WO2011079264A2 - High expansion metallic seal - Google Patents

High expansion metallic seal Download PDF

Info

Publication number
WO2011079264A2
WO2011079264A2 PCT/US2010/062004 US2010062004W WO2011079264A2 WO 2011079264 A2 WO2011079264 A2 WO 2011079264A2 US 2010062004 W US2010062004 W US 2010062004W WO 2011079264 A2 WO2011079264 A2 WO 2011079264A2
Authority
WO
WIPO (PCT)
Prior art keywords
seal
pips
downhole
downhole seal
soft material
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/US2010/062004
Other languages
French (fr)
Other versions
WO2011079264A3 (en
Inventor
Sean L. Gaudette
Clint E. Mickey
Michael J. Loughlin
Larry J. Urban
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Baker Hughes Holdings LLC
Original Assignee
Baker Hughes Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Baker Hughes Inc filed Critical Baker Hughes Inc
Publication of WO2011079264A2 publication Critical patent/WO2011079264A2/en
Publication of WO2011079264A3 publication Critical patent/WO2011079264A3/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21BEARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B33/00Sealing or packing boreholes or wells
    • E21B33/10Sealing or packing boreholes or wells in the borehole

Definitions

  • a downhole seal includes a seal body; two or more pips extending in a direction from the seal body associated with an intended sealing surface, the two or more pips defining nonparallel facing surfaces when in a run in position.
  • Figure 1 is a schematic cross sectional representation of a prior art seal in a run in position
  • Figure 2 is a schematic cross sectional representation of the same seal shown in Figure 1 but in a set position;
  • Figure 3 is a schematic cross sectional representation of a seal configuration as disclosed herein in a run in position;
  • Figure 4 is a schematic cross sectional representation of the same seal shown in Figure 3 but in a set position
  • Figure 5 is a schematic cross sectional representation of another seal configuration as disclosed herein in a run in position
  • Figure 6 is a schematic cross sectional representation of the same seal shown in Figure 5 but in a set position;
  • Figure 7 is a schematic cross sectional representation of another seal configuration as disclosed herein in a run in position
  • Figure 8 is a schematic cross sectional representation of the same seal shown in Figure 7 but in a set position;
  • Figure 9 is a schematic cross sectional representation of another seal configuration as disclosed herein in a run in position
  • Figure 10 is a schematic cross sectional representation of the same seal shown in Figure 9 but in a set position;
  • Figure 11 is a schematic cross sectional representation of the seal configuration shown in Figure 3 with an optional sleeve, as disclosed herein in a run in position;
  • Figure 12 is a schematic cross sectional representation of the same seal shown in Figure 1 1 but in a set position;
  • Figures 13-20 are schematic cross sectional representations of alternate elastomer configurations for the seal embodiments of Figures 3-12.
  • a prior art seal 10 includes pips 12 and 14. The pips together define parallel facing surfaces 16 and 18. Once the seal 10 is set, the pips 12 and 14 are moved to a position illustrated in Figure 2, with the surfaces 16 and 18 moving to a splayed open position as shown. In the prior art this was considered a positive occurrence and hence is the state of the art.
  • a seal body 110 comprises a relatively rigid material such as a metal material.
  • the material is a steel alloy such as stainless steel or inconel.
  • the seal body 110 includes a set of depending pips 112 and 114 that extend radially relative to an axis of the seal body 110 and in one embodiment, as illustrated, extend radially outwardly.
  • the pips 112 and 114 each define nonparallel facing surfaces 116 and 118, respectively. These surfaces are oriented to generally oppose each other but they are not parallel to each other in the run in condition.
  • the surfaces grow closer to one another as distance from the seal body 110 increases.
  • the surfaces 116 to 118 form an acute angle with respect to a centerline 119 of the seal body as displayed in the Figures.
  • Pips having angled surfaces, as illustrated more reliably achieve metal-to -metal contact with a casing inside surface (casing ID) 120.
  • the angled surfaces 116 and 118 help to minimize a radial extrusion gap between the pip 112 or 114 contact surface 122 or 124, respectively, and casing ID 120 than does the prior art seal shown in Figures 1 and 2.
  • the acute angle of the pips also helps to self-energize the seal, in an embodiment where soft material filler 130 is included, with the application of differential pressure.
