WO2010105749A2 - A method of rolling rails, apparatus for rolling rails and rail produced according to said method - Google Patents
A method of rolling rails, apparatus for rolling rails and rail produced according to said method Download PDFInfo
- Publication number
- WO2010105749A2 WO2010105749A2 PCT/EP2010/001426 EP2010001426W WO2010105749A2 WO 2010105749 A2 WO2010105749 A2 WO 2010105749A2 EP 2010001426 W EP2010001426 W EP 2010001426W WO 2010105749 A2 WO2010105749 A2 WO 2010105749A2
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- blank
- rail
- rolling
- mill
- stands
- Prior art date
Links
Classifications
-
- E—FIXED CONSTRUCTIONS
- E01—CONSTRUCTION OF ROADS, RAILWAYS, OR BRIDGES
- E01B—PERMANENT WAY; PERMANENT-WAY TOOLS; MACHINES FOR MAKING RAILWAYS OF ALL KINDS
- E01B31/00—Working rails, sleepers, baseplates, or the like, in or on the line; Machines, tools, or auxiliary devices specially designed therefor
- E01B31/02—Working rail or other metal track components on the spot
- E01B31/12—Removing metal from rails, rail joints, or baseplates, e.g. for deburring welds, reconditioning worn rails
- E01B31/13—Removing metal from rails, rail joints, or baseplates, e.g. for deburring welds, reconditioning worn rails by milling
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21B—ROLLING OF METAL
- B21B1/00—Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations
- B21B1/08—Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations for rolling structural sections, i.e. work of special cross-section, e.g. angle steel
- B21B1/085—Rail sections
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21B—ROLLING OF METAL
- B21B13/00—Metal-rolling stands, i.e. an assembly composed of a stand frame, rolls, and accessories
- B21B13/08—Metal-rolling stands, i.e. an assembly composed of a stand frame, rolls, and accessories with differently-directed roll axes, e.g. for the so-called "universal" rolling process
Definitions
- This invention relates to a method of rolling rails.
- the invention also relates to an apparatus for carrying out said method, and to a product produced therewith.
- Rails are formed by three general methods of rolling :
- the plane of symmetry of the rail coincides with the pass line or is perpendicular thereto.
- the diagonal or angular method differs from the first method in that the shaping of the rail begins with the first pass in the roughing stand, and instead of first compressing the bloom through a smaller size and then forming the section partly through compression and partly through spreading, the process is one of compression from beginning to end.
- the universal method employs both horizontal and vertical rolls in one stand to effect shaping of the work piece. In some cases, a semi-universal stand is used comprising two horizontal rolls and one vertical roll.
- the work rolls of a universal stand, particularly the vertical work rolls may be backed up by back-up rolls, usually of a larger diameter than the work rolls.
- the universal rolling method allows a greater degree of hot working of the head and flange of a rail by compression than can be obtained when horizontal rolls alone are used.
- the traditional or conventional style of rolling rails is to use horizontal rolls either two-high (i.e. two work rolls) or three-high (i.e. three work rolls) typically in a cross country style mill.
- the process comprises the bloom being deformed into a "top hat” before being turned onto its side.
- This "top hat” can be described as a bar having a trapezoidal cross-section.
- the tail and head of the bar is subsequently knifed to begin the rolling process where the head portion, web portion and foot portion of the rail are formed.
- the consequence of this method is that the deformations of the head and foot portion are relatively low during some of the passes.
- the conventional universal rolling method also starts by first producing the "top hat", and further using two-high rolls to form the "top hat” pass through knifing into a rail blank shape before completion through universal stands.
- These universal stands use shaped vertical rolls for the formation of the head and or a combination of open closed grooves of the universal to form the foot. Again the deformations of the head and foot portion are relatively low during some of the passes.
- the material may be rolled either in a reversible manner rather than one-way only, depending on the set-up and lay-out of the mill.
