WO2010048411A2 - Distributed measurement of mud temperature - Google Patents
Distributed measurement of mud temperature Download PDFInfo
- Publication number
- WO2010048411A2 WO2010048411A2 PCT/US2009/061693 US2009061693W WO2010048411A2 WO 2010048411 A2 WO2010048411 A2 WO 2010048411A2 US 2009061693 W US2009061693 W US 2009061693W WO 2010048411 A2 WO2010048411 A2 WO 2010048411A2
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- temperature
- heat transfer
- wellbore
- sub
- drill string
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01K—MEASURING TEMPERATURE; MEASURING QUANTITY OF HEAT; THERMALLY-SENSITIVE ELEMENTS NOT OTHERWISE PROVIDED FOR
- G01K1/00—Details of thermometers not specially adapted for particular types of thermometer
- G01K1/02—Means for indicating or recording specially adapted for thermometers
- G01K1/026—Means for indicating or recording specially adapted for thermometers arrangements for monitoring a plurality of temperatures, e.g. by multiplexing
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01K—MEASURING TEMPERATURE; MEASURING QUANTITY OF HEAT; THERMALLY-SENSITIVE ELEMENTS NOT OTHERWISE PROVIDED FOR
- G01K1/00—Details of thermometers not specially adapted for particular types of thermometer
- G01K1/02—Means for indicating or recording specially adapted for thermometers
- G01K1/022—Means for indicating or recording specially adapted for thermometers for recording
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH OR ROCK DRILLING; MINING
- E21B—EARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B47/00—Survey of boreholes or wells
- E21B47/06—Measuring temperature or pressure
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH OR ROCK DRILLING; MINING
- E21B—EARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B47/00—Survey of boreholes or wells
- E21B47/06—Measuring temperature or pressure
- E21B47/07—Temperature
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01K—MEASURING TEMPERATURE; MEASURING QUANTITY OF HEAT; THERMALLY-SENSITIVE ELEMENTS NOT OTHERWISE PROVIDED FOR
- G01K7/00—Measuring temperature based on the use of electric or magnetic elements directly sensitive to heat ; Power supply therefor, e.g. using thermoelectric elements
- G01K7/42—Circuits effecting compensation of thermal inertia; Circuits for predicting the stationary value of a temperature
Definitions
- the invention disclosed herein relates to exploration for oil and gas and, in particular, to evaluation of temperature profiles downhole.
- elevated temperatures present a harsh environment to equipment downhole, but, the elevated temperatures may be indicative of properties of materials downhole.
- An embodiment of the invention includes a method for estimating a temperature within sub-surface materials traversed by a wellbore, the method including: obtaining temperature data from a plurality of measurements of temperature taken within the wellbore; calculating an overall heat transfer coefficient from the measurement data; calculating a geothermal gradient from the overall heat transfer coefficient; and using the geothermal gradient to estimate the temperature within the sub-surface materials.
- Another embodiment of the invention includes a system for determining a temperature of sub-surface materials, the system including: a plurality of temperature sensors distributed along a drill string, the drill string providing for a wellbore that traverses the sub-surface materials; and a processor for receiving temperature data from the from the plurality of temperature sensors along at least a portion of the wellbore and for implementing machine executable instructions for calculating an overall heat transfer coefficient from the measurement data; calculating a geothermal gradient from the overall heat transfer coefficient; and using the geothermal gradient to estimate the temperature within the sub-surface materials.
- Yet another embodiment of the invention includes a computer program product stored on machine readable media and including machine executable instructions for estimating a temperature in sub-surface materials, by implementing a method including: receiving temperature data from a plurality of measurements of temperature taken within a wellbore traversed by a logging instrument; calculating an overall heat transfer coefficient from the measurement data; calculating a geothermal gradient from the overall heat transfer coefficient; using the geothermal gradient to estimate the temperature within the sub-surface materials; and outputting the estimate to a user.
