WO2003089122A1 - Device and method of creating hydrodynamic cavitation in fluids - Google Patents
Device and method of creating hydrodynamic cavitation in fluids Download PDFInfo
- Publication number
- WO2003089122A1 WO2003089122A1 PCT/US2003/012410 US0312410W WO03089122A1 WO 2003089122 A1 WO2003089122 A1 WO 2003089122A1 US 0312410 W US0312410 W US 0312410W WO 03089122 A1 WO03089122 A1 WO 03089122A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- orifice
- liquid
- liquid jet
- flow
- cavitation
- Prior art date
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/008—Processes for carrying out reactions under cavitation conditions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/20—Jet mixers, i.e. mixers using high-speed fluid streams
- B01F25/23—Mixing by intersecting jets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/40—Static mixers
- B01F25/42—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
- B01F25/43—Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction
- B01F25/433—Mixing tubes wherein the shape of the tube influences the mixing, e.g. mixing tubes with varying cross-section or provided with inwardly extending profiles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/40—Static mixers
- B01F25/42—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
- B01F25/43—Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction
- B01F25/433—Mixing tubes wherein the shape of the tube influences the mixing, e.g. mixing tubes with varying cross-section or provided with inwardly extending profiles
- B01F25/4335—Mixers with a converging-diverging cross-section
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/40—Static mixers
- B01F25/45—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/40—Static mixers
- B01F25/45—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads
- B01F25/452—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads characterised by elements provided with orifices or interstitial spaces
- B01F25/4521—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads characterised by elements provided with orifices or interstitial spaces the components being pressed through orifices in elements, e.g. flat plates or cylinders, which obstruct the whole diameter of the tube
- B01F25/45211—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads characterised by elements provided with orifices or interstitial spaces the components being pressed through orifices in elements, e.g. flat plates or cylinders, which obstruct the whole diameter of the tube the elements being cylinders or cones which obstruct the whole diameter of the tube, the flow changing from axial in radial and again in axial
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/26—Nozzle-type reactors, i.e. the distribution of the initial reactants within the reactor is effected by their introduction or injection through nozzles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F2215/00—Auxiliary or complementary information in relation with mixing
- B01F2215/04—Technical information in relation with mixing
- B01F2215/0413—Numerical information
- B01F2215/0436—Operational information
- B01F2215/0468—Numerical pressure values
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F2215/00—Auxiliary or complementary information in relation with mixing
- B01F2215/04—Technical information in relation with mixing
- B01F2215/0413—Numerical information
- B01F2215/0436—Operational information
- B01F2215/0472—Numerical temperature values
Definitions
- the present invention relates to a device and method for creating hydrodynamic cavitation in fluids.
- This device and method according to the present invention may find application in mixing, synthesis, assisting in chemical reactions, and sonochemical reactions in the chemical, food, pharmaceuticals, cosmetics processing, and other types of industry.
- Cavitation is the formation of bubbles and cavities within a liquid stream resulting from a localized pressure drop in the liquid flow. If the pressure at some point decreases to a magnitude under which the liquid reaches the boiling point for this fluid, then a great number of vapor-filled cavities and bubbles are formed. As the pressure of the liquid then increases, vapor condensation takes place in the cavities and bubbles, and they collapse, creating very large pressure impulses and very high temperatures. According to some estimations, the temperature within the bubbles attains a magnitude on the order of 5000°C and a pressure of approximately 500 kg/cm 2 . Cavitation involves the entire sequence of events beginning with bubble formation through the collapse of the bubble. Because of this high energy level, cavitation has been studied for its ability to mix materials and aid in chemical reactions.
- cavitation there are several different ways to produce cavitation in a fluid.
- the way known to most people is the cavitation resulting from a propeller blade moving at a critical speed through water. If a sufficient pressure drop occurs at the blade surface, cavitation will result.
- the movement of a fluid through a restriction such as an orifice plate can also generate cavitation if the pressure drop across the orifice is sufficient. Both of these methods are commonly referred to as hydrodynamic cavitation.
- Cavitation may also be generated in a fluid by the use of ultrasound.