- the traditional roughing process requires particular techniques to reduce, twist and turn the bar to manipulate the bar into the correct shape and orientation. Up to 12 to 14 passes must be made through the passes, all of which may or may not be through shaped rolls. Usually the number of roughing stands is small, usually two, wherein the work rolls are provided with several pass grooves for subsequent passes and consequently this first stage of the rail rolling process accounts for a considerable time in the mill.
- Figure 1 represents a typical example of a cross country style mill.
- the "top hat” is indicated with the dashed ellipsoid.
- the current practice for universal rolling contains a number of steps: universal rolling with two horizontals and two verticals of which the roll which forms the head of the rail is shaped to the particular rail profile being rolled; edger rolling, head rolling and foot rolling within separate stands.
- the greater part of the reductions of the head and foot are typically performed within the universal stands containing two horizontal rolls and two vertical rolls in a thickness orientation around the profile of the rail section.
- the breakdown obtained in this method has a larger section that is substantially similar to the desired rail in shape, as shown in Figures 2 and 3.
- the difference in width between the head and foot must be accomplished in the roughing operation as indicated by the pass grooves on the roughing stands as shown in Figures 2 and 3.
- One or more of the objects are achieved by a method of rolling steel rails comprising :
- finishing mill comprising at least three four-roll universal stands (Ul, U2 and U3) and at least two two-roll edger stands (El, E2), wherein the universal stands contain a vertical roll for forming the lower foot portion and a vertical roll for forming the head portion of the rail, and two shaped horizontal rolls for forming the sides of the rail and particularly the web portion of the rail, wherein the rail blank is passed only once through said finishing mill, and wherein at least the vertical rolls in all universal stands for forming the lower foot portion are flat rolls, and wherein at least one of universal stands contains a flat vertical roll for forming the head portion.
- a rail blank is transferred to the fully continuous multi-stand finishing mill, preferably consisting of at least five stands.
- the universal stands and the edger stands are used in alternation (e.g. Ul-El- U2-E2-U3).
- the stands of the finishing mill are operated in tandem, i.e. after threading the product to be rolled is rolled in all stands at the same time. It is noted that this fully-continuous tandem rolling requires careful choice of the rolling schedule and rolling speeds of the respective stands, because the amount of material passing through each stand must be the same at any given time.
- At least one of the vertical rolls in the universal stands in the finishing mill comprises a vertical roll for working the head portion of the rail.
- the prior to rolling the blank is brought to a suitable rolling temperature.
- the reheating temperature for steel rails is chosen such that the finishing temperature (i.e. the temperature at which the last deformation is given) is still in the austenitic range, i.e. above Ar 3 .
- the rail may be cooled in still air (natural cooling) or in a water spray, mist, forced air, or submersion in a coolant (accelerated cooling). These cooling regimes are known.
- the terms vertical and horizontal are used to indicate which rolls are meant.
- the horizontal rolls have a rotational axis which is about horizontal
- the vertical rolls have a rotational axis which is about perpendicular to the horizontal. All embodiments are described such that the web of the blank is substantially horizontal. It should be pointed out however that the invention could also be performed with the web of the blank in the vertical direction, particularly in the finishing mill. It is important to apply forging action to the head portion whilst in the universal stands and then apply forming action.
- the width thickness of the head portion is worked: the web portion and head portion are worked thickness wise as well as the foot, no work is completed lengthwise on the rail in these stands or passes: the distance between the head crown and the lower portion of the foot remains unchanged.
- the forging action within the universal stands provides a direct application of pressure on the head portion in the crown area (the surface contacting the wheel of the train when in use), and this prevents the occurrence of rolling imperfections as the rail is reduced to the desired dimensions.
- the length of the distance between the head crown and the lower portion of the foot is reduced.
- the foot portion is reduced in the same direction as the head portion as a result of the opposing force exerted by the vertical flat roll which works the foot portion.
- the head portion is reduced in two directions i.e. crown and sides.
- the head crown is only worked with very slight force applied in the direction as applied by the universal method.
- the universal method actively forges the head portion in this invention at least 4 times with direct pressure applied to the head crown in three instances with the vertical rolls.
- the roll working the head portion in the universal stand arrangement is profiled and shaped to suit each particular section.