- FIG. 1 depicts aspects of a drilling apparatus, and shows a flow of drilling fluid within a borehole
- FIG. 2 is a flow chart providing an exemplary method for estimating temperatures related to a borehole
- FIG. 3 depicts aspects of a temperature profile within a drillstring and a wellbore
- FIG. 4 depicts relationships of temperature parameters as a function of depth
- FIG. 5 depicts aspects of temperature averaging. DETAILED DESCRIPTION OF THE INVENTION
- Measurement of pipe and bore fluid temperatures along a drill string can be used to infer the far-field formation temperature gradient, which is affected by the volume of contained water, and hence pore pressure.
- the temperature data may be used for cementing operations in estimation of the needed cement properties, monitoring of the setting of the cement, and for other aspects as deemed appropriate.
- Knowledge of the far-field temperature and temperature gradient is therefore important for pore pressure prediction, cementing operations, and correction of measurements made by wireline or measurement-while-drilling tools, among others.
- the term "far-field” as used herein relates to being away from the influence or effects of the borehole.
- the techniques take advantage of flow line measurement data, and assume conditions of steady state heat flow within the borehole. That is, it is considered that heat flow across the various thermal resistances within the borehole is relatively constant, and therefore independent of time. It is recognized that, in general, under normal operational wellsite conditions, that such assumptions are more reliable once the wellbore has been circulated continuously for at least one circulation. Before discussing the invention in detail, some context is provided.
- FIG. 1 an exemplary embodiment of an apparatus for performing logging while drilling is shown.
- a section of earth 1 which includes at least one formation 2, is penetrated by a drill string 3.
- the drill string 3 drives a drill bit 4.
- the drill bit 4 also provides a flow of a drilling fluid 5, such as drilling mud. That is, the drilling fluid 5 may be pumped downhole through the drilling pipe 8, and thus resulting in a flow of drilling fluid 6 that is provided upward within a borehole 7 (also referred to as a "wellbore").
- a drilling fluid 5 such as drilling mud
- the drill string 3 may include a plurality of sections of the drill pipe 8.
- the drill pipe 8 may include wired pipe providing users with a communications channel.
- Included within the drill string 3 may be at least one logging apparatus 9.
- Exemplary logging apparatus include devices implementing resistivity, nuclear magnetic resonance, acoustic, seismic and other such technologies.
- a package of downhole electronics 10 included with the logging apparatus 9 is a package of downhole electronics 10.
- the downhole electronics 10 generally provide for collection and/or communication of downhole data to a package of surface based electronics 11.
- Included in this drill string 3 is a plurality of temperature sensors 12.
- the drill string 3 may also be referred to as "drill stem,” and by other similar terms.
- the logging apparatus 9 and the associated electronics 10, 11 provide for such tasks as imaging of the at least one formation 2.
- the logging apparatus 9 and the associated electronics 10, 11 may provide for collection and/or communication of other information, such as temperature from each of the temperature sensors 12.
- each of the temperature sensors 12 is disposed such that the respective temperature sensor 12 is operable for detection of local temperature, including a temperature of the drilling fluid 5.
- Each of the temperature sensors 12 provides a signal to at least one of the electronics units 10, 11.
- each temperature sensor 12 communicates an identity with the sensor output.
- the electronics units 10, 11 are provided with adequate information for determining a temperature gradient within the borehole 7.
- each of the electronics unit(s) 10, 11 may, alone or in combination, further estimate a far-field temperature (i.e., a temperature within some portion of the earth 1 and/or the formation 2).
- bore temperature and annulus temperature is measured at an outlet and an inlet (suction pit), and at several locations along the drillstring 3. These measurements, which may be made in real-time, are used by a temperature model to predict the far-field temperature. Since abnormal temperature gradients occur above and through intervals of abnormal pore-pressure, the predictions of far-field temperature may be used in real-time, such as while drilling. In some embodiments, modeling calls for use of other measurements, such as revolutions per minute (RPM), and formation properties (such as porosity). Accordingly, now consider certain input information useful for modeling far- field temperature. [0016] Inputs useful for modeling far-field temperature include geometry of the borehole 7 (also referred to as a "wellbore").
- the information may include, for example, presence, number, dimensions and/or quality of: casing strings, holes, cemented intervals and other such information.