- a sound wave consists of compression and decompression cycles. If the pressure during the decompression cycle is low enough, bubbles may be formed. These bubbles will grow during the decompression cycle and contract or even implode during the compression cycle.
- U.S. Patent No. 5,931,771 introduced a method of producing ultra-thin emulsions and dispersions, which in accordance with the invention is comprised of the passage of a hydrodynamic liquid flow containing dispersed components through a flow-through channel, internally having at least one nozzle.
- a buffer channel which is directed by its open end in the nozzle side.
- a high velocity primary liquid jet which enters into the buffer channel at a minimal distance from the nozzle.
- a secondary liquid jet is formed, which moves in the buffer channel towards the primary jet and forms with the surface of the primary jet a high intensity vortex contact layer.
- collapsing cavitation caverns and bubbles are generated which disperse emulsions and dispersions to submicron sizes.
- U.S. Patent No. 5,720,551 features a method for use in causing emulsification in a fluid.
- a jet of fluid is directed along a first path, and a structure is interposed in the first path to cause the fluid to be redirected in a controlled flow along a new path, the first path and the new path being oriented to cause shear and cavitation in the fluid.
- the first path and the new path may be oriented in essentially opposite directions.
- the coherent flow may be a cylinder surrounding the jet.
- the interposed structure may have a reflecting surface that is generally semi-spherical, or is generally tapered, and lies at the end of a well.
- Adjustments may be made to the pressure in the well, in the distance from the opening of the well to the reflecting surface, and in the size of the opening to the well.
- the controlled flow, as it exits the well may be directed in an annular sheet away from the opening of the well.
- An annular flow of a coolant may be directed in a direction opposite to the direction of the annular sheet.
- a method for causing a reaction between two or more reactive substances comprises the step of colliding a flow of one reactive substance against a flow of another reactive substance at a high flow rate to cause a reaction between them. Furious turbulence and cavitation occur when the jet flows collide together at high speeds.
- the present invention provides a device for creating hydrodynamic cavitation in fluids comprising a chamber formed by a wall where the wall has a first orifice and an opposing second orifice that are both in fluid communication with said chamber.
- the first orifice and the second orifice share the same center-line and the first orifice has a diameter smaller than that of the second orifice.
- the device may further comprise a second pair of opposing orifices disposed in the wall such that the second pair of opposing orifices is in fluid communication with the chamber.
- a device for creating hydrodynamic cavitation in fluids comprises a flow-through channel having a wall wherein the wall has a first orifice that is in communication with the flow-through channel for introducing a first liquid stream into the flow- through channel and a second orifice opposite the first orifice that is in communication with the flow-through channel for introducing a second liquid stream into the flow-through channel.
- the first orifice and second orifice share the same center-line and the first orifice has a diameter smaller than that of the second orifice.
- the flow-through channel is configured for passing a hydrodynamic liquid through the flow-through channel.
- the first liquid stream comprises a first liquid and the second liquid stream comprises a second liquid, where the first and second liquids may be the same or different.
- the present invention provides for a device for creating hydrodynamic cavitation in fluids comprising a flow-through channel for passing a hydrodynamic liquid where the flow-through channel has an outlet, a cavitation chamber situated within the flow-through channel where the cavitation chamber is defined by a wall and an exit orifice, and a restriction wall in physical communication with the wall and the flow-through channel to prevent the hydrodynamic liquid from exiting the flow-through channel before entering the first and second orifices.
- the wall includes a pair of opposing orifices wherein the first and second orifices share the same center-line and are in communication with the chamber and the first orifice has a diameter smaller than that of the second orifice.
- the device may further comprise a second cavitation chamber situated within the flow-through channel in series with the first cavitation chamber, the second cavitation chamber having a pair of opposing orifices that share the same center-line and have different diameters.
- the wall may further include a second pair of opposing orifices that share the same center-line and have different diameters.
- the present invention provides for a method of creating hydrodynamic cavitation in fluids comprising: providing a first orifice and a second opposing orifice in a wall of a chamber such that the first and second orifices share the same center-line and the first orifice has a diameter smaller than that of the second orifice; introducing a first liquid stream through the first orifice to create a first liquid jet; introducing a second liquid stream through the second orifice to create a second liquid jet; creating a high shear intensity vortex contact layer when the first liquid jet interacts with and penetrates the second liquid jet; and creating and collapsing cavitation caverns and bubbles in the high shear intensity vortex contact layer.
