WO2009056286A1 - Material sheet and process for its preparation - Google Patents
Material sheet and process for its preparation Download PDFInfo
- Publication number
- WO2009056286A1 WO2009056286A1 PCT/EP2008/009121 EP2008009121W WO2009056286A1 WO 2009056286 A1 WO2009056286 A1 WO 2009056286A1 EP 2008009121 W EP2008009121 W EP 2008009121W WO 2009056286 A1 WO2009056286 A1 WO 2009056286A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- fibers
- material sheet
- monolayer
- less
- bonding agent
- Prior art date
Links
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F41—WEAPONS
- F41H—ARMOUR; ARMOURED TURRETS; ARMOURED OR ARMED VEHICLES; MEANS OF ATTACK OR DEFENCE, e.g. CAMOUFLAGE, IN GENERAL
- F41H5/00—Armour; Armour plates
- F41H5/02—Plate construction
- F41H5/04—Plate construction composed of more than one layer
- F41H5/0471—Layered armour containing fibre- or fabric-reinforced layers
- F41H5/0485—Layered armour containing fibre- or fabric-reinforced layers all the layers being only fibre- or fabric-reinforced layers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B37/00—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding
- B32B37/10—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by the pressing technique, e.g. using action of vacuum or fluid pressure
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B37/00—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding
- B32B37/14—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by the properties of the layers
- B32B37/144—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by the properties of the layers using layers with different mechanical or chemical conditions or properties, e.g. layers with different thermal shrinkage, layers under tension during bonding
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B37/00—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding
- B32B37/14—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by the properties of the layers
- B32B37/16—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by the properties of the layers with all layers existing as coherent layers before laminating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B5/00—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts
- B32B5/02—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by structural features of a fibrous or filamentary layer
- B32B5/022—Non-woven fabric
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B5/00—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts
- B32B5/02—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by structural features of a fibrous or filamentary layer
- B32B5/06—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by structural features of a fibrous or filamentary layer characterised by a fibrous or filamentary layer mechanically connected, e.g. by needling to another layer, e.g. of fibres, of paper
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B5/00—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts
- B32B5/02—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by structural features of a fibrous or filamentary layer
- B32B5/12—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by structural features of a fibrous or filamentary layer characterised by the relative arrangement of fibres or filaments of different layers, e.g. the fibres or filaments being parallel or perpendicular to each other
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B5/00—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts
- B32B5/22—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by the presence of two or more layers which are next to each other and are fibrous, filamentary, formed of particles or foamed
- B32B5/24—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by the presence of two or more layers which are next to each other and are fibrous, filamentary, formed of particles or foamed one layer being a fibrous or filamentary layer
- B32B5/26—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by the presence of two or more layers which are next to each other and are fibrous, filamentary, formed of particles or foamed one layer being a fibrous or filamentary layer another layer next to it also being fibrous or filamentary
- B32B5/262—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by the presence of two or more layers which are next to each other and are fibrous, filamentary, formed of particles or foamed one layer being a fibrous or filamentary layer another layer next to it also being fibrous or filamentary characterised by one fibrous or filamentary layer being a woven fabric layer
-
- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D1/00—Woven fabrics designed to make specified articles
- D03D1/0035—Protective fabrics
- D03D1/0052—Antiballistic fabrics
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H5/00—Non woven fabrics formed of mixtures of relatively short fibres and yarns or like filamentary material of substantial length
- D04H5/08—Non woven fabrics formed of mixtures of relatively short fibres and yarns or like filamentary material of substantial length characterised by the method of forming fleeces or layers, e.g. reorientation of fibres or yarns
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F41—WEAPONS
- F41H—ARMOUR; ARMOURED TURRETS; ARMOURED OR ARMED VEHICLES; MEANS OF ATTACK OR DEFENCE, e.g. CAMOUFLAGE, IN GENERAL
- F41H5/00—Armour; Armour plates
- F41H5/02—Plate construction
- F41H5/04—Plate construction composed of more than one layer
- F41H5/0471—Layered armour containing fibre- or fabric-reinforced layers
- F41H5/0478—Fibre- or fabric-reinforced layers in combination with plastics layers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2260/00—Layered product comprising an impregnated, embedded, or bonded layer wherein the layer comprises an impregnation, embedding, or binder material
- B32B2260/02—Composition of the impregnated, bonded or embedded layer
- B32B2260/021—Fibrous or filamentary layer
- B32B2260/023—Two or more layers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2262/00—Composition or structural features of fibres which form a fibrous or filamentary layer or are present as additives
- B32B2262/02—Synthetic macromolecular fibres
- B32B2262/0253—Polyolefin fibres
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/50—Properties of the layers or laminate having particular mechanical properties
- B32B2307/558—Impact strength, toughness
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2323/00—Polyalkenes
- B32B2323/04—Polyethylene
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2405/00—Adhesive articles, e.g. adhesive tapes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2571/00—Protective equipment
- B32B2571/02—Protective equipment defensive, e.g. armour plates, anti-ballistic clothing
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/24—Structurally defined web or sheet [e.g., overall dimension, etc.]