- Mud composition may be used as an input and may consider, for example: particle properties, constituent identities and types, oil percentage, heat capacity, etc,... Also of interest is the temperature inside the drill string 3 and outside of the drill string 3.
- Output of models used for estimating the far-field temperature include: a far- field formation temperature gradient; a drilled interval formation temperature gradient; a bottom hole circulating temperature; and a formation temperature.
- T P K ⁇ e c ' x) + K 2 e C2X) + G ⁇ + ⁇ s - GA (i)
- T a K>Cj c ' K) + K 2 C 4 e C2X) + Gx + T s ⁇ ?>>
- T p represents temperature in the drillstem at depth (x), in degrees Farenheit (°F); T a represents temperature in the annulus at depth (x), in degrees
- A m * Cp/(2 ⁇ * rp 0 * up 0 ) (4)
- B rU a / (rp o * upo) (5) where m represents mass flow rate, in lb/hr;
- C p represents mud heat capacity, in Btu (lb-°F); rpo radius of drillpipe (outer diameter), in ft; upo overall heat transfer coefficient across the drillpipe, in - 0 F - hr); r represents hole radius, in ft; and,
- H represents total well depth (i.e., bit depth), in ft; Tp 1n represents mud inlet temperature, in ° F; T HP represents drill stem temperature at depth H; T Ha represents annulus temperature at depth H.
- Ta Ta 0 Ut (B3) where Ta 0Ut represents flowline temperature, in °F.
- T fnm H * G + Ts (10).
- the method 20 includes six stages (21- 26).
- a first stage 21 geometry of the borehole 7 is used (along with knowledge of aspects of a composition of the drilling fluid 5) to calculate heat transfer coefficients for each section of the borehole 7.
- the heat transfer coefficients are averaged, using as a base the amount of time the fluid is in each section of the hole.
- a third stage 23 the temperature inside the drill string 3 and the temperature outside of the drill string 3 is averaged.
- a geothermal gradient is calculated at a total depth. This may be calculated, for example, by using Eqs. (3, 4, 5 and 8).
- a temperature of the formation is calculated at the total depth. This may be calculated, for example, by using Eq. (10).
- a bottom hole circulating temperature (BHCT) is calculated. This may be calculated, for example, by using Eqs. (6, 7 and either 1 or 2).
- the heat transfer coefficients are "combined.” That is, for example, the heat transfer coefficients may be fit, such as by use of a linear fit, logarithmic fit, exponential fit, a fit to a power function, a weighted fit or some other type of relationship.
- Cp Heat capacity of mud, (Cp), may be calculated using the weight by volume of the individual components in the mud.
- API gravity refers to a measure of how heavy or light a petroleum liquid is compared to water
- a j represents 2 ⁇ rp o * AL , or the surface area, outside wall drillstem; and ⁇ T j represents (Tf - Tp) or the temperature of fluid at the formation and wellbore interface - temperature of fluid in the pipe.
- Tp represents temperature of the fluid inside the pipe, 0 F
- Tp 1 represents temperature, inside pipe wall, 0 F
- K p ⁇ e represents thermal conductivity, drillpipe, Btu/(hr-ft-°F)
- Ta annular fluid temperature
- Tp 0 represents temperature outside pipe wall, 0 F
- ⁇ L represents length of section of interest
- FIG. 3 for a graphic depiction of certain relationships between some of these parameters.
- Equation (14) can be rearranged as follows: dT Q i r J J r y and,
- hj represents a film coefficient of the annulus wall.
- the overall heat transfer coefficients can be evaluated based on film coefficients and the thermal conductivities of the "solid" wellbore geometry elements.
- the thermal conductivities for various materials are listed below; a general method for evaluating film coefficients is given later herein.
- K 011 ⁇ 77 [i _ o.OOO3(r - 32)]. Btu/(hr - f t - 0 F);
- Kc thermal conductivity, continuous phase
- ⁇ represents porosity, fractional
- NNU aNRE b NpR c when
- coefficients a, b, and c depend on the flow regime (laminar, transition, turbulent), defined as follows:
- NNU * c ; where a, b, and c are coefficients
- a solution for the film coefficient in the transition flow regime may be further approximated by the following equation:
- some embodiments further take into account at least one operational factor, such as an RPM of the drill string 3, length of interest, radius, flow rate, volume (such as of drilling mud within the drill string 3, or total volume within the wellbore) and others.