- a method of creating hydrodynamic cavitation in fluids comprising: passing a hydrodynamic liquid through a flow-through channel having a wall; providing a first orifice and a second opposing orifice in the wall of the flow-through channel such that the first and second orifices share the same center-line, the first orifice has a diameter smaller than that of the second orifice; introducing a first liquid stream through the first orifice to create a first liquid jet; introducing a second liquid stream through the second orifice to create a second liquid jet; creatmg a high shear intensity vortex contact layer when the first liquid jet interacts with and penetrates the second liquid jet; and creating and collapsing cavitation caverns and bubbles in the high shear intensity vortex contact layer.
- a method of creating hydrodynamic cavitation in fluids comprising: passing a hydrodynamic liquid through a flow-through channel having an outlet; providing a cavitation chamber situated within the flow-through channel having a wall and an exit orifice; directing the liquid through the first orifice to create a first liquid jet; directing the liquid through the second orifice to create a second liquid jet; creating a high shear intensity vortex contact layer when the first liquid jet interacts with and penetrates the second liquid jet; and creating and collapsing cavitation caverns and bubbles in the high shear intensity vortex contact layer-:
- the wall includes a pair of opposing orifices wherein the first orifice and the second orifice share the same center- line and are in communication with the chamber and the first orifice has a diameter smaller than that of the second orifice.
- the method may further comprise: directing the liquid exiting from the exit orifice of the chamber towards a second cavitation chamber situated downstream of the chamber in the flow-through channel; directing the liquid through the first orifice of the second cavitation chamber to create a third liquid jet; directing the liquid through the second orifice of the second cavitation chamber to create a fourth liquid jet; creatmg a second high shear intensity vortex contact layer when the third liquid jet interacts with and. penetrates the fourth liquid jet; and creating and collapsing cavitation caverns and bubbles in the second high shear intensity vortex contact layer.
- the second cavitation chamber includes a wall having a pair of opposing orifices disposed therein wherein the first orifice and the second orifice share the same center- line and are in communication with the second chamber and the first orifice has a diameter smaller than that of the second orifice.
- the method may further comprise: directing the hydrodynamic liquid through a third orifice in the wall of the chamber to create a third liquid jet; directing the liquid through a fourth orifice in the wall of the chamber opposite the third orifice to create a fourth liquid jet, the third and fourth orifices share the same center- line and the third orifice has a diameter that is smaller than the fourth orifice; creating a second high shear intensity vortex contact layer when the third liquid jet interacts with and penetrates the fourth liquid jet; and creating and collapsing cavitation caverns and bubbles in the second high shear intensity vortex contact layer.
- FIG. 1 is a longitudinal cross-section of a first embodiment of the device according to the present invention wherein the device comprises a flow-through channel that includes a cavitation chamber having two opposed jetting orifices that empty into the chamber,
- FIG- 2 is a longitudinal cross-section of a second embodiment of the device according to the present invention wherein two opposed jetting orifices are provided in a flow-through channel wherein the two opposed jetting orifices are the only two inlets.
- FIG. 3 is a longitudinal cross-section of a third embodiment of the device according to the present invention wherein two opposed jetting orifices are provided in a flow-through channel having an inlet wherein the two opposed jetting orifices are secondary inlets.
- FIG. 4 is a modification of the first embodiment of the device according to the present invention wherein the device comprises three pairs of opposing jetting orifices.
- FIG. 5 is a modification of the first embodiment of the device according to the present invention wherein the device further comprises a second cavitation chamber situated in the flow- through channel in series with the first cavitation chamber.
- FIG. 1 illustrates a longitudinal cross-sectional view of a first embodiment of the device 10 comprising a flow-through channel 15 having an inlet 20 and an outlet 25.
- a cylindrical cavitation chamber 30 Situated within the flow-through channel 15 is a cylindrical cavitation chamber 30 defined by a front wall 35 perpendicular to the flow-through channel 15, a wall 40 parallel to the flow-through channel 15, and an exit orifice 45 in communication with the outlet 25.
