WO2012103651A1 - Production d'un sel cristallisé de nickel à partir de plantes hyperaccumulatrices - Google Patents

Production d'un sel cristallisé de nickel à partir de plantes hyperaccumulatrices Download PDF

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Publication number
WO2012103651A1
WO2012103651A1 PCT/CA2012/050059 CA2012050059W WO2012103651A1 WO 2012103651 A1 WO2012103651 A1 WO 2012103651A1 CA 2012050059 W CA2012050059 W CA 2012050059W WO 2012103651 A1 WO2012103651 A1 WO 2012103651A1
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WO
WIPO (PCT)
Prior art keywords
nickel
salt
solution
crystallized
ash
Prior art date
Application number
PCT/CA2012/050059
Other languages
English (en)
French (fr)
Inventor
Guy Mercier
Romain Barbaroux
Édouard PLASARI
Jean-François BLAIS
Marie-Odile Simonnot
Jean-Louis Morel
Original Assignee
Institut National De La Recherche Scientifique
Université De Lorraine
Institut National De La Recherche Agronomique
Centre National De La Recherche Scientifique
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to CA2,731,457 priority Critical
Priority to CA2731457A priority patent/CA2731457A1/fr
Application filed by Institut National De La Recherche Scientifique, Université De Lorraine, Institut National De La Recherche Agronomique, Centre National De La Recherche Scientifique filed Critical Institut National De La Recherche Scientifique
Publication of WO2012103651A1 publication Critical patent/WO2012103651A1/fr

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Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00Compounds of nickel
    • C01G53/10Sulfates
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01FCOMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F5/00Compounds of magnesium
    • C01F5/26Magnesium halides
    • C01F5/28Fluorides
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00Compounds of nickel
    • C01G53/08Halides
    • C01G53/09Chlorides
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00Obtaining nickel or cobalt
    • C22B23/04Obtaining nickel or cobalt by wet processes
    • C22B23/0407Leaching processes
    • C22B23/0415Leaching processes with acids or salt solutions except ammonium salts solutions
    • C22B23/043Sulfurated acids or salts thereof
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B7/00Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
    • C22B7/006Wet processes
    • C22B7/007Wet processes by acid leaching
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74Iron group metals
    • B01J23/755Nickel
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/02Sulfur, selenium or tellurium; Compounds thereof
    • B01J27/053Sulfates
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02Impregnation, coating or precipitation
    • B01J37/03Precipitation; Co-precipitation
    • B01J37/031Precipitation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/06Washing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08Heat treatment
    • B01J37/082Decomposition and pyrolysis
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/70Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling
PCT/CA2012/050059 2011-02-04 2012-02-03 Production d'un sel cristallisé de nickel à partir de plantes hyperaccumulatrices WO2012103651A1 (fr)

Priority Applications (2)

Application Number Priority Date Filing Date Title
CA2,731,457 2011-02-04
CA2731457A CA2731457A1 (fr) 2011-02-04 2011-02-04 Procede de production d'un sel de sulfate double de nickel et d'ammonium a partir de plantes hyperaccumulatrices

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP12741883.8A EP2670707A4 (fr) 2011-02-04 2012-02-03 Production d'un sel cristallisé de nickel à partir de plantes hyperaccumulatrices

Publications (1)

Publication Number Publication Date
WO2012103651A1 true WO2012103651A1 (fr) 2012-08-09

Family

ID=46599580

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/CA2012/050059 WO2012103651A1 (fr) 2011-02-04 2012-02-03 Production d'un sel cristallisé de nickel à partir de plantes hyperaccumulatrices

Country Status (3)

Country Link
EP (1) EP2670707A4 (ja)
CA (1) CA2731457A1 (ja)
WO (1) WO2012103651A1 (ja)