  • the acute angle of the pips allows for a larger cross sectional area between the two pips for a given dimension between distal ends 121 and 123 of the pips, which will provide larger volume of soft material than the geometry of the prior art such as illustrated in Figure 1.
  • the performance increase is due to the pips 112 and 114 having higher contact pressure against a casing ID 120 or to the pips 112 and 114 attaining a final set position in closer proximity to the casing.
  • the orientation of the pips 112 and 114 creates an acute angle between surface 116 and 120 when measuring the angle toward the left side of the drawing and an acute angle between surface 118 and 120 when measuring the angle toward the right side of the drawing.
  • the configuration of Figures 5 and 6 are repeated except the pips 128 and 131 have a reduced diameter (reduced prominence) that is less than the diameter of the center pip 126 (prominent pip).
  • the advantage to reducing the diameter of the outer pips 128 and 131 is that metal-to-metal contact between the center pip 126 and the casing ID 120 is even more reliably achieved.
  • the pips 128 and 131 still provide for soft material filler anchoring to help prevent washing away of the soft material.
  • the shorter pips encourage the soft material to flow between the pips and the casing ID 120. This helps with sealing small irregularities in the surface 120.
  • the angled inner surfaces of the pips of the foregoing embodiments may be used but are permissive rather than required.
  • the pips need not have the angled surfaces 116 and 118 as in the foregoing embodiments but could be configured with surfaced 16 and 18 as in the prior art.
  • the volume of the area defined by the pips, surface 134 and casing surface 120 will change during setting of he seal 110 and therefore consideration of the amount of soft material is important to ensure that it does not prevent metal to metal contact of the seal with the casing 120, something that can occur as a result of excessive squeezing of the soft material.
  • an additional optional sleeve 136 is contemplated.
  • an illustration of a seal configuration like that of Figures 3 and 4 is used to illustrate the sleeve 136.
  • the illustration is certainly by way of illustration rather than limitation since the sleeve may be used on any of the embodiments disclosed herein or others.
  • the sleeve 136 comprises non-metallic material although metallic material having appropriate structural characteristics could be substituted. Structural characteristics that are desired include toughness to resist borehole impacts during running and softness to promote sealing at pip contact surfaces 122 and 124.
  • the sealing function of the sleeve 136 occurs similarly to that of the soft material 130 in that it flows into small irregularities at casing surface 120 but is located at the pips as opposed to between the pips.
  • each of the embodiments disclosed may be used with or without a soft material 130.
  • Each of the foregoing seal configurations used alone will create a reliable seal.
  • These configurations when endowed with a softer material 130 (see Figures 13-20) than the material from which the seal itself is constructed, that softer material being positioned between pip 112 and pip 114 or 128 and 130 exhibit different sealing properties that may be helpful in tubular structures having a pitted surface, for example.
  • Softer materials contemplated include but are not limited to nonmetallic materials such as polytetrafluoroethylene, rubber, plastic, and soft metallic materials such as lead, gold, silver, etc. Each of these materials tends to flow relatively easily under stress.
  • the configurations of the pips as described above enhance the utility and reliability of these softer materials by helping to keep them contained between the pips rather than to allow the material to flow to a position where it is between the pips and the casing 120, where it can have a detrimental affect on sealing.
  • the material is a single piece of material ( Figures 13, 17, 18 and 19) while in other embodiments the material 130 is configured as more than one piece of material ( Figures 14, 15, 16, and 20). It is further to be appreciated that in Figure 20, O-rings are illustrated having different cross sectional diameters. O-rings with the same cross sectional diameters can also be used as well as different numbers of O-rings. All of the configurations shown Figures 13-20 may have soft material that is molded into a separate ring and placed onto the seal body or molded and bonded directly onto the seal body.

