WO2012065467A1 - Process integration system for led chip and processing method thereof - Google Patents

Process integration system for led chip and processing method thereof Download PDF

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Publication number
WO2012065467A1
WO2012065467A1 PCT/CN2011/078773 CN2011078773W WO2012065467A1 WO 2012065467 A1 WO2012065467 A1 WO 2012065467A1 CN 2011078773 W CN2011078773 W CN 2011078773W WO 2012065467 A1 WO2012065467 A1 WO 2012065467A1
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WO
WIPO (PCT)
Prior art keywords
layer deposition
epitaxial layer
chamber
led substrate
temperature
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PCT/CN2011/078773
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French (fr)
Chinese (zh)
Inventor
奚明
Original Assignee
理想能源设备(上海)有限公司
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Priority to KR1020137011679A priority Critical patent/KR20130105671A/en
Publication of WO2012065467A1 publication Critical patent/WO2012065467A1/en

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Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/67Apparatus specially adapted for handling semiconductor or electric solid state devices during manufacture or treatment thereof; Apparatus specially adapted for handling wafers during manufacture or treatment of semiconductor or electric solid state devices or components ; Apparatus not specifically provided for elsewhere
    • H01L21/67005Apparatus not specifically provided for elsewhere
    • H01L21/67011Apparatus for manufacture or treatment
    • H01L21/67155Apparatus for manufacturing or treating in a plurality of work-stations
    • H01L21/67161Apparatus for manufacturing or treating in a plurality of work-stations characterized by the layout of the process chambers
    • H01L21/67173Apparatus for manufacturing or treating in a plurality of work-stations characterized by the layout of the process chambers in-line arrangement
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L33/00Semiconductor devices with at least one potential-jump barrier or surface barrier specially adapted for light emission; Processes or apparatus specially adapted for the manufacture or treatment thereof or of parts thereof; Details thereof
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/67Apparatus specially adapted for handling semiconductor or electric solid state devices during manufacture or treatment thereof; Apparatus specially adapted for handling wafers during manufacture or treatment of semiconductor or electric solid state devices or components ; Apparatus not specifically provided for elsewhere
    • H01L21/67005Apparatus not specifically provided for elsewhere
    • H01L21/67011Apparatus for manufacture or treatment
    • H01L21/67155Apparatus for manufacturing or treating in a plurality of work-stations
    • H01L21/67161Apparatus for manufacturing or treating in a plurality of work-stations characterized by the layout of the process chambers
    • H01L21/67167Apparatus for manufacturing or treating in a plurality of work-stations characterized by the layout of the process chambers surrounding a central transfer chamber
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/67Apparatus specially adapted for handling semiconductor or electric solid state devices during manufacture or treatment thereof; Apparatus specially adapted for handling wafers during manufacture or treatment of semiconductor or electric solid state devices or components ; Apparatus not specifically provided for elsewhere
    • H01L21/67005Apparatus not specifically provided for elsewhere
    • H01L21/67011Apparatus for manufacture or treatment
    • H01L21/67155Apparatus for manufacturing or treating in a plurality of work-stations
    • H01L21/67207Apparatus for manufacturing or treating in a plurality of work-stations comprising a chamber adapted to a particular process

Definitions

  • the present invention relates to the field of semiconductor technology, and in particular, to an LED chip process integration system and a processing method thereof.
  • the LED chip includes: an LED substrate 10, the material of the LED substrate 10 is sapphire; an N-type GaN layer 11 on which the N-type GaN layer 11 is located; a multi-quantum well active layer 12, located at On the N-type GaN layer 11; a P-type GaN layer 13 on the multiple quantum well active layer 12; a conductive layer 14 on the P-type GaN layer 13; and a P-type GaN electrode layer 15, located in the On the conductive layer 14; an N-type GaN electrode layer 16 on the N-type GaN layer 11; a protective layer 17 between the N-type GaN electrode layer 16 and the P-type GaN electrode layer 15, the protective layer 17 covers the conductive layer 14.
  • the N-type GaN layer 11, the multiple quantum well active layer 12, and the P-type GaN layer 13 are referred to as epitaxial layers.
  • the epitaxial layer is typically fabricated using an epitaxial layer deposition apparatus.
  • the LED substrate is first placed from the clean room on the loading and unloading device of the epitaxial layer deposition apparatus; and then a vacuuming step is performed to remove the LED substrate from the loading and unloading device.
  • an epitaxial layer deposition chamber disposed in the epitaxial layer deposition apparatus; and then performing a heating step by using the epitaxial layer deposition chamber, that is, the LED substrate is raised from a room temperature (10 to 30 degrees Celsius) to a high temperature, and the high temperature range is 800 ⁇ 1300 degrees Celsius; then using the epitaxial layer deposition chamber for epitaxial layer deposition
  • the epitaxial layer deposition step includes depositing the N-type GaN layer 11, the multiple quantum well active layer 12, and the P-type GaN layer 13 shown in FIG.
  • the LED substrate of the epitaxial layer is subjected to a cooling step of lowering the LED substrate from the high temperature to room temperature; then performing a vacuuming operation to place the LED substrate on the loading and unloading device; and finally moving the LED substrate to The clean room is thereby completed to deposit epitaxial layers of the LED substrate.
  • the method includes: first performing a vacuuming step of placing the LED substrate from a clean room in a conductive layer deposition chamber of a conductive layer deposition apparatus; and then performing heating by using the conductive layer deposition chamber, even if the LED substrate is Raising the temperature to 200-500 degrees Celsius at room temperature; then performing a conductive layer deposition step using the conductive layer deposition chamber; then performing a cooling step using the conductive layer deposition chamber, cooling the LED substrate to room temperature; and then pumping again
  • the LED substrate is placed on the loading and unloading device by vacuum action; finally, the LED substrate is moved to a clean room to complete deposition of a conductive layer of the LED substrate.
  • the deposition time of the epitaxial layer deposition chamber is long, usually 3-6 hours, which affects the production efficiency of the epitaxial layer deposition equipment, thereby affecting the production efficiency of the LED chip, thereby making the existing LED
  • the output of the chip is not high, which also causes the existing LED chips to be more expensive;
  • the steps of heating and cooling the LED substrate are respectively required, and the existing heating step and cooling step are performed by using the epitaxial layer deposition chamber. This occupies the time for depositing the epitaxial layer in the epitaxial layer deposition chamber, further reducing the production efficiency of the existing epitaxial layer deposition apparatus, affecting the output of the LED chip, and increasing the cost of the LED chip;
  • the heating step and the temperature decreasing step are performed by using the epitaxial layer deposition chamber, and the repeated temperature rise and temperature reduction shortens the service life of the epitaxial layer deposition chamber, and the epitaxial layer deposition chamber needs to be frequently maintained. , reducing the utilization time of the epitaxial layer deposition equipment (uptime), and failing to meet actual needs;
  • the epitaxial layer deposition apparatus and the conductive layer deposition apparatus are independently disposed such that the LED substrate needs to perform at least four vacuuming operations before entering and leaving the epitaxial layer deposition apparatus and the conductive layer deposition apparatus, thereby reducing the production of the LED substrate.
  • An object of the present invention is to provide an LED chip process integration system and a processing method thereof, which solve the problems of low production efficiency and high production cost of an epitaxial layer deposition process of an LED chip existing in the prior art.
  • the present invention provides an LED chip process integration system, comprising: a loading and unloading device for loading or unloading a processed or processed LED substrate; and a vacuum transmission device for providing a vacuum transmission environment for transmission The LED substrate to be processed or processed;
  • At least one epitaxial layer deposition chamber is disposed at a periphery of the vacuum transmission device, and the epitaxial layer deposition chamber is configured to perform epitaxial layer deposition on the LED substrate to be processed;
  • the pre-processing chamber is located at a periphery of the vacuum transmission device for heating, cleaning or cooling the LED substrate to be processed or cooling the processed LED substrate.
  • the pre-processing chamber is provided with a heating stage for heating the LED substrate to raise the LED substrate from a first temperature to a second temperature.
  • the temperature of the first temperature ranges from 10 to 30 degrees Celsius
  • the temperature of the second temperature ranges from 700 to 1300 degrees Celsius.
  • the pre-treatment chamber is provided with at least one air inlet and at least one air outlet, and the air inlet is configured to pass one or more of a reducing gas or a protective gas, the reducing property A gas or protective gas is used to clean the LED substrate.
  • the reducing gas is hydrogen or ammonia
  • the protective gas is one or more of an inert gas or nitrogen.
  • the pre-processing chamber is provided with a temperature control device, and the temperature control device is configured to control the heating station to heat the LED substrate from the first temperature to the first in 5 to 15 minutes. Two temperatures, and maintaining the LED substrate at the second temperature for 1 to 25 minutes;
  • the air inlet is configured to pass the reducing property when the LED substrate maintains the second temperature One or more of a gas or a protective gas.
  • the deposition time of the epitaxial layer deposition chamber ranges from 0.5 to 6.5 hours.
  • the ratio of the number of the pre-treatment chamber to the number of epitaxial layer deposition chambers is
  • the ratio of the number of the pre-treatment chambers to the epitaxial layer deposition chamber is 1/3.
  • the method further includes: a conductive layer deposition chamber located at a periphery of the vacuum transfer device and the epitaxial layer deposition chamber, the conductive layer deposition chamber for depositing a conductive layer.
  • the vacuum transfer device is linear in shape, and the loading and unloading device, the pretreatment chamber, the epitaxial layer deposition chamber, and the conductive layer deposition chamber are linearly arranged around the periphery of the vacuum transfer device.
  • the vacuum transmission device has a polygonal or circular shape, and the loading and unloading device, the pretreatment chamber, the epitaxial layer deposition chamber, and the conductive layer deposition chamber are located at a periphery of the vacuum transmission device.
  • the pretreatment chamber is connected to the vacuum transmission device, the conductive layer deposition chamber is linearly connected to the pretreatment chamber, and the conductive layer deposition chamber is located in the pretreatment chamber Aside from the side of the vacuum transmission device.
  • the conductive layer is a metal layer or a transparent conductive layer
  • the metal layer is one or more of a gold-nickel alloy, a gold-titanium alloy or another metal
  • the transparent conductive layer is in ITO, ⁇ One or more.
  • the epitaxial layer deposition chamber and the conductive layer deposition chamber are respectively provided with independent exhaust systems.
  • the deposition time of the conductive layer deposition chamber ranges from 10 to 40 minutes.
  • the ratio of the number of epitaxial layer deposition chambers to the number of conductive layer deposition chambers ranges from 2/1 to 12/1.
  • the ratio of the number of epitaxial layer deposition chambers to the number of conductive layer deposition chambers ranges from 4/1 to 12/1.
  • the ratio of the number of epitaxial layer deposition chambers to the number of conductive layer deposition chambers ranges from 8/1 to 12/1.
  • the epitaxial layer deposition chamber is configured to deposit a ⁇ -type GaN layer, a multiple quantum well active layer, and a P-type GaN layer, wherein the N-type GaN layer, the multiple quantum well active layer, and the P-type GaN layer are formed The epitaxial layer.
  • the number of the epitaxial layer deposition chambers is at least three, including: N-type GaN layer sinking An accumulation chamber, a multiple quantum well active layer deposition chamber, and a P-type GaN layer deposition chamber for depositing an N-type GaN layer, the multiple quantum well active layer deposition chamber And a P-type GaN layer deposition chamber for depositing a P-type GaN layer, wherein the N-type GaN layer, the multiple quantum well active layer, and the P-type GaN layer constitute the epitaxial layer .
  • the present invention further provides a processing method of an LED chip process integration system, comprising: placing an LED substrate to be processed on a loading and unloading device;
  • Epitaxial layer deposition is performed in the epitaxial layer deposition chamber.
  • the pre-processing comprises heating, cooling or cleaning the LED substrate.
  • the method further includes:
  • the pretreatment chamber performs a first cooling process on the LED substrate
  • the first cooled LED substrate is transferred to a conductive layer deposition chamber for depositing a conductive layer.
  • the method further includes: transmitting the LED substrate deposited with the conductive layer to the pretreatment chamber for performing a second cooling process.
  • the preprocessing includes:
  • one or more of a reducing gas or a protective gas is introduced into the pretreatment chamber.
  • the reducing gas is hydrogen or ammonia
  • the protective gas is one or more of an inert gas or nitrogen.
  • the method further includes transmitting the LED substrate deposited with the epitaxial layer to the pretreatment chamber for performing a cooling process, wherein the cooling process is to reduce the temperature of the LED substrate from a second temperature to a first temperature,
  • the temperature of the first temperature ranges from 10 to 30 degrees Celsius, and the temperature range of the second temperature is 700 ⁇ 1300 degrees Celsius.
  • the first cooling process is to reduce the temperature of the LED substrate from a second temperature to a third temperature, and the second temperature has a temperature range of 700 to 1300 degrees Celsius, and the temperature range of the third temperature It is 100 ⁇ 400 degrees Celsius.
  • the epitaxial layer is deposited for a time ranging from 0.5 to 6.5 hours.
  • the method further includes:
  • Conductive layer deposition is performed on the LED substrate using the conductive layer deposition chamber.
  • the second cooling process is to cool the LED substrate from 100-400 degrees Celsius to
  • the epitaxial layer comprises an N-type GaN layer, a multiple quantum well active layer, and a P-type GaN layer.
  • the epitaxial layer deposits an N-type GaN layer, a multiple quantum well active layer, and a P-type GaN layer by using the epitaxial layer deposition chamber or deposits N-type GaN by using the three epitaxial layer deposition chambers respectively. Layer, multiple quantum well active layer and P-type GaN layer.
  • the epitaxial layer deposition chamber deposits the N-type GaN layer in a temperature range of 1000-1300 degrees Celsius, and the time range is 100-200 minutes, and the formed N-type GaN layer has a thickness ranging from 1 to 3 Micron
  • the P-type GaN layer is formed to have a temperature range of 850 to 950 degrees Celsius and a time range of 20 to 80 minutes, and the P-type GaN layer is formed to have a thickness ranging from 0.2 to 0.6 ⁇ m.
  • the present invention has the following advantages:
  • the LED chip process integration system comprises a pre-processing chamber outside the deposition chamber of the epitaxial layer, the pre-processing chamber is used for pre-treating the LED substrate, so that the epitaxial layer deposition chamber is only used for Epitaxial layer deposition increases the time for depositing the epitaxial layer in the epitaxial layer deposition chamber, and also improves the production efficiency of the epitaxial layer deposition, correspondingly increasing the production efficiency of the LED chip and the yield of the LED chip;
  • the layer deposition chamber is only used for epitaxial layer deposition, which avoids the influence of its repeated heating and cooling on its service life, thereby prolonging the service life of the epitaxial layer deposition chamber and reducing the deposition chamber of the epitaxial layer.
  • the utilization rate of the layer deposition chamber satisfies the actual needs; since the transmission of the LED substrate between the epitaxial layer deposition chamber and the pretreatment chamber is performed by using a vacuum transmission environment, the LED substrate is protected from external contaminants. Pollution;
  • the pre-treatment chamber can also be used for cleaning the surface of the LED substrate to remove contaminants such as particles, organic matter, inorganic substances and water vapor on the surface of the LED substrate, thereby improving subsequent deposition.
  • the quality of the epitaxial layer, and the adhesion between the epitaxial layer and the LED substrate is improved, and the reliability of the LED substrate is improved;
  • the cleaning step of the pretreatment chamber has a time range of 10 to 40 minutes, and the deposition time of the epitaxial layer deposition chamber ranges from 0.5 to 6.5 hours, and the pretreatment chamber and the epitaxy are disposed.
  • the ratio of the number of layer deposition chambers ranges from 1/2 to 1/5, so that the pretreatment chamber cooperates with the deposition chamber of the epitaxial layer to improve the processing speed of the LED substrate and improve the production efficiency and yield of the LED chip. ;
  • the ratio of the number of the pre-treatment chamber to the epitaxial layer deposition chamber is 1/3, which comprehensively considers the cost of the epitaxial layer deposition chamber and improves the production efficiency of the epitaxial layer deposition chamber, so that More reasonable cost to obtain higher production efficiency;
  • the LED chip process integration system further comprises a conductive layer deposition chamber, such that the deposited LED substrate of the epitaxial layer does not need to be subjected to repeated vacuuming steps, and enters the conductive layer deposition chamber for conducting conductive layer deposition in a vacuum environment.
  • the production efficiency of the conductive layer deposition is improved, the production efficiency and the yield of the LED chip are further improved, and on the other hand, the LED substrate is prevented from being exposed to the clean room, and the LED substrate is prevented from being contaminated by the clean room.
  • the adhesion between the conductive layer and the epitaxial layer is improved, and the yield and reliability of the LED chip are improved;
  • the shape of the vacuum transmission device is linear, and the loading and unloading device, the pretreatment chamber, the epitaxial layer deposition chamber, and the conductive layer deposition chamber are linearly arranged on the periphery of the vacuum transmission device, thereby
  • the integration of the LED chip process integration system is improved, the space occupied by the clean room is less, the cost of the clean room is reduced, and the manufacturing cost of the LED chip is reduced;
  • the vacuum transmission device has a polygonal shape
  • the pretreatment chamber is located on a side of the vacuum transmission device opposite to the epitaxial layer deposition chamber
  • the conductive layer deposition chamber is located in the pretreatment The device is away from the side of the vacuum transmission device and the epitaxial deposition chamber, so that the integration of the LED chip process integration system is increased, the space occupied by the clean room is less, the cost of the clean room is reduced, and the LED chip is reduced. cost;
  • the epitaxial layer deposition chamber and the conductive layer deposition chamber are respectively provided with independent exhaust systems, thereby improving the processing speed of the epitaxial layer deposition chamber and the conductive layer deposition chamber, and improving the processing speed. LED substrate production efficiency and output;
  • the ratio of the number of epitaxial layer deposition chambers to the number of conductive layer deposition chambers ranges from 8/1 to 12/1 such that the epitaxial layer deposition chamber and the conductive layer deposition chamber The number is matched such that the utilization of the epitaxial layer deposition chamber and the conductive layer deposition chamber is improved, and the epitaxial layer deposition chamber or the conductive layer deposition chamber is prevented from being idle or overburdened.
  • 1 is a schematic structural view of a conventional LED chip device
  • FIG. 2 is a schematic structural view of a LED chip process integration system according to a first embodiment of the present invention
  • FIG. 3 is a schematic flow chart of a processing method of the LED chip process integration system according to the first embodiment of the present invention
  • FIG. 4 is a schematic structural view of a LED chip process integration system according to a second embodiment of the present invention
  • FIG. 5 is a schematic structural view of a LED chip process integration system according to a third embodiment of the present invention
  • FIG. 6 is a process integration of an LED chip according to a fourth embodiment of the present invention
  • FIG. 7 is a schematic structural diagram of an LED chip process integration system according to a fifth embodiment of the present invention
  • FIG. 8 is a schematic structural view of a LED chip process integration system according to a sixth embodiment of the present invention.
  • the present invention provides an LED chip process integration system, including:
  • Loading and unloading device for loading or unloading the LED substrate to be processed or processed; vacuum conveying device for providing a vacuum transmission environment for transmitting the LED substrate to be processed or processed;
  • At least one epitaxial layer deposition chamber is disposed at a periphery of the vacuum transmission device, and the epitaxial layer deposition chamber is configured to perform epitaxial layer deposition on the LED substrate to be processed;
  • FIG. 2 is a schematic structural diagram of an LED chip process integration system according to a first embodiment of the present invention.
  • the LED chip process integration system 100 includes:
  • Loading and unloading device 101 for loading or unloading the LED substrate to be processed or processed; vacuum transmitting device 104 for providing a vacuum transmission environment for transmitting the LED substrate to be processed or processed;
  • At least one epitaxial layer deposition chamber 102 is located at a periphery of the vacuum transfer device 104, and the epitaxial layer deposition chamber 102 is configured to perform epitaxial layer deposition on the LED substrate to be processed;
  • At least one pretreatment chamber 103 is configured to pretreat the LED substrate to be processed or processed.
  • FIG. 3 is a schematic flowchart of a processing method of the LED chip process integration system according to the first embodiment of the present invention.
  • the processing method includes:
  • Step S1 placing the LED substrate to be processed on the loading and unloading device
  • Step S2 the LED substrate to be processed is placed in the pre-processing chamber by using a vacuum transfer device; Step S3, pre-processing the LED substrate to be processed by using the pre-processing chamber; Step S4, pre-processing The latter LED substrate is placed in an epitaxial layer deposition chamber;
  • Step S5 performing epitaxial layer deposition in the epitaxial layer deposition chamber.
  • the existing epitaxial layer deposition apparatus requires a step of pretreating the LED substrate to be processed in the epitaxial layer deposition chamber before performing the epitaxial layer deposition process, the pretreatment including heating, cooling or cleaning treatment, etc.
  • heating the LED substrate to be processed causes the LED substrate to be processed to reach a high temperature condition for performing epitaxial layer deposition from room temperature, the room temperature ranges from 10 to 30 degrees Celsius, and the high temperature ranges from 700 to 1300. Celsius;
  • the processed (ie, deposited epitaxial layer) LED substrate needs to be cooled to lower the temperature of the high temperature LED substrate to room temperature.
  • the existing epitaxial layer deposition chamber is expensive, and the pretreatment of the LED substrate to be processed is utilized.
  • One of the defects is that the equipment is costly and the production cost is large, because the epitaxial layer deposition chamber is occupied.