- shaped vertical work rolls mean that the rolls are stand specific. Also, wear of the shaped vertical work roll will affect the surface quality of the head portion of the rail.
- both the vertical rolls working the foot portion are flat and at least one of the rolls working the head portion is flat. The need for shaped vertical rolls is reduced, thereby reducing the need for stand specific rolls. Also, maintenance of the vertical rolls is simplified because there is no need to provide them with a contour during grinding of the roll to remove the worn parts. This allows flexibility between not only products but also between stands.
- any roll can be chosen for any stand. Also as part of the universal process with flat verticals it may not be necessary to change stands for rolling similar products, whereas with shaped verticals the profile of the crown will change and thus a stand change may be required.
- the flat vertical work rolls would simply require a change to the schedule settings. This flexibility in using work rolls for various rolling schedules and in different rolling stands saves both time and money. Also better dimensional tolerances of the rails are obtainable.
- An advantage of the process according to the invention is that surface defects within the head portion are prevented as a result of the larger working of the head in comparison to the known process. As the head undergoes more direct work in the crown area, any potential surface defects caused by rolling are rolled out and hence not in the finished product.
- the number of replacement sets may be reduced.
- one of the universal stands in the finishing mill comprises a shaped vertical roll for forming the head portion. All other vertical rolls for forming the head portion in the other universal stands in the finishing mill are flat rolls. In a preferable embodiment all universal stands in the finishing mill comprise two flat vertical rolls. These embodiments successively increase the benefits and advantages obtained by replacing the shaped vertical rolls by flat vertical rolls. In an embodiment the finishing mill comprises four universal stands
- the two-roll edger stands in the finishing mill are two-high stands or four-high stands, or the finishing mill may comprise combinations of two-high and four-high edger stands.
- the last universal stand of the finishing mill is a semi-universal stand consisting of two shaped horizontal rolls for working the head portion and the web portion, one flat vertical roll for working the lower foot portion and one flat vertical dummy roll opposite the flat vertical roll for working the lower foot portion. The dummy roll does not work the head crown of the rail.
- the final stand is semi-universal and part of the continuous rolling train.
- the final universal stand rolls the section to the final dimensions as required by the customer.
- the use of a semi universal stand in the final stand allows the finished products to have excellent tolerance and surface quality around the head and foot of the rail.
- the rail blank is provided by casting a cast steel rail blank.
- the rail blank from an alternative source, either in addition to rolled rail blanks, or instead of rolled rail blanks, the dependence on the roughing mills to provide the rail blanks is reduced.
- the productivity of the finishing mill can hereby be significantly increased.
- the rail blank may be hot charged into a reheating furnace prior to rolling thereby obtaining a potential energy saving.
- the cast rail blank may be asymmetrical or symmetrical with respect to the centreline of the web portion of the rail blank.
- the rail blank is provided by: - breakdown rolling a bloom in a roughing mill, preferably having a square or rectangular cross-section, to a substantially H-shaped blank, the blank comprising a foot portion, a head portion and a web portion connecting the foot portion to the head portion, the blank having a symmetrical cross-section with respect to the centreline of the web portion followed by forming the rail blank from the H-shaped blank in an intermediate mill, or by
- - casting a substantially H-shaped cast blank comprising a foot portion, a head portion and a web portion connecting the foot portion to the head portion, the blank having a symmetrical cross- section with respect to the centreline of the web portion followed by forming the rail blank from the H-shaped blank in an intermediate mill.
- the roughing mill should be understood to comprise a breakdown mill for converting a bloom into a substantially H- shaped blank and an intermediate mill for converting the substantially H- shaped blank into a rail blank.
- the cast shape or beam blank is taken from the breakdown mill and passed to the intermediate mill where the head and foot will be given different widths and thicknesses formed in the intermediate reversing operation according to the roll-pass design. Accordingly, the rail blank from the intermediate mill resembles the rail to be manufactured in shape, but is larger in dimensions than the finished rail product. Since the head and foot of a rail are of an almost equal cross sectional area, the required H-shaped blank from the breakdown mill or caster can feed the intermediate mill to produce a rail blank. One flange of the beam blank will be formed into the head of the rail and the remaining flange formed into the foot of the rail.
