可选地,在根据本发明的提取设备中,所述罐体的顶部和底部分别设有第一导气管和第二导气管,以便向罐体内导入蒸汽和/或空压气体。
可选地,在根据本发明的提取设备中,还包括:集液器,分别与所述第一冷凝器和罐体连通;溶剂蒸汽在第一冷凝器内冷凝后流入所述集液器,并由集液器回流至所述罐体内。
可选地,在根据本发明的提取设备中,还包括:水箱,与所述集液器连通;流入所述集液器的空压气体,适于流经所述水箱水洗后排出。
可选地,在根据本发明的提取设备中,所述罐体的顶部设有排气口;所述排气口与所述第一冷凝器之间连接有排气管,所述排气管上连接有进水管;所述排气管靠近所述排气口的一端设有滤网装置。
可选地,在根据本发明的提取设备中,所述提取罐还包括:筛板,可拆卸安装于所述罐体内,所述筛板上适于放置植物香料;所述罐体底部适于导入蒸气,以便对所述植物香料进行蒸馏形成蒸馏气,蒸馏气适于通过所述第一冷凝器冷凝形成蒸馏液。
可选地,在根据本发明的提取设备中,还包括:油水分离器,与所述第一冷凝器连通,并适于对所述蒸馏液进行油水分离,以便提取香油。
可选地,在根据本发明的提取设备中,所述夹套上设有进水口和出水口,所述提取设备还包括:水循环温度控制机,通过热水管分别与所述夹套的进水口和出水口连通,以便向所述夹套内通入循环热水。
可选地,在根据本发明的提取设备中,还包括:蒸汽加热器,通过蒸汽管分别与所述第一导气管和第二导气管连通,以便向所述罐体内导入蒸汽。
可选地,在根据本发明的提取设备中,还包括:空气储罐,分别与所述第一导气管和第二导气管连通,以便向所述罐体内通入空压气体;以及空压机,与所述空气储罐连接,所述空压机适于压缩气体,以便形成空压气体通入所述空气储罐中。
可选地,在根据本发明的提取设备中,还包括:储液罐,适于储存提取液;过滤器,分别与所述罐体和储液罐连接,以便提取液从所述罐体流经所述过滤器过滤后进入所述储液罐。
可选地,在根据本发明的提取设备中,还包括:浓缩器,适于对所述提 取液进行浓缩,所述浓缩器为单效浓缩器或多效浓缩器。
可选地,在根据本发明的提取设备中,所述浓缩器包括:加热室,适于导入待浓缩的提取液并适于通入蒸汽对提取液进行加热;蒸发室,与加热室通过循环管连通,以便提取液经加热室加热后流入所述蒸发室,并在蒸发室分离为二次蒸汽和提取液,且分离后的提取液可通过所述循环管回流至加热室;第二冷凝器,与所述蒸发室连通,以便蒸发室内的二次蒸汽进入第二冷凝器冷凝;以及收液罐,位于所述第二冷凝器下方并与所述第二冷凝器通过导管连接,以便经第二冷凝器冷凝后的液体通过所述导管导入收液罐。
可选地,在根据本发明的提取设备中,所述收液罐包括上下两层,且上下两层通过导液管连通。
可选地,在根据本发明的提取设备中,还包括:抽真空装置,与所述第二冷凝器连接,以便抽取由所述蒸发室流入第二冷凝器中的气体。
可选地,在根据本发明的提取设备中,所述抽真空装置包括:真空泵;第三冷凝器,分别通过抽真空管与所述第二冷凝器和真空泵连接;以及真空缓冲罐,位于所述第三冷凝器下方并与所述第三冷凝器连通;其中,所述真空泵适于将所述蒸发室、第二冷凝器及第三冷凝器抽成真空;经第三冷凝器冷凝后的液体进入所述真空缓冲罐。
可选地,在根据本发明的提取设备中,还包括:萃取罐,与所述浓缩器连通。
根据本发明的技术方案,提供了一种提取设备,先通过向提取罐内导入蒸汽直接对料液直接加热,并加热到提取温度,进而向提取罐的夹套内通入循环热水对料液进行辅助加热,使料液稳定维持在提取温度。而且,在提取过程中,还向罐体的顶部或底部导入空压气体对料液进行搅动,从而使料液搅拌更充分,获取更高的提取效率。通过设置与罐体连通的第一冷凝器,能对提取过程中排放的空压气体夹带的溶剂蒸汽进行冷凝回收,并能在提取完成后对物料残渣吸附的溶剂进行冷凝回收,从而能降低溶剂的损耗,避免溶剂直接排放而污染环境。另外,本发明的提取设备,通过设置可拆卸的筛板放置植物香料,并通过向罐体底部导入水蒸气,从而能对植物香料进行蒸馏提取而获得香油。本发明的提取设备还包括浓缩器,从而在获得提取液后能 直接对提取液进行浓缩分离,一步到位。