  • the yield of the epitaxial layer deposition chamber is reduced, which affects the production efficiency of the LED chip;
  • another drawback is that the deposition chamber is deposited by the epitaxial layer due to the limitation of the structure of the epitaxial layer deposition chamber. Heating rate and cooling The cooling rate of the treatment is slow.
  • the inventors propose to pre-treat the LED substrate by using a special chamber, that is, pretreating the LED substrate to be processed by using the pre-processing chamber 103 of the present invention, the pre-processing including the waiting for the The processed LED substrate is subjected to heating, cooling or cleaning.
  • the pretreatment chamber 103 of the present invention is disposed outside of the epitaxial layer deposition chamber 102, which is disposed independently of the epitaxial layer deposition chamber 102.
  • the pretreatment chamber 103 may be disposed at a circumference of the vacuum transmission device 104 or disposed at the vacuum transmission on the premise that the pretreatment chamber 103 is located outside the epitaxial layer deposition chamber 102. Within device 104.
  • the pre-treatment chamber 103 is disposed at a periphery of the vacuum transfer device 104.
  • the pretreatment chamber 103 of the present invention has a lower cost than the price of the epitaxial layer deposition chamber 102 because it does not need to have the function of epitaxial layer deposition.
  • the pretreatment chamber of the present invention The price of 103 is only 1/15 ⁇ 1/20 of the price of the epitaxial layer deposition chamber 102, so that the cost can be reduced, and the time for the epitaxial layer deposition chamber 102 to perform epitaxial layer deposition is increased, and the epitaxy is increased.
  • the throughput of the layer deposition chamber 102 increases the utilization of the epitaxial layer deposition chamber 102.
  • the pre-processing chamber 103 is provided with a heating station for heating the LED substrate to be processed, so that the LED substrate to be processed is from the first temperature. Raise to the second temperature.
  • the first temperature range is 10 to 30 degrees Celsius, and the second temperature should generally be equal to or close to the temperature at which the epitaxial layer deposition chamber 102 performs epitaxial layer deposition.
  • the second temperature range is 700 to 1300 degrees Celsius.
  • the pre-treatment chamber 103 is provided with at least one air inlet and at least one air outlet for introducing one or more of a reducing gas or a protective gas.
  • the reducing gas or protective gas is used to clean the LED substrate.
  • the organic matter on the LED substrate to be processed may be reduced to a gas, and the gas is discharged through the air outlet to remove the organic matter.
  • the reducing gas may be hydrogen, ammonia or a mixture of hydrogen and ammonia. Combined with gas.
  • the protective gas can remove particles on the LED substrate to be processed, that is, the particles on the LED substrate to be processed are blown away and discharged through the air outlet, and on the other hand, the reduction can be prevented.
  • the nature of the gas is lively and affects the safety of the equipment. In the case of high temperature, the water vapor and inorganic contaminants on the LED substrate to be treated are volatilized into a gas, and therefore, the water vapor and inorganic contaminants can also be removed.
  • the protective gas may be an inert gas, nitrogen or a mixed gas of an inert gas and nitrogen.
  • the inert gas may be one of helium, argon or helium or a mixture of two of helium, argon and helium or a mixture of helium, argon and helium.
  • the protective gas is preferably a lower priced nitrogen gas.
  • the air inlet may only pass a reducing gas or a protective gas.
  • the air inlet is provided with a mixed gas of the reducing gas and the protective gas.
  • the organic pollutants, inorganic pollutants, water vapor and the like on the LED substrate to be processed can be removed, but also the safety of the device is ensured.
  • the price of the reducing gas is high, and the reducing gas is diluted by the protective gas, and the production cost is lowered without affecting the removal of the organic pollutant.
  • the air inlet is supplied with a mixed gas of a reducing gas and a protective gas, for example, a mixed gas of hydrogen and a relatively low-priced nitrogen gas or a mixed gas of ammonia gas and a relatively low-priced nitrogen gas.
  • a mixed gas of a reducing gas and a protective gas for example, a mixed gas of hydrogen and a relatively low-priced nitrogen gas or a mixed gas of ammonia gas and a relatively low-priced nitrogen gas.
  • the pretreatment chamber 103 is provided with a temperature control device for controlling the heating station to heat the LED substrate to be processed.
  • the pre-processing chamber 103 can also be used to perform cleaning processing on the LED substrate to be processed while heating the LED substrate to be processed.
  • the pre-processing chamber 103 is for the to-be-processed
  • the pretreatment of the LED substrate includes:
  • the time required for heating the LED is in the range of 5 to 15 minutes, preferably 8 to 13 minutes, for example, 10 minutes; after the LED substrate to be processed reaches the second temperature, the temperature of the pretreatment chamber 103
  • the control device controls the heating station to insulate the LED substrate to be processed, that is, the LED substrate to be processed is kept at the temperature for a period of time, and the time range is 1 to 25 minutes, preferably 5 to 15 minutes.
  • the air inlet of the pre-treatment chamber 103 is introduced into one or more of the reducing gas or the protective gas (for example, a mixed gas of hydrogen and nitrogen or a mixed gas of ammonia and nitrogen).
  • the vent may also pass one or more of the reducing gas or the protective gas when the temperature of the LED substrate to be processed is the first temperature, so that Producing the effect of cleaning the LED substrate to be processed, but only one or more of the reducing gas or the protective gas is introduced when the LED substrate to be processed maintains the second temperature, saving The amount of gas used reduces production costs.
  • the pre-processing chamber 103 of the present invention firstly raises the LED substrate to be processed from 20 degrees Celsius to 950 to 1150 degrees Celsius, for example, 1050 degrees Celsius, for the required time. 5 to 15 minutes, for example, 10 minutes; then, the LED substrate to be treated is kept at the high temperature for 1 to 25 minutes, for example, 5 minutes or 15 minutes, and hydrogen and nitrogen are introduced while being kept warm.
  • the mixed gas (the volume ratio of hydrogen to nitrogen in the mixed gas may be 2% to 50%); and then transferred to the epitaxial layer deposition chamber 102 through the vacuum transfer device 104 to perform epitaxial layer deposition.
  • the deposition time of the epitaxial layer deposition chamber 102 is generally long, the time range is usually 0.5 to 6.5 hours, and the cleaning processing time of the pretreatment chamber 103 is usually in the range of 10 to 40 minutes. If the ratio of the number of epitaxial layer deposition chambers 102 to the pretreatment chambers 103 is set to 1/1, it may cause a portion of the LED substrate to occupy the epitaxial layer deposition chamber 102 for a long time, so that the pretreatment chamber passes through the pretreatment chamber. The LED substrate after the cleaning process has no corresponding epitaxial layer deposition chamber 102 for epitaxial layer deposition, and the maximum LED chip production efficiency cannot be obtained.
  • the inventors propose to provide a plurality of epitaxial layer deposition chambers 102, specifically the ratio of the number of the pre-treatment chambers 103 to the epitaxial layer deposition chambers 102 is less than 1/1, for example, the ratio may be in the range of 1/2 ⁇ 1/5.
  • the inventors have considered that increasing the number of epitaxial layer deposition chambers 102 can speed up the processing speed of the LED substrate to be processed, but since the epitaxial layer deposition chamber 102 is expensive, this also increases LED chip process integration.
  • the cost of the system 100 therefore, the inventors comprehensively consider the cost of the LED chip process integration system and the production efficiency of the conductive layer deposition process, preferably setting the ratio of the number of the pre-treatment chambers 103 to the number of epitaxial layer deposition chambers 102 It is 1/3. Since the number of the pre-processing chambers 103 is one in this embodiment, the number of corresponding epitaxial layer deposition chambers 102 is three. At the above ratio, the production efficiency of higher epitaxial layer deposition can be obtained at a reasonable cost.
  • the ratio of the number of pre-treatment chambers 103 to the epitaxial layer deposition chamber 102 may be other values, depending on the particular application.
  • the pre-processing chamber 103 pre-places the LED substrate
  • the method further includes cooling the processed LED substrate.
  • the cooling process is to cool the LED substrate on which the epitaxial layer is deposited from the second temperature to the first temperature.
  • the second temperature range is 700 to 1300 degrees Celsius
  • the first temperature range is 10 to 30 degrees Celsius.
  • the cooling treatment removes heat from the surface of the processed LED substrate by using a protective gas by introducing a protective gas into the epitaxial layer deposition chamber 102, compared to placing the LED substrate on the epitaxial layer.
  • the deposition of the layer deposition chamber 102 increases the time for the epitaxial layer deposition chamber 102 to perform epitaxial layer deposition, and improves the efficiency of the epitaxial layer deposition process; the LED substrate deposited in the epitaxial layer is placed in a clean room or vacuum The conveyor is cooled to increase the rate of cooling.
  • the vacuum transmission device 104 is linear in shape, and the loading and unloading device 101, the pretreatment chamber 103, and the epitaxial layer deposition chamber 102 are linearly arranged in the The periphery of the vacuum transfer device 104.
  • the vacuum transmission device 104 is a sealed cavity, and at least is provided with a vacuum pump, a robot arm and at least three sealing doors, and each sealing door corresponds to the loading and unloading device 101 and the pre-processing chamber 103, respectively.
  • An epitaxial layer deposition chamber 102 is used as a channel for the LED substrate to be transferred from the loading and unloading device 101, the pretreatment chamber 103, and the epitaxial layer deposition chamber 102 to the vacuum transmission device. Taking the LED substrate to be processed placed on the loading and unloading device 101 as an example, a sealing door corresponding to the loading and unloading device 101 is opened, and the robot arm takes out the LED substrate to be processed from the loading and unloading device 101.
  • the sealing door is closed, the vacuum pump vacuums the vacuum transmission device 104, so that the cavity of the vacuum transmission device 104 satisfies a certain degree of vacuum, and then the robot arm will treat the to-be-processed Moving the LED substrate to a sealed door of the vacuum transfer device 104 corresponding to the pre-treatment chamber 103, and then opening the sealed door, and placing the LED substrate to be processed in the pre-treatment chamber
  • the LED substrate to be processed is transferred to the epitaxial layer deposition chamber by the same method as described above. Room 102.
  • the loading and unloading device 101, the pre-processing chamber 103, and the epitaxial layer deposition chamber 102 are linearly arranged on both sides of the vacuum transmission device 104, and the linear arrangement is beneficial to improve the LED chip process integration system.
  • the integration of 100 reduces the space occupied by the clean room, thereby reducing the cost of the clean room and reducing the cost of manufacturing the LED chip.
  • the loading and unloading device 101, the pre-processing chamber 103 is located at one side of the vacuum transmission device 104, and the epitaxial layer deposition chamber 102 is located at the vacuum transmission device.
  • the other side of the 104 is opposite the loading and unloading device 101 and the pretreatment chamber 103.
  • the vacuum transmission device 104 provides a vacuum transmission environment for transporting the LED substrate to be processed or processed, thereby causing a transmission environment between the pretreatment chamber 103 and the epitaxial layer deposition chamber 102.
  • the vacuum environment prevents the LED substrate from being exposed to the clean room and is contaminated by contaminants in the clean room, thereby improving the between the epitaxial layer deposited in the epitaxial layer deposition chamber 102 and the LED substrate. Adhesion prevents failure of the LED chip due to contamination of the contaminant or affects the yield of the LED chip.
  • the epitaxial layer deposition chamber 102 performs epitaxial layer deposition.
  • the epitaxial layer is a multi-layered structure.
  • the epitaxial layer is a multi-layered structure in which an N-type GaN layer, a multiple quantum well active layer, and a P-type GaN layer are stacked. Therefore, the epitaxial layer deposition chamber 102 needs to deposit an N-type GaN layer, a multiple quantum well active layer, and a P-type GaN layer on the LED substrate to be processed.
  • the epitaxial layer deposition chamber 102 deposits an epitaxial layer at a temperature ranging from 700 to 1300 degrees Celsius.
  • the N-type GaN layer, the multiple quantum well active layer, and the P-type GaN layer may be deposited using an epitaxial layer deposition chamber 102.
  • the N-type GaN layer deposition chamber is for depositing an N-type GaN layer
  • the multiple quantum well active layer deposition chamber is for depositing a multiple quantum well active layer
  • the P-type GaN layer deposition chamber is used for A P-type GaN layer is deposited, and the N-type GaN layer, the multiple quantum well active layer, and the P-type GaN layer constitute the epitaxial layer.
  • the N-type GaN layer deposition chamber, the multiple quantum well active layer deposition chamber, and the P-type GaN layer deposition chamber may be provided with independent source material supply devices for providing source materials, forming and The film material corresponding to the source material can avoid cross-contamination between the plurality of source materials.
  • the N-type GaN layer deposition chamber, the multiple quantum well active layer deposition chamber, and the P-type GaN layer deposition chamber may be provided with independent heating stages and temperature control devices for each thin film layer (N-type GaN layer, multiple The temperature control device of the deposition chamber 102 of the quantum well active layer or the P-type GaN layer independently controls the heating station to independently heat the LED substrate, facilitating independent temperature control according to each of the thin film layer deposition chambers 102.
  • the N-type GaN layer deposition chamber, the multiple quantum well active layer deposition chamber, and the P-type GaN layer deposition chamber deposit different film layers, so that the corresponding N-type GaN layer deposition chamber and the multiple quantum wells have
  • the temperature of the source layer deposition chamber and the P-type GaN layer deposition chamber are different, such that the N-type GaN layer deposition chamber, the multiple quantum well active layer deposition chamber, and the P-type GaN layer deposition chamber
  • the temperature of the chamber only needs to be set to a relatively fixed temperature, avoiding the need to repeatedly adjust the temperature of depositing various thin film layers by using one epitaxial layer deposition chamber, thereby saving process time, and due to the N-type GaN layer deposition chamber
  • the temperature of the multiple quantum well active layer deposition chamber is relatively stable, thereby facilitating the corresponding deposition of the N-type GaN layer deposition chamber and the multiple quantum well active layer deposition chamber on different LED substrates. Uniformity of the thin film layer (N-type GaN layer, multiple quantum
  • the processing method of the LED chip process integration system of the present invention is specifically as follows:
  • the LED substrate to be processed is transferred to the pre-processing chamber 103 by the vacuum transmission device 104, and the LED substrate to be processed is heated and cleaned by the pre-processing chamber 103, and heated.
  • the pretreatment chamber 103 for the principle and method of the cleaning process, please refer to the description of the pretreatment chamber 103 in this embodiment.
  • the surface of the LED substrate to be processed after being heated and cleaned is clean and has a certain degree. a temperature, the temperature ranges from 700 to 1300 degrees Celsius, and the temperature may correspond to a temperature of the epitaxial layer deposition process, for example, the temperature may be 1050 degrees Celsius;
  • the vacuum transfer device 104 transfers the heated and cleaned LED substrate to be processed to the epitaxial layer deposition chamber 102, and the epitaxial layer deposition chamber 102 performs epitaxial layer deposition, epitaxial layer deposition.
  • the parameters will be explained in detail later;
  • the processed (ie, deposited epitaxial layer) LED substrate is transferred to the pre-processing chamber 103 by the vacuum transfer device 104, and the processed LED substrate is performed by the pre-processing chamber 103.
  • Cooling treatment in this embodiment, the cooling treatment is to cool from the second temperature (700-1300 degrees Celsius) to the first temperature, and the required cooling time ranges from 1 to 25 minutes, preferably 10 to 15 minutes;
  • the vacuum transfer device 104 transfers the processed LED substrate to the load unloading device 101.
  • the epitaxial layer of the present invention may form an N-type GaN layer, a multiple quantum well active layer and a P-type GaN layer by using an epitaxial layer deposition chamber 102, or may form an N-type GaN layer by using three epitaxial layer deposition chambers respectively. , a multiple quantum well active layer and a P-type GaN layer.
  • the epitaxial layer deposition chamber 102 performs N-type GaN layer deposition, multiple quantum well active layer deposition, and P-type GaN deposition.
  • the temperature of the N-type GaN layer formed by the epitaxial layer deposition chamber 102 ranges from 700 to 1300 degrees Celsius, preferably from 1000 to 1300 degrees Celsius, preferably from 1000 to 1150 degrees Celsius, for example, 1100 degrees Celsius or 1050 degrees Celsius; It is 100 to 200 minutes, preferably 100 to 150 minutes, for example, 100 minutes, 125 minutes or 150 minutes; the thickness of the N-type GaN layer formed ranges from 1 to 3 meters, preferably from 1 to 2 meters, for example 1 ⁇ 2 ⁇ ; For example, when the deposition temperature of the N-type GaN layer is 1050 degrees Celsius, the time is 120 minutes, the corresponding formed N-type GaN layer has a thickness of 1.5 microns;
  • the temperature range of the epitaxial layer deposition chamber 102 forming the multiple quantum well active layer is
  • the time range is 30-80 minutes, preferably 40-50 minutes, and the formed multi-quantum well active layer has a thickness ranging from 600 to 900 angstroms, preferably 700-800 angstroms;
  • the deposition temperature of the multiple quantum well active layer is 750 degrees Celsius and the time is 40 minutes, the corresponding formed N-type GaN layer has a thickness of 750 angstroms;
  • the epitaxial layer deposition chamber 102 forms the P-type GaN layer in a temperature range of 800 to 1000 degrees Celsius, preferably 850 to 950 degrees Celsius, for example, 800 degrees Celsius, 900 degrees Celsius or 950 degrees Celsius, and the time range is 20 to 80 minutes.
  • the thickness of the P-type GaN layer formed is in the range of 0.2 to 0.6 ⁇ m, preferably 0.3 to 0.5 ⁇ m; for example, when the deposition temperature of the multi-P-type GaN layer is 900 ° C, the time is 25 minutes.
  • the corresponding formed N-type GaN layer has a thickness of 0.4 ⁇ m.
  • the three epitaxial layer deposition chambers 102 are respectively an N-type GaN layer deposition chamber, a multiple quantum well active layer deposition chamber, and a P-type GaN layer deposition.
  • the chamber is deposited.
  • the N-type GaN layer deposition chamber forms a process parameter of the N-type GaN layer
  • the multi-quantum well active layer deposition chamber forms a process parameter of the multi-quantum well active layer epitaxial layer
  • the P-type GaN layer deposition chamber forms a P-type
  • the process parameters of the GaN layer please refer to the parameters of the epitaxial layer formed by using an epitaxial deposition chamber 102, which will not be described herein.
  • FIG. 4 is a schematic structural view of a process integration system for an LED chip according to a second embodiment of the present invention, wherein the same structures as those of the first embodiment are denoted by the same reference numerals.
  • the LED chip process integration system 100 includes:
  • At least one epitaxial layer deposition chamber 102 is located at a periphery of the vacuum transfer device 104, and the epitaxial layer deposition chamber 102 is configured to perform epitaxial layer deposition on the LED substrate to be processed;
  • the conductive layer deposition chamber 105 is used to deposit a conductive layer.
  • the LED chip process integration system adds the conductive layer deposition chamber 105, and the rest of the structure is the same as that of the first embodiment.
  • the LED chip process integration system adds the conductive layer deposition chamber 105, and the rest of the structure is the same as that of the first embodiment.
  • the conductive layer deposition chamber 105 is used for conducting a conductive layer on the LED substrate, and the conductive layer may be made of a metal layer or a transparent conductive layer, and the metal layer is one of a gold-nickel alloy, a gold-titanium alloy or another metal.
  • the transparent conductive layer comprises one or more of ITO and ⁇ .
  • the LED chip process integration system integrates the epitaxial layer deposition process and the conductive layer deposition process in the same system, thereby the LED substrate is deposited in the epitaxial layer chamber 102 and the conductive layer deposition chamber.
  • the transmission between the 105 is vacuum transmission, eliminating the need to move the LED substrate to the clean room, avoiding contamination of the LED substrate, and eliminating the need for repeated vacuuming.
  • the conductive layer deposition chamber 105 is disposed on a side of the vacuum transfer device 104 opposite to the epitaxial layer deposition chamber 102.
  • the deposition time of the conductive layer deposition chamber 105 ranges from 10 to 40 minutes, and the deposition time of the epitaxial layer deposition chamber 102 ranges from 0.5 to 6.5 hours, the deposition time of the conductive layer deposition chamber 105 is shorter.
  • the deposition time of the epitaxial layer deposition chamber 102 is long, so that the conductive layer deposition chamber 105 may have a problem of insufficient utilization, so the inventors optimized the number of the conductive layer deposition chambers 105 to improve the conductive layer.
  • the utilization rate of the deposition chamber 105 is increased, and the integration degree of the LED chip process integration system of the present invention and the production efficiency of the LED chip are improved.
  • the ratio of the number of the epitaxial layer deposition chambers 102 to the number of the conductive layer deposition chambers 105 ranges from 2/1 to 12/1, more preferably from 4/1 to 12/1, for example, the ratio Can be 8/1 ⁇ 12/1.
  • the epitaxial layer deposition chamber 102 and the conductive layer deposition chamber 105 are respectively provided with independent exhaust systems. In other embodiments, the epitaxial layer deposition chamber 102 may also share an exhaust system with the conductive layer deposition chamber 105.