- the arrangement of the cavitation chamber 30 within the flow-through channel 15 creates an annular opening 33.
- Wall 40 has a first jetting orifice 50 and a second jetting orifice 55 oriented directly opposite the first jetting orifice 50 such that the first jetting orifice 50 and the second jetting orifice 55 directly face each other and share the same center-line X.
- the diameter of the first jetting orifice 50 is smaller than the diameter of the second jetting orifice 55.
- the cavitation chamber 30 also includes a flange 60 in communication with wall 40 and the flow-through channel 15 to direct fluid into the cavitation chamber 30 and restrict fluid from exiting the flow-through channel without being directed into the first jetting orifice 50 or second jetting orifice 55.
- a hydrodynamic liquid stream moves along the direction, indicated by arrow A, through the inlet 20 and flows into flow-through channel 15. As the liquid stream approaches the front wall 35, the liquid stream is directed towards the annular opening 33. One portion of the liquid stream, indicated by arrow B, passes through the annular opening 33 and enters the first jetting orifice 50 forming a high velocity liquid jet 65 (hereinafter referred to as "smaller liquid jet 65" because this liquid jet exits the smaller diameter jetting orifice 50).
- the other portion of the liquid stream passes through the annular opening 33 and enters the second jetting orifice 55 forming a high velocity liquid jet 70 (hereinafter referred to as "larger liquid jet 70" because this liquid jet exits the larger diameter jetting orifice 55).
- Both smaller liquid jet 65 and larger liquid jet 70 flow into chamber 30 where they impinge along center-line X. Once the smaller liquid jet 65 and the larger liquid jet 70 impinge, smaller liquid jet 65 penetrates and interacts with larger liquid jet 70 thereby creating a high shear intensity vortex contact layer 75 between the liquid jets 65, 70. Cavitation caverns and bubbles are created in the high shear intensity vortex contact layer 75. During the collapse of cavitation caverns and bubbles, high localized pressures, up to 1000 MPa, arise and the level of energy dissipation in the flow-through channel 205 attains a magnitude in the range of 1 10 - 1 15 watt/kg.
- the first embodiment includes only one pair of opposing jetting orifices, it is possible to provide two or more pairs of opposing jetting orifices within the wall 340 and in communication with the chamber 330.
- the first opposing jetting orifice of each pair has a diameter smaller than that of the second opposing jetting orifice.
- This alternate design is shown as device 300 in FIG. 4, with arrow A representing the flow of hydrodynamic fluid through the flow-through channel 305.
- Wall 340 includes a first pair of opposing jettmg orifices 350, 355, a second pair of opposing jetting orifices 360, 365, and a third pair of opposing jetting orifices 370, 375.
- the device 300 is structurally and functionally identical to the device 10 of the first embodiment, except for the addition of two pairs of opposing jetting orifices 370, 375.
- the first embodiment includes only one cavitation chamber 30, it is possible to provide two or more cavitation chambers in series within the flow-through chamber.
- This alternate design is shown as device 400 in FIG. 5, with arrow A representing the flow of hydrodynamic fluid through the flow-through channel 405.
- the device 400 includes a first cavitation chamber 430 defined by a front wall 435, a wall 440 having a pair of opposing jetting orifices 450, 455, and an exit orifice 445.
- the device 400 includes a second cavitation chamber 460 defined by a front wall 465, a wall 470 having a pair of opposing jetting orifices 475, 480, and an exit orifice 485.
- the device 400 is structurally and functionally identical to the device 10 of the first embodiment, except for the addition of the second chamber 460.
- the preferred cavitation chamber 30 is cylindrical in shape, it is contemplated that any shape may be possible provided that the liquid flow is permitted to enter the cavitation chamber 30. Such shapes may include cubical, conical, spherical, semi-spherical, or rectangular.
- FIG. 2 represents a second embodiment according to the present invention.
- FIG. 2 illustrates a longitudinal cross-sectional view of the device 100 comprising a flow through channel 105 having a first inlet 110, a second inlet 115, and an outlet 120.
- the first inlet 110 includes a first jetting orifice 125 and the second inlet 115 includes a second jetting orifice 130.