上述说明仅是本发明技术方案的概述,为了能够更清楚了解本发明的技术手段,而可依照说明书的内容予以实施,并且为了让本发明的上述和其它目的、特征和优点能够更明显易懂,以下特举本发明的具体实施方式。
为了实现上述以及相关目的,本文结合下面的描述和附图来描述某些说明性方面,这些方面指示了可以实践本文所公开的原理的各种方式,并且所有方面及其等效方面旨在落入所要求保护的主题的范围内。通过结合附图阅读下面的详细描述,本公开的上述以及其它目的、特征和优势将变得更加明显。涉及本公开,相同的附图标记通常指代相同的部件或元素。
图1示出了根据本发明一个实施例的提取设备300的结构示意图;
图2示出了根据本发明一个实施例中的提取模块100的局部图;
图3示出了根据本发明一个实施例中的提取罐110的局部图;
图4示出了根据本发明一个实施例中的浓缩器200的局部图。
下面将参照附图更详细地描述本公开的示例性实施例。虽然附图中显示了本公开的示例性实施例,然而应当理解,可以以各种形式实现本公开而不应被这里阐述的实施例所限制。相反,提供这些实施例是为了能够更透彻地理解本公开,并且能够将本公开的范围完整的传达给本领域的技术人员。
如前文所述,现有技术中用于中草药的提取设备,在使用过程中或多或少存在一定的功能缺陷,因此本发明提出了一种性能更优化的提取设备300。图1示出了本发明的提取设备300的结构示意图。
如图1所示,提取设备300包括适于提取物料的提取模块100,提取模块100适于对物料与溶剂混合后的料液进行提取,以形成提取液并储存。需要说明的是,本发明中的物料例如可以是中草药等,但不限于此。提取物料所采用的溶剂可以是纯水或自来水,也可以是甲醇溶液或乙醇溶液,但不限于此。
根据一个实施例,如图1所示,提取模块100包括提取罐110以及与提取罐110连通的第一冷凝器120。提取罐110包括罐体111,罐体110内适于装入物料与溶剂混合后的料液,罐体111的壁部设有夹套112。罐体111的顶部和底部分别设有第一导气管113和第二导气管114,第一导气管113、第二导气管114均分别与蒸汽管和空压气管连接,且蒸汽管和空压气管上分别设有阀门,从而通过控制阀门的开关控制蒸汽、空压气体向第一导气管113、第二导气管114导入,并由第一导气管113和第二导气管114向罐体111内导入蒸汽和/或空压气体。另外,罐体111顶部的第一导气管113还设有喷气管119,喷气管119由第一导气管113向下延伸至罐体111的下部,从而由第一导气管113导入的蒸汽或空压气体,能通过喷气管119从罐体111的下部流入罐体111内。
在提取过程中,先通过第一导气管113或第二导气管114导入蒸汽直接对料液进行加热,并将料液加热到提取温度,以便在提取温度对料液进行提取得到提取液。需要说明的是,提取液是通过在提取温度下持续通过空压气体搅动料液,使物料与溶剂充分、均匀混合后,物料中的有效成分被提取到溶剂中所得到的提取溶液。其中,提取温度、加热时间等参数可以由本领域技术人员自行设置,本发明对此不做限制。
进而,在通过蒸汽将料液加热到提取温度后,停止导入蒸汽,并向提取罐110的夹套112内循环通入预定温度的热水,对使罐体111内的料液辅助加热,使维持在稳定的提取温度。这样,在蒸汽直接对料液加热到提取温度后,通过循环热水对提取罐110的夹套112进行辅助加热,有利于稳定地控制提取温度,而且节约能量。应当指出,在加热过程中,还通过第一导气管113从罐体110的顶部导入空压气体,或者通过第二导气管114从罐体110的底部导入空压气体,通过导入空压气体对料液进行搅动,从而使料液的空间温度均匀,同时使提取物料中的有效成分充分进入提取液中,获取更高的提取效率。
