WO2010035883A1 - Method for forming deformed cross-section and formed article of quadrilateral cross-section exhibiting excellent spot weldability - Google Patents
Method for forming deformed cross-section and formed article of quadrilateral cross-section exhibiting excellent spot weldability Download PDFInfo
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- WO2010035883A1 WO2010035883A1 PCT/JP2009/067123 JP2009067123W WO2010035883A1 WO 2010035883 A1 WO2010035883 A1 WO 2010035883A1 JP 2009067123 W JP2009067123 W JP 2009067123W WO 2010035883 A1 WO2010035883 A1 WO 2010035883A1
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21D—WORKING OR PROCESSING OF SHEET METAL OR METAL TUBES, RODS OR PROFILES WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21D26/00—Shaping without cutting otherwise than using rigid devices or tools or yieldable or resilient pads, i.e. applying fluid pressure or magnetic forces
- B21D26/02—Shaping without cutting otherwise than using rigid devices or tools or yieldable or resilient pads, i.e. applying fluid pressure or magnetic forces by applying fluid pressure
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21D—WORKING OR PROCESSING OF SHEET METAL OR METAL TUBES, RODS OR PROFILES WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21D26/00—Shaping without cutting otherwise than using rigid devices or tools or yieldable or resilient pads, i.e. applying fluid pressure or magnetic forces
- B21D26/02—Shaping without cutting otherwise than using rigid devices or tools or yieldable or resilient pads, i.e. applying fluid pressure or magnetic forces by applying fluid pressure
- B21D26/033—Deforming tubular bodies
- B21D26/041—Means for controlling fluid parameters, e.g. pressure or temperature
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21D—WORKING OR PROCESSING OF SHEET METAL OR METAL TUBES, RODS OR PROFILES WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21D26/00—Shaping without cutting otherwise than using rigid devices or tools or yieldable or resilient pads, i.e. applying fluid pressure or magnetic forces
- B21D26/02—Shaping without cutting otherwise than using rigid devices or tools or yieldable or resilient pads, i.e. applying fluid pressure or magnetic forces by applying fluid pressure
- B21D26/033—Deforming tubular bodies
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21D—WORKING OR PROCESSING OF SHEET METAL OR METAL TUBES, RODS OR PROFILES WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21D51/00—Making hollow objects
- B21D51/02—Making hollow objects characterised by the structure of the objects
- B21D51/06—Making hollow objects characterised by the structure of the objects folded objects
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21D—WORKING OR PROCESSING OF SHEET METAL OR METAL TUBES, RODS OR PROFILES WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21D51/00—Making hollow objects
- B21D51/16—Making hollow objects characterised by the use of the objects
Definitions
- the conventional profile forming technology using hydroforming has a problem that it is difficult to obtain a molded product having a profile with a high dimensional accuracy and excellent spot weldability.
- the irregular cross section refers to a cross section such as a quadrangular cross section other than a circular form.
- a method for forming an irregular cross-section characterized in that: (4) In any one of the above (1) to (3), a modified cross-section forming method characterized by using a steel pipe having a thickness / outer diameter ratio t / D of 0.05 or less as the pipe material. (5) A quadrilateral cross-section molded product having one or two parallel two sides formed by molding a tubular material by the modified cross-section molding method according to any one of (1) to (4) above, One or two parallel 2 excellent in spot weldability, characterized in that (hollow depth on flat surface or depth of hollow on flat surface) is 0.5 mm or less, and further, the corner radius of curvature R is 10 mm or less. A quadrilateral cross-section molded product with sides.
- the tube material is a tube material having a tensile strength of 690 MPa or more, and after crushing with the deformed section mold, the tube material is deformed by continuously applying an internal pressure with the liquid.
- the maximum internal pressure is an internal pressure that satisfies both Pmin and more and more than 50 MPa, and the peripheral length increase rate after molding is A% or more and 11.0% or less below.
- A 4.167 ⁇ 10 ⁇ 3 ⁇ (TS-590)
- TS Tensile strength of pipe (MPa)
- TS Tensile strength of pipe (MPa)
- a steel pipe having a tensile strength of 780 MPa or more is used as the pipe material, and molding is performed such that the peripheral length increase rate after molding is A% or more and 10.0% or less below.
- a modified cross-section molding method characterized.
- A 4.167 ⁇ 10 ⁇ 3 ⁇ (TS-590)
- TS Tensile strength of pipe (MPa)
- (12) In combination with the internal pressure load after the crushing process, the tube end is loaded with a compressive force in the tube axis direction, and the tube end is pushed toward the center in the tube axis direction. Section forming method. (13) In the above (11) or (12), a steel pipe having a tensile strength of 780 MPa or more is used as the pipe, and the peripheral length increase rate after forming is formed to be A% or more and 10.0% or less below.
- a modified cross-section molding method characterized by the above.
- FIG. 1 is an explanatory diagram showing an outline of the method of the present invention.
- a metal tube having a tensile strength (abbreviated as TS (tensile strength)) of 590 MPa or more, for example, a steel tube is used.
- TS tensile strength
- the tube material 10 is loaded into a mold having at least one flat portion, for example, a mold 1A having a pair of upper and lower flat portions.
- the mold cross-sectional shape of the molds 1 and 1 ⁇ / b> A is a cross-sectional shape different from that of the tube material 10.
- the tube material 10 may be either preformed or not.
- the method without an internal pressure load on the pipe material includes two cases where the liquid is not contained in the pipe and the case where no internal pressure is generated by the liquid even if the liquid is contained in the pipe. .