- the first jetting orifice 125 is oriented directly opposite the second jetting orifice 130 such that the first jetting orifice 125 and the second jetting orifice 130 directly face each other and share the same center-line X.
- the diameter of the first jetting orifice 125 is smaller than the diameter of the second jetting orifice 130.
- a first hydrodynamic liquid stream enters the first inlet 110 and passes through the first jetting orifice 125 forming a high velocity liquid jet 135 (hereinafter referred to as "smaller liquid jet 135" because this liquid jet exits the smaller diameter jetting orifice 125) that flows into flow-through channel 105.
- a second hydrodynamic liquid stream enters the second inlet 115 and passes through the second jetting orifice 130 forming a high velocity liquid jet 140 (hereinafter referred to as "larger liquid jet 140" because this liquid jet exits the larger diameter jetting orifice 130) that flows into flow-through channel 105.
- Both the smaller liquid jet 135 and the larger liquid jet 140 flow into the flow-through channell05 where they impinge along center-line X. Once the smaller liquid jet 135 and the larger liquid jet 140 impinge, smaller liquid jet 135 penetrates and interacts with larger liquid jet 140 thereby creating a high shear intensity vortex contact layer 145 between the liquid jets 135, 140. Cavitation caverns and bubbles are created in the high shear intensity vortex contact layer 145. During the collapse of cavitation caverns and bubbles, high localized pressures, up to 1000 MPa, arise and the level of energy dissipation in the flow- through channel 205 attains a magnitude in the range of 1 10 - 1 15 watt/kg.
- the device 100 is capable of receiving liquids having the same or different characteristics, which provides the operator with the ability to modify and control the desired cavitation effects.
- the first and second hydrodynamic liquid streams discussed above comprise a first and second liquid, respectively.
- the first and second liquids may be the same liquid, different liquids, or any combination thereof.
- Each liquid may be a pure liquid, a liquid containing solid particles, a liquid containing droplets, an emulsion of multiple materials, a slurry, or a suspension.
- each liquid may be introduced to the device under different physical conditions and chemical compositions. Such physical conditions may include pressure, temperature, viscosity, and density.
- Such chemical compositions may include different chemical formulations and concentrations.
- the second embodiment illustrates a flow-through channel having a pair of opposing jetting orifices disposed therein
- any chamber maybe provided with a pair of opposing jetting orifices to practice the present invention.
- Such chambers may include tank, a pipe, a spherical vessel, a cylindrical vessel such as a drum, or any other desired shape. It is also contemplated that any size and shape may be possible provided that the liquid flow is permitted to enter the chamber.
- Such shapes may include cubical, conical, spherical, semi-spherical, or rectangular.
- FIG. 3 represents a third embodiment according to the present invention.
- FIG. 3 illustrates a longitudinal cross-sectional view of the device 200 comprising a flow through chamber 205 having an inlet 207 and an outlet 220.
- the flow-through channel also includes a first ancillary inlet 210 and a second ancillary inlet 215.
- the first ancillary inlet 210 includes a first jetting orifice 225 and the second ancillary inlet 215 includes a second jetting orifice 230.
- the first jetting orifice 225 is oriented directly opposite the second jetting orifice 230 such that the first jetting orifice 225 and the second jetting orifice 230 directly face each other and share the same center-line X.
- the diameter of the first jetting orifice 225 is smaller than the diameter of the second jetting orifice 230.
- a first hydrodynamic liquid stream moves along the direction, indicated by arrow A, through the inlet 207 and flows into the flow-through channel 205.
- a second hydrodynamic liquid stream enters the first ancillary inlet 210 and passes through the first jetting orifice 225 forming a high velocity liquid jet 235 (hereinafter refened to as "smaller liquid jet 235" because this liquid jet exits the smaller diameter jetting orifice 225) that flows into flow-through channel 205.
- a third hydrodynamic liquid stream enters the second ancillary inlet 215 and passes through the second jetting orifice 230 forming a high velocity liquid jet 240 (hereinafter referred to as "larger liquid jet 240" because this liquid jet exits the larger diameter jetting orifice 230) that flows into flow-through channel 205.
- large liquid jet 240 a high velocity liquid jet 240
- Both the smaller liquid jet 235 and the larger liquid jet 240 flow into the flow-through chamber 205 where they impinge along center-line X.