- the H-shaped cast blank may be hot charged into a reheating furnace prior to rolling thereby obtaining a potential energy saving.
- This process is comparable to the known method for producing rail, albeit that the bloom is not converted into a "top-hat”-configuration but into a substantially H-shaped blank (or beam blank).
- the blank may also be in a cast form.
- H-shaped blanks from an alternative source, either in addition to rolled H-shaped blanks, or instead of rolled H-shaped blanks, the dependence on the breakdown mill to provide the blanks is reduced.
- the productivity of the finishing mill can hereby be significantly increased.
- the method does not require any increase in the number of roughing or intermediate passes and, therefore, requires no additional stands.
- the use of H-shaped blanks with a simple cross section makes it possible to use the roughing operation with only a single roughing stand and a single intermediate stand thus removing any potentially difficult twist or turn operations as in the "top-hat" method.
- the roughing mill is a reversing mill.
- the thickness and width of the head portion and the thickness of the foot portion and the thickness of the web portion of the H-shaped blank is larger than the respective thickness and width of the corresponding portions in the finished rail.
- the length of the web portion of the H-shaped blank (i.e. the distance between the heat and the foot portion) is smaller than the corresponding length in the finished rail and/or wherein the width of the foot portion of the H-shaped blank is larger than the respective width of the corresponding portion in the finished rail.
- the intermediate mill forms the H-shaped blank into a rail blank which is asymmetrical with respect to the centreline of the web portion of the rail blank.
- a rolling mill for rolling rail in accordance with the method described above is provided.
- a rolling mill for rolling rail starting from a substantially H-shaped blank in accordance with the method described above is provided which is convertible into a rolling mill for rolling H-beam sections starting from a substantially H-shaped blank produced either by breakdown rolling a bloom (8) in a roughing mill, preferably having a square or rectangular cross-section, to a substantially H-shaped blank (X), the blank comprising a foot portion (2), a head portion (3) and a web portion (4) connecting the foot portion to the head portion, the blank having a symmetrical cross-section with respect to the centreline of the web portion followed by forming a beam blank (1) from the H-shaped blank in an intermediate mill, or by
- the substantially H-shaped cast blank (or beam blank) can be rolled into an H-section or I-section using the same finishing mill not only from the same blank as used for rolling rails but also using the same flat vertical rolls in the four roll universal configuration.
- the shaped horizontal rolls in the universal stands are exchanged for rolls which perform the forming action of the I- section or H-section. This exchange can be done much more quickly, thus reducing the downtime of the mill. Costs for rolls are also reduced, because the vertical rolls are the same. The mill also has become more flexible.
- a rail is provided produced according to the method described above.
- the final microstructure of the head in the finished rail is finer.
- Figure 1 represents a typical example of a cross country style mill.
- the "top hat” is indicated with the dashed ellipsoid.
- Shaped vertical rolls are used for the shaping of the head portion of the rail in U1-U4 and UF.
- Three edger stands are used in the configuration E2-U1-U3-E1-U2-U4-E3-UF.
- Figure 2 represents a typical example of a mill using grooves and involving turning actions.
- the "top hat” is indicated with the dashed ellipsoid.
- Figure 3 is a schematic representation of the evolution of a substantially H-shaped blank 1 (or beam blank) into a rail.
- the foot of the rail is just as wide as the flange of the blank, but this is not a necessity.
- the foot may be wider or narrower than the flange of the blank.
- the blank in Figure 3a comprises a foot portion 2, a head portion 3 and a web portion 4 connecting the foot portion 2 to the head portion 3.
- the blank has a symmetrical cross-section with respect to the centreline
- a rail blank (5) has a shape between the shape presented in Figure 3a and the final rail (6). This rail blank as such is not shown in Figure 3. However, the rail blank also comprises a foot portion 2, a head portion 3 and a web portion 4 connecting the foot portion 2 to the head portion 3.
- the lower portion of the foot of the rail 6 is indicated with 2a.