- preparation by injecting liquid is performed while crushing.
- a recess (referred to as a flat portion recess) is formed in the tube wall portion facing the flat portion of the mold, and the tube wall portion facing the corner portion of the mold is loosely formed. Corner R is formed.
- the pipe is continuously loaded with an internal pressure that causes the maximum internal pressure to be equal to or higher than the following P min [MPa] while being clamped of upper of die and lower die, so that the pipe has a deformed cross-sectional shape. Molding is performed (FIG. 1C).
- P min 0.045 ⁇ TS (1)
- P min lower limit of maximum internal pressure [MPa]
- TS tensile strength of pipe material [MPa]
- the coefficient on the right side is 0.09 instead of 0.045, more preferably 0.12, because the shape of the molded product is further improved.
- the maximum internal pressure is usually about 100 to 200 MPa for the following reason.
- the performance of a pressure intensifier that applies internal pressure is 200 MPa at maximum.
- the projected area (or mold cavity projected area) in the horizontal plane of the molded product is excessive, it may be set to less than 200 MPa, for example, 150 MPa due to the limitation of the press force of the pressure intensifier. If there is no restriction as described above and the raw tube is thin and low in strength, sufficient straightening may be possible at 100 MPa.
- the peripheral length increase rate after molding is 2.0% or more and 10.0% or less.
- the flat portion dent amount tends to increase as the t / D increases, so that the t / D of the pipe material is 0. It is preferable to use a steel pipe of .05 or less.
- the radius of curvature R (see FIG. The definition is shown in Fig. 2.
- the specific measurement method is to cut a cross-section molded product with a plane perpendicular to the longitudinal direction, capture cross-sectional photographs of all corners in the image, and draw circles with various radii of curvature.
- the curvature radius R of all corners was obtained by overlapping the corners, and the maximum radius R was set as the corner curvature radius R.) was 10 mm or less.
- the reason why the lower limit P min [MPa] of the internal pressure (maximum internal pressure) when the internal pressure applied after crushing is maximized in the present invention is defined as the value of the above equation (1) will be described.
- the flat portion dent amount of the molded product is 0.
- the molding conditions were examined so that the corner radius of curvature R would be 10 mm or less.
- both the flat portion dent amount and the corner radius of curvature R decrease. It was found that this should be the lower limit of the maximum internal pressure.
- the relationship between this lower limit and the TS of the pipe material is as shown in FIG. 4. From FIG. 4, when TS is 590 MPa or more, the lower limit P min of the maximum internal pressure is expressed by the above formula (1).
- the flat part dent amount and the peripheral length increase rate dependency of the corner R were obtained, and the following knowledge was obtained. That is, when the maximum internal pressure after crushing is set to P min or more and the tube TS is 780 MPa or more, the flat portion dent amount is further reduced when the product peripheral length increase rate is 2.0% or more. Further, it is a finding that when the product peripheral length increase rate is 10.0% or less, the corner radius of curvature R is further reduced.
- the peripheral length increase rate after molding is 2.0 to 10.0%. It is better to mold it.
- the internal pressure used for molding after crushing is determined by finding the correspondence between the maximum internal pressure and the peripheral length increase rate by FEM (finite element method) analysis and experiment, and this correspondence corresponds to the target peripheral length increase rate. It is better to set the maximum internal pressure.
- tensile If strength is used tubing 10 above 690 MPa, as described above, maximum pressure is the by the liquid to continue tube while clamping (1) a defined P min [MPa ]
- An internal pressure satisfying both the above-described internal pressure and over 50 MPa is loaded, and molding is performed so that the peripheral length increase rate after hydroforming is not less than A% and not more than 11.0%.
- the circumference increase rate is given by the following equation.
- a flat part dent further reduces, and a corner (R material) overhangs a corner R part, and becomes a sharper (small curvature radius) R shape.
- the coefficient on the right side is 4.8 ⁇ 10 ⁇ 3 instead of 4.167 ⁇ 10 ⁇ 3 , the shape of the molded product (flat recess or corner R portion) is further improved. This is preferable.
- the material when the internal pressure is applied after crushing, the material may overhang, resulting in an excessive reduction in the thickness near the corner R.
- a compressive force in the tube axis direction is applied to the tube end and the tube end is pushed toward the center in the tube axis direction (this is referred to as “shaft pushing”). Therefore, it is possible to reduce the thickness reduction.
- the preferable condition for “shaft pushing” is to adjust the cylinder stroke (cylinder stroke) of the press machine for shaft pushing so that the push-in amount (stroke) is 0 to the length of the molded part of the final product after hydrofume processing. About 10% is preferable.
- the flat portion dent amount tends to increase as the t / D increases, so that the t / D of the pipe material is 0. It is preferable to use a steel pipe of .05 or less.
- the corner radius of curvature R decreases as the circumference increase rate increases, and the circumference increase rate when the corner radius of curvature R becomes 10 mm is the upper limit.
- the peripheral length increase rate is preferably 11.0% or less.
- the peripheral length increase rate is preferably 10.0% or less.
- a tube material having the TS and size shown in Table 1 was formed into a deformed cross section in the following steps.
- the pipe materials used were all ERW steel pipes.
- Table 2 shows the composition of the steel sheets of materials 1-33 and the manufacturing method of the steel sheets.
- the length of the steel pipe used for the Example was 300 mm.
- the steel plate 12 is placed on the upper flat portion of the product 11, and the electrode 3 is pressed against it with a constant pressure (50 to 200 Kgf) to perform one-side spot welding for each three pieces.