具体地,提取设备300包括蒸汽加热器160,蒸汽加热器160通过蒸汽管分别与第一导气管113、第二导气管114连通,以便向罐体111内导入蒸汽为料液提供热量。蒸汽加热器160可以为电热炉。
如图1所示,提取设备300还包括水循环温度控制机170,夹套112上设 有进水口和出水口。水循环温度控制机170通过热水管分别与夹套112的进水口和出水口连通,从而形成密封循环的加热体系,向夹套112内通入循环热水,对罐体内的料液进行辅助加热,使料液处于稳定的提取温度。水循环温度控制机170可以是微控数值化加热设备,其可以按需求设置水温且水循环温度控制机170上设有数字化显示的进水温度、出水温度、当前水温度以及设置水温度,从而能自动调控加热温度或者停止加热。可选地,水循环温度控制机170的加热温控范围为25~98℃。
提取设备300还包括空气储罐140和空压机145,空压机145与空气储罐145连接,空压机145适于压缩气体,以形成空压气体通入到空气储罐中储存。空气储罐140通过空压气管分别与第一导气管113、第二导气管114连通,从而由空压气管输出的空压气体可通过第一导气管113或第二导气管114导入至罐体111内。空压气体可包括空气、氮气、惰性气体等。
进一步地,空气储罐140还连接有空气油水分离器141。由于空压机145压缩空气会产生含油废水,通过设置空气油水分离器141,能过滤空气储罐140输出的空压气体夹带的含油废水,从而净化空压气体,提高通入至罐体111内的空压气体的纯净度。
另外,如图2和图3所示,罐体111的底部设有排渣口101,排渣口101处设有适于封堵排渣口的排渣口盖102。根据一种实施方式,提取罐110还包括气动装置105,并适于通过该气动装置105控制排渣口盖102打开或关闭,排渣口盖102的开启动力源是空压气体。
根据一个实施例,如图1所示,罐体111的顶部设有排气口115,罐体111内导入的空压气体会通过排气口115排放。该排气口115与第一冷凝器120之间连接有排气管117,从而,第一冷凝器120与罐体111通过该排气管117连通。由于空压气体在排放时会夹带溶剂蒸汽,通过设置与罐体111连通的第一冷凝器120,使空压气体与夹带的溶剂蒸汽均通过排气管117进入第一冷凝器120,并通过第一冷凝器120对溶剂蒸汽冷凝后回收,从而能防止提取罐110内的溶剂损失。
进一步地,如图1所示,第一冷凝器120的下方设有集液器125。集液器125的顶部(进液口)与冷凝器用管连通,集液器125的底部(出液口)与罐 体111连通。空压气体夹带的溶剂蒸汽在第一冷凝器120内冷凝后,会流入集液器125内回收,并能从集液器125的出液口回流至罐体111内提取物料。这样,随空压气体排放的溶剂能重新被利用,一方面减少了溶剂的流失,另一方面防止溶剂排放到大气中污染环境。
如图1所示,提取模块100还包括水箱130,水箱130与集液器125连通。未经第一冷凝器120冷凝的空压气体以及少部分未冷凝的溶剂蒸汽,在进入集液器125后,会继续流经水箱130水洗后排出,进一步防止溶剂蒸汽直接排放到大气中污染环境。
另外,如图1所示,排气管117上还连接有进水管,该进水管上设有手动阀,以便通过手动阀控制进水管开启后,能向排气管117内通入水流,从而清洗排气管117内的物料残渣。此外,排气管117上靠近排气口115的一端还设有滤网装置116,滤网装置116能拦截空压气体排放时夹带的物料颗粒,防止物料颗粒随空压气体进入第一冷凝器120内。
需要说明的是,在对料液提取完成后,还可继续向罐体111内导入空压气体和水蒸气,空压气体和水蒸气可形成合力,并携带走物料残渣吸附的溶剂从排气口115排出、并进入第一冷凝器120冷凝,冷凝后的溶剂进入集液器125,未冷凝的气体则流经水箱130水洗后排放。这样,能实现对物料残渣吸附的溶剂进行回收,降低溶剂的损耗,也避免了溶剂直接排放而污染环境。