- at least one operational factor such as an RPM of the drill string 3, length of interest, radius, flow rate, volume (such as of drilling mud within the drill string 3, or total volume within the wellbore) and others.
- the individual heat transfer coefficients may be averaged based on the time the mud packet is in each section.
- U 31 be the i ⁇ drillpipe and wellbore heat transfer coefficient. In this case:
- At 1 is the time, in minutes, that the mud packet is in any distinct wellbore section having a constant Up 0 or Ua. ⁇ t, can be calculated from:
- an average flow rate may be given by:
- Q represents mud read flow rate
- gpm and ⁇ tr represents mud sample interval, time (seconds or minutes).
- Ad be a depth increment.
- Formation temperature is represented as the average temperature over the interval Ad. This is reasonably accurate if Ad is small in relation to D. Refer to FIG. 4.
- the model assumes a linear geothermal gradient and the mud packet must pass over a length of formation (wellbore wall) equal to Z) + Ad.
- Average mud temperature out for a depth increment Ad is simply the lagged mud temperature for the depth, or D + Ad.
- ⁇ S represents an averaging base.
- the averaging is triggered “on” when the return depth is D and triggered “off when the return depth is D + ⁇ d.
- the average temperature in is, however, not so straightforward. As the mud packet is being circulated to the surface, it is influenced by the temperature in the drillstem, which is governed by the temperature in over the circulation period. At the start of the drilled interval, however, the drillstem contains mud which entered the pipe while the prior interval was being drilled.
- the "temperature in,” which influences the temperature out, may therefore be represented as being the average of: 1. average mud temperature in for a volume equivalent to the volume of the drillstem at depth D; 2. average mud temperature in during the drilled interval ⁇ d; and 3. average mud temperature in while the mud packet for depth D + ⁇ d is being circulated out.
- Item 1 requires the prediction of the depth D for online averaging (unless raw data is stored in arrays). Its contribution to the overall average is however small, and it may be ignored.
- the average mud temperature in is therefore:
- ⁇ S represents an averaging base.
- the averaging is triggered “on” when the bit is at depth D and triggered “off when the returns depth is Z) + ⁇ d. This is shown diagrammatically in FIG. 5. However, it should be noted that there will be overlap in the average temperature in for sequential depth increments, and the monitor will contain N average temperature in values (being updated "simultaneously") for N mud packets in the wellbore annulus.
- the foregoing equations represent, in detail, a straightforward method of calculating formation temperatures and both annular and drillstem circulating temperatures.
- the method provided is illustrative. For example, finite difference methods or finite element methods may be used. In general, the method provides results that are within a few degrees. Also, note that temperature measurements made at locations along the drill string 3 may be used to specify other boundary conditions and the model may be modified, or another model developed to include them.
- the term “formations” may refer to the various features and materials that may be encountered in a subsurface environment. Accordingly, it should be considered that while the term “formation” generally refers to geologic formations of interest, that the term “formations,” as used herein, may, in some instances, include any geologic points or volumes of interest (such as a survey area). In general, the terms formation, formations, and other such terms are in reference to any volume of sub-surface materials that may be of interest.
- a logging instrument such as a instrument deployed in wireline logging of a wellbore - or by a drill string
- a drill string may make use of the technology provided herein.
- generation of data in "real time” is taken to mean generation of data at a rate that is useful or adequate for making decisions during or concurrent with processes such as production, experimentation, verification, and other types of surveys or uses as may be opted for by a user or operator.
- real-time measurements and calculations may provide users with information necessary to make desired adjustments during the drilling process.
- adjustments are enabled on a continuous basis (at the rate of drilling), while in another embodiment, adjustments may require periodic cessation of drilling for assessment of data. Such adjustments may also be useful in geosteering applications.
- various analysis components may be used, including digital and/or an analog systems.