- This is the part of the rail which rests on the sleeper or the rail bed.
- the head crown i.e. the part which eventually comes into contact with the wheels of a train, is indicated with 3a.
- the edges of the web part are indicated with 4a and 4b, whereas 7a and 7b represent the entire side curvature starting at the head crown, and ending at the lower portion of the foot.
- 7a and 7b are the parts formed by the horizontal rolls. 4a is therefore a part of 7a.
- 2a and 3a are the parts formed by the vertical rolls.
- Figure 4 is a schematic representation of a process according to the invention.
- the finishing mill is represented which, starting from a rail blank produces a finished rail in a 7-stands continuous tandem mill of a U1-E1-U2-E2-U3-E3-U4, wherein all vertical rolls are flat rolls, and wherein U4 is a semi-universal stand with a dummy vertical flat roll on the left hand side.
- Figure 4b represents the evolution of an H-shaped blank into a rail blank in an intermediate mill
- Figure 4a represents the evolution of a bloom into an H-shaped blank in a breakdown mill. The breakdown mill and the intermediate mill jointly form the roughing mill.
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- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Architecture (AREA)
- Civil Engineering (AREA)
- Structural Engineering (AREA)
- Metal Rolling (AREA)
Abstract
Description
Claims
Priority Applications (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
AP2011005934A AP2011005934A0 (en) | 2009-03-16 | 2010-03-08 | A method of rolling rails, apparatus for rolling rails and rail produced according to said method. |
RU2011141776/02A RU2530609C2 (en) | 2009-03-16 | 2010-03-08 | Method of rail rolling, device for rail rolling and rail thus made |
EP10709165A EP2408967A2 (en) | 2009-03-16 | 2010-03-08 | A method of rolling rails, apparatus for rolling rails and rail produced according to said method |
UAA201112010A UA103795C2 (en) | 2009-03-16 | 2010-03-08 | Method of rolling rails, device for rolling rails and rail manufactured by said method |
ZA2011/06122A ZA201106122B (en) | 2009-03-16 | 2011-08-19 | A method of rolling rails, apparatus for rolling rails and rail produced according to said method |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP09003746 | 2009-03-16 | ||
EP09003746.6 | 2009-03-16 |
Publications (2)
Publication Number | Publication Date |
---|---|
WO2010105749A2 true WO2010105749A2 (en) | 2010-09-23 |
WO2010105749A3 WO2010105749A3 (en) | 2011-01-27 |
Family
ID=40897681
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/EP2010/001426 WO2010105749A2 (en) | 2009-03-16 | 2010-03-08 | A method of rolling rails, apparatus for rolling rails and rail produced according to said method |
Country Status (6)
Country | Link |
---|---|
EP (1) | EP2408967A2 (en) |
AP (1) | AP2011005934A0 (en) |
RU (1) | RU2530609C2 (en) |
UA (1) | UA103795C2 (en) |
WO (1) | WO2010105749A2 (en) |
ZA (1) | ZA201106122B (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2014117519A1 (en) * | 2013-02-01 | 2014-08-07 | 中冶赛迪工程技术股份有限公司 | Compact universal vertical steel rail rolling method |
RU2784961C1 (en) * | 2021-12-27 | 2022-12-01 | Акционерное общество "ЕВРАЗ Объединенный Западно-Сибирский металлургический комбинат", АО "ЕВРАЗ ЗСМК" | Roughing pass system for rolling railway rails |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
RU2569624C2 (en) * | 2013-12-11 | 2015-11-27 | Федеральное Государственное Бюджетное Образовательное Учреждение Высшего Профессионального Образования "Пензенский Государственный Университет Архитектуры И Строительства" | Method of rail production |