- Y10T428/24132—Structurally defined web or sheet [e.g., overall dimension, etc.] including grain, strips, or filamentary elements in different layers or components parallel
Definitions
- the adjacent fibers within the same monolayer are preferably in intimate contact along their substantial length.
- at least 80wt%, 90wt% or 95wt% of the adjacent fibers within the same monolayer are mechanically fused together.
- Mechanical fusion is observed through the formation of an integral monolayer without the addition of a material that integrally connects all the fibers together along their substantial length (i.e preferably at least 40, 60 or 80% of the length of the adjacent fibers) as seen by the eye, or by a (scanning electron) microscope.
- the use of mechanical fusion enables the bonding agent to be applied locally, typically in the transverse direction to the unidirectional fibers.
- the bonding agent preferably does not function as a matrix forming material, but as an initial monolayer stabiliser.
- the high pressures are applied to the plurality of fibers for at least 45 seconds, more preferably at least 1 minute or at least 5 minutes and most preferably at least 10 minutes.
- the contact time under high pressure is required to promote sufficient mechanical fusing between adjacent fibers, such that an integral material sheet is formed with a minimal content of bonding agent i.e less than 13,1 1 , 10, 9, 7, 5 or 3wt% compared to the total weight of the material sheet.
- the lower the bonding agent content the higher the anti-ballistic performance of the material sheet.
- Figure 1 is a schematic drawing of process in accordance with the present invention of preparing at least one monolayer
- Figure 2 is a graph illustrating ballistic performance versus monolayer thickness
- Figure 3 is a Differential scanning calorimetry spectrograph illustrating the presence of an endothermic effect consistent with partial melt recrystallisation of the fibers
- the receiving plate (4) in Figure 1 is preferably loaded on both sides with at least one monolayer and is placed in a high pressure device and subjected to pressures of at least 100 bar
- the applied pressure is preferable applied in a one step process, with the pressure quickly (preferably within 30 seconds, more preferably within 20, 10 or 5 seconds) ramped up the target operating pressure to avoid melt bonding.
- the temperature is preferably maintained within the preferred temperature range (below the melting point of the fibers) for compression under high pressure.
- Analysis of the first heating curve is used.