- the system may have components such as a processor, storage media, memory, input, output, communications link (wired, wireless, pulsed mud, optical or other), user interfaces, software programs, signal processors (digital or analog) and other such components (such as resistors, capacitors, inductors and others) to provide for operation and analyses of the apparatus and methods disclosed herein in any of several manners well-appreciated in the art.
- teachings may be, but need not be, implemented in conjunction with a set of computer executable instructions stored on a computer readable medium, including memory (ROMs, RAMs), optical (CD-ROMs), or magnetic (disks, hard drives), or any other type that when executed causes a computer to implement the method of the present invention.
- ROMs, RAMs random access memory
- CD-ROMs compact disc-read only memory
- magnetic (disks, hard drives) any other type that when executed causes a computer to implement the method of the present invention.
- These instructions may provide for equipment operation, control, data collection and analysis and other functions deemed relevant by a system designer, owner, user or other such personnel, in addition to the functions described in this disclosure.
- a sample line, sample storage, sample chamber, sample exhaust, pump, piston, power supply e.g., at least one of a generator, a remote supply and a battery
- vacuum supply e.g., at least one of a generator, a remote supply and a battery
- refrigeration i.e., cooling
- heating component e.g., heating component
- motive force such as a translational force, propulsional force or a rotational force
- magnet electromagnet
- sensor electrode
- transmitter, receiver, transceiver e.g., transceiver
- antenna e.g., a transceiver
- controller e.g., optical unit, electrical unit or electromechanical unit
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- Mining & Mineral Resources (AREA)
- General Physics & Mathematics (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Fluid Mechanics (AREA)
- Environmental & Geological Engineering (AREA)
- Geochemistry & Mineralogy (AREA)
- Geophysics (AREA)
- Measuring Temperature Or Quantity Of Heat (AREA)
- Investigating Or Analyzing Materials Using Thermal Means (AREA)
- Geophysics And Detection Of Objects (AREA)
- Fertilizers (AREA)
- Excavating Of Shafts Or Tunnels (AREA)
Abstract
Description
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Priority Applications (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB1105037.4A GB2476749B (en) | 2008-10-22 | 2009-10-22 | Distributed measurement of mud temperature |
| BRPI0920127A BRPI0920127A2 (en) | 2008-10-22 | 2009-10-22 | distributed temperature measurement of mud |
| NO20110503A NO343253B1 (en) | 2008-10-22 | 2011-04-01 | Distributed measurement of temperature in drilling mud during well drilling |
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10737508P | 2008-10-22 | 2008-10-22 | |
| US61/107,375 | 2008-10-22 | ||
| US12/582,742 US8543336B2 (en) | 2008-10-22 | 2009-10-21 | Distributed measurement of mud temperature |
| US12/582,742 | 2009-10-21 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| WO2010048411A2 true WO2010048411A2 (en) | 2010-04-29 |
| WO2010048411A3 WO2010048411A3 (en) | 2010-07-08 |
Family
ID=42118313
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PCT/US2009/061693 Ceased WO2010048411A2 (en) | 2008-10-22 | 2009-10-22 | Distributed measurement of mud temperature |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US8543336B2 (en) |
| BR (1) | BRPI0920127A2 (en) |
| GB (1) | GB2476749B (en) |
| NO (1) | NO343253B1 (en) |
| WO (1) | WO2010048411A2 (en) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2397649A1 (en) * | 2010-06-10 | 2011-12-21 | BP Exploration Operating Company Limited | Method and system for determining relative mass fluxes |
| MY182683A (en) * | 2013-06-20 | 2021-01-29 | Halliburton Energy Services Inc | Device and method for temperature detection and measurement using integrated computational elements |