  • the method for processing the LED substrate includes:
  • the LED substrate to be processed is placed in the pretreatment chamber 103;
  • the pre-processing chamber 103 heats and cleans the LED substrate to be processed, so that the surface of the LED substrate to be processed after the heating and cleaning process is clean and has a certain temperature, and the temperature range is 700 ⁇ 1300 degrees Celsius, specifically corresponding to the temperature of the epitaxial layer deposition process, in this embodiment, the temperature is 1100 degrees Celsius or 1050 degrees Celsius;
  • the vacuum transfer device 104 places the LED substrate to be processed in the epitaxial layer deposition chamber 102 for epitaxial layer deposition;
  • the vacuum transfer device 104 places the processed (i.e., deposited epitaxial layer) LED substrate in the pretreatment chamber 103;
  • the pre-processing chamber 103 performs a first cooling on the LED substrate, and the first cooling is specifically to reduce the LED substrate on which the epitaxial layer is deposited from a second temperature to a third temperature, and the second temperature is a temperature at which the epitaxial layer deposition process is performed, the second temperature ranges from 700 to 1100 degrees Celsius, for example, 1100 degrees Celsius or 1050 degrees Celsius, and the third temperature is a temperature at which the conductive layer deposition process is performed, for example, 100 to 400 degrees Celsius. Preferably 150 to 350 degrees Celsius;
  • the vacuum transfer device 104 places the first cooled LED substrate in the conductive layer deposition chamber 105;
  • the conductive layer deposition chamber 105 deposits a conductive layer on the epitaxial layer of the first cooled LED substrate
  • the vacuum transfer device 104 places the processed (i.e., deposited conductive layer) LED substrate in the pretreatment chamber 103;
  • the pre-processing chamber 103 performs second cooling on the processed LED substrate, and the second cooling is to reduce the third temperature when the LED substrate is deposited from the conductive layer to a first temperature;
  • the vacuum transfer device 104 transfers the second cooled LED substrate to a loading and unloading device to complete an epitaxial layer and a conductive layer deposition process.
  • FIG. 5 is a schematic structural diagram of an LED chip process integration system according to a third embodiment of the present invention, wherein the same structures as those in the first embodiment and the second embodiment are given the same reference numerals.
  • Place The LED chip process integration system 100 includes:
  • Loading and unloading device 101 for loading or unloading the LED substrate to be processed or processed; vacuum transmitting device 104 for providing a vacuum transmission environment for transmitting the LED substrate to be processed or processed;
  • At least one epitaxial layer deposition chamber 102 is located at a periphery of the vacuum transfer device 104, and the epitaxial layer deposition chamber 102 is configured to perform epitaxial layer deposition on the LED substrate to be processed;
  • a conductive layer deposition chamber 105 is located at a periphery of the vacuum transfer device 104 and the epitaxial layer deposition chamber 102 for depositing a conductive layer.
  • the vacuum transmission device has a polygonal shape, and the pretreatment chamber 103, the loading and unloading device 101, the epitaxial layer deposition chamber 102, and the conductive layer deposition chamber 105 are arranged. At the periphery of the vacuum transmission device 104.
  • the vacuum transfer device may also be circular, elliptical, trapezoidal, rhombic or other polygonal shape.
  • the pre-processing chamber 103 is connected to the vacuum transmission device 104, and the conductive layer deposition chamber 105 is linearly connected to the pre-processing chamber 103, and the conductive layer deposition chamber
  • the chamber 105 is located on a side of the pretreatment chamber 103 remote from the vacuum transmission device 104, which can reduce the space of the clean room occupied by the LED chip process integration system 100 and reduce the cost of the clean room.
  • the pretreatment chamber 103 the loading and unloading device 101, and the epitaxial layer deposition chamber
  • the structure of the conductive layer deposition chamber 105 and the vacuum transmission device 104 are the same as those of the first embodiment and the second embodiment. Please refer to the related content in the first embodiment and the second embodiment of the present invention, and details are not described herein again. .
  • FIG. 6 is a schematic structural diagram of an LED chip process integration system according to a fourth embodiment of the present invention, wherein the same structures as those of the first embodiment, the second embodiment, and the third embodiment are denoted by the same reference numerals.
  • the chip process integration system 100 includes: a loading and unloading device 101 for placing an LED substrate to be processed and a processed LED substrate; Loading and unloading device 101 for loading or unloading the LED substrate to be processed or processed; vacuum transmission device 104 for providing a vacuum transmission environment for transmitting the LED substrate to be processed or processed;
  • At least one epitaxial layer deposition chamber 102 is located at a periphery of the vacuum transfer device 104, and the epitaxial layer deposition chamber 102 is configured to perform epitaxial layer deposition on the LED substrate to be processed;
  • the conductive layer deposition chamber 105 is used to deposit a conductive layer.
  • the shape of the vacuum transfer device 104 in the present embodiment and the vacuum transfer device 104 in the second embodiment are both linear.
  • the difference between this embodiment and the second embodiment is that the number of the load unloading devices 101 is plural. , the figure shows three.
  • the loading and unloading device 101 is located at one side of the vacuum transfer device 104, and the epitaxial layer deposition chamber 102 and the conductive layer deposition chamber 105 are located opposite to the loading and unloading device 101 of the vacuum transfer device 104. One side.
  • FIG. 7 is a schematic structural diagram of an LED chip process integration system according to a fifth embodiment of the present invention.
  • the present embodiment differs from the fourth embodiment in that the conductive layer deposition chamber 105 is located on a side of the vacuum transfer device 103 that is different from the load unloading device 101 and the epitaxial layer deposition chamber 102.
  • FIG. 8 is a schematic view showing the structure of an LED chip process integration system according to a sixth embodiment of the present invention, and the same structures as those in the first to fifth embodiments are denoted by the same reference numerals.
  • the difference between this embodiment and the second embodiment is that the conductive layer deposition chamber 105 is different in position of the LED chip process integration system, and the conductive layer deposition chamber 105 is located at the periphery of the vacuum transmission device 104. And the conductive layer deposition chamber 105 is located between the transfer unloading device 101 and the epitaxial layer deposition chamber 102.
  • the LED chip process integration system of the present invention includes a loading and unloading device, a pretreatment chamber, an epitaxial layer deposition chamber, and a vacuum transmission device, wherein the pretreatment chamber Located outside the epitaxial layer deposition chamber, the pre-treatment chamber is dedicated to pre-treating the LED substrate, thereby saving the step of pre-treating the LED substrate by the epitaxial layer deposition chamber, and adding an epitaxial layer deposition chamber.
  • the time for depositing the epitaxial layer reduces the cost and improves the production efficiency of the epitaxial layer deposition chamber, and the invention greatly reduces the cost of manufacturing the LED chip.
  • the output of the LED chip is increased, and in a preferred embodiment, the present invention also integrates the conductive layer deposition chamber into the LED chip process system, further improving the production efficiency of the LED chip manufacturing and increasing the yield of the LED chip.

Abstract

A process integration system for an LED chip and a processing method thereof are provided. The process integration system comprises: a loading/unloading device (101), for loading or unloading an LED base plate which needs to be processed or has been processed; a vacuum transmission device (104), for providing a vacuum transmission environment to transmit the LED base plate which needs to be processed or has been processed; at least one epitaxial layer deposition chamber (102), which is located at a peripheral part of the vacuum transmission device (104) and is used for epitaxial layer deposition onto the LED base plate to be processed; and at least one pre-processing chamber (103), for the pre-processing of the LED base plate which needs to be processed or has been processed. The present invention improves productivity in the epitaxial layer deposition process of LED base plates, improves the productivity and yield of LED chips, reduces the cost of LED chips, and improves the service life and utilization rate of the epitaxial layer deposition chamber.

Description

LED芯片工艺集成系统及其处理方法 本申请要求于 2010年 11 月 19 日提交中国国家知识产权局、 申请号为 201010552412.8、发明名称为" LED芯片工艺集成系统及其处理方法"的中国专 利申请的优先权, 其全部内容通过引用结合在本申请中。 技术领域  LED chip process integration system and processing method thereof The present application claims to be filed on November 19, 2010 by the Chinese National Intellectual Property Office, the application number is 201010552412.8, and the invention name is "LED chip process integration system and its processing method" Priority is hereby incorporated by reference in its entirety. Technical field
本发明涉及半导体技术领域, 特别涉及一种 LED芯片工艺集成系统及其 处理方法。  The present invention relates to the field of semiconductor technology, and in particular, to an LED chip process integration system and a processing method thereof.
背景技术 Background technique
随着第三代半导体材料氮化镓的突破和蓝、 绿、 白光发光二极管的问世, 继半导体技术引发微电子革命之后, 又在孕育一场新的产业革命一照明革命, 其标志是半导体灯将逐步替代白炽灯和荧光灯。 而寿命可以延长 100倍。 因此 半导体照明具有节能、 长寿命、 环保等优点。  With the breakthrough of the third-generation semiconductor material GaN and the advent of blue, green and white light-emitting diodes, following the microelectronic revolution triggered by semiconductor technology, a new industrial revolution-lighting revolution was born, which is marked by semiconductor lamps. Gradually replace incandescent and fluorescent lamps. And the life expectancy can be extended by 100 times. Therefore, semiconductor lighting has the advantages of energy saving, long life and environmental protection.
请参考图 1 , 为现有的 LED芯片器件结构示意图。 所述 LED芯片包括: LED基板 10, 所述 LED基板 10的材质为蓝宝石; N型 GaN层 11 , 所述 N 型 GaN层 11位于所述 LED基板 10上; 多量子阱有源层 12, 位于所述 N型 GaN层 11上; P型 GaN层 13, 位于所述多量子阱有源层 12上; 导电层 14, 位于所述 P型 GaN层 13上; P型 GaN电极层 15, 位于所述导电层 14上; N 型 GaN电极层 16, 位于所述 N型 GaN层 11上; 保护层 17, 位于所述 N型 GaN电极层 16和 P型 GaN电极层 15之间, 所述保护层 17覆盖所述导电层 14。  Please refer to Figure 1 for a schematic diagram of the structure of the existing LED chip device. The LED chip includes: an LED substrate 10, the material of the LED substrate 10 is sapphire; an N-type GaN layer 11 on which the N-type GaN layer 11 is located; a multi-quantum well active layer 12, located at On the N-type GaN layer 11; a P-type GaN layer 13 on the multiple quantum well active layer 12; a conductive layer 14 on the P-type GaN layer 13; and a P-type GaN electrode layer 15, located in the On the conductive layer 14; an N-type GaN electrode layer 16 on the N-type GaN layer 11; a protective layer 17 between the N-type GaN electrode layer 16 and the P-type GaN electrode layer 15, the protective layer 17 covers the conductive layer 14.
为了便于说明, 将所述 N型 GaN层 11、 多量子阱有源层 12、 P型 GaN 层 13称为外延层。 所述外延层通常利用外延层沉积设备制作。 现有的外延层 沉积设备在制作所述外延层时, 首先将 LED基板从洁净室放置于外延层沉积 设备的装载卸载装置; 然后进行抽真空步骤, 将所述 LED基板从所述装载卸 载装置放置于所述外延层沉积设备的外延层沉积腔室;接着利用所述外延层沉 积腔室进行加热步骤, 即将所述 LED基板从室温 (10~30摄氏度)升至高温, 所 述高温范围为 800~1300摄氏度; 然后利用所述外延层沉积腔室进行外延层沉 积步骤, 所述外延层沉积步骤包括沉积所述图 1所示的 N型 GaN层 11、 多量 子阱有源层 12、 P型 GaN层 13; 接着利用所述外延层沉积腔室对沉积了外延 层的 LED基板进行冷却步骤, 即将所述 LED基板从所述高温降至室温; 接着 再次进行抽真空动作, 将所述 LED基板放置于所述装载卸载装置; 最后将所 述 LED基板移至洁净室, 从而完成所述 LED基板的外延层沉积。 For convenience of explanation, the N-type GaN layer 11, the multiple quantum well active layer 12, and the P-type GaN layer 13 are referred to as epitaxial layers. The epitaxial layer is typically fabricated using an epitaxial layer deposition apparatus. In the conventional epitaxial layer deposition apparatus, when the epitaxial layer is formed, the LED substrate is first placed from the clean room on the loading and unloading device of the epitaxial layer deposition apparatus; and then a vacuuming step is performed to remove the LED substrate from the loading and unloading device. And an epitaxial layer deposition chamber disposed in the epitaxial layer deposition apparatus; and then performing a heating step by using the epitaxial layer deposition chamber, that is, the LED substrate is raised from a room temperature (10 to 30 degrees Celsius) to a high temperature, and the high temperature range is 800~1300 degrees Celsius; then using the epitaxial layer deposition chamber for epitaxial layer deposition The epitaxial layer deposition step includes depositing the N-type GaN layer 11, the multiple quantum well active layer 12, and the P-type GaN layer 13 shown in FIG. 1; and then depositing the deposition chamber by using the epitaxial layer The LED substrate of the epitaxial layer is subjected to a cooling step of lowering the LED substrate from the high temperature to room temperature; then performing a vacuuming operation to place the LED substrate on the loading and unloading device; and finally moving the LED substrate to The clean room is thereby completed to deposit epitaxial layers of the LED substrate.
按照现有技术, 在外延层沉积后, 需要将 LED基板从洁净室放置于导电 层沉积设备的装载卸载装置, 进行导电层沉积。 具体地, 包括: 首先进行抽真 空步骤,将所述 LED基板从洁净室放置于导电层沉积设备的导电层沉积腔室; 接着利用所述导电层沉积腔室进行加热, 即使所述 LED 基板从室温升至 200~500摄氏度; 然后利用所述导电层沉积腔室进行导电层沉积步骤; 接着利 用所述导电层沉积腔室进行冷却步骤, 将所述 LED基板冷却至室温; 然后再 次进行抽真空动作, 将所述 LED基板放置于所述装载卸载装置; 最后将所述 LED基板移至洁净室, 从而完成所述 LED基板的导电层沉积。  According to the prior art, after the epitaxial layer is deposited, it is necessary to place the LED substrate from the clean room on the loading and unloading device of the conductive layer deposition apparatus to perform deposition of the conductive layer. Specifically, the method includes: first performing a vacuuming step of placing the LED substrate from a clean room in a conductive layer deposition chamber of a conductive layer deposition apparatus; and then performing heating by using the conductive layer deposition chamber, even if the LED substrate is Raising the temperature to 200-500 degrees Celsius at room temperature; then performing a conductive layer deposition step using the conductive layer deposition chamber; then performing a cooling step using the conductive layer deposition chamber, cooling the LED substrate to room temperature; and then pumping again The LED substrate is placed on the loading and unloading device by vacuum action; finally, the LED substrate is moved to a clean room to complete deposition of a conductive layer of the LED substrate.
在实际中发现, 现有技术至少存在以下问题:  In practice, it has been found that the prior art has at least the following problems:
第一, 所述外延层沉积腔室沉积外延层的时间较长, 通常为 3~6小时, 影 响了外延层沉积设备的生产效率, 从而影响了 LED芯片的生产效率, 从而使 得现有的 LED芯片的产量不高, 也造成了现有的 LED芯片的价格较贵;  First, the deposition time of the epitaxial layer deposition chamber is long, usually 3-6 hours, which affects the production efficiency of the epitaxial layer deposition equipment, thereby affecting the production efficiency of the LED chip, thereby making the existing LED The output of the chip is not high, which also causes the existing LED chips to be more expensive;
第二,在外延层沉积腔室开始沉积外延层前和外延层沉积后, 分别需要对 LED基板进行加热和冷却的步骤, 而现有的加热步骤和冷却步骤利用所述外 延层沉积腔室进行, 这占用了所述外延层沉积腔室用于沉积外延层的时间, 进 一步降低了现有的外延层沉积设备的生产效率, 影响 LED芯片的产量, 也增 加了 LED芯片的成本;  Second, before the epitaxial layer deposition chamber begins to deposit the epitaxial layer and after the epitaxial layer is deposited, the steps of heating and cooling the LED substrate are respectively required, and the existing heating step and cooling step are performed by using the epitaxial layer deposition chamber. This occupies the time for depositing the epitaxial layer in the epitaxial layer deposition chamber, further reducing the production efficiency of the existing epitaxial layer deposition apparatus, affecting the output of the LED chip, and increasing the cost of the LED chip;
第三, 利用所述外延层沉积腔室进行所述加热步骤和降温步骤,反复的升 温和降温缩短了所述外延层沉积腔室的使用寿命,需要经常对所述外延层沉积 腔室进行维护, 降低了所述外延层沉积设备的利用率 (uptime), 无法满足实际 的需要;  Third, the heating step and the temperature decreasing step are performed by using the epitaxial layer deposition chamber, and the repeated temperature rise and temperature reduction shortens the service life of the epitaxial layer deposition chamber, and the epitaxial layer deposition chamber needs to be frequently maintained. , reducing the utilization time of the epitaxial layer deposition equipment (uptime), and failing to meet actual needs;
第四, 外延层沉积设备和导电层沉积设备独立设置, 使得 LED基板在进 入和离开所述外延层沉积设备和导电层沉积设备之前,需要进行至少 4次抽真 空的动作, 降低 LED基板的生产效率和 LED基板的产量; 并且 LED基板从 所述外延层沉积设备移至导电层时, 需要暴露在洁净室中,使得洁净室中的有 机污染物、无机污染物和水蒸气可能污染外延层,从而影响导电层与外延层之 间的可靠性。 Fourth, the epitaxial layer deposition apparatus and the conductive layer deposition apparatus are independently disposed such that the LED substrate needs to perform at least four vacuuming operations before entering and leaving the epitaxial layer deposition apparatus and the conductive layer deposition apparatus, thereby reducing the production of the LED substrate. Efficiency and yield of the LED substrate; and when the LED substrate is moved from the epitaxial layer deposition device to the conductive layer, it needs to be exposed in the clean room so that there is Machine contaminants, inorganic contaminants, and water vapor may contaminate the epitaxial layer, thereby affecting the reliability between the conductive layer and the epitaxial layer.
发明内容 Summary of the invention
本发明的目的是提供一种 LED芯片工艺集成系统及其处理方法, 以解决 现有技术中存在的 LED芯片的外延层沉积工艺的生产效率低下且生产成本高 的问题。  SUMMARY OF THE INVENTION An object of the present invention is to provide an LED chip process integration system and a processing method thereof, which solve the problems of low production efficiency and high production cost of an epitaxial layer deposition process of an LED chip existing in the prior art.
为解决上述问题, 本发明提供了一种 LED芯片工艺集成系统, 包括: 装载卸载装置, 用于装载或卸载待处理的或处理完毕的 LED基板; 真空传输装置,用于提供真空传输环境以传输所述待处理的或处理完毕的 LED基板;  In order to solve the above problems, the present invention provides an LED chip process integration system, comprising: a loading and unloading device for loading or unloading a processed or processed LED substrate; and a vacuum transmission device for providing a vacuum transmission environment for transmission The LED substrate to be processed or processed;
至少一个外延层沉积腔室,位于所述真空传输装置周沿, 所述外延层沉积 腔室用于对所述待处理的 LED基板进行外延层沉积;  At least one epitaxial layer deposition chamber is disposed at a periphery of the vacuum transmission device, and the epitaxial layer deposition chamber is configured to perform epitaxial layer deposition on the LED substrate to be processed;
至少一个预处理腔室, 用于对所述待处理的或处理完毕的 LED基板进行 预处理。  At least one pretreatment chamber for pretreating the LED substrate to be processed or processed.
可选地, 所述预处理腔室位于所述真空传输装置周沿, 用于对所述待处理 的 LED基板进行加热、清洁或冷却处理或对所述处理完毕的 LED基板进行冷 却处理。  Optionally, the pre-processing chamber is located at a periphery of the vacuum transmission device for heating, cleaning or cooling the LED substrate to be processed or cooling the processed LED substrate.
可选地, 所述预处理腔室设置有加热台, 所述加热台用于对 LED基板进 行加热处理, 使得所述 LED基板从第一温度升至第二温度。  Optionally, the pre-processing chamber is provided with a heating stage for heating the LED substrate to raise the LED substrate from a first temperature to a second temperature.
可选地,所述第一温度的温度范围为 10~30摄氏度, 所述第二温度的温度 范围为 700~1300摄氏度。  Optionally, the temperature of the first temperature ranges from 10 to 30 degrees Celsius, and the temperature of the second temperature ranges from 700 to 1300 degrees Celsius.
可选地, 所述预处理腔室设置有至少一个进风口和至少一个出风口, 所述 进风口用于通入还原性气体或保护性气体的中的一种或多种,所述还原性气体 或保护性气体用于对 LED基板进行清洁处理。  Optionally, the pre-treatment chamber is provided with at least one air inlet and at least one air outlet, and the air inlet is configured to pass one or more of a reducing gas or a protective gas, the reducing property A gas or protective gas is used to clean the LED substrate.
可选地, 所述还原性气体为氢气或氨气, 所述保护性气体为惰性气体或氮 气中的一种或多种。  Optionally, the reducing gas is hydrogen or ammonia, and the protective gas is one or more of an inert gas or nitrogen.
可选地, 所述预处理腔室设置有温控装置, 所述温控装置用于控制所述加 热台在 5~15分钟内将所述 LED基板从所述第一温度加热至所述第二温度,且 使所述 LED基板保持所述第二温度 1~25分钟;  Optionally, the pre-processing chamber is provided with a temperature control device, and the temperature control device is configured to control the heating station to heat the LED substrate from the first temperature to the first in 5 to 15 minutes. Two temperatures, and maintaining the LED substrate at the second temperature for 1 to 25 minutes;
在所述 LED基板保持所述第二温度时, 所述进风口用于通入所述还原性 气体或保护性气体的一种或多种。 The air inlet is configured to pass the reducing property when the LED substrate maintains the second temperature One or more of a gas or a protective gas.
可选地, 所述外延层沉积腔室的沉积时间范围为 0.5~6.5小时。  Optionally, the deposition time of the epitaxial layer deposition chamber ranges from 0.5 to 6.5 hours.
