WO2008126364A1 - 非水電解液二次電池用マンガン酸リチウム及びその製造方法、並びに非水電解液二次電池 - Google Patents

非水電解液二次電池用マンガン酸リチウム及びその製造方法、並びに非水電解液二次電池 Download PDF

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WO2008126364A1
WO2008126364A1 PCT/JP2008/000763 JP2008000763W WO2008126364A1 WO 2008126364 A1 WO2008126364 A1 WO 2008126364A1 JP 2008000763 W JP2008000763 W JP 2008000763W WO 2008126364 A1 WO2008126364 A1 WO 2008126364A1
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secondary battery
aqueous electrolyte
electrolyte secondary
lithium manganese
production
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PCT/JP2008/000763
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English (en)
French (fr)
Inventor
Masayuki Uegami
Akihisa Kajiyama
Kazutoshi Ishizaki
Hideaki Sadamura
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Toda Kogyo Corporation
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Priority to KR1020097020224A priority Critical patent/KR101456313B1/ko
Priority to US12/594,110 priority patent/US8440113B2/en
Priority to CN2008800105468A priority patent/CN101652883B/zh
Priority to EP08720642.1A priority patent/EP2157640B1/en
Priority to CA2682942A priority patent/CA2682942C/en
Priority to ES08720642.1T priority patent/ES2659389T3/es
Publication of WO2008126364A1 publication Critical patent/WO2008126364A1/ja
Priority to US13/787,863 priority patent/US8821766B2/en

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    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/50—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
    • H01M4/505—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
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    • H01M4/50—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
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    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G45/00—Compounds of manganese
    • C01G45/12—Manganates manganites or permanganates
    • C01G45/1221—Manganates or manganites with a manganese oxidation state of Mn(III), Mn(IV) or mixtures thereof
    • C01G45/1242—Manganates or manganites with a manganese oxidation state of Mn(III), Mn(IV) or mixtures thereof of the type [Mn2O4]-, e.g. LiMn2O4, Li[MxMn2-x]O4
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G51/00—Compounds of cobalt
    • C01G51/40—Cobaltates
    • C01G51/42—Cobaltates containing alkali metals, e.g. LiCoO2
    • C01G51/44—Cobaltates containing alkali metals, e.g. LiCoO2 containing manganese
    • C01G51/54—Cobaltates containing alkali metals, e.g. LiCoO2 containing manganese of the type [Mn2O4]-, e.g. Li(CoxMn2-x)04, Li(MyCoxMn2-x-y)O4
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • C10G45/02—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
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    • H—ELECTRICITY
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    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
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    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
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    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
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    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
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  • Chemical & Material Sciences (AREA)
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  • Inorganic Chemistry (AREA)
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  • Electrochemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Secondary Cells (AREA)

Abstract

　本発明は、高出力で高温安定性に優れたマンガン酸リチウムを提供することを目的とする。上記課題は、一次粒子径が１μｍ以上、挙動粒子の平均粒径（Ｄ５０）が１μｍ以上、１０μｍ以下で、実質的に単結晶粒子を形成するマンガン酸リチウム粒子粉末であり、化学式Ｌｉ１＋ｘＭｎ２－ｘ－ｙＹｙＯ４（Ｙ＝Ａｌ、Ｍｇ、Ｃｏ、０．０３≦ｘ≦０．１５、０．０５≦ｙ≦０．２０）であり、Ｙ元素が粒子内部に均一に分散しており、且つ、Ｉ（４００）／Ｉ（１１１）が３３％以上であってＩ（４４０）／Ｉ（１１１）が１６％以上であることを特徴とするマンガン酸リチウム粒子粉末により解決される。
PCT/JP2008/000763 2007-03-30 2008-03-27 非水電解液二次電池用マンガン酸リチウム及びその製造方法、並びに非水電解液二次電池 WO2008126364A1 (ja)

Priority Applications (7)

Application Number Priority Date Filing Date Title
KR1020097020224A KR101456313B1 (ko) 2007-03-30 2008-03-27 비수전해액 이차 전지용 망간산리튬 및 그의 제조 방법, 및 비수전해액 이차 전지
US12/594,110 US8440113B2 (en) 2007-03-30 2008-03-27 Lithium manganate for non-aqueous electrolyte secondary battery, process for producing the same, and non-aqueous electrolyte secondary battery
CN2008800105468A CN101652883B (zh) 2007-03-30 2008-03-27 非水电解液二次电池用锰酸锂及其制造方法、以及非水电解液二次电池
EP08720642.1A EP2157640B1 (en) 2007-03-30 2008-03-27 Lithium manganese for non-aqueous electrolyte secondary battery, method for production thereof, and non-aqueous electrolyte secondary battery
CA2682942A CA2682942C (en) 2007-03-30 2008-03-27 Lithium manganate for non-aqueous electrolyte secondary battery, process for producing the same, and non-aqueous electrolyte secondary battery
ES08720642.1T ES2659389T3 (es) 2007-03-30 2008-03-27 Litio manganeso para batería secundaria de electrolito no acuoso, método para la producción del mismo, y batería secundaria de electrolito no acuoso
US13/787,863 US8821766B2 (en) 2007-03-30 2013-03-07 Lithium manganate for non-aqueous electrolyte secondary battery, process for producing the same, and non-aqueous electrolyte secondary battery