根据一个实施例,本发明的提取设备300还能通过蒸馏法从植物香料中提取香油。植物香料例如可以是植物花瓣、植物枝叶、根皮等,但不限于此。具体地,提取罐110还包括筛板118,筛板118可拆卸地安装于罐体111内。当需要通过蒸馏法从植物香料中提取香油时,通过将筛板118安装在罐体111内,在筛板118上放置要提取的植物香料。通过第二导气管114从罐体111的底部导入蒸气,从而,植物香料中的有效成分随蒸汽蒸馏形成蒸馏气,实现对植物香料中的有效成分进行蒸馏提取。
进一步地,如图1至图3所示,提取模块100还包括油水分离器160,油水分离器160与第一冷凝器120连通。植物香料中的有效成分随蒸汽蒸馏形成的蒸馏气由排气管117流入第一冷凝器120,并通过第一冷凝器120冷凝形成蒸馏液,进而,蒸馏液流入油水分离器160,并在油水分离器160内进行油 水分离,从而提取香油。另外,油水分离器160上还设有出油口161,从而将提取的香油从出油口161导出。
需要说明的是,在通过蒸馏法从植物香料中提取香油时,也可以通过第一导气管113或第二导气管114向罐体111内导入空压气体,从而空压气体和水蒸气可形成合力,有助于更快速、充分地对植物香料中的有效成分进行蒸馏提取。
此外,如图1所示,提取模块100还包括储液罐150和过滤器155,储液罐150适于储存提取完成后的提取液。具体地,罐体111的底部连接有提取液管151,并通过提取液管151与过滤器155的进液口连通,过滤器155的出液口与储液罐150连通。这样,过滤器155分别与罐体111和储液罐150连接,当罐体111内的料液提取完成后,通过开启提取液管151,将提取液从罐体111内导出并进入过滤器155过滤,进而,过滤后的提取液再导入储液罐150。
根据一个实施例,提取设备300还包括浓缩器200,浓缩器200适于对提取液进行浓缩。可选地,浓缩器200为单效浓缩器或多效浓缩器。
根据一种实施方式,如图1所示,浓缩器200为单效浓缩器,该单效浓缩器包括加热室210、蒸发室220、第二冷凝器230以及收液罐240。
其中,加热室210可与储液罐150连通,从而储液罐150内的提取液可导入加热室210内,且加热室210通过蒸汽管与蒸汽加热器160连接,从而加热室210可通入蒸汽对提取液进行加热。需要说明的是,加热室210与储液罐150之间也可以是不连通的独立状态,储液罐150内的提取液可通过药液泵抽入加热室210内,并在加热室210内通过蒸汽进行加热。
另外,加热室210的上部与下部分别通过循环管与蒸发室220连通,蒸发室220的顶部与第二冷凝器230连通,收液罐240位于第二冷凝器230下方并与第二冷凝器230通过导管连接。这样,提取液经加热室210加热,并借助抽真空外力从上部的循环管流入蒸发室220,并在蒸发室220分离为二次蒸汽和提取液。经蒸发室220分离后的提取液可通过下部的循环管回流到加热室210内,再次经加热室210加热后流入蒸发室220,形成对提取液的循环加热和蒸发,实现提取液的浓缩。而经蒸发室220分离后的二次蒸汽会进入 第二冷凝器230冷凝为液体,并通过导管导入收液罐240内。
根据一种实施方式,如图4所示,收液罐240为双层结构,包括上下两层,且上下两层通过导液管245连通,收液罐240上层的液体可通过导液管245导入至下层,导液管245上设有阀门。这样,当下层液体收集到一定量时,可关闭导液管245阀门,将下层的液体排出,进而再打开阀门,使收液罐240的上下两层连通,上层液体又能通过导液管245导入至下层。可见,本发明通过浓缩器200能对提取液中的溶剂不断蒸发并冷凝回收到收液罐240内,进而实现对提取液持续的浓缩。