- the empty pan measurement is subtracted from the sample curve to correct for baseline curvature. Correction of the slope of the sample curve is performed by aligning the baseline at the flat part before and after the peaks (at 60 and 190 0 C for
Landscapes
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Mechanical Engineering (AREA)
- Physics & Mathematics (AREA)
- Fluid Mechanics (AREA)
- Aiming, Guidance, Guns With A Light Source, Armor, Camouflage, And Targets (AREA)
- Laminated Bodies (AREA)
- Nonwoven Fabrics (AREA)
- Casting Or Compression Moulding Of Plastics Or The Like (AREA)
Abstract
Description
Claims
Priority Applications (10)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
BRPI0819237-5A BRPI0819237B1 (en) | 2007-11-01 | 2008-10-29 | MATERIAL SHEET, PROCESS FOR PREPARATION, RIBBON UNDERSTANDING A PLURALITY OF FIBERS AND BALISTIC RESISTANT ARTICLE |
EP08829956.5A EP2205928B1 (en) | 2007-11-01 | 2008-10-29 | Material sheet and process for its preparation |
KR1020167011522A KR101756608B1 (en) | 2007-11-01 | 2008-10-29 | Material sheet and process for its preparation |
US12/740,490 US9541351B2 (en) | 2007-11-01 | 2008-10-29 | Material sheet and process for its preparation |
DK08829956.5T DK2205928T3 (en) | 2007-11-01 | 2008-10-29 | MATERIAL FILM AND METHOD OF PRODUCING THEREOF |
AU2008317959A AU2008317959B2 (en) | 2007-11-01 | 2008-10-29 | Material sheet and process for its preparation |
CN200880114518.0A CN101861508B (en) | 2007-11-01 | 2008-10-29 | Material sheet and process for its preparation |
IL204951A IL204951A (en) | 2007-11-01 | 2010-04-08 | Material sheet and process for its preparation |
US15/371,100 US10663265B2 (en) | 2007-11-01 | 2016-12-06 | Material sheet and process for its preparation |
US16/118,401 US11009317B2 (en) | 2007-11-01 | 2018-08-30 | Material sheet and process for its preparation |
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US99610707P | 2007-11-01 | 2007-11-01 | |
EP07021357.4 | 2007-11-01 | ||
US60/996,107 | 2007-11-01 | ||
EP07021357 | 2007-11-01 |
Related Child Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US12/740,490 A-371-Of-International US9541351B2 (en) | 2007-11-01 | 2008-10-29 | Material sheet and process for its preparation |
US15/371,100 Continuation US10663265B2 (en) | 2007-11-01 | 2016-12-06 | Material sheet and process for its preparation |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2009056286A1 true WO2009056286A1 (en) | 2009-05-07 |
Family
ID=39509687
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/EP2008/009121 WO2009056286A1 (en) | 2007-11-01 | 2008-10-29 | Material sheet and process for its preparation |
Country Status (10)
Country | Link |
---|---|
US (3) | US9541351B2 (en) |
EP (2) | EP2205928B1 (en) |
KR (2) | KR101618816B1 (en) |
CN (1) | CN101861508B (en) |
AU (1) | AU2008317959B2 (en) |
BR (1) | BRPI0819237B1 (en) |
DK (2) | DK2693159T3 (en) |
IL (1) | IL204951A (en) |
TW (1) | TWI547608B (en) |
WO (1) | WO2009056286A1 (en) |
Cited By (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2205928A1 (en) | 2007-11-01 | 2010-07-14 | DSM IP Assets B.V. | Material sheet and process for its preparation |
WO2011019512A2 (en) | 2009-08-11 | 2011-02-17 | Honeywell International Inc. | High strength ultra-high molecular weight polyethylene tape articles |
WO2012080274A1 (en) | 2010-12-14 | 2012-06-21 | Dsm Ip Assets B.V. | Tape and products containing the same |
DE102011075798B4 (en) * | 2010-06-08 | 2012-10-04 | Toyota Boshoku Kabushiki Kaisha | Fiber structure article and method of manufacture of this |
WO2012139934A1 (en) | 2011-04-13 | 2012-10-18 | Dsm Ip Assets B.V. | Creep-optimized uhmwpe fiber |
WO2013087827A1 (en) | 2011-12-14 | 2013-06-20 | Dsm Ip Assets B.V. | Ultra -high molecular weight polyethylene multifilament yarn |