- the device 200 is capable of receiving liquids having the same or different characteristics, which provides the operator with the ability to modify and control the desired cavitation effects.
- the first and second hydrodynamic liquid streams discussed above comprise a first and second liquid, respectively.
- the first and second liquids may be the same liquid, different liquids, or any combination thereof.
- Each liquid may be a pure liquid, a liquid containing solid particles, a liquid containing droplets, an emulsion of multiple materials, a slurry, or a suspension.
- each liquid may be introduced to the device under different physical conditions and chemical compositions. Such physical conditions may include pressure, temperature, viscosity, and density.
- Such chemical compositions may include different chemical formulations and concentrations.
- the third embodiment illustrates a flow-through channel having a pair of opposing jetting orifices disposed therein
- any chamber may be provided with a pair of opposing jetting orifices to practice the present invention.
- Such chambers may include tank, a pipe, a spherical vessel, a cylindrical vessel such as a drum, or any other desired shape. It is also contemplated that any size and shape may be possible provided that the liquid flow is permitted to enter the chamber.
- Such shapes may include cubical, conical, spherical, semi-spherical, or rectangular.
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Dispersion Chemistry (AREA)
- Organic Chemistry (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Structures Of Non-Positive Displacement Pumps (AREA)
Abstract
Description
Claims
Priority Applications (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CA002482459A CA2482459A1 (en) | 2002-04-22 | 2003-04-22 | Device and method of creating hydrodynamic cavitation in fluids |
AU2003228638A AU2003228638A1 (en) | 2002-04-22 | 2003-04-22 | Device and method of creating hydrodynamic cavitation in fluids |
DE60323480T DE60323480D1 (en) | 2002-04-22 | 2003-04-22 | DEVICE AND METHOD FOR GENERATING HYDRODYNAMIC CAVITATION IN FLUIDS |
EP03726399A EP1501626B1 (en) | 2002-04-22 | 2003-04-22 | Device and method of creating hydrodynamic cavitation in fluids |
MXPA04010449A MXPA04010449A (en) | 2002-04-22 | 2003-04-22 | Device and method of creating hydrodynamic cavitation in fluids. |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/131,512 | 2002-04-22 | ||
US10/131,512 US20030199595A1 (en) | 2002-04-22 | 2002-04-22 | Device and method of creating hydrodynamic cavitation in fluids |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2003089122A1 true WO2003089122A1 (en) | 2003-10-30 |
Family
ID=29215572
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/US2003/012410 WO2003089122A1 (en) | 2002-04-22 | 2003-04-22 | Device and method of creating hydrodynamic cavitation in fluids |
Country Status (8)
Country | Link |
---|---|
US (2) | US20030199595A1 (en) |
EP (1) | EP1501626B1 (en) |
AT (1) | ATE407732T1 (en) |
AU (1) | AU2003228638A1 (en) |
CA (1) | CA2482459A1 (en) |
DE (1) | DE60323480D1 (en) |
MX (1) | MXPA04010449A (en) |
WO (1) | WO2003089122A1 (en) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2939423B1 (en) * | 2008-12-09 | 2011-12-09 | Yves Lecoffre | METHOD AND DEVICE FOR TREATING AT LEAST ONE COMPOUND TRANSPORTED IN A LIQUID |
SG163454A1 (en) * | 2009-01-30 | 2010-08-30 | Neftech Pte Ltd | A method and apparatus for increasing the fuel efficiency of mixed fuels |
US9126176B2 (en) | 2012-05-11 | 2015-09-08 | Caisson Technology Group LLC | Bubble implosion reactor cavitation device, subassembly, and methods for utilizing the same |