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Geology (AREA)
  • Mining & Mineral Resources (AREA)
  • Physics & Mathematics (AREA)
  • Environmental & Geological Engineering (AREA)
  • Fluid Mechanics (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Gasket Seals (AREA)

Abstract

A downhole seal includes a seal body; two or more pips extending in a direction from the seal body associated with an intended sealing surface, the two or more pips defining nonparallel facing surfaces when in a run in position.

Description

HIGH EXPANSION METALLIC SEAL
CROSS REFERENCE TO RELATED APPLICATION
This application claims the benefit of the filing date of United States Patent Application Serial Number 12/646,421 filed December 23, 2009, for "HIGH EXPANSION METALLIC SEAL."
BACKGROUND
[0001] In the downhole drilling and completion arts, sealing of various things such as an annulus between a mandrel or basepipe and a casing, for example is a common requirement. Many different types of seals have been developed and have used many different types of material and/or combinations of material. More recently, high expansion metal seals have become of interest to the industry yet while they suffer little from the deleterious effects of the downhole environment and relatively easily resist mechanical insults such as pressure inversions, extrusion, and the ravages of time, they present greater difficulty with regard to establishing a competent seal to begin with. Various means have been used to assist in the creating of the seal each having effective success to some degree.
[0002] None of the known solutions has proven a panacea in all situations and consequently, the art still seeks alternative solutions and well receives those proposed.
SUMMARY
[0003] A downhole seal includes a seal body; two or more pips extending in a direction from the seal body associated with an intended sealing surface, the two or more pips defining nonparallel facing surfaces when in a run in position.
BRIEF DESCRIPTION OF THE DRAWINGS
[0004] Referring now to the drawings wherein like elements are numbered alike in the several Figures:
[0005] Figure 1 is a schematic cross sectional representation of a prior art seal in a run in position;
[0006] Figure 2 is a schematic cross sectional representation of the same seal shown in Figure 1 but in a set position; [0007] Figure 3 is a schematic cross sectional representation of a seal configuration as disclosed herein in a run in position;
[0008] Figure 4 is a schematic cross sectional representation of the same seal shown in Figure 3 but in a set position;
[0009] Figure 5 is a schematic cross sectional representation of another seal configuration as disclosed herein in a run in position;
[0010] Figure 6 is a schematic cross sectional representation of the same seal shown in Figure 5 but in a set position;
[0011] Figure 7 is a schematic cross sectional representation of another seal configuration as disclosed herein in a run in position;
[0012] Figure 8 is a schematic cross sectional representation of the same seal shown in Figure 7 but in a set position;
[0013] Figure 9 is a schematic cross sectional representation of another seal configuration as disclosed herein in a run in position;
[0014] Figure 10 is a schematic cross sectional representation of the same seal shown in Figure 9 but in a set position;
[0015] Figure 11 is a schematic cross sectional representation of the seal configuration shown in Figure 3 with an optional sleeve, as disclosed herein in a run in position;
[0016] Figure 12 is a schematic cross sectional representation of the same seal shown in Figure 1 1 but in a set position; and
[0017] Figures 13-20 are schematic cross sectional representations of alternate elastomer configurations for the seal embodiments of Figures 3-12.
DETAILED DESCRIPTION
[0018] In order to enhance understanding of the invention disclosed herein initial reference will be made to the prior art, represented in Figures 1 and 2. A prior art seal 10 includes pips 12 and 14. The pips together define parallel facing surfaces 16 and 18. Once the seal 10 is set, the pips 12 and 14 are moved to a position illustrated in Figure 2, with the surfaces 16 and 18 moving to a splayed open position as shown. In the prior art this was considered a positive occurrence and hence is the state of the art.
[0019] Referring now to Figures 3 and 4, a first embodiment of the seal concept disclosed herein is illustrated. A seal body 110 comprises a relatively rigid material such as a metal material. In one embodiment the material is a steel alloy such as stainless steel or inconel. The seal body 110 includes a set of depending pips 112 and 114 that extend radially relative to an axis of the seal body 110 and in one embodiment, as illustrated, extend radially outwardly. Significantly, the pips 112 and 114 each define nonparallel facing surfaces 116 and 118, respectively. These surfaces are oriented to generally oppose each other but they are not parallel to each other in the run in condition. Moreover, as can be appreciated from the Figures, the surfaces grow closer to one another as distance from the seal body 110 increases. The surfaces 116 to 118 form an acute angle with respect to a centerline 119 of the seal body as displayed in the Figures. Pips having angled surfaces, as illustrated, more reliably achieve metal-to -metal contact with a casing inside surface (casing ID) 120. Further the angled surfaces 116 and 118 help to minimize a radial extrusion gap between the pip 112 or 114 contact surface 122 or 124, respectively, and casing ID 120 than does the prior art seal shown in Figures 1 and 2. The acute angle of the pips also helps to self-energize the seal, in an embodiment where soft material filler 130 is included, with the application of differential pressure. The acute angle of the pips allows for a larger cross sectional area between the two pips for a given dimension between distal ends 121 and 123 of the pips, which will provide larger volume of soft material than the geometry of the prior art such as illustrated in Figure 1. The performance increase is due to the pips 112 and 114 having higher contact pressure against a casing ID 120 or to the pips 112 and 114 attaining a final set position in closer proximity to the casing. As can be appreciated in Figure 4, the orientation of the pips 112 and 114 creates an acute angle between surface 116 and 120 when measuring the angle toward the left side of the drawing and an acute angle between surface 118 and 120 when measuring the angle toward the right side of the drawing.