可选地, 所述预处理腔室与所述外延层沉积腔室的数目的比例范围为 Optionally, the ratio of the number of the pre-treatment chamber to the number of epitaxial layer deposition chambers is
1/2~1/5。 1/2~1/5.
可选地, 所述预处理腔室与所述外延层沉积腔室的数目的比例为 1/3。 可选地, 还包括: 导电层沉积腔室, 位于所述真空传输装置和外延层沉积 腔室的周沿, 所述导电层沉积腔室用于沉积导电层。  Optionally, the ratio of the number of the pre-treatment chambers to the epitaxial layer deposition chamber is 1/3. Optionally, the method further includes: a conductive layer deposition chamber located at a periphery of the vacuum transfer device and the epitaxial layer deposition chamber, the conductive layer deposition chamber for depositing a conductive layer.
可选地, 所述真空传输装置的形状为线性, 所述装载卸载装置、 预处理腔 室、 外延层沉积腔室和导电层沉积腔室线性排布于所述真空传输装置周沿。  Optionally, the vacuum transfer device is linear in shape, and the loading and unloading device, the pretreatment chamber, the epitaxial layer deposition chamber, and the conductive layer deposition chamber are linearly arranged around the periphery of the vacuum transfer device.
可选地, 所述真空传输装置的形状为多边形或圆形, 所述装载卸载装置、 预处理腔室、 外延层沉积腔室和导电层沉积腔室位于所述真空传输装置周沿。  Optionally, the vacuum transmission device has a polygonal or circular shape, and the loading and unloading device, the pretreatment chamber, the epitaxial layer deposition chamber, and the conductive layer deposition chamber are located at a periphery of the vacuum transmission device.
可选地, 所述预处理腔室与所述真空传输装置相连接, 所述导电层沉积腔 室与所述预处理腔室线性连接,所述导电层沉积腔室位于所述预处理腔室的远 离所述真空传输装置的一侧。  Optionally, the pretreatment chamber is connected to the vacuum transmission device, the conductive layer deposition chamber is linearly connected to the pretreatment chamber, and the conductive layer deposition chamber is located in the pretreatment chamber Aside from the side of the vacuum transmission device.
可选地, 所述导电层为金属层或透明导电层, 所述金属层为金镍合金、 金 钛合金或其他金属中的一种或多种, 所述透明导电层为 ITO、 ΖηΟ中的一种或 多种。  Optionally, the conductive layer is a metal layer or a transparent conductive layer, and the metal layer is one or more of a gold-nickel alloy, a gold-titanium alloy or another metal, and the transparent conductive layer is in ITO, ΖηΟ One or more.
可选地,所述外延层沉积腔室与所述导电层沉积腔室分别设置有独立的排 气系统。  Optionally, the epitaxial layer deposition chamber and the conductive layer deposition chamber are respectively provided with independent exhaust systems.
可选地, 所述导电层沉积腔室的沉积时间范围为 10~40分钟。  Optionally, the deposition time of the conductive layer deposition chamber ranges from 10 to 40 minutes.
可选地,所述外延层沉积腔室的数目与导电层沉积腔室的数目的比例范围 为 2/1-12/1„  Optionally, the ratio of the number of epitaxial layer deposition chambers to the number of conductive layer deposition chambers ranges from 2/1 to 12/1.
可选地,所述外延层沉积腔室的数目与导电层沉积腔室的数目的比例范围 为 4/1-12/1„  Optionally, the ratio of the number of epitaxial layer deposition chambers to the number of conductive layer deposition chambers ranges from 4/1 to 12/1.
可选地,所述外延层沉积腔室的数目与导电层沉积腔室的数目的比例范围 为 8/1-12/1„  Optionally, the ratio of the number of epitaxial layer deposition chambers to the number of conductive layer deposition chambers ranges from 8/1 to 12/1.
可选地, 所述外延层沉积腔室用于沉积 Ν型 GaN层、 多量子阱有源层和 P型 GaN层, 所述 N型 GaN层、 多量子阱有源层和 P型 GaN层构成所述外 延层。  Optionally, the epitaxial layer deposition chamber is configured to deposit a Ν-type GaN layer, a multiple quantum well active layer, and a P-type GaN layer, wherein the N-type GaN layer, the multiple quantum well active layer, and the P-type GaN layer are formed The epitaxial layer.
可选地, 所述外延层沉积腔室的数目至少为 3个, 包括: N型 GaN层沉 积腔室、多量子阱有源层沉积腔室和 P型 GaN层沉积腔室,所述 N型 GaN层 沉积腔室用于沉积 N型 GaN层, 所述多量子阱有源层沉积腔室用于沉积多量 子阱有源层,所述 P型 GaN层沉积腔室用于沉积 P型 GaN层,所述 N型 GaN 层、 多量子阱有源层和 P型 GaN层构成所述外延层。 Optionally, the number of the epitaxial layer deposition chambers is at least three, including: N-type GaN layer sinking An accumulation chamber, a multiple quantum well active layer deposition chamber, and a P-type GaN layer deposition chamber for depositing an N-type GaN layer, the multiple quantum well active layer deposition chamber And a P-type GaN layer deposition chamber for depositing a P-type GaN layer, wherein the N-type GaN layer, the multiple quantum well active layer, and the P-type GaN layer constitute the epitaxial layer .
相应地, 本发明还提供一种 LED芯片工艺集成系统的处理方法, 包括: 将待处理的 LED基板放置于装载卸载装置;  Correspondingly, the present invention further provides a processing method of an LED chip process integration system, comprising: placing an LED substrate to be processed on a loading and unloading device;
利用真空传输装置将所述待处理的 LED基板放置于预处理腔室; 利用所述预处理腔室对所述待处理的 LED基板进行预处理;  Disposing the LED substrate to be processed in a pretreatment chamber by using a vacuum transfer device; pretreating the LED substrate to be processed by using the pretreatment chamber;
将预处理后的所述 LED基板放置于外延层沉积腔室;  Depositing the pretreated LED substrate in an epitaxial layer deposition chamber;
在所述外延层沉积腔室中进行外延层沉积。  Epitaxial layer deposition is performed in the epitaxial layer deposition chamber.
可选地, 所述预处理包括对所述 LED基板进行加热、 冷却或者清洁处理。 可选地, 还包括:  Optionally, the pre-processing comprises heating, cooling or cleaning the LED substrate. Optionally, the method further includes:
利用所述真空传输装置将沉积有外延层的 LED 基板传输至所述预处理 室;  Transmitting an LED substrate deposited with an epitaxial layer to the pretreatment chamber by using the vacuum transfer device;
所述预处理室对所述 LED基板进行第一冷却处理;  The pretreatment chamber performs a first cooling process on the LED substrate;
将所述第一冷却处理后的 LED基板传输到导电层沉积腔室用于沉积导电 层。  The first cooled LED substrate is transferred to a conductive layer deposition chamber for depositing a conductive layer.
可选地, 还包括: 将沉积有导电层的 LED基板传输至所述预处理室进行 第二冷却处理。  Optionally, the method further includes: transmitting the LED substrate deposited with the conductive layer to the pretreatment chamber for performing a second cooling process.
可选地, 所述预处理包括:  Optionally, the preprocessing includes:
利用温控装置将所述加热台在 5~15分钟内将所述 LED基板从第一温度加 热至第二温度;  Heating the LED substrate from the first temperature to the second temperature in 5 to 15 minutes by using a temperature control device;
使所述 LED基板保持所述第二温度 1~25分钟;  Holding the LED substrate at the second temperature for 1 to 25 minutes;
在所述 LED基板保持所述第二温度的同时, 向所述预处理腔室内通入还 原性气体或保护性气体的一种或多种。  While the LED substrate maintains the second temperature, one or more of a reducing gas or a protective gas is introduced into the pretreatment chamber.
可选地, 所述还原性气体为氢气或氨气, 所述保护性气体为惰性气体或氮 气中的一种或多种。  Optionally, the reducing gas is hydrogen or ammonia, and the protective gas is one or more of an inert gas or nitrogen.
可选地, 还包括将所述沉积有外延层的 LED基板传输至所述预处理室进 行冷却处理, 所述冷却处理为将所述 LED基板的温度从第二温度降低为第一 温度,所述第一温度的温度范围为 10~30摄氏度,所述第二温度的温度范围为 700~1300摄氏度。 Optionally, the method further includes transmitting the LED substrate deposited with the epitaxial layer to the pretreatment chamber for performing a cooling process, wherein the cooling process is to reduce the temperature of the LED substrate from a second temperature to a first temperature, The temperature of the first temperature ranges from 10 to 30 degrees Celsius, and the temperature range of the second temperature is 700~1300 degrees Celsius.
可选地, 所述第一冷却处理为将所述 LED基板的温度从第二温度降低为 第三温度, 所述第二温度的温度范围为 700~1300摄氏度, 所述第三温度的温 度范围为 100~400摄氏度。  Optionally, the first cooling process is to reduce the temperature of the LED substrate from a second temperature to a third temperature, and the second temperature has a temperature range of 700 to 1300 degrees Celsius, and the temperature range of the third temperature It is 100~400 degrees Celsius.
可选地, 所述外延层沉积的时间范围为 0.5~6.5小时。  Optionally, the epitaxial layer is deposited for a time ranging from 0.5 to 6.5 hours.
可选地, 还包括:  Optionally, the method further includes:
利用所述真空传输装置将所述冷却后的 LED 基板放置于导电层沉积腔 室;  Depositing the cooled LED substrate in a conductive layer deposition chamber by using the vacuum transfer device;
利用所述导电层沉积腔室对所述 LED基板进行导电层沉积。  Conductive layer deposition is performed on the LED substrate using the conductive layer deposition chamber.
可选地, 所述第二冷却处理为将所述 LED基板从 100-400摄氏度冷却至 Optionally, the second cooling process is to cool the LED substrate from 100-400 degrees Celsius to
10~30摄氏度。 10 to 30 degrees Celsius.
可选地, 所述外延层包括 N型 GaN层、 多量子阱有源层和 P型 GaN层。 可选地, 所述外延层利用一个所述外延层沉积腔室沉积 N型 GaN层、 多 量子阱有源层和 P型 GaN层或利用 3个所述外延层沉积腔室分别沉积 N型 GaN层、 多量子阱有源层和 P型 GaN层。  Optionally, the epitaxial layer comprises an N-type GaN layer, a multiple quantum well active layer, and a P-type GaN layer. Optionally, the epitaxial layer deposits an N-type GaN layer, a multiple quantum well active layer, and a P-type GaN layer by using the epitaxial layer deposition chamber or deposits N-type GaN by using the three epitaxial layer deposition chambers respectively. Layer, multiple quantum well active layer and P-type GaN layer.
可选地, 所述外延层沉积腔室沉积所述 N 型 GaN 层的温度范围为 1000-1300摄氏度, 时间范围为 100~200分钟, 形成的所述 N型 GaN层的厚 度范围为 1~3微米;  Optionally, the epitaxial layer deposition chamber deposits the N-type GaN layer in a temperature range of 1000-1300 degrees Celsius, and the time range is 100-200 minutes, and the formed N-type GaN layer has a thickness ranging from 1 to 3 Micron
形成所述多量子阱有源层的温度范围为 700~800 摄氏度, 时间范围为 30~80分钟, 形成的多量子阱有源层的厚度范围为 600~900埃;  Forming the multi-quantum well active layer at a temperature ranging from 700 to 800 degrees Celsius and a time range of 30 to 80 minutes, and forming a multi-quantum well active layer having a thickness ranging from 600 to 900 angstroms;
形成所述 P型 GaN层的温度范围为 850~950摄氏度, 时间范围为 20~80 分钟, 形成的 P型 GaN层的厚度范围为 0.2~0.6微米。  The P-type GaN layer is formed to have a temperature range of 850 to 950 degrees Celsius and a time range of 20 to 80 minutes, and the P-type GaN layer is formed to have a thickness ranging from 0.2 to 0.6 μm.
与现有技术相比, 本发明具有以下优点:  Compared with the prior art, the present invention has the following advantages:
本发明提供的 LED芯片工艺集成系统包括位于外延层沉积室之外的预处 理腔室, 所述预处理腔室用于对 LED基板进行预处理, 从而使得所述外延层 沉积腔室仅用于外延层沉积,增加了所述外延层沉积腔室用于沉积外延层的时 间 ,也提高了外延层沉积的生产效率,相应提高了 LED芯片的生产效率和 LED 芯片的产量; 并且由于所述外延层沉积腔室仅用于外延层沉积, 避免了其反复 升温和降温对其使用寿命的影响, 从而延长了所述外延层沉积腔室的使用寿 命, 减少了对所述外延层沉积腔室的维护的人力成本和时间成本,提高了外延 层沉积腔室的利用率, 满足了实际的需要; 由于所述 LED基板在外延层沉积 腔室、 预处理腔室之间的传输利用真空传输环境进行, 避免了 LED基板受到 外部的污染物的污染; The LED chip process integration system provided by the present invention comprises a pre-processing chamber outside the deposition chamber of the epitaxial layer, the pre-processing chamber is used for pre-treating the LED substrate, so that the epitaxial layer deposition chamber is only used for Epitaxial layer deposition increases the time for depositing the epitaxial layer in the epitaxial layer deposition chamber, and also improves the production efficiency of the epitaxial layer deposition, correspondingly increasing the production efficiency of the LED chip and the yield of the LED chip; The layer deposition chamber is only used for epitaxial layer deposition, which avoids the influence of its repeated heating and cooling on its service life, thereby prolonging the service life of the epitaxial layer deposition chamber and reducing the deposition chamber of the epitaxial layer. Maintenance of labor costs and time costs, improved the extension The utilization rate of the layer deposition chamber satisfies the actual needs; since the transmission of the LED substrate between the epitaxial layer deposition chamber and the pretreatment chamber is performed by using a vacuum transmission environment, the LED substrate is protected from external contaminants. Pollution;
进一步优化地, 所述预处理腔室还可以用于对所述 LED基板表面进行清 洁处理, 从而去除 LED基板表面的污染物, 例如颗粒、 有机物、 无机物和水 蒸气等,从而提高了后续沉积的外延层的质量,并且改善了所述外延层与 LED 基板之间的粘附性, 提高 LED基板的可靠性;  Further preferably, the pre-treatment chamber can also be used for cleaning the surface of the LED substrate to remove contaminants such as particles, organic matter, inorganic substances and water vapor on the surface of the LED substrate, thereby improving subsequent deposition. The quality of the epitaxial layer, and the adhesion between the epitaxial layer and the LED substrate is improved, and the reliability of the LED substrate is improved;
进一步优化地,所述预处理腔室的清洁步骤的时间范围为 10~40分钟,所 述外延层沉积腔室的沉积时间范围为 0.5~6.5小时, 设置所述预处理腔室与所 述外延层沉积腔室的数目比例范围为 1/2~1/5 , 使得所述预处理腔室与所述外 延层沉积腔室配合工作, 提高 LED基板的处理速度, 提高 LED芯片的生产效 率和产量;  Further preferably, the cleaning step of the pretreatment chamber has a time range of 10 to 40 minutes, and the deposition time of the epitaxial layer deposition chamber ranges from 0.5 to 6.5 hours, and the pretreatment chamber and the epitaxy are disposed. The ratio of the number of layer deposition chambers ranges from 1/2 to 1/5, so that the pretreatment chamber cooperates with the deposition chamber of the epitaxial layer to improve the processing speed of the LED substrate and improve the production efficiency and yield of the LED chip. ;
进一步优化地,所述预处理腔室与所述外延层沉积腔室的数目比例为 1/3 , 综合考虑了外延层沉积腔室的成本与提高外延层沉积腔室的生产效率,从而可 以以较为合理的成本获得较高的生产效率;  Further optimized, the ratio of the number of the pre-treatment chamber to the epitaxial layer deposition chamber is 1/3, which comprehensively considers the cost of the epitaxial layer deposition chamber and improves the production efficiency of the epitaxial layer deposition chamber, so that More reasonable cost to obtain higher production efficiency;
进一步优化地, 所述 LED芯片工艺集成系统还包括导电层沉积腔室, 使 得所述外延层沉积后的 LED基板无需进行反复抽真空步骤, 在真空环境中进 入导电层沉积腔室进行导电层沉积, 一方面提高了导电层沉积的生产效率, 进 一步提高了 LED芯片的生产效率和产量, 另一方面, 避免了所述 LED基板暴 露在洁净室中, 防止所述 LED基板受到洁净室的污染, 改善了导电层与外延 层之间的粘附性, 提高了所述 LED芯片的良率和可靠性;  Further preferably, the LED chip process integration system further comprises a conductive layer deposition chamber, such that the deposited LED substrate of the epitaxial layer does not need to be subjected to repeated vacuuming steps, and enters the conductive layer deposition chamber for conducting conductive layer deposition in a vacuum environment. On the one hand, the production efficiency of the conductive layer deposition is improved, the production efficiency and the yield of the LED chip are further improved, and on the other hand, the LED substrate is prevented from being exposed to the clean room, and the LED substrate is prevented from being contaminated by the clean room. The adhesion between the conductive layer and the epitaxial layer is improved, and the yield and reliability of the LED chip are improved;
进一步优化地, 所述真空传输装置的形状为线性, 所述装载卸载装置、 预 处理腔室、外延层沉积腔室和导电层沉积腔室线性排布于所述真空传输装置周 沿, 从而使得所述 LED芯片工艺集成系统的集成度提高, 占用洁净室的空间 较少, 降低了洁净室成本投入, 降低了 LED芯片的制造成本;  Further optimized, the shape of the vacuum transmission device is linear, and the loading and unloading device, the pretreatment chamber, the epitaxial layer deposition chamber, and the conductive layer deposition chamber are linearly arranged on the periphery of the vacuum transmission device, thereby The integration of the LED chip process integration system is improved, the space occupied by the clean room is less, the cost of the clean room is reduced, and the manufacturing cost of the LED chip is reduced;
进一步优化地, 所述真空传输装置的形状为多边形, 所述预处理腔室位于 所述真空传输装置的与外延层沉积腔室相对的一侧,所述导电层沉积腔室位于 所述预处理装置远离所述真空传输装置和外延沉积腔室的一侧,从而使得所述 LED 芯片工艺集成系统的集成度提高, 占用洁净室的空间较少, 降低了洁净 室成本投入, 降低了 LED芯片的成本; 进一步优化地,所述外延层沉积腔室与所述导电层沉积腔室分别设置有独 立的排气系统, 从而提高了所述外延层沉积腔室与导电层沉积腔室的处理速 度, 提高了 LED基板的生产效率和产量; Further preferably, the vacuum transmission device has a polygonal shape, the pretreatment chamber is located on a side of the vacuum transmission device opposite to the epitaxial layer deposition chamber, and the conductive layer deposition chamber is located in the pretreatment The device is away from the side of the vacuum transmission device and the epitaxial deposition chamber, so that the integration of the LED chip process integration system is increased, the space occupied by the clean room is less, the cost of the clean room is reduced, and the LED chip is reduced. cost; Further optimized, the epitaxial layer deposition chamber and the conductive layer deposition chamber are respectively provided with independent exhaust systems, thereby improving the processing speed of the epitaxial layer deposition chamber and the conductive layer deposition chamber, and improving the processing speed. LED substrate production efficiency and output;
进一步优化地,所述外延层沉积腔室的数目与导电层沉积腔室的数目的比 例范围为 8/1~12/1 ,使得所述外延层沉积腔室与所述导电层沉积腔室的数目匹 配,从而使得提高了外延层沉积腔室与所述导电层沉积腔室的利用率, 避免外 延层沉积腔室或所述导电层沉积腔室闲置或负担过重的情况。  Further preferably, the ratio of the number of epitaxial layer deposition chambers to the number of conductive layer deposition chambers ranges from 8/1 to 12/1 such that the epitaxial layer deposition chamber and the conductive layer deposition chamber The number is matched such that the utilization of the epitaxial layer deposition chamber and the conductive layer deposition chamber is improved, and the epitaxial layer deposition chamber or the conductive layer deposition chamber is prevented from being idle or overburdened.
附图说明 DRAWINGS
图 1是现有的 LED芯片器件结构示意图;  1 is a schematic structural view of a conventional LED chip device;
图 2是本发明第一实施例的 LED芯片工艺集成系统结构示意图; 图 3是本发明第一实施例的 LED芯片工艺集成系统的处理方法流程示意 图;  2 is a schematic structural view of a LED chip process integration system according to a first embodiment of the present invention; FIG. 3 is a schematic flow chart of a processing method of the LED chip process integration system according to the first embodiment of the present invention;
图 4是本发明第二实施例的 LED芯片工艺集成系统结构示意图; 图 5是本发明第三实施例的 LED芯片工艺集成系统结构示意图; 图 6是本发明第四实施例的 LED芯片工艺集成系统结构示意图; 图 7是本发明第五实施例的 LED芯片工艺集成系统结构示意图; 图 8是本发明第六实施例的 LED芯片工艺集成系统结构示意图。  4 is a schematic structural view of a LED chip process integration system according to a second embodiment of the present invention; FIG. 5 is a schematic structural view of a LED chip process integration system according to a third embodiment of the present invention; FIG. 6 is a process integration of an LED chip according to a fourth embodiment of the present invention; FIG. 7 is a schematic structural diagram of an LED chip process integration system according to a fifth embodiment of the present invention; FIG. 8 is a schematic structural view of a LED chip process integration system according to a sixth embodiment of the present invention.