- a constant pressure 50 to 200 Kgf
- welding conditions energization time: 10 to 20 cycles (50 Hz), welding current: 5 to 10 KA
- Whether or not spot weldability is determined is determined by the presence or absence of nugget formation and a tensile shear test (JIS).
- JIS tensile shear test
- Z 3136 is performed with a tensile shear load, and the following two-stage evaluation of ⁇ and ⁇ is made.
- the pipe after crushing using the upper and lower molding dies, the pipe is continuously loaded with an internal pressure by a liquid, and the maximum internal pressure is in an appropriate range, more preferably, the rate of increase in peripheral length after molding is in the appropriate range.
- the tubular material can be formed into a deformed cross-sectional shape having a curvature radius R of a corner with a small flat portion dent amount and a sharp outline (small curvature radius). Since the obtained deformed cross-section molded product has a small flat portion dent amount, it is excellent in one-side spot weldability with a metal plate. Further, the deformation of the springback after unloading is suppressed, and a deformed cross-section molded product with high dimensional accuracy is obtained.
Abstract
Description
ここで、異形断面とは円形(circular form)以外の、例えば、四辺形断面のような断面をいう。 In other words, the conventional profile forming technology using hydroforming has a problem that it is difficult to obtain a molded product having a profile with a high dimensional accuracy and excellent spot weldability.
Here, the irregular cross section refers to a cross section such as a quadrangular cross section other than a circular form.
(1)引張強さ590MPa以上の管材に、内圧を負荷しない状態もしくは液体により50MPa以下の内圧を負荷した状態で、少なくとも1つの面が平坦部を有する異形断面金型にて潰し加工を行い、引続き前記液体により最高内圧が下記Pmin[MPa]以上になる内圧を負荷して、前記管材を異形断面形状に成形することを特徴とする異形断面成形方法。 The inventors have intensively studied to solve the above-mentioned problems. As a result, the inventors have conceived a means for realizing a high-dimensional precision deformed cross-section molded article that facilitates spot welding by hydroforming, and have made the present invention. That is, the present invention is as follows.
(1) In a state where no internal pressure is applied to a pipe material having a tensile strength of 590 MPa or more or an internal pressure of 50 MPa or less is applied with a liquid, crushing is performed with a deformed cross-section mold having at least one flat surface, A deformed cross-section forming method, wherein the tube is formed into a deformed cross-sectional shape by continuously applying an internal pressure at which the maximum internal pressure is equal to or higher than the following P min [MPa] by the liquid.
Pmin=0.045×TS
Pmin:最高内圧の下限[MPa]、TS:管材の引張強さ[MPa]
(2)前記潰し加工後の内圧負荷と併せて、管端(tube end)に管軸方向(tube axis direction)の圧縮力(compression force)を負荷して管端を管軸方向中央側に押し込むことを特徴とする上記(1)に記載の異形断面成形方法。
(3)上記(1)または(2)において、前記管材として引張強さ780MPa以上の鋼管を用い、成形後の周長増加率(increasing rate of girth)が2.0%以上10.0%以下となるように成形することを特徴とする異形断面成形方法。
(4)上記(1)~(3)のいずれかにおいて、前記管材として肉厚/外径比t/Dが0.05以下である鋼管を用いることを特徴とする異形断面成形方法。
(5)管材を上記(1)~(4)のいずれかに記載の異形断面成形方法で成形してなる一又は二の平行2辺を有する四辺形断面成形品であって、平坦部凹み量(hollow depth on flat surface or depth of hollow on flat surface)が0.5mm以下であり、さらにコーナーの曲率半径Rが10mm以下であることを特徴とするスポット溶接性に優れた一又は二の平行2辺を有する四辺形断面成形品。
(6)上記(1)において、前記管材が引張強さ690MPa以上の管材であり、前記異形断面金型にて潰し加工を行った後、引続き前記液体により内圧を負荷して、前記管材を異形断面形状に成形するにあたり、前記最高内圧が、Pmin以上および、50MPa超えの両方を満足する内圧を加え、さらに、成形後の周長増加率が下記A%以上11.0%以下となるように成形することを特徴とする異形断面成形方法。 P min = 0.045 × TS
P min : lower limit of maximum internal pressure [MPa], TS: tensile strength of pipe material [MPa]
(2) Along with the internal pressure load after the crushing process, a tube axis direction compression force is applied to the tube end and the tube end is pushed toward the center in the tube axis direction. The method for forming an irregular cross-section as described in (1) above, wherein
(3) In the above (1) or (2), a steel pipe having a tensile strength of 780 MPa or more is used as the pipe material, and an increasing rate of circumference after molding is 2.0% or more and 10.0% or less. A method for forming an irregular cross-section, characterized in that:
(4) In any one of the above (1) to (3), a modified cross-section forming method characterized by using a steel pipe having a thickness / outer diameter ratio t / D of 0.05 or less as the pipe material.
(5) A quadrilateral cross-section molded product having one or two parallel two sides formed by molding a tubular material by the modified cross-section molding method according to any one of (1) to (4) above, One or two parallel 2 excellent in spot weldability, characterized in that (hollow depth on flat surface or depth of hollow on flat surface) is 0.5 mm or less, and further, the corner radius of curvature R is 10 mm or less. A quadrilateral cross-section molded product with sides.