[0020] In another embodiment, referring to Figures 5 and 6, the configuration of Figures 3 and 4 is repeated except for the addition of an additional pip 126. The additional pip 126 is configured to contact the casing 120 as shown in Figure 6. The advantages to adding a center pip is that it offers the potential of a third metal-to -metal contact point or reduced extrusion gap and it controls the set volume of soft material 130, which prevents excessive squeeze.
[0021] In another embodiment, referring to Figures 7 and 8, the configuration of Figures 5 and 6 are repeated except the pips 128 and 131 have a reduced diameter (reduced prominence) that is less than the diameter of the center pip 126 (prominent pip). The advantage to reducing the diameter of the outer pips 128 and 131 is that metal-to-metal contact between the center pip 126 and the casing ID 120 is even more reliably achieved. The pips 128 and 131 still provide for soft material filler anchoring to help prevent washing away of the soft material. In this embodiment however, the shorter pips encourage the soft material to flow between the pips and the casing ID 120. This helps with sealing small irregularities in the surface 120. Further, it is to be appreciated that in this embodiment the angled inner surfaces of the pips of the foregoing embodiments may be used but are permissive rather than required. Stated alternatively, in embodiments with reduced prominence pips, the pips need not have the angled surfaces 116 and 118 as in the foregoing embodiments but could be configured with surfaced 16 and 18 as in the prior art.
[0022] In another embodiment, referring to Figures 9 and 10, the configuration of Figures 3 and 4 is repeated except a span surface 134 between pips 112 and 114 is not perpendicular to the centerline 119 of the seal but rather has a concave shape with respect to the centerline of the seal as illustrated. The concavity of span surface 134 alters the set volume of the seal 110 and allows for greater selection in soft material volume. It is to be understood however, that the volume of the area defined by the pips, surface 134 and casing surface 120 will change during setting of he seal 110 and therefore consideration of the amount of soft material is important to ensure that it does not prevent metal to metal contact of the seal with the casing 120, something that can occur as a result of excessive squeezing of the soft material.
[0023] In all embodiments Figures 3-10, an additional optional sleeve 136 is contemplated. Referring to Figures 11 and 12, an illustration of a seal configuration like that of Figures 3 and 4 is used to illustrate the sleeve 136. The illustration is certainly by way of illustration rather than limitation since the sleeve may be used on any of the embodiments disclosed herein or others. In one embodiment the sleeve 136 comprises non-metallic material although metallic material having appropriate structural characteristics could be substituted. Structural characteristics that are desired include toughness to resist borehole impacts during running and softness to promote sealing at pip contact surfaces 122 and 124. The sealing function of the sleeve 136 occurs similarly to that of the soft material 130 in that it flows into small irregularities at casing surface 120 but is located at the pips as opposed to between the pips.
[0024] As has been alluded to hereinabove, each of the embodiments disclosed may be used with or without a soft material 130. Each of the foregoing seal configurations used alone will create a reliable seal. These configurations when endowed with a softer material 130 (see Figures 13-20) than the material from which the seal itself is constructed, that softer material being positioned between pip 112 and pip 114 or 128 and 130 exhibit different sealing properties that may be helpful in tubular structures having a pitted surface, for example. Softer materials contemplated include but are not limited to nonmetallic materials such as polytetrafluoroethylene, rubber, plastic, and soft metallic materials such as lead, gold, silver, etc. Each of these materials tends to flow relatively easily under stress. They are therefore helpful in ensuring sealing in smaller discontinuities of the sealing surface. The configurations of the pips as described above enhance the utility and reliability of these softer materials by helping to keep them contained between the pips rather than to allow the material to flow to a position where it is between the pips and the casing 120, where it can have a detrimental affect on sealing. Reference is made to a number of embodiments of soft material 130. The embodiments are self explanatory, each of which being configured to provide for good sealing characteristics while exhibiting an unstressed shape that allows space into which the stressed material 120 may flow to avoid flow of that material between the pips 112 and 114 and the casing 120. It is to be appreciated that in some illustrated embodiments the material is a single piece of material (Figures 13, 17, 18 and 19) while in other embodiments the material 130 is configured as more than one piece of material (Figures 14, 15, 16, and 20). It is further to be appreciated that in Figure 20, O-rings are illustrated having different cross sectional diameters. O-rings with the same cross sectional diameters can also be used as well as different numbers of O-rings. All of the configurations shown Figures 13-20 may have soft material that is molded into a separate ring and placed onto the seal body or molded and bonded directly onto the seal body.
[0025] While one or more embodiments have been shown and described, modifications and substitutions may be made thereto without departing from the spirit and scope of the invention. Accordingly, it is to be understood that the present invention has been described by way of illustrations and not limitation.