具体实施方式 detailed description
针对现有 LED基板的外延层沉积工艺的生产效率不高,使得 LED芯片的 生产效率和 LED芯片的产量较低,导致现有的 LED芯片的成本较高以及现有 的外延层沉积腔室的使用寿命和利用率较低的情况, 本发明提供一种 LED芯 片工艺集成系统, 包括:  The production efficiency of the epitaxial layer deposition process for the existing LED substrate is not high, so that the production efficiency of the LED chip and the output of the LED chip are low, resulting in high cost of the existing LED chip and the existing epitaxial layer deposition chamber. In the case of low service life and utilization, the present invention provides an LED chip process integration system, including:
装载卸载装置, 用于装载或卸载待处理的或处理完毕的 LED基板; 真空传输装置,用于提供真空传输环境以传输所述待处理的或处理完毕的 LED基板;  Loading and unloading device for loading or unloading the LED substrate to be processed or processed; vacuum conveying device for providing a vacuum transmission environment for transmitting the LED substrate to be processed or processed;
至少一个外延层沉积腔室,位于所述真空传输装置周沿, 所述外延层沉积 腔室用于对所述待处理的 LED基板进行外延层沉积;  At least one epitaxial layer deposition chamber is disposed at a periphery of the vacuum transmission device, and the epitaxial layer deposition chamber is configured to perform epitaxial layer deposition on the LED substrate to be processed;
至少一个预处理腔室, 用于对所述待处理的或处理完毕的 LED基板进行 预处理。  At least one pretreatment chamber for pretreating the LED substrate to be processed or processed.
下面将结合具体的实施例对本发明的技术方案进行详细的说明。 请参考图 2, 为本发明第一实施例的 LED芯片工艺集成系统结构示意图。 所述 LED芯片工艺集成系统 100包括: The technical solution of the present invention will be described in detail below with reference to specific embodiments. Please refer to FIG. 2 , which is a schematic structural diagram of an LED chip process integration system according to a first embodiment of the present invention. The LED chip process integration system 100 includes:
装载卸载装置 101 , 用于装载或卸载待处理的或处理完毕的 LED基板; 真空传输装置 104, 用于提供真空传输环境以传输所述待处理的或处理完 毕的 LED基板;  Loading and unloading device 101 for loading or unloading the LED substrate to be processed or processed; vacuum transmitting device 104 for providing a vacuum transmission environment for transmitting the LED substrate to be processed or processed;
至少一个外延层沉积腔室 102, 位于所述真空传输装置 104的周沿, 所述 外延层沉积腔室 102用于对所述待处理的 LED基板进行外延层沉积;  At least one epitaxial layer deposition chamber 102 is located at a periphery of the vacuum transfer device 104, and the epitaxial layer deposition chamber 102 is configured to perform epitaxial layer deposition on the LED substrate to be processed;
至少一个预处理腔室 103, 用于对所述待处理的或处理完毕的 LED基板 进行预处理。 At least one pretreatment chamber 103 is configured to pretreat the LED substrate to be processed or processed.
为了更好地说明本发明的 LED芯片工艺集成系统 100的工作过程, 请结 合图 3 , 图 3为本发明第一实施例的 LED芯片工艺集成系统的处理方法流程 示意图。 所述处理方法包括:  In order to better illustrate the operation of the LED chip process integration system 100 of the present invention, please refer to FIG. 3, which is a schematic flowchart of a processing method of the LED chip process integration system according to the first embodiment of the present invention. The processing method includes:
步骤 S1 , 将待处理的 LED基板放置于装载卸载装置;  Step S1, placing the LED substrate to be processed on the loading and unloading device;
步骤 S2,利用真空传输装置将所述待处理的 LED基板放置于预处理腔室; 步骤 S3 , 利用所述预处理腔室对所述待处理的 LED基板进行预处理; 步骤 S4, 将预处理后的所述 LED基板放置于外延层沉积腔室;  Step S2, the LED substrate to be processed is placed in the pre-processing chamber by using a vacuum transfer device; Step S3, pre-processing the LED substrate to be processed by using the pre-processing chamber; Step S4, pre-processing The latter LED substrate is placed in an epitaxial layer deposition chamber;
步骤 S5 , 在所述外延层沉积腔室中进行外延层沉积。  Step S5, performing epitaxial layer deposition in the epitaxial layer deposition chamber.
下面将结合 LED芯片工艺集成系统的处理方法对本发明的 LED芯片工艺 集成系统的结构进行详细的说明。  The structure of the LED chip process integration system of the present invention will be described in detail below in conjunction with the processing method of the LED chip process integration system.
发明人发现,现有的外延层沉积设备在进行外延层沉积工艺前, 需要在外 延层沉积腔室中对待处理的 LED基板进行预处理的步骤, 所述预处理包括加 热、 冷却或清洁处理等, 例如对所述待处理的 LED基板加热使得所述待处理 的 LED基板从室温达到进行外延层沉积的高温条件,所述室温的范围为 10~30 摄氏度, 所述高温的范围为 700~1300摄氏度; 在外延层沉积后, 需要对所述 处理完毕的 (即沉积了外延层的) LED基板进行冷却处理, 使得高温的 LED 基板的温度降为室温。但是现有的外延层沉积腔室价格昂贵, 利用其对所述待 处理的 LED基板进行预处理, 缺陷之一是设备成本大、 产量成本大, 因为这 样占用了所述外延层沉积腔室用于沉积外延层的时间,降低了所述外延层沉积 腔室的产量, 影响了 LED芯片的生产效率; 又一缺陷是由于外延层沉积腔室 的结构的限制,利用所述外延层沉积腔室进行加热处理的升温速率和进行冷却 处理的降温速率较慢, 以加热为例, 利用现有的外延层沉积腔室将 LED基板 从室温升至高温, 需要 15~40分钟, 占用了外延层沉积腔室用于沉积外延层的 时间; 再一缺陷是, 利用外延层沉积腔室进行加热和冷却处理容易损伤外延层 沉积腔室的寿命,需要投入人力、财力和时间对外延层沉积腔室进行维护保养, 从而降低了外延层沉积腔室的利用率。 The inventors have found that the existing epitaxial layer deposition apparatus requires a step of pretreating the LED substrate to be processed in the epitaxial layer deposition chamber before performing the epitaxial layer deposition process, the pretreatment including heating, cooling or cleaning treatment, etc. For example, heating the LED substrate to be processed causes the LED substrate to be processed to reach a high temperature condition for performing epitaxial layer deposition from room temperature, the room temperature ranges from 10 to 30 degrees Celsius, and the high temperature ranges from 700 to 1300. Celsius; After the epitaxial layer is deposited, the processed (ie, deposited epitaxial layer) LED substrate needs to be cooled to lower the temperature of the high temperature LED substrate to room temperature. However, the existing epitaxial layer deposition chamber is expensive, and the pretreatment of the LED substrate to be processed is utilized. One of the defects is that the equipment is costly and the production cost is large, because the epitaxial layer deposition chamber is occupied. During the deposition of the epitaxial layer, the yield of the epitaxial layer deposition chamber is reduced, which affects the production efficiency of the LED chip; another drawback is that the deposition chamber is deposited by the epitaxial layer due to the limitation of the structure of the epitaxial layer deposition chamber. Heating rate and cooling The cooling rate of the treatment is slow. Taking the heating as an example, using the existing epitaxial layer deposition chamber to raise the LED substrate from room temperature to high temperature takes 15 to 40 minutes, occupying the epitaxial layer deposition chamber for depositing the epitaxial layer. Time; another drawback is that the use of the epitaxial layer deposition chamber for heating and cooling treatment is likely to damage the life of the epitaxial layer deposition chamber, requiring labor, financial resources and time to maintain the epitaxial layer deposition chamber, thereby reducing the epitaxial layer Utilization of the deposition chamber.
针对上述缺陷, 发明人提出利用专门的腔室对 LED基板进行预处理, 即 利用本发明的预处理腔室 103对所述待处理的 LED基板进行预处理, 所述预 处理包括对所述待处理的 LED基板进行加热、 冷却或清洁处理。 本发明所述 的预处理腔室 103设置于外延层沉积腔室 102之外,其与所述外延层沉积腔室 102独立设置。 在保证所述预处理腔室 103位于所述外延层沉积腔室 102之外 的前提下,所述预处理腔室 103可以设置于所述真空传输装置 104的周沿或设 置于所述真空传输装置 104内。  In view of the above drawbacks, the inventors propose to pre-treat the LED substrate by using a special chamber, that is, pretreating the LED substrate to be processed by using the pre-processing chamber 103 of the present invention, the pre-processing including the waiting for the The processed LED substrate is subjected to heating, cooling or cleaning. The pretreatment chamber 103 of the present invention is disposed outside of the epitaxial layer deposition chamber 102, which is disposed independently of the epitaxial layer deposition chamber 102. The pretreatment chamber 103 may be disposed at a circumference of the vacuum transmission device 104 or disposed at the vacuum transmission on the premise that the pretreatment chamber 103 is located outside the epitaxial layer deposition chamber 102. Within device 104.
请继续参考图 2, 作为本发明的一个实施例, 所述预处理腔室 103设置于 所述真空传输装置 104的周沿。本发明所述的预处理腔室 103由于不需要具有 外延层沉积的功能, 因此其价格与所述外延层沉积腔室 102的价格相比较低, 具体地, 本发明所述的预处理腔室 103 的价格仅为所述外延层沉积腔室 102 价格的 1/15~1/20, 这样就可以减少成本, 并增加所述外延层沉积腔室 102进 行外延层沉积的时间,提高所述外延层沉积腔室 102的产量,提高所述外延层 沉积腔室 102的利用率。  With continued reference to FIG. 2, as an embodiment of the present invention, the pre-treatment chamber 103 is disposed at a periphery of the vacuum transfer device 104. The pretreatment chamber 103 of the present invention has a lower cost than the price of the epitaxial layer deposition chamber 102 because it does not need to have the function of epitaxial layer deposition. Specifically, the pretreatment chamber of the present invention The price of 103 is only 1/15~1/20 of the price of the epitaxial layer deposition chamber 102, so that the cost can be reduced, and the time for the epitaxial layer deposition chamber 102 to perform epitaxial layer deposition is increased, and the epitaxy is increased. The throughput of the layer deposition chamber 102 increases the utilization of the epitaxial layer deposition chamber 102.
作为本发明的一个实施例, 所述预处理腔室 103设置有加热台, 所述加热 台用于对所述待处理的 LED基板进行加热处理,使得所述待处理的 LED基板 从第一温度升至第二温度。所述第一温度范围为 10~30摄氏度,所述第二温度 通常应等于或接近所述外延层沉积腔室 102进行外延层沉积的温度。作为本发 明的一个实施例, 所述第二温度范围为 700~1300摄氏度。  As an embodiment of the present invention, the pre-processing chamber 103 is provided with a heating station for heating the LED substrate to be processed, so that the LED substrate to be processed is from the first temperature. Raise to the second temperature. The first temperature range is 10 to 30 degrees Celsius, and the second temperature should generally be equal to or close to the temperature at which the epitaxial layer deposition chamber 102 performs epitaxial layer deposition. As an embodiment of the present invention, the second temperature range is 700 to 1300 degrees Celsius.
作为本发明的一个实施例,所述预处理腔室 103上设置有至少一个进风口 和至少一个出风口,所述进风口用于通入还原性气体或保护性气体中的一种或 多种。 所述还原性气体或保护性气体用于对所述 LED基板进行清洁处理。  As an embodiment of the present invention, the pre-treatment chamber 103 is provided with at least one air inlet and at least one air outlet for introducing one or more of a reducing gas or a protective gas. . The reducing gas or protective gas is used to clean the LED substrate.
所述还原性气体在高温( 700~1300摄氏度 )时,可以将所述待处理的 LED 基板上的有机物还原为气体,通过所述出风口将所述气体排出而将所述有机物 去除。 作为一个实施例, 所述还原性气体可以为氢气、 氨气或氢气与氨气的混 合气体。 When the reducing gas is at a high temperature (700 to 1300 degrees Celsius), the organic matter on the LED substrate to be processed may be reduced to a gas, and the gas is discharged through the air outlet to remove the organic matter. As an embodiment, the reducing gas may be hydrogen, ammonia or a mixture of hydrogen and ammonia. Combined with gas.
所述保护性气体一方面可以去除所述待处理的 LED基板上的颗粒, 即将 所述待处理的 LED基板上的颗粒吹走, 并通过所述出风口排出, 另一方面可 以防止所述还原性气体的性质活泼而影响设备安全。在高温的情况下, 所述待 处理的 LED基板上的水蒸气和无机污染物由于挥发为气体, 因此, 所述水蒸 气和无机污染物也可以被去除。 所述保护性气体可以为惰性气体、 氮气或惰性 气体与氮气的混合气体。 所述惰性气体可以为氦气、 氩气、 氙气中的一种或氦 气、 氩气、 氙气中的两种的混合或氦气、 氩气、 氙气的混合气体。 作为优选的 实施例, 所述保护性气体优选为价格较低的氮气。  On the one hand, the protective gas can remove particles on the LED substrate to be processed, that is, the particles on the LED substrate to be processed are blown away and discharged through the air outlet, and on the other hand, the reduction can be prevented. The nature of the gas is lively and affects the safety of the equipment. In the case of high temperature, the water vapor and inorganic contaminants on the LED substrate to be treated are volatilized into a gas, and therefore, the water vapor and inorganic contaminants can also be removed. The protective gas may be an inert gas, nitrogen or a mixed gas of an inert gas and nitrogen. The inert gas may be one of helium, argon or helium or a mixture of two of helium, argon and helium or a mixture of helium, argon and helium. As a preferred embodiment, the protective gas is preferably a lower priced nitrogen gas.
需要说明的是, 所述进风口可以仅通入还原性气体或保护性气体,但是作 为优选的实施例,所述进风口通入的是所述还原性气体与保护性气体的混合气 体, 这样不仅可以去除所述待处理的 LED基板上的有机污染物、 无机污染物、 水蒸气等, 而且, 保证了设备的安全。 并且还原性气体的价格较高, 利用保护 性气体对还原性气体进行稀释, 在不影响去除有机污染物的前提下, 降低生产 成本。 因此优选地, 所述进风口通入还原性气体与保护性气体的混合气体, 例 如氢气与价格较低的氮气的混合气体或氨气与价格较低的氮气的混合气体。  It should be noted that the air inlet may only pass a reducing gas or a protective gas. However, as a preferred embodiment, the air inlet is provided with a mixed gas of the reducing gas and the protective gas. Not only the organic pollutants, inorganic pollutants, water vapor and the like on the LED substrate to be processed can be removed, but also the safety of the device is ensured. Moreover, the price of the reducing gas is high, and the reducing gas is diluted by the protective gas, and the production cost is lowered without affecting the removal of the organic pollutant. Therefore, preferably, the air inlet is supplied with a mixed gas of a reducing gas and a protective gas, for example, a mixed gas of hydrogen and a relatively low-priced nitrogen gas or a mixed gas of ammonia gas and a relatively low-priced nitrogen gas.
所述预处理腔室 103设置有温控装置,所述温控装置用于控制所述加热台 对所述待处理的 LED基板进行加热。 所述预处理腔室 103还可用于在对所述 待处理的 LED基板进行加热的同时,对所述待处理的 LED基板进行清洁处理。  The pretreatment chamber 103 is provided with a temperature control device for controlling the heating station to heat the LED substrate to be processed. The pre-processing chamber 103 can also be used to perform cleaning processing on the LED substrate to be processed while heating the LED substrate to be processed.
以加热和清洁处理为例, 具体地, 所述预处理腔室 103 对所述待处理的 Taking the heating and cleaning process as an example, specifically, the pre-processing chamber 103 is for the to-be-processed
LED基板进行的预处理包括: The pretreatment of the LED substrate includes:
利用所述预处理腔室 103 的温控装置控制所述加热台对所述待处理的 LED基板进行加热, 从而使得所述待处理的 LED基板的温度从第一温度升至 第二温度, 所述 LED加热所需时间范围为 5~15分钟, 优选为 8~13分钟, 例 如为 10分钟; 在所述待处理的 LED基板达到所述第二温度后, 所述预处理腔 室 103的温控装置控制所述加热台对所述待处理的 LED基板进行保温, 即使 得所述待处理的 LED基板保持所述温度一段时间 ,所述时间范围为 1~25分钟, 优选为 5~15分钟, 例如为 12分钟, 在所述待处理的 LED基板保持所述第二 温度时,所述预处理腔室 103的进风口通入所述还原性气体或保护性气体的一 种或多种 (例如氢气与氮气的混合气体或氨气与氮气的混合气体)。 需要说明的是, 上述过程中, 所述通风口也可以在所述待处理的 LED基 板的温度为第一温度时通入所述还原性气体或保护性气体的一种或多种,从而 同样产生了清洁所述待处理的 LED基板的效果, 但是仅在所述待处理的 LED 基板保持所述第二温度时通入所述还原性气体或保护性气体的一种或多种,节 约了气体用量, 降低了生产成本。 作为优选的实施例, 本发明所述的预处理腔 室 103在进行预处理步骤时,首先将所述待处理的 LED基板从 20摄氏度升至 950~1150摄氏度, 例如为 1050摄氏度, 所需时间为 5~15分钟, 例如为 10分 钟; 然后进行在所述高温下对所述待处理的 LED基板保温 1~25分钟, 例如为 5分钟或 15分钟, 并且在保温的同时通入氢气和氮气的混合气体(所述混合 气体中氢气与氮气的体积比例可以为 2%~50% ); 然后通过真空传输装置 104 传送至外延层沉积腔室 102, 进行外延层沉积。 Controlling, by the temperature control device of the pre-processing chamber 103, the heating station to heat the LED substrate to be processed, so that the temperature of the LED substrate to be processed is raised from the first temperature to the second temperature. The time required for heating the LED is in the range of 5 to 15 minutes, preferably 8 to 13 minutes, for example, 10 minutes; after the LED substrate to be processed reaches the second temperature, the temperature of the pretreatment chamber 103 The control device controls the heating station to insulate the LED substrate to be processed, that is, the LED substrate to be processed is kept at the temperature for a period of time, and the time range is 1 to 25 minutes, preferably 5 to 15 minutes. For example, for 12 minutes, when the LED substrate to be processed maintains the second temperature, the air inlet of the pre-treatment chamber 103 is introduced into one or more of the reducing gas or the protective gas ( For example, a mixed gas of hydrogen and nitrogen or a mixed gas of ammonia and nitrogen). It should be noted that, in the above process, the vent may also pass one or more of the reducing gas or the protective gas when the temperature of the LED substrate to be processed is the first temperature, so that Producing the effect of cleaning the LED substrate to be processed, but only one or more of the reducing gas or the protective gas is introduced when the LED substrate to be processed maintains the second temperature, saving The amount of gas used reduces production costs. As a preferred embodiment, the pre-processing chamber 103 of the present invention firstly raises the LED substrate to be processed from 20 degrees Celsius to 950 to 1150 degrees Celsius, for example, 1050 degrees Celsius, for the required time. 5 to 15 minutes, for example, 10 minutes; then, the LED substrate to be treated is kept at the high temperature for 1 to 25 minutes, for example, 5 minutes or 15 minutes, and hydrogen and nitrogen are introduced while being kept warm. The mixed gas (the volume ratio of hydrogen to nitrogen in the mixed gas may be 2% to 50%); and then transferred to the epitaxial layer deposition chamber 102 through the vacuum transfer device 104 to perform epitaxial layer deposition.
发明人考虑到, 由于所述外延层沉积腔室 102的沉积时间通常较长, 所述 时间范围通常为 0.5~6.5小时, 而预处理腔室 103的清洁处理时间范围通常为 10-40分钟。 若将外延层沉积腔室 102与预处理腔室 103的数目比例按照 1/1 设置, 则可能会使得部分 LED基板长时间地占用外延层沉积腔室 102, 而使 得经过所述预处理腔室 103清洁处理后的 LED基板没有对应的外延层沉积腔 室 102进行外延层沉积, 无法获得最大的 LED芯片的生产效率。 因此, 发明 人提出设置多个外延层沉积腔室 102, 具体为所述预处理腔室 103与所述外延 层沉积腔室 102的数目的比例小于 1/1 , 例如所述比例的范围可以为 1/2~1/5。  The inventors contemplate that since the deposition time of the epitaxial layer deposition chamber 102 is generally long, the time range is usually 0.5 to 6.5 hours, and the cleaning processing time of the pretreatment chamber 103 is usually in the range of 10 to 40 minutes. If the ratio of the number of epitaxial layer deposition chambers 102 to the pretreatment chambers 103 is set to 1/1, it may cause a portion of the LED substrate to occupy the epitaxial layer deposition chamber 102 for a long time, so that the pretreatment chamber passes through the pretreatment chamber. The LED substrate after the cleaning process has no corresponding epitaxial layer deposition chamber 102 for epitaxial layer deposition, and the maximum LED chip production efficiency cannot be obtained. Therefore, the inventors propose to provide a plurality of epitaxial layer deposition chambers 102, specifically the ratio of the number of the pre-treatment chambers 103 to the epitaxial layer deposition chambers 102 is less than 1/1, for example, the ratio may be in the range of 1/2~1/5.