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR843270A (fr) * 1937-09-11 1939-06-28 Seri Holding Sa Procédé d'obtention de magnésium très pur à partir de minerais de magnésium
GB567260A (en) * 1943-05-29 1945-02-05 Ocean Salts Products Ltd Improvements relating to the production of magnesium fluoride
WO1998059080A1 (en) * 1997-06-20 1998-12-30 University Of Maryland College Park Method for phytomining of nickel, cobalt and other metals from soil
US7268273B2 (en) * 1995-06-06 2007-09-11 The University Of Maryland Recovering metals from soil
WO2009038379A2 (en) * 2007-09-21 2009-03-26 Research Institute Of Industrial Science & Technology Method of manufacturing fe and ni containing material and cobalt containing material using recycling residue of spent catalyst and method of manufacturing raw material for stainless using the fe and ni containing material and method of manufacturing fe-ni alloy
RU2356836C1 (ru) * 2007-09-11 2009-05-27 Открытое Акционерное Общество "Российский научно-исследовательский и проектный институт титана и магния" (ОАО "РИТМ") Способ комплексной переработки серпентинита

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2520958A (en) * 1947-01-14 1950-09-05 Poole Henry Gordon Nickel recovery
GB1604768A (en) * 1978-05-31 1981-12-16 Johnson Mattheys & Co Ltd Recovery of platinum group metal values
DE10252951A1 (de) * 2002-11-14 2004-05-27 Kali-Umwelttechnik Gmbh Verfahren zur Rückgewinnung von Nickelsalzen
JP4216657B2 (ja) * 2003-06-26 2009-01-28 新日本製鐵株式会社 ニッケル含有廃液スラッジからの硫酸ニッケルの回収方法
EP1979063A4 (en) * 2006-01-17 2010-03-10 Yissum Res Dev Co Method of removal of heavy metal ions from water
WO2011064462A1 (fr) * 2009-11-26 2011-06-03 Centre National De La Recherche Scientifique Utilisation de plantes accumulatrices de metaux pour la preparation de catalyseurs utilisables dans des reactions chimiques
CN103946401A (zh) * 2011-11-22 2014-07-23 住友金属矿山株式会社 高纯度硫酸镍的制造方法

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR843270A (fr) * 1937-09-11 1939-06-28 Seri Holding Sa Procédé d'obtention de magnésium très pur à partir de minerais de magnésium
GB567260A (en) * 1943-05-29 1945-02-05 Ocean Salts Products Ltd Improvements relating to the production of magnesium fluoride
US7268273B2 (en) * 1995-06-06 2007-09-11 The University Of Maryland Recovering metals from soil
WO1998059080A1 (en) * 1997-06-20 1998-12-30 University Of Maryland College Park Method for phytomining of nickel, cobalt and other metals from soil
RU2356836C1 (ru) * 2007-09-11 2009-05-27 Открытое Акционерное Общество "Российский научно-исследовательский и проектный институт титана и магния" (ОАО "РИТМ") Способ комплексной переработки серпентинита
WO2009038379A2 (en) * 2007-09-21 2009-03-26 Research Institute Of Industrial Science & Technology Method of manufacturing fe and ni containing material and cobalt containing material using recycling residue of spent catalyst and method of manufacturing raw material for stainless using the fe and ni containing material and method of manufacturing fe-ni alloy

Non-Patent Citations (5)

* Cited by examiner, † Cited by third party
Title
BARBAROUX ET AL.: "Chemical leaching of nickel from the seeds of the metal hyperaccumulator plant.", ALYSSUM MURALE. HYDROMETALLURGY, vol. 100, no. 1-2, 2009, pages 10 - 14, XP026769628 *
MULLIN ET AL.: "Nickel ammonium sulfate crystal growth rates in aqueous solution", J. CHEM.ENG. DATA, vol. 18, no. 4, 1973, pages 353 - 355, XP055124044 *
PHILLIPS ET AL.: "Growth of nickel sulfate in a laboratoiy-scale fluidized-bed crystallizer.", AICHE JOURNAL., vol. 20, no. 4, July 1974 (1974-07-01), pages 678 - 687, XP055124031 *
ROBINSON ET AL.: "The nickel hyperaccumulator plant Alyssum bertolonii as a potential agent for phytoremediation and phytomining of nickel", JOURNAL OF GEOCHEMICAL EXPLORATION, vol. 59, no. 2, June 1997 (1997-06-01), pages 75 - 86, XP055124028 *
See also references of EP2670707A4 *

Also Published As

Publication number Publication date
CA2731457A1 (fr) 2012-08-04
EP2670707A1 (fr) 2013-12-11
EP2670707A4 (fr) 2015-12-23

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