如图1所示,蒸发室220的壁部也设有蒸发室夹套222,该蒸发室夹套222与水循环温度控制机170也通过热水管连通,从而通过向蒸发室夹套222内通入循环热水,为蒸发室220内分离后的提取液提供热量,保证循环进入加热室210的提取液具有较高的温度,提高浓缩效率。
此外,如图1所示,提取设备300还包括抽真空装置250,抽真空装置250与第二冷凝器230连接,能抽取蒸发室220中蒸发的气体。换言之,蒸发室220中蒸发的气体流入第二冷凝器230中,并被抽真空装置250抽走。具体地,抽真空装置250包括第三冷凝器251、真空缓冲罐252和真空泵253,真空泵253可以是水环真空泵,但不限于此。第三冷凝器251分别通过抽真空管与第二冷凝器230和真空泵253连接。真空缓冲罐252位于第三冷凝器251下方并与第三冷凝器251连通。这样,通过真空泵253能将蒸发室220中蒸发的气体(经过第二冷凝器230)抽取至第三冷凝器251中进一步冷凝,并将第三冷凝器251中未冷凝的气体抽走;经第三冷凝器251冷凝后的液体则进入真空缓冲罐252中。
应当理解,真空泵253可将蒸发室220、第二冷凝器230及第三冷凝器251均抽成真空状态。通过抽真空装置250抽取蒸发室220中蒸发的气体,能使浓缩器200内处于负压环境,使提取液在负压环境下更快速地达到浓缩要求。另外,通过设置第三冷凝器251和真空缓冲罐252,对第二冷凝器230中未冷凝的气体进一步冷凝,从而使浓缩器200内达到稳定的真空度,而且能缓冲浓缩罐内外的压力差,防止倒灌。
根据一个实施例,提取设备300还可以设置萃取罐(图中未示出),通 过将萃取罐与浓缩器200连通,具体可与加热室210的出口连通,从而,在浓缩器200中的提取液浓缩完成后,通过对浓缩器200加压、或者对萃取罐减压,使浓缩器200与萃取罐之间产生压力差,从而便于将浓缩器200中的浓缩流体导入萃取罐内,并在萃取罐内对浓缩液进行萃取。
本说明书的描述中,除非另有明确的规定和限定,术语“连接”、“固定”等均应做广义理解。此外,术语“上”、“下”、“内”、“外”、“顶”、“底”等指示的方位或位置关系是基于附图所示的方位或位置关系,仅是为了便于描述本发明和简化描述,而不是指示或暗示所指的设备或单元必须具有特定的方向、以特定的方位构造和操作,因此,不能理解为对本发明的限制。
在本说明书的描述中,术语“一个实施例”、“一些实施例”、“具体实施例”等的描述意指结合该实施例或示例描述的具体特征、结构、材料或特点包含于本发明的至少一个实施例或示例中。在本说明书中,对上述术语的示意性表述不一定指的是相同的实施例或示例。而且,描述的具体特征、结构、材料或特点可以在任何的一个或多个实施例或示例中以合适的方式结合。
在此处所提供的说明书中,说明了大量具体细节。然而,能够理解,本发明的实施例可以在没有这些具体细节的情况下被实践。在一些实例中,并未详细示出公知的方法、结构和技术,以便不模糊对本说明书的理解。
Claims (17)
- 一种提取设备,包括:提取罐,包括罐体,所述罐体的壁部设有夹套;所述罐体适于装入物料与溶剂混合后的料液,并适于导入蒸汽对料液加热,以使料液加热到提取温度;所述罐体还适于导入空压气体对料液进行搅动;所述夹套适于在料液加热到提取温度后通入循环热水,以使料液维持在提取温度;以及第一冷凝器,与所述罐体连通,适于对空压气体排放时夹带的溶剂蒸汽进行冷凝,以便回收溶剂。
- 如权利要求1所述的提取设备,其中:所述罐体的顶部和底部分别设有第一导气管和第二导气管,以便向罐体内导入蒸汽和/或空压气体。
- 如权利要求1所述的提取设备,其中,还包括:集液器,分别与所述第一冷凝器和罐体连通;溶剂蒸汽在第一冷凝器内冷凝后流入所述集液器,并由集液器回流至所述罐体内。
- 如权利要求3所述的提取设备,其中,还包括:水箱,与所述集液器连通;流入所述集液器的空压气体,适于流经所述水箱水洗后排出。