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2007-092619 2007-03-30
JP2007092619A JP5344111B2 (ja) 2007-03-30 2007-03-30 非水電解液二次電池用マンガン酸リチウムの製造方法、並びに非水電解液二次電池

Related Child Applications (2)

Application Number Title Priority Date Filing Date
US12/594,110 A-371-Of-International US8440113B2 (en) 2007-03-30 2008-03-27 Lithium manganate for non-aqueous electrolyte secondary battery, process for producing the same, and non-aqueous electrolyte secondary battery
US13/787,863 Division US8821766B2 (en) 2007-03-30 2013-03-07 Lithium manganate for non-aqueous electrolyte secondary battery, process for producing the same, and non-aqueous electrolyte secondary battery

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WO2008126364A1 true WO2008126364A1 (ja) 2008-10-23

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US (2) US8440113B2 (ja)
EP (1) EP2157640B1 (ja)
JP (1) JP5344111B2 (ja)
KR (1) KR101456313B1 (ja)
CN (1) CN101652883B (ja)
CA (1) CA2682942C (ja)
ES (1) ES2659389T3 (ja)
WO (1) WO2008126364A1 (ja)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20160248089A1 (en) * 2008-10-01 2016-08-25 Toda Kogyo Corporation Lithium manganate particles for non-aqueous electrolyte secondary battery, process for producing the same, and nonaqueous electrolyte secondary battery
US9515314B2 (en) 2010-09-20 2016-12-06 Lg Chem, Ltd. Cathode active material comprising lithium manganese-based oxide and non-aqueous electrolyte secondary battery based upon the same
WO2020044652A1 (ja) * 2018-08-31 2020-03-05 パナソニックＩｐマネジメント株式会社 正極活物質およびそれを備えた電池

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JP5344111B2 (ja) * 2007-03-30 2013-11-20 戸田工業株式会社 非水電解液二次電池用マンガン酸リチウムの製造方法、並びに非水電解液二次電池
WO2010084855A1 (ja) 2009-01-20 2010-07-29 戸田工業株式会社 非水電解液二次電池用正極活物質およびその製造方法、非水電解液二次電池
JP5273617B2 (ja) * 2009-10-22 2013-08-28 国立大学法人福井大学 リチウムイオン二次電池正極活物質の製造方法
KR101337365B1 (ko) * 2010-09-20 2013-12-05 주식회사 엘지화학 도전성이 개선된 고용량 양극 활물질 및 이를 포함하는 비수 전해질 이차전지
EP2698351B1 (en) * 2011-04-14 2017-12-27 Toda Kogyo Corp. Li-Ni COMPOSITE OXIDE PARTICLE POWDER AND PROCESS FOR PRODUCING SAME, AND NON-AQUEOUS ELECTROLYTE SECONDARY BATTERY
JP6123391B2 (ja) * 2012-03-22 2017-05-10 東ソー株式会社 四三酸化マンガン及びその製造方法
US10109857B2 (en) 2012-04-05 2018-10-23 Tosoh Corporation Metal-containing trimanganese tetraoxide composite particles and method for producing same
JP6221310B2 (ja) * 2012-04-05 2017-11-01 東ソー株式会社 四三酸化マンガン組成物及びその製造方法並びにその用途
JP2013230967A (ja) * 2012-04-05 2013-11-14 Tosoh Corp 四三酸化マンガン組成物及びその製造法、並びにそれを用いたリチウムマンガン系複合酸化物の製造方法
US20160126547A1 (en) * 2012-11-13 2016-05-05 Kazumichi Koga Lithium manganate particles for non-aqueous electrolyte secondary batteries and process for producing the same, and non-aqueous electrolyte secondary battery
CN103746109B (zh) * 2014-01-16 2016-09-14 昆明理工大学 一种液相法包覆锂离子电池正极材料锰酸锂的方法
JP6417888B2 (ja) 2014-11-20 2018-11-07 戸田工業株式会社 非水電解質二次電池用正極活物質粒子粉末とその製造方法、および非水電解質二次電池
JP6428192B2 (ja) 2014-11-20 2018-11-28 戸田工業株式会社 非水電解質二次電池用正極活物質粒子粉末とその製造方法、および非水電解質二次電池
CN105576232B (zh) * 2016-03-01 2018-06-19 北京理工大学 一种锂离子电池正极材料暴露(111)活性晶面空心多级结构锰酸锂立方体的制备方法
JP7110647B2 (ja) * 2018-03-22 2022-08-02 住友金属鉱山株式会社 リチウムニッケル含有複合酸化物とその製造方法、および、リチウムイオン二次電池、並びに、リチウムニッケル含有複合酸化物の評価方法
CN112993236A (zh) * 2019-12-18 2021-06-18 天津国安盟固利新材料科技股份有限公司 一种单颗粒锰酸锂正极材料及其制备方法

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