Claims

1. A downhole seal comprising:
a seal body;
two or more pips extending in a direction from the seal body associated with an intended sealing surface, the two or more pips defining nonparallel facing surfaces when in a run in position.
2. A downhole seal as claimed in claim 1 wherein the nonparallel facing surfaces define a dimension therebetween that diminishes with increasing distance from the seal body.
3. A downhole seal as claimed in claim 1 wherein the two or more pips nonparallel facing surfaces each define acute angles with a surface of a tubular in which the seal is installed.
4. A downhole seal as claimed in claim 1 wherein the two or more pips each include a selected contact surface.
5. A downhole seal as claimed in claim 4 wherein the contact surface has an angle relative to an axis of the seal body.
6. A downhole seal as claimed in claim 1 further comprising an additional pip located between the two or more pips.
7. A downhole seal as claimed in claim 6 wherein the additional pip is of symmetrical geometry relative to an annular path along which it extends.
8. A downhole seal as claimed in claim 1 further comprising a soft material disposed between the two or more pips.
9. A downhole seal as claimed in claim 8 wherein the soft material is a nonmetal material.
10. A downhole seal as claimed in claim 8 wherein the soft material is a metallic material.
11. A downhole seal as claimed in claim 8 wherein the soft material is configured in a single piece.
12. A downhole seal as claimed in claim 11 wherein the single piece is bonded directly to the seal body.
13. A downhole seal as claimed in claim 8 wherein the soft material is configured in a plurality of pieces.
14. A downhole seal as claimed in claim 13 wherein the plurality of pieces are bonded directly to the seal body.
15. A downhole seal as claimed in claim 8 wherein the soft material is one or more O-rings.
16. A downhole seal as claimed in claim 6 wherein the two or more pips are of lesser prominence than the additional pip.
17. A downhole seal as claimed in claim 1 wherein the seal further comprises a sleeve disposed about the seal body.
18. A downhole seal as claimed in claim 17 wherein the sleeve comprises tough soft material.
19. A downhole seal as claimed in claim 17 wherein the sleeve facilitates sealing at a contact surface of each pip.
20. A downhole seal as claimed in claim 1 wherein the seal body further includes a concave span surface between the two or more pips.
PCT/US2010/062004 2009-12-23 2010-12-23 High expansion metallic seal Ceased WO2011079264A2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US12/646,421 US20110148043A1 (en) 2009-12-23 2009-12-23 High expansion metallic seal
US12/646,421 2009-12-23