发明人考虑到,增加所述外延层沉积腔室 102的数目, 可以加快对所述待 处理的 LED基板的处理速度, 但是由于外延层沉积腔室 102价格昂贵, 这样 也会增加 LED芯片工艺集成系统 100的成本, 因此, 发明人综合考虑 LED芯 片工艺集成系统的成本与导电层沉积工艺的生产效率 ,优选地设置所述预处理 腔室 103与所述外延层沉积腔室 102的数目的比例为 1/3。 由于本实施例中, 所述预处理腔室 103的数目为 1个, 因此对应的外延层沉积腔室 102的数目 为 3个。在上述的数目比例时, 可以用合理的成本获得较高的外延层沉积的生 产效率。  The inventors have considered that increasing the number of epitaxial layer deposition chambers 102 can speed up the processing speed of the LED substrate to be processed, but since the epitaxial layer deposition chamber 102 is expensive, this also increases LED chip process integration. The cost of the system 100, therefore, the inventors comprehensively consider the cost of the LED chip process integration system and the production efficiency of the conductive layer deposition process, preferably setting the ratio of the number of the pre-treatment chambers 103 to the number of epitaxial layer deposition chambers 102 It is 1/3. Since the number of the pre-processing chambers 103 is one in this embodiment, the number of corresponding epitaxial layer deposition chambers 102 is three. At the above ratio, the production efficiency of higher epitaxial layer deposition can be obtained at a reasonable cost.
在其他的实施例中,根据具体的应用需要, 所述预处理腔室 103与所述外 延层沉积腔室 102的数目比值还可以为其他的数值。  In other embodiments, the ratio of the number of pre-treatment chambers 103 to the epitaxial layer deposition chamber 102 may be other values, depending on the particular application.
作为本发明的优选实施例, 所述预处理腔室 103对所述 LED基板的预处 理还包括对处理后的 LED基板进行冷却处理。 本实施例中, 所述冷却处理为 将沉积了外延层的 LED基板从第二温度冷却为第一温度。 所述第二温度范围 为 700~1300摄氏度, 所述第一温度范围为 10~30摄氏度。 所述冷却处理通过 向所述外延层沉积腔室 102 内通入保护性气体, 利用保护性气体将处理后的 LED基板表面的热量带走, 相比于将所述 LED基板放置于所述外延层沉积腔 室 102进行冷却,提高了外延层沉积腔室 102进行外延层沉积的时间,提高了 外延层沉积工艺的效率; 相比于所述沉积了外延层的 LED基板放置于洁净室 或真空传输装置进行冷却, 提高了冷却的速度。 As a preferred embodiment of the present invention, the pre-processing chamber 103 pre-places the LED substrate The method further includes cooling the processed LED substrate. In this embodiment, the cooling process is to cool the LED substrate on which the epitaxial layer is deposited from the second temperature to the first temperature. The second temperature range is 700 to 1300 degrees Celsius, and the first temperature range is 10 to 30 degrees Celsius. The cooling treatment removes heat from the surface of the processed LED substrate by using a protective gas by introducing a protective gas into the epitaxial layer deposition chamber 102, compared to placing the LED substrate on the epitaxial layer. The deposition of the layer deposition chamber 102 increases the time for the epitaxial layer deposition chamber 102 to perform epitaxial layer deposition, and improves the efficiency of the epitaxial layer deposition process; the LED substrate deposited in the epitaxial layer is placed in a clean room or vacuum The conveyor is cooled to increase the rate of cooling.
请继续参考图 2, 作为本发明的优选实施例, 所述真空传输装置 104的形 状为线性, 所述装载卸载装置 101、 预处理腔室 103、 外延层沉积腔室 102线 性排布于所述真空传输装置 104的周沿。  With continued reference to FIG. 2, as a preferred embodiment of the present invention, the vacuum transmission device 104 is linear in shape, and the loading and unloading device 101, the pretreatment chamber 103, and the epitaxial layer deposition chamber 102 are linearly arranged in the The periphery of the vacuum transfer device 104.
具体地, 所述真空传输装置 104为一密封的腔体, 并至少设置有真空泵、 机械手臂和至少 3个密封门, 每一密封门分别对应与所述装载卸载装置 101、 预处理腔室 103、 外延层沉积腔室 102, 所述密封门作为 LED基板从所述装载 卸载装置 101、 预处理腔室 103、 外延层沉积腔室 102传输至所述真空传输装 置的通道。 以待处理的 LED基板放置于所述装载卸载装置 101为例, 与所述 装载卸载装置 101相对应的密封门打开, 机械手臂将所述待处理的 LED基板 从所述装载卸载装置 101取出, 然后, 所述密封门闭合, 所述真空泵对所述真 空传输装置 104进行抽真空,使得所述真空传输装置 104的腔体满足一定的真 空度, 然后, 所述机械手臂将所述待处理的 LED基板移至所述真空传输装置 104的与所述预处理腔室 103对应的密封门处, 接着, 将所述密封门打开, 并 将所述待处理的 LED基板放置于所述预处理腔室 103内, 在所述预处理腔室 103 内对所述待处理的 LED基板进行加热和清洁后, 利用与上述方法相同的 方法将所述待处理的 LED基板传送至所述外延层沉积腔室 102。  Specifically, the vacuum transmission device 104 is a sealed cavity, and at least is provided with a vacuum pump, a robot arm and at least three sealing doors, and each sealing door corresponds to the loading and unloading device 101 and the pre-processing chamber 103, respectively. An epitaxial layer deposition chamber 102 is used as a channel for the LED substrate to be transferred from the loading and unloading device 101, the pretreatment chamber 103, and the epitaxial layer deposition chamber 102 to the vacuum transmission device. Taking the LED substrate to be processed placed on the loading and unloading device 101 as an example, a sealing door corresponding to the loading and unloading device 101 is opened, and the robot arm takes out the LED substrate to be processed from the loading and unloading device 101. Then, the sealing door is closed, the vacuum pump vacuums the vacuum transmission device 104, so that the cavity of the vacuum transmission device 104 satisfies a certain degree of vacuum, and then the robot arm will treat the to-be-processed Moving the LED substrate to a sealed door of the vacuum transfer device 104 corresponding to the pre-treatment chamber 103, and then opening the sealed door, and placing the LED substrate to be processed in the pre-treatment chamber In the chamber 103, after the LED substrate to be processed is heated and cleaned in the pre-processing chamber 103, the LED substrate to be processed is transferred to the epitaxial layer deposition chamber by the same method as described above. Room 102.
作为一个实施例, 所述装载卸载装置 101、 预处理腔室 103、 外延层沉积 腔室 102线性排布于所述真空传输装置 104的两侧,采用线性排布有利于提高 LED芯片工艺集成系统 100的集成度, 减小占用的洁净室的空间, 从而降低 洁净室的成本, 减小 LED芯片制造的成本。  As an embodiment, the loading and unloading device 101, the pre-processing chamber 103, and the epitaxial layer deposition chamber 102 are linearly arranged on both sides of the vacuum transmission device 104, and the linear arrangement is beneficial to improve the LED chip process integration system. The integration of 100 reduces the space occupied by the clean room, thereby reducing the cost of the clean room and reducing the cost of manufacturing the LED chip.
较为优选地, 请参考图 2, 所述装载卸载装置 101、 预处理腔室 103位于 所述真空传输装置 104的一侧,所述外延层沉积腔室 102位于所述真空传输装 置 104的与所述装载卸载装置 101、 预处理腔室 103相对的另一侧。 所述真空传输装置 104提供的真空传输环境用于传输待处理的或处理完 毕的 LED基板,从而使得所述 LED基板在所述预处理腔室 103和外延层沉积 腔室 102之间的传输环境为真空环境, 从而避免了所述 LED基板暴露于洁净 室中而受到洁净室中的污染物的污染,提高了所述外延层沉积腔室 102中沉积 的外延层与所述 LED基板之间的粘附性,防止由于污染物的污染使得 LED芯 片失效或影响 LED芯片的良率。 Preferably, referring to FIG. 2, the loading and unloading device 101, the pre-processing chamber 103 is located at one side of the vacuum transmission device 104, and the epitaxial layer deposition chamber 102 is located at the vacuum transmission device. The other side of the 104 is opposite the loading and unloading device 101 and the pretreatment chamber 103. The vacuum transmission device 104 provides a vacuum transmission environment for transporting the LED substrate to be processed or processed, thereby causing a transmission environment between the pretreatment chamber 103 and the epitaxial layer deposition chamber 102. The vacuum environment prevents the LED substrate from being exposed to the clean room and is contaminated by contaminants in the clean room, thereby improving the between the epitaxial layer deposited in the epitaxial layer deposition chamber 102 and the LED substrate. Adhesion prevents failure of the LED chip due to contamination of the contaminant or affects the yield of the LED chip.
所述外延层沉积腔室 102进行外延层沉积。所述外延层为多层结构, 本实 施例,所述外延层是由 N型 GaN层、多量子阱有源层和 P型 GaN层堆叠成的 多层结构。 因此, 所述外延层沉积腔室 102需要在待处理的 LED基板上沉积 N型 GaN层、 多量子阱有源层和 P型 GaN层。 所述外延层沉积腔室 102沉积 外延层的温度范围为 700~1300摄氏度。  The epitaxial layer deposition chamber 102 performs epitaxial layer deposition. The epitaxial layer is a multi-layered structure. In this embodiment, the epitaxial layer is a multi-layered structure in which an N-type GaN layer, a multiple quantum well active layer, and a P-type GaN layer are stacked. Therefore, the epitaxial layer deposition chamber 102 needs to deposit an N-type GaN layer, a multiple quantum well active layer, and a P-type GaN layer on the LED substrate to be processed. The epitaxial layer deposition chamber 102 deposits an epitaxial layer at a temperature ranging from 700 to 1300 degrees Celsius.
需要说明的是,作为本发明的一个实施例, 可以利用一个外延层沉积腔室 102沉积所述 N型 GaN层、 多量子阱有源层和 P型 GaN层。  It should be noted that, as an embodiment of the present invention, the N-type GaN layer, the multiple quantum well active layer, and the P-type GaN layer may be deposited using an epitaxial layer deposition chamber 102.
在本发明的其他的实施例中,当所述外延层沉积腔室 102的数目大于等于 In other embodiments of the invention, when the number of epitaxial layer deposition chambers 102 is greater than or equal to
3个时, 至少包括: N型 GaN层沉积腔室、 多量子阱有源层沉积腔室和 P型 GaN层沉积腔室。 其中所述 N型 GaN层沉积腔室用于沉积 N型 GaN层, 所 述多量子阱有源层沉积腔室用于沉积多量子阱有源层, 所述 P型 GaN层沉积 腔室用于沉积 P型 GaN层, 所述 N型 GaN层、 多量子阱有源层和 P型 GaN 层构成所述外延层。 所述 N型 GaN层沉积腔室、 多量子阱有源层沉积腔室和 P型 GaN层沉积腔室可以设置独立的源材料供给装置, 所述源材料供给装置 用于提供源材料, 形成与所述源材料相对应的薄膜层, 这样可以避免多种源材 料之间的交叉污染。 所述 N型 GaN层沉积腔室、 多量子阱有源层沉积腔室和 P型 GaN层沉积腔室可以设置独立的加热台和温控装置,便于每一薄膜层(N 型 GaN层、 多量子阱有源层或 P型 GaN层)的沉积腔室 102的温控装置独立 控制所述加热台独立对 LED基板进行加热, 有利于根据每一薄膜层沉积腔室 102进行独立的温度控制。 所述 N型 GaN层沉积腔室、 多量子阱有源层沉积 腔室和 P型 GaN层沉积腔室沉积的薄膜层不同,从而对应的所述 N型 GaN层 沉积腔室、 多量子阱有源层沉积腔室和 P型 GaN层沉积腔室的温度不同, 使 得所述 N型 GaN层沉积腔室、多量子阱有源层沉积腔室和 P型 GaN层沉积腔 室的温度仅需要设置为一个相对固定的温度,避免了利用一个外延层沉积腔室 沉积多种薄膜层的温度需要反复调整, 从而节约了工艺时间, 并且由于所述 N 型 GaN层沉积腔室、 多量子阱有源层沉积腔室的温度相对稳定, 从而可有利 于提高所述 N型 GaN层沉积腔室、 多量子阱有源层沉积腔室的在不同的 LED 基板上沉积的相应的薄膜层( N型 GaN层、 多量子阱有源层或 P型 GaN层 ) 的均匀度。 At least three, at least: an N-type GaN layer deposition chamber, a multiple quantum well active layer deposition chamber, and a P-type GaN layer deposition chamber. Wherein the N-type GaN layer deposition chamber is for depositing an N-type GaN layer, the multiple quantum well active layer deposition chamber is for depositing a multiple quantum well active layer, and the P-type GaN layer deposition chamber is used for A P-type GaN layer is deposited, and the N-type GaN layer, the multiple quantum well active layer, and the P-type GaN layer constitute the epitaxial layer. The N-type GaN layer deposition chamber, the multiple quantum well active layer deposition chamber, and the P-type GaN layer deposition chamber may be provided with independent source material supply devices for providing source materials, forming and The film material corresponding to the source material can avoid cross-contamination between the plurality of source materials. The N-type GaN layer deposition chamber, the multiple quantum well active layer deposition chamber, and the P-type GaN layer deposition chamber may be provided with independent heating stages and temperature control devices for each thin film layer (N-type GaN layer, multiple The temperature control device of the deposition chamber 102 of the quantum well active layer or the P-type GaN layer independently controls the heating station to independently heat the LED substrate, facilitating independent temperature control according to each of the thin film layer deposition chambers 102. The N-type GaN layer deposition chamber, the multiple quantum well active layer deposition chamber, and the P-type GaN layer deposition chamber deposit different film layers, so that the corresponding N-type GaN layer deposition chamber and the multiple quantum wells have The temperature of the source layer deposition chamber and the P-type GaN layer deposition chamber are different, such that the N-type GaN layer deposition chamber, the multiple quantum well active layer deposition chamber, and the P-type GaN layer deposition chamber The temperature of the chamber only needs to be set to a relatively fixed temperature, avoiding the need to repeatedly adjust the temperature of depositing various thin film layers by using one epitaxial layer deposition chamber, thereby saving process time, and due to the N-type GaN layer deposition chamber The temperature of the multiple quantum well active layer deposition chamber is relatively stable, thereby facilitating the corresponding deposition of the N-type GaN layer deposition chamber and the multiple quantum well active layer deposition chamber on different LED substrates. Uniformity of the thin film layer (N-type GaN layer, multiple quantum well active layer or P-type GaN layer).
作为一个实施例, 请结合图 2, 本发明的 LED芯片工艺集成系统的处理 方法具体为:  As an embodiment, with reference to FIG. 2, the processing method of the LED chip process integration system of the present invention is specifically as follows:
首先, 提供待处理的 LED基板, 将所述待处理的 LED基板放置于所述装 载卸载装置 101 ;  First, providing an LED substrate to be processed, and placing the LED substrate to be processed on the loading and unloading device 101;
然后, 利用所述真空传输装置 104将所述待处理的 LED基板传送到达所 述预处理腔室 103 , 由所述预处理腔室 103对所述待处理的 LED基板进行加 热和清洁处理,加热和清洁处理的原理以及方法请参考本实施例关于预处理腔 室 103的描述,在此不做详细的说明, 经过加热和清洁处理后的所述待处理的 LED基板表面清洁,并具有一定的温度,所述温度的范围为 700~1300摄氏度, 所述温度可以与外延层沉积工艺的温度对应, 例如所述温度可以为 1050摄氏 度;  Then, the LED substrate to be processed is transferred to the pre-processing chamber 103 by the vacuum transmission device 104, and the LED substrate to be processed is heated and cleaned by the pre-processing chamber 103, and heated. For the principle and method of the cleaning process, please refer to the description of the pretreatment chamber 103 in this embodiment. Without detailed description, the surface of the LED substrate to be processed after being heated and cleaned is clean and has a certain degree. a temperature, the temperature ranges from 700 to 1300 degrees Celsius, and the temperature may correspond to a temperature of the epitaxial layer deposition process, for example, the temperature may be 1050 degrees Celsius;
然后, 所述真空传输装置 104将所述加热和清洁处理后的待处理的 LED 基板传送到达所述外延层沉积腔室 102, 由所述外延层沉积腔室 102进行外延 层沉积, 外延层沉积的参数将在后续进行详细地说明;  Then, the vacuum transfer device 104 transfers the heated and cleaned LED substrate to be processed to the epitaxial layer deposition chamber 102, and the epitaxial layer deposition chamber 102 performs epitaxial layer deposition, epitaxial layer deposition. The parameters will be explained in detail later;
接着,利用所述真空传输装置 104将处理完毕的(即沉积了外延层的)LED 基板传送至所述预处理腔室 103 , 由所述预处理腔室 103 对所述处理完毕的 LED基板进行冷却处理,本实施例中, 所述冷却处理为从第二温度 ( 700-1300 摄氏度)冷却至第一温度, 所需的冷却时间范围为 1~25分钟, 优选为 10~15 分钟;  Then, the processed (ie, deposited epitaxial layer) LED substrate is transferred to the pre-processing chamber 103 by the vacuum transfer device 104, and the processed LED substrate is performed by the pre-processing chamber 103. Cooling treatment, in this embodiment, the cooling treatment is to cool from the second temperature (700-1300 degrees Celsius) to the first temperature, and the required cooling time ranges from 1 to 25 minutes, preferably 10 to 15 minutes;
最后, 所述真空传输装置 104将所述处理完毕的 LED基板传送至装载卸 载装置 101。  Finally, the vacuum transfer device 104 transfers the processed LED substrate to the load unloading device 101.
本发明所述的外延层可以利用一个外延层沉积腔室 102形成 N型 GaN层、 多量子阱有源层和 P型 GaN层, 也可以利用 3个外延层沉积腔室分别形成 N 型 GaN层、 多量子阱有源层和 P型 GaN层。 当利用一个外延层沉积腔室 102形成所述外延层时,所述外延层沉积腔室 102进行 N型 GaN层沉积、 多量子阱有源层沉积和 P型 GaN沉积。 其中: 所述外延层沉积腔室 102形成所述 N型 GaN层的温度范围为 700~1300 摄氏度, 优选为 1000~1300摄氏度, 优选为 1000~1150摄氏度, 例如为 1100 摄氏度或 1050摄氏度; 时间范围为 100~200分钟, 优选为 100~150分钟, 例 如为 100分钟、 125分钟或 150分钟; 形成的所述 N型 GaN层的厚度范围为 l~3 米, 优选为 l~2 米, 例如为 1 敫米或2敫米; 例如, 当所述 N型 GaN 层的沉积温度为 1050摄氏度, 时间为 120分钟时, 对应的形成的 N型 GaN 层的厚度为 1.5微米; The epitaxial layer of the present invention may form an N-type GaN layer, a multiple quantum well active layer and a P-type GaN layer by using an epitaxial layer deposition chamber 102, or may form an N-type GaN layer by using three epitaxial layer deposition chambers respectively. , a multiple quantum well active layer and a P-type GaN layer. When the epitaxial layer is formed using an epitaxial layer deposition chamber 102, the epitaxial layer deposition chamber 102 performs N-type GaN layer deposition, multiple quantum well active layer deposition, and P-type GaN deposition. Wherein: the temperature of the N-type GaN layer formed by the epitaxial layer deposition chamber 102 ranges from 700 to 1300 degrees Celsius, preferably from 1000 to 1300 degrees Celsius, preferably from 1000 to 1150 degrees Celsius, for example, 1100 degrees Celsius or 1050 degrees Celsius; It is 100 to 200 minutes, preferably 100 to 150 minutes, for example, 100 minutes, 125 minutes or 150 minutes; the thickness of the N-type GaN layer formed ranges from 1 to 3 meters, preferably from 1 to 2 meters, for example 1 敫米或2敫米; For example, when the deposition temperature of the N-type GaN layer is 1050 degrees Celsius, the time is 120 minutes, the corresponding formed N-type GaN layer has a thickness of 1.5 microns;
所述外延层沉积腔室 102 形成所述多量子阱有源层的温度范围为 The temperature range of the epitaxial layer deposition chamber 102 forming the multiple quantum well active layer is
700~1300摄氏度, 优选为 700~800摄氏度, 时间范围为 30~80分钟, 优选为 40~50分钟, 形成的多量子阱有源层的厚度范围为 600~900埃, 优选 700~800 埃; 例如, 当所述多量子阱有源层的沉积温度为 750摄氏度, 时间为 40分钟 时, 对应的形成的 N型 GaN层的厚度为 750埃; 700~1300 degrees Celsius, preferably 700~800 degrees Celsius, the time range is 30-80 minutes, preferably 40-50 minutes, and the formed multi-quantum well active layer has a thickness ranging from 600 to 900 angstroms, preferably 700-800 angstroms; For example, when the deposition temperature of the multiple quantum well active layer is 750 degrees Celsius and the time is 40 minutes, the corresponding formed N-type GaN layer has a thickness of 750 angstroms;
所述外延层沉积腔室 102形成所述 P型 GaN层的温度范围为 800~1000摄 氏度,优选为 850~950摄氏度,例如为 800摄氏度、 900摄氏度或 950摄氏度, 时间范围为 20~80分钟, 优选为 20~30分钟, 形成的 P型 GaN层的厚度范围 为 0.2~0.6微米, 优选为 0.3~0.5微米; 例如, 当所述多 P型 GaN层的沉积温 度为 900摄氏度, 时间为 25分钟时, 对应的形成的 N型 GaN层的厚度为 0.4 微米。  The epitaxial layer deposition chamber 102 forms the P-type GaN layer in a temperature range of 800 to 1000 degrees Celsius, preferably 850 to 950 degrees Celsius, for example, 800 degrees Celsius, 900 degrees Celsius or 950 degrees Celsius, and the time range is 20 to 80 minutes. Preferably, the thickness of the P-type GaN layer formed is in the range of 0.2 to 0.6 μm, preferably 0.3 to 0.5 μm; for example, when the deposition temperature of the multi-P-type GaN layer is 900 ° C, the time is 25 minutes. The corresponding formed N-type GaN layer has a thickness of 0.4 μm.