| CA2980439A1 (en) * | 2015-06-15 | 2016-12-22 | Halliburton Energy Services, Inc. | Application of time derivative of distributed temperature survey (dts) in identifying cement curing time and cement top |
| CN105134179B (en) * | 2015-08-21 | 2018-02-02 | 中国石油天然气股份有限公司 | A Calculation Method of Distribution Data of Wellbore Pressure and Temperature of Natural Gas Well |
| EP3428745A1 (en) * | 2017-07-11 | 2019-01-16 | Endress+Hauser Wetzer GmbH+CO. KG | Determination of a spatial distribution of a process variable |
| US11920464B2 (en) * | 2020-01-31 | 2024-03-05 | Halliburton Energy Services, Inc. | Thermal analysis of temperature data collected from a distributed temperature sensor system for estimating thermal properties of a wellbore |
| CN112528218B (en) * | 2020-11-20 | 2022-04-15 | 西南石油大学 | Method for determining cement curing temperature of underground real environment |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2538849A1 (en) * | 1982-12-30 | 1984-07-06 | Schlumberger Prospection | METHOD AND DEVICE FOR DETERMINING THE FLOW PROPERTIES OF A FLUID IN A WELL FROM TEMPERATURE MEASUREMENTS |
| US4575261A (en) * | 1983-06-30 | 1986-03-11 | Nl Industries, Inc. | System for calculating formation temperatures |
| US4765183A (en) * | 1987-03-12 | 1988-08-23 | Coury Glenn E | Apparatus and method for taking measurements while drilling |
| US6206108B1 (en) * | 1995-01-12 | 2001-03-27 | Baker Hughes Incorporated | Drilling system with integrated bottom hole assembly |
| US5892860A (en) * | 1997-01-21 | 1999-04-06 | Cidra Corporation | Multi-parameter fiber optic sensor for use in harsh environments |
| GB9916022D0 (en) * | 1999-07-09 | 1999-09-08 | Sensor Highway Ltd | Method and apparatus for determining flow rates |
| US6585408B2 (en) * | 2001-07-30 | 2003-07-01 | General Electric Company | Method and apparatus for measuring local heat transfer distribution on a surface |
| US6789937B2 (en) * | 2001-11-30 | 2004-09-14 | Schlumberger Technology Corporation | Method of predicting formation temperature |
| WO2005035943A1 (en) * | 2003-10-10 | 2005-04-21 | Schlumberger Surenco Sa | System and method for determining flow rates in a well |
| US20050149264A1 (en) * | 2003-12-30 | 2005-07-07 | Schlumberger Technology Corporation | System and Method to Interpret Distributed Temperature Sensor Data and to Determine a Flow Rate in a Well |
| JP4789450B2 (en) * | 2004-11-04 | 2011-10-12 | パナソニック株式会社 | Line quality reporting method, base station apparatus and communication terminal |
| CA2503268C (en) * | 2005-04-18 | 2011-01-04 | Core Laboratories Canada Ltd. | Systems and methods for acquiring data in thermal recovery oil wells |
| US20070278009A1 (en) * | 2006-06-06 | 2007-12-06 | Maximo Hernandez | Method and Apparatus for Sensing Downhole Characteristics |
| US7937999B2 (en) * | 2006-09-26 | 2011-05-10 | Baker Hughes Incorporated | Estimating formation temperature near a borehole and using same for estimating a property of the formation |
| WO2010031052A2 (en) * | 2008-09-15 | 2010-03-18 | Bp Corporation North America Inc. | Method of determining borehole conditions from distributed measurement data |
| US8727035B2 (en) * | 2010-08-05 | 2014-05-20 | Schlumberger Technology Corporation | System and method for managing temperature in a wellbore |
-
2009
- 2009-10-21 US US12/582,742 patent/US8543336B2/en active Active
- 2009-10-22 BR BRPI0920127A patent/BRPI0920127A2/en not_active IP Right Cessation
- 2009-10-22 GB GB1105037.4A patent/GB2476749B/en active Active
- 2009-10-22 WO PCT/US2009/061693 patent/WO2010048411A2/en not_active Ceased
-
2011
- 2011-04-01 NO NO20110503A patent/NO343253B1/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| US8543336B2 (en) | 2013-09-24 |
| NO20110503A1 (en) | 2011-05-02 |
| GB201105037D0 (en) | 2011-05-11 |
| GB2476749A (en) | 2011-07-06 |
| US20100106421A1 (en) | 2010-04-29 |
| NO343253B1 (en) | 2018-12-27 |
| WO2010048411A3 (en) | 2010-07-08 |
| GB2476749B (en) | 2015-07-08 |
| BRPI0920127A2 (en) | 2017-10-24 |
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