(6) In the above (1), the tube material is a tube material having a tensile strength of 690 MPa or more, and after crushing with the deformed section mold, the tube material is deformed by continuously applying an internal pressure with the liquid. When forming into a cross-sectional shape, the maximum internal pressure is an internal pressure that satisfies both Pmin and more and more than 50 MPa, and the peripheral length increase rate after molding is A% or more and 11.0% or less below. A method for forming an irregular cross section, characterized by forming.
A=4.167×10−3×(TS−590)
A:周長増加率の下限(%)、TS:管材の引張強さ(MPa)
(7)前記潰し加工後の内圧負荷と併せて、管端に管軸方向の圧縮力を負荷して管端を管軸方向中央側に押し込むことを特徴とする(6)に記載の異形断面成形方法。
(8)(6)または(7)において、前記管材として引張強さ780MPa以上の鋼管を用い、成形後の周長増加率が下記A%以上10.0%以下となるように成形することを特徴とする異形断面成形方法。 A = 4.167 × 10 −3 × (TS-590)
A: Lower limit of perimeter increase rate (%), TS: Tensile strength of pipe (MPa)
(7) The deformed cross section according to (6), wherein a compressive force in the tube axis direction is applied to the tube end together with the internal pressure load after the crushing process, and the tube end is pushed toward the center in the tube axis direction. Molding method.
(8) In (6) or (7), a steel pipe having a tensile strength of 780 MPa or more is used as the pipe material, and molding is performed such that the peripheral length increase rate after molding is A% or more and 10.0% or less below. A modified cross-section molding method characterized.
A=4.167×10−3×(TS−590)
A:周長増加率の下限(%)、TS:管材の引張強さ(MPa)
(9)(6)~(8)のいずれかにおいて、前記管材として肉厚/外径比t/Dが0.05以下である鋼管を用いることを特徴とする異形断面成形方法。
(10)管材を(6)~(9)のいずれかに記載の異形断面成形方法で成形してなる一又は二の平行2辺を有する四辺形断面成形品であって、平坦部凹み量が0.5mm以下であり、さらにコーナーの曲率半径Rが10mm以下であることを特徴とするスポット溶接性に優れた一又は二の平行2辺を有する四辺形断面成形品。
(11)引張強さ690MPa以上の管材に、内圧を負荷しない状態もしくは液体により50MPa以下の内圧を負荷した状態で、少なくとも1つの面が平坦部を有する異形断面金型にて潰し加工を行い、引続き前記液体により最高内圧が、50MPa超である内圧を負荷して、前記管材を異形断面形状に成形するにあたり、成形後の周長増加率が下記A%以上11.0%以下となるように成形することを特徴とする異形断面成形方法。
記
A=4.167×10−3×(TS−590)
A:周長増加率の下限(%)、TS:管材の引張強さ(MPa)
(12)前記潰し加工後の内圧負荷と併せて、管端に管軸方向の圧縮力を負荷して管端を管軸方向中央側に押し込むことを特徴とする前記(11)に記載の異形断面成形方法。
(13)前記(11)または(12)において、前記管材として引張強さ780MPa以上の鋼管を用い、成形後の周長増加率が下記A%以上10.0%以下となるように成形することを特徴とする異形断面成形方法。
記
A=4.167×10−3×(TS−590)
A:周長増加率の下限(%)、TS:管材の引張強さ(MPa)
(14)前記(11)~(13)のいずれかにおいて、前記管材として肉厚/外径比t/Dが0.05以下である鋼管を用いることを特徴とする異形断面成形方法。
(15)管材を前記(11)~(14)のいずれかに記載の異形断面成形方法で成形してなる一又は二の平行2辺を有する四辺形断面成形品であって、平坦部凹み量が0.5mm以下であり、さらにコーナーの曲率半径Rが10mm以下であることを特徴とするスポット溶接性に優れた一又は二の平行2辺を有する四辺形断面成形品。 A = 4.167 × 10 −3 × (TS-590)
A: Lower limit of perimeter increase rate (%), TS: Tensile strength of pipe (MPa)
(9) The modified cross-section forming method according to any one of (6) to (8), wherein a steel pipe having a thickness / outer diameter ratio t / D of 0.05 or less is used as the pipe material.
(10) A quadrilateral cross-sectional molded product having one or two parallel two sides formed by molding a tubular material by the modified cross-section molding method according to any one of (6) to (9), wherein the flat portion dent amount is A quadrilateral cross-sectional molded article having one or two parallel two sides excellent in spot weldability, characterized by being 0.5 mm or less and having a corner radius of curvature R of 10 mm or less.
(11) In a state where no internal pressure is applied to a pipe material having a tensile strength of 690 MPa or more or an internal pressure of 50 MPa or less is applied with a liquid, crushing is performed with a deformed cross-section die having at least one flat surface, When the tube is formed into a deformed cross-sectional shape by continuously applying an internal pressure with a maximum internal pressure of more than 50 MPa with the liquid, the peripheral length increase rate after molding is from A% to 11.0% below. A method for forming an irregular cross section, characterized by forming.
A = 4.167 × 10 −3 × (TS-590)
A: Lower limit of perimeter increase rate (%), TS: Tensile strength of pipe (MPa)
(12) In combination with the internal pressure load after the crushing process, the tube end is loaded with a compressive force in the tube axis direction, and the tube end is pushed toward the center in the tube axis direction. Section forming method.
(13) In the above (11) or (12), a steel pipe having a tensile strength of 780 MPa or more is used as the pipe, and the peripheral length increase rate after forming is formed to be A% or more and 10.0% or less below. A modified cross-section molding method characterized by the above.