当分别利用 3个外延层沉积腔室沉积外延层时,所述 3个外延层沉积腔室 102分别为 N型 GaN层沉积腔室、 多量子阱有源层沉积腔室和 P型 GaN层沉 积腔室沉积。 所述 N型 GaN层沉积腔室形成 N型 GaN层的工艺参数、 多量 子阱有源层沉积腔室形成多量子阱有源层外延层的工艺参数和 P型 GaN层沉 积腔室形成 P型 GaN层的工艺参数请参考本发明所述的利用一个外延沉积腔 室 102形成外延层的参数, 在此不做赘述。  When the epitaxial layers are deposited by using three epitaxial layer deposition chambers respectively, the three epitaxial layer deposition chambers 102 are respectively an N-type GaN layer deposition chamber, a multiple quantum well active layer deposition chamber, and a P-type GaN layer deposition. The chamber is deposited. The N-type GaN layer deposition chamber forms a process parameter of the N-type GaN layer, the multi-quantum well active layer deposition chamber forms a process parameter of the multi-quantum well active layer epitaxial layer, and the P-type GaN layer deposition chamber forms a P-type For the process parameters of the GaN layer, please refer to the parameters of the epitaxial layer formed by using an epitaxial deposition chamber 102, which will not be described herein.
请参考图 4, 图 4为本发明第二实施例的 LED芯片工艺集成系统结构示 意图, 其中与第一实施例相同的结构以相同的标号标出。 所述 LED芯片工艺 集成系统 100包括:  Referring to FIG. 4, FIG. 4 is a schematic structural view of a process integration system for an LED chip according to a second embodiment of the present invention, wherein the same structures as those of the first embodiment are denoted by the same reference numerals. The LED chip process integration system 100 includes:
装载卸载装置 101 , 用于装载或卸载待处理的或处理完毕的 LED基板; 真空传输装置 104, 用于提供真空传输环境以传输所述待处理的或处理完 毕的 LED基板; Loading and unloading device 101 for loading or unloading the LED substrate to be processed or processed; a vacuum transmission device 104, configured to provide a vacuum transmission environment to transmit the LED substrate to be processed or processed;
至少一个外延层沉积腔室 102, 位于所述真空传输装置 104的周沿, 所述 外延层沉积腔室 102用于对所述待处理的 LED基板进行外延层沉积;  At least one epitaxial layer deposition chamber 102 is located at a periphery of the vacuum transfer device 104, and the epitaxial layer deposition chamber 102 is configured to perform epitaxial layer deposition on the LED substrate to be processed;
至少一个预处理腔室 103 , 用于对所述待处理的或处理完毕的 LED基板 进行预处理; 导电层沉积腔室 105 , 位于所述真空传输装置 104和外延层沉积 腔室 102的周沿, 所述导电层沉积腔室 105用于沉积导电层。  At least one pre-processing chamber 103 for pre-treating the processed or processed LED substrate; a conductive layer deposition chamber 105 located at a periphery of the vacuum transfer device 104 and the epitaxial layer deposition chamber 102 The conductive layer deposition chamber 105 is used to deposit a conductive layer.
本实施例中与第一实施例的区别在于所述 LED芯片工艺集成系统增加了 导电层沉积腔室 105 , 其余结构与第一实施例相同, 具体请参考第一实施例的 描述, 在此不做赘述。  The difference between the embodiment and the first embodiment is that the LED chip process integration system adds the conductive layer deposition chamber 105, and the rest of the structure is the same as that of the first embodiment. For details, please refer to the description of the first embodiment. Make a statement.
所述导电层沉积腔室 105用于在 LED基板上导电层, 所述导电层的材质 可以为金属层或透明导电层, 所述金属层为金镍合金、金钛合金或其他金属中 的一种或多种, 所述透明导电层包括 ITO、 ΖηΟ中的一种或多种。  The conductive layer deposition chamber 105 is used for conducting a conductive layer on the LED substrate, and the conductive layer may be made of a metal layer or a transparent conductive layer, and the metal layer is one of a gold-nickel alloy, a gold-titanium alloy or another metal. The transparent conductive layer comprises one or more of ITO and ΖηΟ.
由于增加了所述导电层沉积腔室 105 , 使得 LED芯片工艺集成系统将外 延层沉积工艺和导电层沉积工艺集成在同一系统内, 从而 LED基板在外延层 沉积腔室 102和导电层沉积腔室 105之间的传输为真空传输, 无需将 LED基 板移至洁净室, 避免了 LED基板受到污染, 并且无需反复的抽真空的动作。  Since the conductive layer deposition chamber 105 is added, the LED chip process integration system integrates the epitaxial layer deposition process and the conductive layer deposition process in the same system, thereby the LED substrate is deposited in the epitaxial layer chamber 102 and the conductive layer deposition chamber. The transmission between the 105 is vacuum transmission, eliminating the need to move the LED substrate to the clean room, avoiding contamination of the LED substrate, and eliminating the need for repeated vacuuming.
较为优选地,所述导电层沉积腔室 105排布于所述真空传输装置 104的与 所述外延层沉积腔室 102相对的一侧。  More preferably, the conductive layer deposition chamber 105 is disposed on a side of the vacuum transfer device 104 opposite to the epitaxial layer deposition chamber 102.
由于所述导电层沉积腔室 105的沉积时间范围为 10~40分钟,而所述外延 层沉积腔室 102的沉积时间范围为 0.5~6.5小时, 导电层沉积腔室 105的沉积 时间较短而外延层沉积腔室 102 的沉积时间较长, 从而使得导电层沉积腔室 105可能存在利用率不足的问题, 因此发明人对导电层沉积腔室 105的数目进 行了优化,以提高所述导电层沉积腔室 105的利用率,并且提高本发明的 LED 芯片工艺集成系统的集成度和 LED芯片的生产效率。 具体地, 所述外延层沉 积腔室 102的数目与导电层沉积腔室 105的数目的比例范围为 2/1~12/1 ,较为 优选地为 4/1~12/1 , 例如所述比例可以为 8/1~12/1。  Since the deposition time of the conductive layer deposition chamber 105 ranges from 10 to 40 minutes, and the deposition time of the epitaxial layer deposition chamber 102 ranges from 0.5 to 6.5 hours, the deposition time of the conductive layer deposition chamber 105 is shorter. The deposition time of the epitaxial layer deposition chamber 102 is long, so that the conductive layer deposition chamber 105 may have a problem of insufficient utilization, so the inventors optimized the number of the conductive layer deposition chambers 105 to improve the conductive layer. The utilization rate of the deposition chamber 105 is increased, and the integration degree of the LED chip process integration system of the present invention and the production efficiency of the LED chip are improved. Specifically, the ratio of the number of the epitaxial layer deposition chambers 102 to the number of the conductive layer deposition chambers 105 ranges from 2/1 to 12/1, more preferably from 4/1 to 12/1, for example, the ratio Can be 8/1~12/1.
为了进一步提高生产效率,在本实施例中, 所述外延层沉积腔室 102与所 述导电层沉积腔室 105分别设置有独立的排气系统。在其他的实施例中, 所述 外延层沉积腔室 102还可以与所述导电层沉积腔室 105共用排气系统。 当采用本实施例的 LED芯片工艺集成系统时,其对 LED基板的处理方法 包括: In order to further improve the production efficiency, in the embodiment, the epitaxial layer deposition chamber 102 and the conductive layer deposition chamber 105 are respectively provided with independent exhaust systems. In other embodiments, the epitaxial layer deposition chamber 102 may also share an exhaust system with the conductive layer deposition chamber 105. When the LED chip process integration system of the embodiment is used, the method for processing the LED substrate includes:
将所述待处理的 LED基板放置于所述装载卸载装置 101 ;  Place the LED substrate to be processed on the loading and unloading device 101;
利用所述真空传输装置 104将所述待处理的 LED基板放置于所述预处理 腔室 103;  Using the vacuum transfer device 104, the LED substrate to be processed is placed in the pretreatment chamber 103;
所述预处理腔室 103对所述待处理的 LED基板进行加热和清洁处理, 使 得加热和清洁处理后的所述待处理的 LED基板表面清洁、 具有一定的温度, 所述温度范围为 700~1300摄氏度, 具体与外延层沉积工艺的温度对应, 本实 施例中, 所述温度为 1100摄氏度或 1050摄氏度;  The pre-processing chamber 103 heats and cleans the LED substrate to be processed, so that the surface of the LED substrate to be processed after the heating and cleaning process is clean and has a certain temperature, and the temperature range is 700~ 1300 degrees Celsius, specifically corresponding to the temperature of the epitaxial layer deposition process, in this embodiment, the temperature is 1100 degrees Celsius or 1050 degrees Celsius;
所述真空传输装置 104将所述待处理的 LED基板放置于所述外延层沉积 腔室 102, 进行外延层沉积;  The vacuum transfer device 104 places the LED substrate to be processed in the epitaxial layer deposition chamber 102 for epitaxial layer deposition;
所述真空传输装置 104将处理后 (即沉积了外延层) 的 LED基板放置于 所述预处理腔室 103;  The vacuum transfer device 104 places the processed (i.e., deposited epitaxial layer) LED substrate in the pretreatment chamber 103;
所述预处理腔室 103对所述 LED基板进行第一冷却, 所述第一冷却具体 为将所述沉积了外延层的 LED基板从第二温度降低为第三温度, 所述第二温 度为进行外延层沉积工艺的温度, 所述第二温度的范围为 700~1100摄氏度, 例如为 1100摄氏度或 1050摄氏度,所述第三温度为进行导电层沉积工艺的温 度, 例如为 100~400摄氏度, 优选为 150~350摄氏度;  The pre-processing chamber 103 performs a first cooling on the LED substrate, and the first cooling is specifically to reduce the LED substrate on which the epitaxial layer is deposited from a second temperature to a third temperature, and the second temperature is a temperature at which the epitaxial layer deposition process is performed, the second temperature ranges from 700 to 1100 degrees Celsius, for example, 1100 degrees Celsius or 1050 degrees Celsius, and the third temperature is a temperature at which the conductive layer deposition process is performed, for example, 100 to 400 degrees Celsius. Preferably 150 to 350 degrees Celsius;
所述真空传输装置 104将所述第一冷却处理后的 LED基板放置于所述导 电层沉积腔室 105;  The vacuum transfer device 104 places the first cooled LED substrate in the conductive layer deposition chamber 105;
所述导电层沉积腔室 105在所述第一冷却处理后的 LED基板的外延层上 沉积导电层;  The conductive layer deposition chamber 105 deposits a conductive layer on the epitaxial layer of the first cooled LED substrate;
所述真空传输装置 104将处理完毕的 (即沉积了导电层) 的所述 LED基 板放置于所述预处理腔室 103;  The vacuum transfer device 104 places the processed (i.e., deposited conductive layer) LED substrate in the pretreatment chamber 103;
所述预处理腔室 103对所述处理完毕的 LED基板进行第二冷却, 所述第 二冷却为将所述 LED基板从导电层沉积时的第三温度降低为第一温度;  The pre-processing chamber 103 performs second cooling on the processed LED substrate, and the second cooling is to reduce the third temperature when the LED substrate is deposited from the conductive layer to a first temperature;
所述真空传输装置 104所述第二冷却处理后的 LED基板传送至装载卸载 装置, 完成外延层和导电层沉积工艺。  The vacuum transfer device 104 transfers the second cooled LED substrate to a loading and unloading device to complete an epitaxial layer and a conductive layer deposition process.
下面请参考图 5 , 图 5是本发明第三实施例的 LED芯片工艺集成系统结 构示意图, 其中与第一实施例和第二实施例中相同的结构采用相同的标号。所 述 LED芯片工艺集成系统 100包括: Referring to FIG. 5, FIG. 5 is a schematic structural diagram of an LED chip process integration system according to a third embodiment of the present invention, wherein the same structures as those in the first embodiment and the second embodiment are given the same reference numerals. Place The LED chip process integration system 100 includes:
装载卸载装置 101 , 用于装载或卸载待处理的或处理完毕的 LED基板; 真空传输装置 104, 用于提供真空传输环境以传输所述待处理的或处理完 毕的 LED基板;  Loading and unloading device 101 for loading or unloading the LED substrate to be processed or processed; vacuum transmitting device 104 for providing a vacuum transmission environment for transmitting the LED substrate to be processed or processed;
至少一个外延层沉积腔室 102, 位于所述真空传输装置 104的周沿, 所述 外延层沉积腔室 102用于对所述待处理的 LED基板进行外延层沉积;  At least one epitaxial layer deposition chamber 102 is located at a periphery of the vacuum transfer device 104, and the epitaxial layer deposition chamber 102 is configured to perform epitaxial layer deposition on the LED substrate to be processed;
至少一个预处理腔室 103, 用于对所述待处理的或处理完毕的 LED基板 进行预处理; At least one pretreatment chamber 103 for pretreating the LED substrate to be processed or processed;
导电层沉积腔室 105 , 位于所述真空传输装置 104和外延层沉积腔室 102 的周沿, 所述导电层沉积腔室 105用于沉积导电层。  A conductive layer deposition chamber 105 is located at a periphery of the vacuum transfer device 104 and the epitaxial layer deposition chamber 102 for depositing a conductive layer.
本实施例与第二实施例的区别在于, 所述真空传输装置的形状为多边形, 所述预处理腔室 103、 装载卸载装置 101、 外延层沉积腔室 102和导电层沉积 腔室 105排布于所述真空传输装置 104周沿。在其他的实施例中, 所述真空传 输装置的形状也可以为圆形、 椭圆形、 梯形、 菱形或其他多边形。  The difference between this embodiment and the second embodiment is that the vacuum transmission device has a polygonal shape, and the pretreatment chamber 103, the loading and unloading device 101, the epitaxial layer deposition chamber 102, and the conductive layer deposition chamber 105 are arranged. At the periphery of the vacuum transmission device 104. In other embodiments, the vacuum transfer device may also be circular, elliptical, trapezoidal, rhombic or other polygonal shape.
具体地, 请参考图 5 , 所述预处理腔室 103与所述真空传输装置 104相连 接, 所述导电层沉积腔室 105与所述预处理腔室 103线性连接, 所述导电层沉 积腔室 105位于所述预处理腔室 103的远离所述真空传输装置 104的一侧,这 样可以减少所述 LED芯片工艺集成系统 100占用的洁净室的空间, 降低洁净 室成本。  Specifically, referring to FIG. 5, the pre-processing chamber 103 is connected to the vacuum transmission device 104, and the conductive layer deposition chamber 105 is linearly connected to the pre-processing chamber 103, and the conductive layer deposition chamber The chamber 105 is located on a side of the pretreatment chamber 103 remote from the vacuum transmission device 104, which can reduce the space of the clean room occupied by the LED chip process integration system 100 and reduce the cost of the clean room.
本实施例中, 所述预处理腔室 103、 装载卸载装置 101、 外延层沉积腔室 In this embodiment, the pretreatment chamber 103, the loading and unloading device 101, and the epitaxial layer deposition chamber
102、 导电层沉积腔室 105、 真空传输装置 104的结构与第一实施例和第二实 施例相同,请参考本发明关于第一实施例和第二实施例中相关内容,在此不再 赘述。 102. The structure of the conductive layer deposition chamber 105 and the vacuum transmission device 104 are the same as those of the first embodiment and the second embodiment. Please refer to the related content in the first embodiment and the second embodiment of the present invention, and details are not described herein again. .
本实施例中的 LED芯片工艺集成系统的在 LED基板上沉积外延层和导电 层的处理方法可以参考第二实施例的 LED芯片工艺集成系统的处理方法, 在 此不再赘述。  For the processing method of depositing the epitaxial layer and the conductive layer on the LED substrate in the LED chip process integration system of this embodiment, reference may be made to the processing method of the LED chip process integration system of the second embodiment, and details are not described herein again.
下面请参考图 6, 图 6是本发明第四实施例的 LED芯片工艺集成系统结 构示意图, 其中与第一实施例、 第二实施例、 第三实施例相同的结构采用相同 的标号标出。 所述芯片工艺集成系统 100包括: 装载卸载装置 101 , 用于放置 待处理的 LED基板和处理完毕的 LED基板; 装载卸载装置 101 , 用于装载或卸载待处理的或处理完毕的 LED基板; 真空传输装置 104, 用于提供真空传输环境以传输所述待处理的或处理完 毕的 LED基板; Please refer to FIG. 6. FIG. 6 is a schematic structural diagram of an LED chip process integration system according to a fourth embodiment of the present invention, wherein the same structures as those of the first embodiment, the second embodiment, and the third embodiment are denoted by the same reference numerals. The chip process integration system 100 includes: a loading and unloading device 101 for placing an LED substrate to be processed and a processed LED substrate; Loading and unloading device 101 for loading or unloading the LED substrate to be processed or processed; vacuum transmission device 104 for providing a vacuum transmission environment for transmitting the LED substrate to be processed or processed;
至少一个外延层沉积腔室 102, 位于所述真空传输装置 104的周沿, 所述 外延层沉积腔室 102用于对所述待处理的 LED基板进行外延层沉积;  At least one epitaxial layer deposition chamber 102 is located at a periphery of the vacuum transfer device 104, and the epitaxial layer deposition chamber 102 is configured to perform epitaxial layer deposition on the LED substrate to be processed;
至少一个预处理腔室 103, 用于对所述待处理的或处理完毕的 LED基板 进行预处理; 导电层沉积腔室 105 , 位于所述真空传输装置 104和外延层沉积 腔室 102的周沿, 所述导电层沉积腔室 105用于沉积导电层。 At least one pre-processing chamber 103 for pre-treating the processed or processed LED substrate; a conductive layer deposition chamber 105 located at a periphery of the vacuum transfer device 104 and the epitaxial layer deposition chamber 102 The conductive layer deposition chamber 105 is used to deposit a conductive layer.
本实施例中的真空传输装置 104 的与第二实施例中的真空传输装置 104 的形状均为线性, 本实施例与第二实施例的区别在于, 所述装载卸载装置 101 的数目为多个, 图中示出的为 3个。所述装载卸载装置 101位于真空传输装置 104的一侧, 所述外延层沉积腔室 102、 所述导电层沉积腔室 105位于所述真 空传输装置 104的与所述装载卸载装置 101相对的另一侧。  The shape of the vacuum transfer device 104 in the present embodiment and the vacuum transfer device 104 in the second embodiment are both linear. The difference between this embodiment and the second embodiment is that the number of the load unloading devices 101 is plural. , the figure shows three. The loading and unloading device 101 is located at one side of the vacuum transfer device 104, and the epitaxial layer deposition chamber 102 and the conductive layer deposition chamber 105 are located opposite to the loading and unloading device 101 of the vacuum transfer device 104. One side.
其中, 所述导电层沉积腔室 105 的位置还可以设置于所述真空传输装置 104的其他位置。 具体请参考图 7 , 图 7是本发明第五实施例的 LED芯片工艺 集成系统结构示意图。本实施例与第四实施例的区别在于, 所述导电层沉积腔 室 105位于所述真空传输装置 103的与所述装载卸载装置 101和外延层沉积腔 室 102不同的一侧。  Wherein, the position of the conductive layer deposition chamber 105 may also be disposed at other positions of the vacuum transmission device 104. For details, please refer to FIG. 7. FIG. 7 is a schematic structural diagram of an LED chip process integration system according to a fifth embodiment of the present invention. The present embodiment differs from the fourth embodiment in that the conductive layer deposition chamber 105 is located on a side of the vacuum transfer device 103 that is different from the load unloading device 101 and the epitaxial layer deposition chamber 102.
请参考图 8, 图 8是本发明第六实施例的 LED芯片工艺集成系统结构示 意图, 图中与第一至第五实施例中相同的结构采用相同的标号表示。本实施例 与所述第二实施例的区别在于所述导电层沉积腔室 105在 LED芯片工艺集成 系统的位置不同,所述导电层沉积腔室 105位于所述真空传输装置 104的周沿, 且所述导电层沉积腔室 105位于所述转载卸载装置 101与外延层沉积腔室 102 之间。  Referring to FIG. 8, FIG. 8 is a schematic view showing the structure of an LED chip process integration system according to a sixth embodiment of the present invention, and the same structures as those in the first to fifth embodiments are denoted by the same reference numerals. The difference between this embodiment and the second embodiment is that the conductive layer deposition chamber 105 is different in position of the LED chip process integration system, and the conductive layer deposition chamber 105 is located at the periphery of the vacuum transmission device 104. And the conductive layer deposition chamber 105 is located between the transfer unloading device 101 and the epitaxial layer deposition chamber 102.