- 如权利要求1所述的提取设备,其中:所述罐体的顶部设有排气口;所述排气口与所述第一冷凝器之间连接有排气管,所述排气管上连接有进水管;所述排气管靠近所述排气口的一端设有滤网装置。
- 如权利要求1所述的提取设备,其中,所述提取罐还包括:筛板,可拆卸安装于所述罐体内,所述筛板上适于放置植物香料;所述罐体底部适于导入蒸气,以便对所述植物香料进行蒸馏形成蒸馏气,蒸馏气适于通过所述第一冷凝器冷凝形成蒸馏液。
- 如权利要求6所述的提取设备,其中,还包括:油水分离器,与所述第一冷凝器连通,并适于对所述蒸馏液进行油水分离,以便提取香油。
- 如权利要求1所述的提取设备,其中,所述夹套上设有进水口和出水口,所述提取设备还包括:水循环温度控制机,通过热水管分别与所述夹套的进水口和出水口连通,以便向所述夹套内通入循环热水。
- 如权利要求2所述的提取设备,其中,还包括:蒸汽加热器,通过蒸汽管分别与所述第一导气管和第二导气管连通,以便向所述罐体内导入蒸汽。
- 如权利要求2所述的提取设备,其中,还包括:空气储罐,分别与所述第一导气管和第二导气管连通,以便向所述罐体内通入空压气体;以及空压机,与所述空气储罐连接,所述空压机适于压缩气体,以便形成空压气体通入所述空气储罐中。
- 如权利要求1所述的提取设备,其中,还包括:储液罐,适于储存提取液;过滤器,分别与所述罐体和储液罐连接,以便提取液从所述罐体流经所述过滤器过滤后进入所述储液罐。
- 如权利要求1所述的提取设备,其中,还包括:浓缩器,适于对所述提取液进行浓缩,所述浓缩器为单效浓缩器或多效浓缩器。
- 如权利要求12所述的提取设备,其中,所述浓缩器包括:加热室,适于导入待浓缩的提取液并适于通入蒸汽对提取液进行加热;蒸发室,与加热室通过循环管连通,以便提取液经加热室加热后流入所述蒸发室,并在蒸发室分离为二次蒸汽和提取液,且分离后的提取液可通过所述循环管回流至加热室;第二冷凝器,与所述蒸发室连通,以便蒸发室内的二次蒸汽进入第二冷凝器冷凝;以及收液罐,位于所述第二冷凝器下方并与所述第二冷凝器通过导管连接,以便经第二冷凝器冷凝后的液体通过所述导管导入收液罐。
- 如权利要求13所述的提取设备,其中:所述收液罐包括上下两层,且上下两层通过导液管连通。
- 如权利要求13所述的提取设备,其中,还包括:抽真空装置,与所述第二冷凝器连接,以便抽取由所述蒸发室流入第二冷凝器中的气体。
- 如权利要求15所述的提取设备,其中,所述抽真空装置包括:真空泵;第三冷凝器,分别通过抽真空管与所述第二冷凝器和真空泵连接;以及真空缓冲罐,位于所述第三冷凝器下方并与所述第三冷凝器连通;其中,所述真空泵适于将所述蒸发室、第二冷凝器及第三冷凝器抽成真空;经第三冷凝器冷凝后的液体进入所述真空缓冲罐。
- 如权利要求12所述的提取设备,其中,还包括:萃取罐,与所述浓缩器连通。
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| CN113057246B (zh) * | 2021-03-26 | 2021-12-07 | 广安万豪生物技术有限公司 | 一种从富硒食用菌中提取硒蛋白的方法 |
| CN113908584B (zh) * | 2021-10-11 | 2025-09-26 | 江中药业股份有限公司 | 一种主动增压提取装置和中药制剂的生产系统 |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1116922A (zh) * | 1995-07-13 | 1996-02-21 | 王金志 | 中药多功能渗漉提取装置 |
| CN2776512Y (zh) * | 2005-03-14 | 2006-05-03 | 邱晔 | 一种植物提取分离罐 |