A = 4.167 × 10 −3 × (TS-590)
A: Lower limit of perimeter increase rate (%), TS: Tensile strength of pipe (MPa)
(14) In any one of the above (11) to (13), a modified cross-section forming method using a steel pipe having a thickness / outer diameter ratio t / D of 0.05 or less as the pipe material.
(15) A quadrilateral cross-sectional molded product having one or two parallel two sides formed by molding a tubular material by the modified cross-section molding method according to any one of (11) to (14) above, Is a quadrilateral cross-sectional molded article having one or two parallel two sides excellent in spot weldability, characterized in that the corner radius of curvature R is 10 mm or less.
記
Pmin=0.045×TS ・・・・(1)
Pmin:最高内圧の下限[MPa]、TS:管材の引張強さ[MPa]
これにより、図1(c)に示すように、平坦部凹みは低減し、コーナーR部は材料(管材の材料)が張り出し、シャープなR形状となる。また、最高内圧を高くするほど残留応力が低減し、除荷後のスプリングバックによる形状変化が小さくなる。 Therefore, the pipe is continuously loaded with an internal pressure that causes the maximum internal pressure to be equal to or higher than the following P min [MPa] while being clamped of upper of die and lower die, so that the pipe has a deformed cross-sectional shape. Molding is performed (FIG. 1C).
P min = 0.045 × TS (1)
P min : lower limit of maximum internal pressure [MPa], TS: tensile strength of pipe material [MPa]
Thereby, as shown in FIG.1 (c), a flat part dent is reduced and material (material of a pipe material) overhangs a corner R part, and becomes a sharp R shape. Further, as the maximum internal pressure is increased, the residual stress is reduced, and the shape change due to the springback after unloading is reduced.
なお、周長増加率は次式の(2)式で与えられる。
周長増加率=(成形品の外周長/成形前の管材の外周長−1)×100(%)‥‥・・・(2) Further, in the present invention, when a steel pipe having a tensile strength of 780 MPa or more is used as the pipe material, it is preferable that the peripheral length increase rate after molding is 2.0% or more and 10.0% or less.
The circumference increase rate is given by the following equation (2).
Perimeter increase rate = (periphery length of molded product / perimeter length of tube material before molding-1) × 100 (%) (2)
また、潰し加工後の成形に用いる内圧は、FEM(finite element method)解析や実験により、最高内圧と周長増加率の対応関係を求めておき、この対応関係において目標の周長増加率に対応する最高内圧に設定するとよい。 A ≦ (L K / L P −1) × 100 ≦ B (3)
In addition, the internal pressure used for molding after crushing is determined by finding the correspondence between the maximum internal pressure and the peripheral length increase rate by FEM (finite element method) analysis and experiment, and this correspondence corresponds to the target peripheral length increase rate. It is better to set the maximum internal pressure.
記
A=4.167×10−3×(TS−590)…(4)
A:周長増加率の下限(%)、TS:管材の引張強さ(MPa) Perimeter increase rate = (periphery length of molded product / perimeter length of tube material before molding-1) × 100 (%) (2)
A = 4.167 × 10 −3 × (TS-590) (4)
A: Lower limit of perimeter increase rate (%), TS: Tensile strength of pipe (MPa)
[工程] 金型に装入→内圧無しの状態または液体により50MPa以下の内圧(No.10と11は、それぞれ 10MPa、13MPa)を負荷した状態で型締めによる潰し加工→表1に示す種々の周長増加率となるように液体により最高内圧が表1に示す値となる内圧を負荷(一部の管材には軸押しを併用(No.12と13は、それぞれ、押し込み量 2.5%、3.0%))。 Using the
[Process] Inserting into mold → No internal pressure or crushing by mold clamping under liquid pressure of 50 MPa or less (No. 10 and 11 are 10 MPa and 13 MPa, respectively) → Various types shown in Table 1 Load the internal pressure so that the maximum internal pressure becomes the value shown in Table 1 by the liquid so that the perimeter increase rate is obtained (Axial push is used in combination with some pipes (No. 12 and 13 are 2.5% push-in amount respectively) 3.0%)).
[スポット溶接性の試験方法] The flat part dent amount and the corner radius of curvature R (see FIG. 2) of the obtained molded product (product) were measured (measurement of the flat part dent amount was performed by measuring each of the deformed cross-section molded products at the center part in the longitudinal direction. For each of the two flat portions, a dent amount of each of the four flat portions was measured using a laser distance meter in a direction perpendicular to the longitudinal direction, and the maximum dent amount was defined as the flat portion dent amount. In the measurement, the cross-section molded product was cut at the center in the longitudinal direction at a plane perpendicular to the longitudinal direction, and cross-sectional photographs of each of the four corners were taken into the image, and circles of various radii were placed at each corner. The radius of curvature R of the four corners was obtained by superimposing them, and the maximum radius R was defined as the radius of curvature R of the corner.) Also, the spot weldability was tested by the following method.