Publications (2)

Publication Number Publication Date
WO2011079264A2 true WO2011079264A2 (en) 2011-06-30
WO2011079264A3 WO2011079264A3 (en) 2011-10-06

Family

ID=44149962

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2010/062004 Ceased WO2011079264A2 (en) 2009-12-23 2010-12-23 High expansion metallic seal

Country Status (2)

Country Link
US (1) US20110148043A1 (en)
WO (1) WO2011079264A2 (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10519740B2 (en) 2017-03-20 2019-12-31 Weatherford Technology Holdings, Llc Sealing apparatus and associated methods of manufacturing
US10472911B2 (en) 2017-03-20 2019-11-12 Weatherford Technology Holdings, LLC. Gripping apparatus and associated methods of manufacturing

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB0016595D0 (en) * 2000-07-07 2000-08-23 Moyes Peter B Deformable member
US7363975B2 (en) * 2000-07-07 2008-04-29 Baker Hughes Incorporated Push/pull belleville stack for use with zertech MTM seal
US6705615B2 (en) * 2001-10-31 2004-03-16 Dril-Quip, Inc. Sealing system and method
US7784797B2 (en) * 2006-05-19 2010-08-31 Baker Hughes Incorporated Seal and slip assembly for expandable downhole tools

Also Published As

Publication number Publication date
WO2011079264A3 (en) 2011-10-06
US20110148043A1 (en) 2011-06-23

Similar Documents

Publication Publication Date Title
JP5232475B2 (en) Pipe threaded fittings with seals
CA2708715C (en) Sealing apparatus having ring member and back-up layer
JP4300187B2 (en) Threaded pipe fittings
US8567492B2 (en) Modified packer with non-extrusion ring
US8381809B2 (en) Packer with non-extrusion ring
US7963321B2 (en) Swellable downhole packer
CN102575508B (en) Annular blocking device
US9376882B2 (en) Self-energizing annular seal
US9464498B2 (en) Extrusion preventing supporting device
BRPI0707924A2 (en) gas-tight tubular fitting
BRPI0416408B1 (en) REALIZATION BY PLASTIC EXPANSION OF TUBULAR SEAL WITH OVERLAYING (S) AND INITIAL (IS)
JP2010533827A (en) Screw joint with elastic seal ring
CN103032047B (en) Bi-directional compression self-tightening axial seal and change connection application
US20160032681A1 (en) High pressure seal with composite anti-extrusion mechanism
BR112016015324B1 (en) threaded joint for ultra thick oil well pipe
WO2016193888A1 (en) Flexible pipe joint having an annular flexible boot thermally or chemically insulating an annular elastomeric flexible element
US9322240B2 (en) Inflatable packer with a reinforced sealing cover
WO2018118273A1 (en) Pressure activated anti-extrusion ring for annular seal, seal configuration, and method
CA2103095A1 (en) Sealing element for inflatable packer
US9140095B2 (en) Packer cup for sealing in multiple wellbore sizes eccentrically
US20110148043A1 (en) High expansion metallic seal
AU2020245138B2 (en) Backup
US10077621B2 (en) Diverter flow line insert packer seal
WO2011079265A2 (en) High expansion metallic seal
CA2521763C (en) Pump plug

Legal Events

Date Code Title Description
121 Ep: the epo has been informed by wipo that ep was designated in this application

Ref document number: 10840161

Country of ref document: EP

Kind code of ref document: A1

NENP Non-entry into the national phase

Ref country code: DE

122 Ep: pct application non-entry in european phase

Ref document number: 10840161

Country of ref document: EP

Kind code of ref document: A2