| CN201267727Y (zh) * | 2008-05-21 | 2009-07-08 | 邓昌沪 | 喷射对流强化溶出提取罐 |
| CN101508710A (zh) * | 2009-03-18 | 2009-08-19 | 天台县满园春农林开发有限公司 | 无患子皂苷动态逆流提取设备及其生产工艺 |
| CN103505902A (zh) * | 2012-06-27 | 2014-01-15 | 永州中农银杏开发有限责任公司 | 多管型大容量微波萃取机及其微波萃取方法 |
| US20170043276A1 (en) * | 2015-03-18 | 2017-02-16 | Nicholas Tennant | Extraction apparatus and method |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2035633U (zh) * | 1988-09-11 | 1989-04-12 | 黄寿干 | 球形旋转提取罐 |
| CN1256163C (zh) * | 2004-08-16 | 2006-05-17 | 邱云彪 | 中药热回流提取、浓缩机组 |
| CN205683639U (zh) * | 2016-06-08 | 2016-11-16 | 陕西森弗天然制品有限公司 | 热回流提取浓缩机 |
| CN205850302U (zh) * | 2016-08-08 | 2017-01-04 | 赵剑芳 | 具有在线抑沫功能的多功能中药提取罐 |
-
2019
- 2019-04-26 CN CN201910346059.9A patent/CN110124349A/zh active Pending
- 2019-05-16 WO PCT/CN2019/087195 patent/WO2020215407A1/zh not_active Ceased
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1116922A (zh) * | 1995-07-13 | 1996-02-21 | 王金志 | 中药多功能渗漉提取装置 |
| CN2776512Y (zh) * | 2005-03-14 | 2006-05-03 | 邱晔 | 一种植物提取分离罐 |
| CN201267727Y (zh) * | 2008-05-21 | 2009-07-08 | 邓昌沪 | 喷射对流强化溶出提取罐 |
| CN101508710A (zh) * | 2009-03-18 | 2009-08-19 | 天台县满园春农林开发有限公司 | 无患子皂苷动态逆流提取设备及其生产工艺 |
| CN103505902A (zh) * | 2012-06-27 | 2014-01-15 | 永州中农银杏开发有限责任公司 | 多管型大容量微波萃取机及其微波萃取方法 |
| US20170043276A1 (en) * | 2015-03-18 | 2017-02-16 | Nicholas Tennant | Extraction apparatus and method |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112494984A (zh) * | 2020-12-09 | 2021-03-16 | 安庆医药高等专科学校 | 一种连续性中药动态提取分离生产工艺 |
| CN112494984B (zh) * | 2020-12-09 | 2022-04-08 | 安庆医药高等专科学校 | 一种连续性中药动态提取分离生产工艺 |
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