[Spot weldability test method]
TSS(N)=1.85×t×TS×(1+0.0059EL)×(ND+2.09)
ただし、tは鋼板12の板厚(mm)
TSは鋼板12の引張強さ(MPa)
ELは鋼板12の伸び(%)
NDは製品11と鋼板12の間のナゲット径(nugget diameter)(mm)
鋼板12は、板厚が1.0mm以下の440MPa級以下の鋼板である。
○:スポット溶接部13にナゲット形成有(ナゲット形成の有無は断面写真から判定)、引張せん断荷重は十分(合格)
×:スポット溶接部13にナゲット形成無、もしくは、引張せん断荷重が不十分 As shown in FIG. 5, the
TSS (N) = 1.85 × t × TS × (1 + 0.0059EL) × (ND + 2.09)
Where t is the thickness of the steel plate 12 (mm)
TS is the tensile strength of steel plate 12 (MPa)
EL is the elongation of steel sheet 12 (%)
ND is the nugget diameter (mm) between the
The
○: Nugget formed on spot weld 13 (presence of nugget formation is determined from cross-sectional photograph), and sufficient tensile shear load (passed)
X: No nugget is formed on the
[工程] 金型に装入→内圧無しの状態または液体により50MPa以下の内圧(No.8と9は、それぞれ10MPa、13MPa)を負荷した状態で型締めによる潰し加工→表3に示す種々の周長増加率となるように液体により50MPa超の内圧を負荷(一部の管材には軸押しを併用(No.10と11は、それぞれ、押し込み量4%、5%))。 In the same manner as in Example 1, using the
[Process] Inserting into mold → No internal pressure or crushing by mold clamping with internal pressure of 50 MPa or less (No. 8 and 9 are 10 MPa and 13 MPa, respectively) with liquid → Various types shown in Table 3 An internal pressure of more than 50 MPa is applied with a liquid so as to increase the peripheral length (shaft pressing is used in combination with some pipe materials (No. 10 and 11 are 4% and 5%, respectively)).
上記測定および試験の結果を表3に示す。表3より、本発明例では、TS690MPa以上の管材からスポット溶接性に優れた高寸法精度の異形断面成形品が得られたことがわかる。なお、本発明例において、t/D≦0.05のものは、t/D>0.05のものに比べ、平坦部凹み量が小さくなっている。 The flat part dent amount and the corner radius of curvature R (see FIG. 2) of the obtained molded product (product) were measured, and spot weldability was tested in the same manner as in Example 1.
The results of the above measurements and tests are shown in Table 3. From Table 3, it can be seen that in the example of the present invention, an irregular cross-section molded article with high dimensional accuracy having excellent spot weldability was obtained from a tube material of TS690 MPa or more. In the example of the present invention, the flat portion dent amount is smaller when t / D ≦ 0.05 than when t / D> 0.05.
1A 金型(下金型)
3 電極
10 管材
11 製品(異形断面成形品、一又は二の平行2辺を有する四辺形断面成形品)
12 鋼板
13 スポット溶接部 1 Mold (Upper mold)
1A mold (lower mold)
3
12
Claims (15)
- 引張強さ590MPa以上の管材に、内圧を負荷しない状態もしくは液体により50MPa以下の内圧を負荷した状態で、少なくとも1つの面が平坦部を有する異形断面金型にて潰し加工を行い、引続き前記液体により最高内圧が下記Pmin[MPa]以上になる内圧を負荷して、前記管材を異形断面形状に成形することを特徴とする異形断面成形方法。
記
Pmin=0.045×TS
Pmin:最高内圧の下限[MPa]、TS:管材の引張強さ[MPa] In a state in which an internal pressure is not applied to a pipe material having a tensile strength of 590 MPa or more or an internal pressure of 50 MPa or less is applied by a liquid, crushing processing is performed with a deformed cross-section mold having at least one flat surface, and the liquid is continuously applied. The deformed cross-section forming method is characterized in that an internal pressure at which the maximum internal pressure is equal to or higher than the following P min [MPa] is applied to form the tube material into a deformed cross-sectional shape.
P min = 0.045 × TS
P min : lower limit of maximum internal pressure [MPa], TS: tensile strength of pipe material [MPa] - 前記潰し加工後の内圧負荷と併せて、管端に管軸方向の圧縮力を負荷して管端を管軸方向中央側に押し込むことを特徴とする請求項1に記載の異形断面成形方法。 The deformed cross-section forming method according to claim 1, wherein together with the internal pressure load after the crushing process, a compressive force in the tube axis direction is applied to the tube end and the tube end is pushed toward the center in the tube axis direction.
- 請求項1または2において、前記管材として引張強さ780MPa以上の鋼管を用い、成形後の周長増加率が2.0%以上10.0%以下となるように成形することを特徴とする異形断面成形方法。 3. The modified shape according to claim 1, wherein a steel pipe having a tensile strength of 780 MPa or more is used as the pipe material, and the peripheral length increase rate after forming is 2.0% or more and 10.0% or less. Section forming method.
- 請求項1~3のいずれか1項において、前記管材として肉厚/外径比t/Dが0.05以下である鋼管を用いることを特徴とする異形断面成形方法。 4. The modified cross-section forming method according to claim 1, wherein a steel pipe having a wall thickness / outer diameter ratio t / D of 0.05 or less is used as the pipe material.
- 管材を請求項1~4のいずれか1項に記載の異形断面成形方法で成形してなる一又は二の平行2辺を有する四辺形断面成形品であって、平坦部凹み量が0.5mm以下であり、さらにコーナーの曲率半径Rが10mm以下であることを特徴とするスポット溶接性に優れた一又は二の平行2辺を有する四辺形断面成形品。 A quadrilateral cross-sectional molded product having one or two parallel two sides formed by molding a tubular material by the modified cross-section molding method according to any one of claims 1 to 4, wherein the flat portion dent amount is 0.5 mm. A quadrilateral cross-sectional molded article having one or two parallel two sides excellent in spot weldability, wherein the corner radius of curvature R is 10 mm or less.