综上, 本发明提供的 LED芯片工艺集成系统的处理方法, 所述 LED芯片 工艺集成系统包括装载卸载装置、 预处理腔室、 外延层沉积腔室、 真空传输装 置, 其中所述预处理腔室位于所述外延层沉积腔室之外, 所述预处理腔室专用 于对 LED基板进行预处理,从而节约了外延层沉积腔室对 LED基板进行预处 理的步骤, 增加了外延层沉积腔室用于沉积外延层的时间, 降低了成本, 提高 了外延层沉积腔室的生产效率, 本发明大大降低了 LED芯片制造的成本, 提 高了 LED芯片的产量, 并且在优选的实施例中, 本发明还将导电层沉积腔室 集成在 LED芯片工艺系统中, 进一步提高了 LED芯片制造的生产效率, 提高 了 LED芯片的产量。 In summary, the LED chip process integration system of the present invention includes a loading and unloading device, a pretreatment chamber, an epitaxial layer deposition chamber, and a vacuum transmission device, wherein the pretreatment chamber Located outside the epitaxial layer deposition chamber, the pre-treatment chamber is dedicated to pre-treating the LED substrate, thereby saving the step of pre-treating the LED substrate by the epitaxial layer deposition chamber, and adding an epitaxial layer deposition chamber. The time for depositing the epitaxial layer reduces the cost and improves the production efficiency of the epitaxial layer deposition chamber, and the invention greatly reduces the cost of manufacturing the LED chip. The output of the LED chip is increased, and in a preferred embodiment, the present invention also integrates the conductive layer deposition chamber into the LED chip process system, further improving the production efficiency of the LED chip manufacturing and increasing the yield of the LED chip.
本发明虽然已以较佳实施例公开如上,但其并不是用来限定本发明,任何 本领域技术人员在不脱离本发明的精神和范围内,都可以利用上述揭示的方法 和技术内容对本发明技术方案做出可能的变动和修改, 因此, 凡是未脱离本发 改、 等同变化及修饰, 均属于本发明技术方案的保护范围。  The present invention has been disclosed in the preferred embodiments as described above, but it is not intended to limit the invention, and the present invention may be utilized by the method and technical contents disclosed above without departing from the spirit and scope of the invention. The technical solutions make possible changes and modifications, and therefore, the scope of protection of the technical solutions of the present invention is not deviated from the present invention.

Claims

权 利 要 求 Rights request
1、 一种 LED芯片工艺集成系统, 包括:  1. An LED chip process integration system, comprising:
装载卸载装置, 用于装载或卸载待处理的或处理完毕的 LED基板; 真空传输装置,用于提供真空传输环境以传输所述待处理的或处理完毕的 Loading an unloading device for loading or unloading a processed or processed LED substrate; a vacuum transfer device for providing a vacuum transmission environment for transmitting the to-be-processed or processed
LED基板; LED substrate;
其特征在于, 还包括:  It is characterized in that it further comprises:
至少一个外延层沉积腔室,位于所述真空传输装置周沿, 所述外延层沉积 腔室用于对所述待处理的 LED基板进行外延层沉积;  At least one epitaxial layer deposition chamber is disposed at a periphery of the vacuum transmission device, and the epitaxial layer deposition chamber is configured to perform epitaxial layer deposition on the LED substrate to be processed;
至少一个预处理腔室, 用于对所述待处理的或处理完毕的 LED基板进行 预处理。  At least one pretreatment chamber for pretreating the LED substrate to be processed or processed.
2、 如权利要求 1所述的 LED芯片工艺集成系统, 其特征在于, 所述预处 理腔室位于所述真空传输装置周沿,用于对所述待处理的 LED基板进行加热、 清洁或冷却处理或对所述处理完毕的 LED基板进行冷却处理。  2. The LED chip process integration system according to claim 1, wherein the pre-processing chamber is located at a periphery of the vacuum transmission device for heating, cleaning or cooling the LED substrate to be processed. The processed LED substrate is processed or cooled.
3、 如权利要求 1或 2所述的 LED芯片工艺集成系统, 其特征在于, 所述 预处理腔室设置有加热台, 所述加热台用于对 LED基板进行加热处理, 使得 所述 LED基板从第一温度升至第二温度。  The LED chip process integration system according to claim 1 or 2, wherein the pre-processing chamber is provided with a heating stage, and the heating stage is configured to heat-process the LED substrate to make the LED substrate It rises from the first temperature to the second temperature.
4、 如权利要求 3所述的 LED芯片工艺集成系统, 其特征在于, 所述第一 温度的温度范围为 10~30摄氏度, 所述第二温度的温度范围为 700~1300摄氏 度。  4. The LED chip process integration system according to claim 3, wherein the temperature of the first temperature ranges from 10 to 30 degrees Celsius, and the temperature of the second temperature ranges from 700 to 1300 degrees Celsius.
5、 如权利要求 3所述的 LED芯片工艺集成系统, 其特征在于, 所述预处 理腔室设置有至少一个进风口和至少一个出风口 ,所述进风口用于通入还原性 气体或保护性气体的中的一种或多种, 所述还原性气体或保护性气体用于对 LED基板进行清洁处理。  The LED chip process integration system according to claim 3, wherein the pre-treatment chamber is provided with at least one air inlet and at least one air outlet, and the air inlet is used for introducing a reducing gas or protecting One or more of the gas, the reducing gas or the protective gas is used for cleaning the LED substrate.
6、 如权利要求 5所述的 LED芯片工艺集成系统, 其特征在于, 所述还原 性气体为氢气或氨气, 所述保护性气体为惰性气体或氮气中的一种或多种。  6. The LED chip process integration system according to claim 5, wherein the reducing gas is hydrogen or ammonia, and the protective gas is one or more of an inert gas or nitrogen.
7、 如权利要求 6所述的 LED芯片工艺集成系统, 其特征在于, 所述预处 理腔室设置有温控装置, 所述温控装置用于控制所述加热台在 5~15分钟内将 所述 LED基板从所述第一温度加热至所述第二温度,且使所述 LED基板保持 所述第二温度 1~25分钟; 在所述 LED基板保持所述第二温度时, 所述进风口用于通入所述还原性 气体或保护性气体的一种或多种。 7. The LED chip process integration system according to claim 6, wherein the pre-processing chamber is provided with a temperature control device, and the temperature control device is configured to control the heating station to be within 5 to 15 minutes. Heating the LED substrate from the first temperature to the second temperature, and maintaining the LED substrate at the second temperature for 1 to 25 minutes; The air inlet is configured to pass one or more of the reducing gas or the protective gas when the LED substrate maintains the second temperature.
8、 如权利要求 7所述的 LED芯片工艺集成系统, 其特征在于, 所述外延 层沉积腔室的沉积时间范围为 0.5~6.5小时。  8. The LED chip process integration system according to claim 7, wherein the deposition time of the epitaxial layer deposition chamber ranges from 0.5 to 6.5 hours.
9、 如权利要求 8所述的 LED芯片工艺集成系统, 其特征在于, 所述预处 理腔室与所述外延层沉积腔室的数目的比例范围为 1/2~1/5。  9. The LED chip process integration system of claim 8, wherein a ratio of the number of pre-processing chambers to the number of epitaxial layer deposition chambers ranges from 1/2 to 1/5.
10、 如权利要求 9所述的 LED芯片工艺集成系统, 其特征在于, 所述预 处理腔室与所述外延层沉积腔室的数目的比例为 1/3。  10. The LED chip process integration system of claim 9, wherein a ratio of the number of pre-processing chambers to the number of epitaxial layer deposition chambers is 1/3.
11、 如权利要求 8所述的 LED芯片工艺集成系统, 其特征在于, 还包括: 导电层沉积腔室,位于所述真空传输装置和外延层沉积腔室的周沿, 所述导电 层沉积腔室用于沉积导电层。  11. The LED chip process integration system of claim 8, further comprising: a conductive layer deposition chamber located at a periphery of the vacuum transfer device and the epitaxial layer deposition chamber, the conductive layer deposition chamber The chamber is used to deposit a conductive layer.
12、 如权利要求 11所述的 LED芯片工艺集成系统, 其特征在于, 所述真 空传输装置的形状为线性, 所述装载卸载装置、 预处理腔室、 外延层沉积腔室 和导电层沉积腔室线性排布于所述真空传输装置周沿。  12. The LED chip process integration system according to claim 11, wherein the vacuum transmission device has a linear shape, the loading and unloading device, the pretreatment chamber, the epitaxial layer deposition chamber, and the conductive layer deposition chamber. The chambers are linearly arranged around the circumference of the vacuum transfer device.
13、 如权利要求 11所述的 LED芯片工艺集成系统, 其特征在于, 所述真 空传输装置的形状为多边形或圆形, 所述装载卸载装置、 预处理腔室、 外延层 沉积腔室和导电层沉积腔室位于所述真空传输装置周沿。  13. The LED chip process integration system according to claim 11, wherein the vacuum transmission device has a polygonal or circular shape, and the loading and unloading device, the pretreatment chamber, the epitaxial layer deposition chamber, and the conductive A layer deposition chamber is located at the periphery of the vacuum transfer device.
14、 如权利要求 13所述的 LED芯片工艺集成系统, 其特征在于, 所述预 处理腔室与所述真空传输装置相连接,所述导电层沉积腔室与所述预处理腔室 线性连接,所述导电层沉积腔室位于所述预处理腔室的远离所述真空传输装置 的一侧。  14. The LED chip process integration system according to claim 13, wherein the pretreatment chamber is connected to the vacuum transmission device, and the conductive layer deposition chamber is linearly connected to the pretreatment chamber. The conductive layer deposition chamber is located on a side of the pretreatment chamber that is remote from the vacuum transfer device.
15、 如权利要求 11所述的 LED芯片工艺集成系统, 其特征在于, 所述导 电层为金属层或透明导电层, 所述金属层为金镍合金、金钛合金或其他金属中 的一种或多种, 所述透明导电层为 ITO、 ΖηΟ中的一种或多种。  The LED chip process integration system according to claim 11, wherein the conductive layer is a metal layer or a transparent conductive layer, and the metal layer is one of a gold-nickel alloy, a gold-titanium alloy or another metal. Or a plurality of, the transparent conductive layer is one or more of ITO and ΖηΟ.
16、 如权利要求 11所述的 LED芯片工艺集成系统, 其特征在于, 所述外 延层沉积腔室与所述导电层沉积腔室分别设置有独立的排气系统。  The LED chip process integration system according to claim 11, wherein the epitaxial layer deposition chamber and the conductive layer deposition chamber are respectively provided with independent exhaust systems.
17、 如权利要求 11所述的 LED芯片工艺集成系统, 其特征在于, 所述导 电层沉积腔室的沉积时间范围为 10~40分钟。  The LED chip process integration system according to claim 11, wherein the deposition time of the conductive layer deposition chamber ranges from 10 to 40 minutes.
18、 如权利要求 17所述的 LED芯片工艺集成系统, 其特征在于, 所述外 延层沉积腔室的数目与导电层沉积腔室的数目的比例范围为 2/1~12/1。 18. The LED chip process integration system of claim 17, wherein the ratio of the number of epitaxial layer deposition chambers to the number of conductive layer deposition chambers ranges from 2/1 to 12/1.
19、 如权利要求 18所述的 LED芯片工艺集成系统, 其特征在于, 所述外 延层沉积腔室的数目与导电层沉积腔室的数目的比例范围为 4/1~12/1。 19. The LED chip process integration system of claim 18, wherein the ratio of the number of epitaxial layer deposition chambers to the number of conductive layer deposition chambers ranges from 4/1 to 12/1.
20、 如权利要求 19所述的 LED芯片工艺集成系统, 其特征在于, 所述外 延层沉积腔室的数目与导电层沉积腔室的数目的比例范围为 8/1~12/1。  20. The LED chip process integration system of claim 19, wherein the ratio of the number of epitaxial layer deposition chambers to the number of conductive layer deposition chambers ranges from 8/1 to 12/1.
21、 如权利要求 1所述的 LED芯片工艺集成系统, 其特征在于, 所述外 延层沉积腔室用于沉积 N型 GaN层、多量子阱有源层和 P型 GaN层,所述 N 型 GaN层、 多量子阱有源层和 P型 GaN层构成所述外延层。  21. The LED chip process integration system of claim 1, wherein the epitaxial layer deposition chamber is for depositing an N-type GaN layer, a multiple quantum well active layer, and a P-type GaN layer, the N-type The GaN layer, the multiple quantum well active layer, and the P-type GaN layer constitute the epitaxial layer.
22、 如权利要求 1所述的 LED芯片工艺集成系统, 其特征在于, 所述外 延层沉积腔室的数目至少为 3个, 包括: N型 GaN层沉积腔室、 多量子阱有 源层沉积腔室和 P型 GaN层沉积腔室,所述 N型 GaN层沉积腔室用于沉积 N 型 GaN层, 所述多量子阱有源层沉积腔室用于沉积多量子阱有源层, 所述 P 型 GaN层沉积腔室用于沉积 P型 GaN层, 所述 N型 GaN层、 多量子阱有源 层和 P型 GaN层构成所述外延层。  The LED chip process integration system according to claim 1, wherein the number of the epitaxial layer deposition chambers is at least three, including: an N-type GaN layer deposition chamber, and a multiple quantum well active layer deposition. a chamber and a P-type GaN layer deposition chamber for depositing an N-type GaN layer, the multiple quantum well active layer deposition chamber for depositing a multi-quantum well active layer, The P-type GaN layer deposition chamber is used to deposit a P-type GaN layer, and the N-type GaN layer, the multiple quantum well active layer, and the P-type GaN layer constitute the epitaxial layer.
23、 一种如权利要求 1所述的 LED芯片工艺集成系统的处理方法, 其特 征在于, 包括:  23. The method of processing an LED chip process integration system according to claim 1, wherein the method comprises:
将待处理的 LED基板放置于装载卸载装置;  Placing the LED substrate to be processed on the loading and unloading device;
利用真空传输装置将所述待处理的 LED基板放置于预处理腔室; 利用所述预处理腔室对所述待处理的 LED基板进行预处理;  Disposing the LED substrate to be processed in a pretreatment chamber by using a vacuum transfer device; pretreating the LED substrate to be processed by using the pretreatment chamber;
将预处理后的所述 LED基板放置于外延层沉积腔室;  Depositing the pretreated LED substrate in an epitaxial layer deposition chamber;
在所述外延层沉积腔室中进行外延层沉积。  Epitaxial layer deposition is performed in the epitaxial layer deposition chamber.
24、如权利要求 23所述的 LED芯片工艺集成系统的处理方法, 其特征在 于, 所述预处理包括对所述 LED基板进行加热、 冷却或者清洁处理。  24. The method of processing an LED chip process integration system according to claim 23, wherein the pre-processing comprises heating, cooling or cleaning the LED substrate.
25、如权利要求 23所述的 LED芯片工艺集成系统的处理方法, 其特征在 于, 还包括:  The processing method of the LED chip process integration system according to claim 23, further comprising:
利用所述真空传输装置将沉积有外延层的 LED 基板传输至所述预处理 室;  Transmitting an LED substrate deposited with an epitaxial layer to the pretreatment chamber by using the vacuum transfer device;
所述预处理室对所述 LED基板进行第一冷却处理;  The pretreatment chamber performs a first cooling process on the LED substrate;
将所述第一冷却处理后的 LED基板传输到导电层沉积腔室用于沉积导电 层。  The first cooled LED substrate is transferred to a conductive layer deposition chamber for depositing a conductive layer.
26、如权利要求 25所述的 LED芯片工艺集成系统的处理方法, 其特征在 于, 还包括: 将沉积有导电层的的 LED基板传输至所述预处理室进行第二冷 却处理。 26. The method of processing an LED chip process integration system according to claim 25, wherein The method further includes: transmitting the LED substrate on which the conductive layer is deposited to the pretreatment chamber for performing a second cooling process.
27、如权利要求 23所述的 LED芯片工艺集成系统的处理方法, 其特征在 于, 所述预处理包括:  The processing method of the LED chip process integration system according to claim 23, wherein the preprocessing comprises:
利用温控装置将所述加热台在 5~15分钟内将所述 LED基板从第一温度加 热至第二温度;  Heating the LED substrate from the first temperature to the second temperature in 5 to 15 minutes by using a temperature control device;
使所述 LED基板保持所述第二温度 1~25分钟;  Holding the LED substrate at the second temperature for 1 to 25 minutes;
在所述 LED基板保持所述第二温度的同时, 向所述预处理腔室内通入还 原性气体或保护性气体的一种或多种。  While the LED substrate maintains the second temperature, one or more of a reducing gas or a protective gas is introduced into the pretreatment chamber.
28、如权利要求 27所述的 LED芯片工艺集成系统的处理方法, 其特征在 于, 所述还原性气体为氢气或氨气, 所述保护性气体为惰性气体或氮气中的一 种或多种。  The processing method of the LED chip process integration system according to claim 27, wherein the reducing gas is hydrogen or ammonia, and the protective gas is one or more of an inert gas or nitrogen. .
29、如权利要求 23所述的 LED芯片工艺集成系统的处理方法, 其特征在 于, 还包括将所述沉积有外延层的 LED基板传输至所述预处理室进行冷却处 理, 所述冷却处理为将所述 LED基板的温度从第二温度降低为第一温度, 所 述第一温度的温度范围为 10~30摄氏度,所述第二温度的温度范围为 700~1300 摄氏度。  The processing method of the LED chip process integration system according to claim 23, further comprising: transmitting the LED substrate on which the epitaxial layer is deposited to the pretreatment chamber for cooling processing, wherein the cooling process is The temperature of the LED substrate is lowered from a second temperature to a first temperature, the first temperature has a temperature range of 10 to 30 degrees Celsius, and the second temperature has a temperature range of 700 to 1300 degrees Celsius.
30、如权利要求 25所述的 LED芯片工艺集成系统的处理方法, 其特征在 于,所述第一冷却处理为将所述 LED基板的温度从第二温度降低为第三温度, 所述第二温度的温度范围为 700~1300摄氏度, 所述第三温度的温度范围为 100~400摄氏度。  The processing method of the LED chip process integration system according to claim 25, wherein the first cooling process is to reduce the temperature of the LED substrate from a second temperature to a third temperature, the second The temperature range of the temperature is 700 to 1300 degrees Celsius, and the temperature of the third temperature ranges from 100 to 400 degrees Celsius.
31、如权利要求 23所述的 LED芯片工艺集成系统的处理方法, 其特征在 于, 所述外延层沉积的时间范围为 0.5~6.5小时。  31. The method of processing an LED chip process integration system according to claim 23, wherein the epitaxial layer is deposited for a time ranging from 0.5 to 6.5 hours.
32、如权利要求 31所述的 LED芯片工艺集成系统的处理方法, 其特征在 于, 还包括:  32. The method of processing an LED chip process integration system according to claim 31, further comprising:
利用所述真空传输装置将所述冷却后的 LED 基板放置于导电层沉积腔 室;  Depositing the cooled LED substrate in a conductive layer deposition chamber by using the vacuum transfer device;
利用所述导电层沉积腔室对所述 LED基板进行导电层沉积。  Conductive layer deposition is performed on the LED substrate using the conductive layer deposition chamber.
33、如权利要求 26所述的 LED芯片工艺集成系统的处理方法, 其特征在 于, 所述第二冷却处理为将所述 LED基板从 100-400摄氏度冷却至 10~30摄 氏度。 The processing method of the LED chip process integration system according to claim 26, wherein the second cooling process is to cool the LED substrate from 100-400 degrees Celsius to 10 to 30 degrees. Degree.
34、如权利要求 23所述的 LED芯片工艺集成系统的处理方法, 其特征在 于, 所述外延层包括 N型 GaN层、 多量子阱有源层和 P型 GaN层。  34. The method of processing an LED chip process integrated system according to claim 23, wherein the epitaxial layer comprises an N-type GaN layer, a multiple quantum well active layer, and a P-type GaN layer.
35、如权利要求 34所述的 LED芯片工艺集成系统的处理方法, 其特征在 于, 所述外延层利用一个所述外延层沉积腔室沉积 N型 GaN层、 多量子阱有 源层和 P型 GaN层或利用 3个所述外延层沉积腔室分别沉积 N型 GaN层、多 量子阱有源层和 P型 GaN层。  The processing method of the LED chip process integration system according to claim 34, wherein the epitaxial layer deposits an N-type GaN layer, a multi-quantum well active layer, and a P-type by using one of the epitaxial layer deposition chambers. The N-type GaN layer, the multiple quantum well active layer, and the P-type GaN layer are respectively deposited by the GaN layer or by using the three epitaxial layer deposition chambers.
36、如权利要求 33所述的 LED芯片工艺集成系统的处理方法, 其特征在 于, 所述外延层沉积腔室沉积所述 N型 GaN层的温度范围为 1000~1300摄氏 度, 时间范围为 100~200分钟, 形成的所述 N型 GaN层的厚度范围为 1~3微 米;  The processing method of the LED chip process integration system according to claim 33, wherein the epitaxial layer deposition chamber deposits the N-type GaN layer at a temperature ranging from 1000 to 1300 degrees Celsius, and the time range is 100~ 200 minutes, the thickness of the N-type GaN layer formed is in the range of 1 to 3 microns;
形成所述多量子阱有源层的温度范围为 700~800 摄氏度, 时间范围为 30~80分钟, 形成的多量子阱有源层的厚度范围为 600~900埃;  Forming the multi-quantum well active layer at a temperature ranging from 700 to 800 degrees Celsius and a time range of 30 to 80 minutes, and forming a multi-quantum well active layer having a thickness ranging from 600 to 900 angstroms;
形成所述 P型 GaN层的温度范围为 850~950摄氏度, 时间范围为 20~80 分钟, 形成的 P型 GaN层的厚度范围为 0.2~0.6微米。  The P-type GaN layer is formed to have a temperature range of 850 to 950 degrees Celsius and a time range of 20 to 80 minutes, and the P-type GaN layer is formed to have a thickness ranging from 0.2 to 0.6 μm.
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