RU2668626C1 (en) * | 2017-05-02 | 2018-10-02 | Федеральное государственное автономное образовательное учреждение высшего образования "Уральский федеральный университет имени первого Президента России Б.Н. Ельцина" | Method of rolling rails |
CN107520249B (en) * | 2017-07-28 | 2020-02-07 | 包头钢铁(集团)有限责任公司 | Method for rolling steel rail by using all-universal four-roller finished hole pattern |
RU2684126C1 (en) * | 2018-02-26 | 2019-04-04 | Акционерное общество "ЕВРАЗ Объединенный Западно-Сибирский металлургический комбинат", АО "ЕВРАЗ ЗСМК" | Method of calibration of inclined calibers with alternative direction of inclination in duo stand rolls for rolling of railways |
RU2717251C1 (en) * | 2019-02-21 | 2020-03-19 | Федеральное государственное автономное образовательное учреждение высшего образования "Уральский федеральный университет имени первого Президента России Б.Н. Ельцина" | Method of rolling rails |
RU2710410C1 (en) * | 2019-05-06 | 2019-12-26 | Акционерное общество "ЕВРАЗ Объединенный Западно-Сибирский металлургический комбинат", АО "ЕВРАЗ ЗСМК" | Method of rolling rails |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2474905A1 (en) * | 1980-02-04 | 1981-08-07 | Sacilor | METHOD FOR PLACING RODS ON ROLLER CYLINDERS, METHOD AND DEVICE FOR FEEDING THESE RODS, ROLLING CYLINDERS HAVING SUCH RODS, ROLLER CAGES PROVIDED WITH SUCH CYLINDERS AND ROLLERS COMPRISING SUCH CAGES |
FR2490115A1 (en) * | 1980-09-15 | 1982-03-19 | Sacilor | METHOD FOR PLACING CANNELS, CYLINDERS, CAGES AND ROLLING MILLS FOR A FINISHED UNIVERSAL OR SEMI-UNIVERSAL CAGE OF REFUSED PASSES FOR RAILS |
US4393680A (en) * | 1981-07-30 | 1983-07-19 | Sms Schloemann-Siemag, Inc. | Method for rolling rails |
FR2543028B1 (en) * | 1983-03-21 | 1985-08-23 | Sacilor | PROCESS FOR FORMING A RAIL OF METAL RAIL |
SU1738394A1 (en) * | 1990-03-05 | 1992-06-07 | Украинский научно-исследовательский институт металлов | Method of rolling t-shapes |
SU1764722A1 (en) * | 1990-05-15 | 1992-09-30 | Челябинский Политехнический Институт Им.Ленинского Комсомола | Method for rolling i-sections |
ITMI20021594A1 (en) * | 2002-07-19 | 2004-01-19 | Danieli Off Mecc | METHOD AND SYSTEM FOR HOT ROLLING OF RAILS |
-
2010
- 2010-03-08 WO PCT/EP2010/001426 patent/WO2010105749A2/en active Application Filing
- 2010-03-08 UA UAA201112010A patent/UA103795C2/en unknown
- 2010-03-08 EP EP10709165A patent/EP2408967A2/en not_active Withdrawn
- 2010-03-08 RU RU2011141776/02A patent/RU2530609C2/en not_active IP Right Cessation
- 2010-03-08 AP AP2011005934A patent/AP2011005934A0/en unknown
-
2011
- 2011-08-19 ZA ZA2011/06122A patent/ZA201106122B/en unknown
Non-Patent Citations (1)
Title |
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None |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2014117519A1 (en) * | 2013-02-01 | 2014-08-07 | 中冶赛迪工程技术股份有限公司 | Compact universal vertical steel rail rolling method |
RU2784961C1 (en) * | 2021-12-27 | 2022-12-01 | Акционерное общество "ЕВРАЗ Объединенный Западно-Сибирский металлургический комбинат", АО "ЕВРАЗ ЗСМК" | Roughing pass system for rolling railway rails |
Also Published As
Publication number | Publication date |
---|---|
RU2011141776A (en) | 2013-04-27 |
UA103795C2 (en) | 2013-11-25 |
EP2408967A2 (en) | 2012-01-25 |
AP2011005934A0 (en) | 2011-10-31 |
RU2530609C2 (en) | 2014-10-10 |
ZA201106122B (en) | 2012-10-31 |
WO2010105749A3 (en) | 2011-01-27 |
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