- 請求項1において、前記管材が引張強さ690MPa以上の管材であり、前記異形断面金型にて潰し加工を行った後、引続き前記液体により内圧を負荷して、前記管材を異形断面形状に成形するにあたり、前記最高内圧が、Pmin以上および、50MPa超えの両方を満足する内圧を加え、さらに、成形後の周長増加率が下記A%以上11.0%以下となるように成形することを特徴とする異形断面成形方法。
記
A=4.167×10−3×(TS−590)
A:周長増加率の下限(%)、TS:管材の引張強さ(MPa) 2. The tube material according to claim 1, wherein the tube material is a tube material having a tensile strength of 690 MPa or more, and after the crushing process is performed with the deformed cross-section mold, an internal pressure is continuously applied by the liquid to form the tube material into a deformed cross-section shape. In doing so, the internal pressure satisfying both the maximum internal pressure of Pmin or more and exceeding 50 MPa is applied, and further, the molding is performed such that the peripheral length increase rate after molding is A% or more and 11.0% or less as follows. A modified cross-section molding method characterized.
A = 4.167 × 10 −3 × (TS-590)
A: Lower limit of perimeter increase rate (%), TS: Tensile strength of pipe (MPa) - 前記潰し加工後の内圧負荷と併せて、管端に管軸方向の圧縮力を負荷して管端を管軸方向中央側に押し込むことを特徴とする請求項6に記載の異形断面成形方法。 The deformed cross-section forming method according to claim 6, wherein together with the internal pressure load after the crushing process, a compressive force in the tube axis direction is applied to the tube end and the tube end is pushed toward the center in the tube axis direction.
- 請求項6または7において、前記管材として引張強さ780MPa以上の鋼管を用い、成形後の周長増加率が下記A%以上10.0%以下となるように成形することを特徴とする異形断面成形方法。
記
A=4.167×10−3×(TS−590)
A:周長増加率の下限(%)、TS:管材の引張強さ(MPa) 8. The modified cross section according to claim 6 or 7, wherein a steel pipe having a tensile strength of 780 MPa or more is used as the pipe material, and the peripheral length increase rate after the forming is A% or more and 10.0% or less below. Molding method.
A = 4.167 × 10 −3 × (TS-590)
A: Lower limit of perimeter increase rate (%), TS: Tensile strength of pipe (MPa) - 請求項6~8のいずれか1項において、前記管材として肉厚/外径比t/Dが0.05以下である鋼管を用いることを特徴とする異形断面成形方法。 9. The modified cross-section forming method according to claim 6, wherein a steel pipe having a thickness / outer diameter ratio t / D of 0.05 or less is used as the pipe material.
- 管材を請求項6~9のいずれか1項に記載の異形断面成形方法で成形してなる一又は二の平行2辺を有する四辺形断面成形品であって、平坦部凹み量が0.5mm以下であり、さらにコーナーの曲率半径Rが10mm以下であることを特徴とするスポット溶接性に優れた一又は二の平行2辺を有する四辺形断面成形品。 A quadrilateral cross-sectional molded product having one or two parallel two sides formed by molding a tubular material by the irregular cross-section molding method according to any one of claims 6 to 9, wherein a flat portion dent amount is 0.5 mm. A quadrilateral cross-sectional molded article having one or two parallel two sides excellent in spot weldability, wherein the corner radius of curvature R is 10 mm or less.
- 引張強さ690MPa以上の管材に、内圧を負荷しない状態もしくは液体により50MPa以下の内圧を負荷した状態で、少なくとも1つの面が平坦部を有する異形断面金型にて潰し加工を行い、引続き前記液体により最高内圧が、50MPa超である内圧を負荷して、前記管材を異形断面形状に成形するにあたり、成形後の周長増加率が下記A%以上11.0%以下となるように成形することを特徴とする異形断面成形方法。
記
A=4.167×10−3×(TS−590)
A:周長増加率の下限(%)、TS:管材の引張強さ(MPa) In a state in which an internal pressure is not applied to a pipe material having a tensile strength of 690 MPa or more or an internal pressure of 50 MPa or less is applied by a liquid, crushing processing is performed with a deformed cross-section mold having at least one flat portion, and the liquid is continuously applied. When forming the pipe material into an irregular cross-sectional shape by applying an internal pressure whose maximum internal pressure is more than 50 MPa, forming the peripheral length increase rate after molding to be A% or more and 11.0% or less below. A modified cross-section molding method characterized by the above.
A = 4.167 × 10 −3 × (TS-590)
A: Lower limit of perimeter increase rate (%), TS: Tensile strength of pipe (MPa) - 前記潰し加工後の内圧負荷と併せて、管端に管軸方向の圧縮力を負荷して管端を管軸方向中央側に押し込むことを特徴とする請求項11に記載の異形断面成形方法。 The deformed cross-section forming method according to claim 11, wherein together with the internal pressure load after the crushing, a compressive force in the tube axis direction is applied to the tube end and the tube end is pushed toward the center in the tube axis direction.
- 請求項11または12において、前記管材として引張強さ780MPa以上の鋼管を用い、成形後の周長増加率が下記A%以上10.0%以下となるように成形することを特徴とする異形断面成形方法。
記
A=4.167×10−3×(TS−590)
A:周長増加率の下限(%)、TS:管材の引張強さ(MPa) 13. The modified cross section according to claim 11 or 12, wherein a steel pipe having a tensile strength of 780 MPa or more is used as the pipe material, and the peripheral length increase rate after forming is A% or more and 10.0% or less below. Molding method.