WO2013131996A1 (en) * | 2012-03-09 | 2013-09-12 | Dsm Ip Assets B.V. | Composite panel |
US8697220B2 (en) | 2009-08-11 | 2014-04-15 | Honeywell International, Inc. | High strength tape articles from ultra-high molecular weight polyethylene |
WO2015193215A1 (en) * | 2014-06-16 | 2015-12-23 | Dsm Ip Assets B.V. | Fibrous tape |
WO2017102618A1 (en) | 2015-12-15 | 2017-06-22 | Dsm Ip Assets B.V. | Low creep fiber |
US9731454B2 (en) | 2009-08-11 | 2017-08-15 | Honeywell International Inc. | Multidirectional fiber-reinforced tape/film articles and the method of making the same |
US9879757B2 (en) | 2013-12-10 | 2018-01-30 | Dsm Ip Assets B.V. | Chain comprising polymeric links and a spacer |
WO2019121209A1 (en) | 2017-12-18 | 2019-06-27 | Dsm Ip Assets B.V. | Ballistic-resistant molded article |
WO2019121204A1 (en) | 2017-12-18 | 2019-06-27 | Dsm Ip Assets B.V. | Ballistic-resistant curved molded article |
US10870930B2 (en) | 2015-05-28 | 2020-12-22 | Dsm Ip Assets B.V. | Hybrid chain link |
Families Citing this family (11)
Publication number | Priority date | Publication date | Assignee | Title |
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US9138961B2 (en) | 2011-10-19 | 2015-09-22 | Honeywell International Inc. | High performance laminated tapes and related products for ballistic applications |
BR112014030653B1 (en) | 2012-06-11 | 2021-11-23 | Dsm Ip Assets B.V. | ARTICLE WITH CONTINUOUS FORMAT, METHOD OF OBTAINING IT AND USE OF THE ARTICLE OR METHOD OF OBTAINING |
KR20150042785A (en) | 2012-08-06 | 2015-04-21 | 허니웰 인터내셔널 인코포레이티드 | Multidirectional fiber-reinforced tape/film articles and the method of making the same |
US20150135937A1 (en) * | 2013-11-18 | 2015-05-21 | E I Du Pont De Nemours And Company | Method to produce ballistic and stab resistant structures for garments and structures produced by the method |
US11242625B2 (en) | 2015-05-28 | 2022-02-08 | Dsm Ip Assets B.V. | Hybrid chain link |
EP3303876A1 (en) | 2015-05-28 | 2018-04-11 | DSM IP Assets B.V. | Polymeric chain link |
US20170297295A1 (en) * | 2016-04-15 | 2017-10-19 | Honeywell International Inc. | Blister free composite materials molding |
JP7163676B2 (en) | 2018-09-03 | 2022-11-01 | 株式会社リコー | Fiber assembly, staple fiber and manufacturing method thereof, and membrane and manufacturing method thereof |
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EP4348157A1 (en) | 2021-06-04 | 2024-04-10 | Avient Protective Materials B.V. | Hybrid ballistic-resistant molded article |
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2008
- 2008-10-29 DK DK13191253.7T patent/DK2693159T3/en active
- 2008-10-29 US US12/740,490 patent/US9541351B2/en active Active
- 2008-10-29 KR KR1020107009483A patent/KR101618816B1/en active IP Right Grant
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Also Published As
Publication number | Publication date |
---|---|
EP2693159B1 (en) | 2017-12-06 |
TW200932968A (en) | 2009-08-01 |
KR101618816B1 (en) | 2016-05-09 |
TWI547608B (en) | 2016-09-01 |
KR20100087305A (en) | 2010-08-04 |
US20100260968A1 (en) | 2010-10-14 |
DK2693159T3 (en) | 2018-03-12 |
US20170082406A1 (en) | 2017-03-23 |
US10663265B2 (en) | 2020-05-26 |
EP2205928B1 (en) | 2016-11-23 |
AU2008317959A1 (en) | 2009-05-07 |
KR20160063389A (en) | 2016-06-03 |
BRPI0819237A2 (en) | 2016-10-11 |
BRPI0819237B1 (en) | 2019-10-15 |
CN101861508B (en) | 2015-05-20 |
US20180372453A1 (en) | 2018-12-27 |
AU2008317959B2 (en) | 2014-01-16 |
EP2205928A1 (en) | 2010-07-14 |
US11009317B2 (en) | 2021-05-18 |
DK2205928T3 (en) | 2017-02-27 |
IL204951A (en) | 2017-09-28 |
EP2693159A1 (en) | 2014-02-05 |
CN101861508A (en) | 2010-10-13 |
US9541351B2 (en) | 2017-01-10 |
KR101756608B1 (en) | 2017-07-10 |
IL204951A0 (en) | 2010-11-30 |
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