A = 4.167 × 10 −3 × (TS-590)
A: Lower limit of perimeter increase rate (%), TS: Tensile strength of pipe (MPa) - 請求項11~13のいずれか1項において、前記管材として肉厚/外径比t/Dが0.05以下である鋼管を用いることを特徴とする異形断面成形方法。 14. The modified cross-section forming method according to claim 11, wherein a steel pipe having a thickness / outer diameter ratio t / D of 0.05 or less is used as the pipe material.
- 管材を請求項11~14のいずれか1項に記載の異形断面成形方法で成形してなる一又は二の平行2辺を有する四辺形断面成形品であって、平坦部凹み量が0.5mm以下であり、さらにコーナーRが10mm以下であることを特徴とするスポット溶接性に優れた一又は二の平行2辺を有する四辺形断面成形品。 A quadrilateral cross-sectional molded product having one or two parallel two sides formed by molding a tubular material by the modified cross-section molding method according to any one of claims 11 to 14, wherein the flat portion dent amount is 0.5 mm. A quadrilateral cross-sectional molded article having one or two parallel two sides excellent in spot weldability, wherein the corner R is 10 mm or less.
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EP09816295.1A EP2351623B1 (en) | 2008-09-25 | 2009-09-24 | Method for forming deformed cross-section and formed article of quadrilateral cross-section exhibiting excellent spot weldability |
KR1020137017515A KR20130083492A (en) | 2008-09-25 | 2009-09-24 | Method for forming deformed cross-section and formed article of quadrilateral cross-section exhibiting excellent spot weldability |
KR1020117006739A KR101322229B1 (en) | 2008-09-25 | 2009-09-24 | Method for forming deformed cross-section and formed article of quadrilateral cross-section exhibiting excellent spot weldability |
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US20150315666A1 (en) | 2014-04-30 | 2015-11-05 | Ford Global Technologies, Llc | Induction annealing as a method for expanded hydroformed tube formability |
US9545657B2 (en) * | 2014-06-10 | 2017-01-17 | Ford Global Technologies, Llc | Method of hydroforming an extruded aluminum tube with a flat nose corner radius |
JP6670543B2 (en) * | 2014-12-11 | 2020-03-25 | 住友重機械工業株式会社 | Molding apparatus and molding method |
CN106311857B (en) * | 2015-12-21 | 2017-11-07 | 青岛世冠装备科技有限公司 | A kind of swollen manufacturing process of complex section hollow member low pressure upsetting |
CN105562516B (en) * | 2016-03-15 | 2018-03-30 | 哈尔滨工业大学 | A kind of variable cross-section special piece topping up method for press forming |
CN107243538A (en) * | 2017-08-08 | 2017-10-13 | 天津天锻航空科技有限公司 | A kind of method that big girth rectangle is shaped by Xiao Zhou's Circular Pipe |
CN111957804B (en) * | 2020-07-20 | 2021-06-29 | 燕山大学 | Device for liquid-filling bending forming of thin-walled tube and forming method thereof |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH1147842A (en) * | 1997-08-06 | 1999-02-23 | Sumitomo Metal Ind Ltd | Liquid pressure bulging method and liquid pressure bulging device for metallic tube |
JP2000246361A (en) | 1999-03-02 | 2000-09-12 | F Tech:Kk | Hydroforming method of pipe material |
JP2001096316A (en) * | 1999-09-27 | 2001-04-10 | Nkk Corp | Hydroforming method for steel pipe |
JP2002220069A (en) * | 2001-01-25 | 2002-08-06 | Mitsubishi Motors Corp | Car body member |
JP2004255445A (en) * | 2003-02-27 | 2004-09-16 | Nippon Steel Corp | Hydroforming method and its metal die |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5339667A (en) * | 1993-04-19 | 1994-08-23 | General Motors Corporation | Method for pinch free tube forming |
JPH10156429A (en) * | 1996-11-29 | 1998-06-16 | Hitachi Ltd | Method for forming tube having complicated special cross section tube |
US6257035B1 (en) * | 1999-12-15 | 2001-07-10 | Ti Corporate Services Limited | Compressive hydroforming |
JP4631130B2 (en) | 2000-05-25 | 2011-02-16 | 住友金属工業株式会社 | Modified tubular product and manufacturing method thereof |
IT1320503B1 (en) * | 2000-06-16 | 2003-12-10 | Iveco Fiat | PROCEDURE FOR THE PRODUCTION OF AXLES FOR INDUSTRIAL VEHICLES. |
JP3854812B2 (en) * | 2001-03-27 | 2006-12-06 | 新日本製鐵株式会社 | Strength members for automobiles |
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Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH1147842A (en) * | 1997-08-06 | 1999-02-23 | Sumitomo Metal Ind Ltd | Liquid pressure bulging method and liquid pressure bulging device for metallic tube |
JP2000246361A (en) | 1999-03-02 | 2000-09-12 | F Tech:Kk | Hydroforming method of pipe material |
JP2001096316A (en) * | 1999-09-27 | 2001-04-10 | Nkk Corp | Hydroforming method for steel pipe |
JP2002220069A (en) * | 2001-01-25 | 2002-08-06 | Mitsubishi Motors Corp | Car body member |
JP2004255445A (en) * | 2003-02-27 | 2004-09-16 | Nippon Steel Corp | Hydroforming method and its metal die |
Non-Patent Citations (1)
Title |
---|
See also references of EP2351623A4 * |
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KR101322229B1 (en) | 2013-10-28 |
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