US9682355B2 (en) * | 2014-06-18 | 2017-06-20 | Arisdyne Systems, Inc. | Method for conducting sonochemical reactions and processes |
EP3442694A4 (en) * | 2016-04-12 | 2019-12-18 | Arisdyne Systems, Inc. | Method and device for cavitationally treating a fluid |
CN107812458A (en) * | 2017-11-28 | 2018-03-20 | 佛山科学技术学院 | A kind of chemical liquid blender |
EA202193079A1 (en) * | 2019-05-10 | 2022-02-11 | Грэфен Стар Лтд | GRAPHENE PRODUCTION METHOD |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3849074A (en) * | 1972-12-07 | 1974-11-19 | Du Pont | Apparatus for mixing quickly reactive materials |
US4996004A (en) * | 1982-08-14 | 1991-02-26 | Bayer Aktiengesellschaft | Preparation of pharmaceutical or cosmetic dispersions |
US5723518A (en) * | 1994-06-03 | 1998-03-03 | Bayer Aktiengesellschaft | Aqueous two-component polyurethane coating compositions and a method for their preparation |
Family Cites Families (33)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US1496858A (en) * | 1923-02-17 | 1924-06-10 | Knollenberg Rudolf | Mixing liquids |
US2137338A (en) * | 1934-03-28 | 1938-11-22 | Gosmann Walther | Apparatus for producing foam for fire extinguishing purposes |
US2751335A (en) * | 1951-02-01 | 1956-06-19 | Exxon Research Engineering Co | Method and apparatus for mixing and contacting fluids |
US2890868A (en) * | 1955-08-01 | 1959-06-16 | Haskelite Mfg Corp | Mixing head |
NL283530A (en) * | 1961-08-19 | |||
US3701484A (en) * | 1970-11-20 | 1972-10-31 | Johns Manville | Apparatus and process for suspending solids |
US3833718A (en) * | 1971-04-02 | 1974-09-03 | Chevron Res | Method of mixing an aqueous aluminum salt solution and an alkaline base solution in a jet mixer to form a hydroxy-aluminum solution |
US3894562A (en) * | 1973-12-20 | 1975-07-15 | Jr Charles D Moseley | Fluid flow controller |
US4043539A (en) * | 1975-03-28 | 1977-08-23 | Texaco Inc. | Method and apparatus for static type fluid mixing |
US4189243A (en) * | 1978-01-25 | 1980-02-19 | Black Wesley F | In-line mud shearing apparatus |
US4908154A (en) * | 1981-04-17 | 1990-03-13 | Biotechnology Development Corporation | Method of forming a microemulsion |
US4533254A (en) * | 1981-04-17 | 1985-08-06 | Biotechnology Development Corporation | Apparatus for forming emulsions |
US4440500A (en) * | 1982-06-21 | 1984-04-03 | Polyurethane Technology Of America-Martin Sweets Company, Inc. | High pressure impingement mixing apparatus |
US5116536A (en) * | 1982-08-14 | 1992-05-26 | Bayer Aktiengesellschaft | Preparation of pharmaceutical or cosmetic dispersions |
DE3242278A1 (en) * | 1982-11-16 | 1984-05-17 | Basf Ag, 6700 Ludwigshafen | DEVICE FOR PRODUCING A MIXTURE FROM AT LEAST TWO PLASTIC COMPONENTS |
DE3633343A1 (en) * | 1986-09-10 | 1988-03-17 | Bayer Ag | METHOD AND DEVICE FOR PRODUCING A PLASTIC, IN PARTICULAR FOAM-MAKING, FLOWABLE REACTION MIXTURE FROM AT LEAST TWO FLOWABLE REACTION COMPONENTS IN A CONTINUOUS PROCESS |
DE4128999A1 (en) * | 1991-08-31 | 1993-03-04 | Adrian Verstallen | Fluid emulsion mixer - subjects the inner phase to high pressure to form thin flat layers which are mixed in a counterflow |
JP2553287B2 (en) * | 1992-07-29 | 1996-11-13 | 幸彦 唐澤 | Emulsifier |
US5417956A (en) * | 1992-08-18 | 1995-05-23 | Worcester Polytechnic Institute | Preparation of nanophase solid state materials |
US5466646A (en) * | 1992-08-18 | 1995-11-14 | Worcester Polytechnic Institute | Process for the preparation of solid state materials and said materials |
US5482369A (en) * | 1993-02-08 | 1996-01-09 | Verstallen; Adrian | Process for homogenizing essentially immiscible liquids for forming an emulsion |
JP2527297B2 (en) * | 1993-10-01 | 1996-08-21 | ナノマイザー株式会社 | Material atomizer |
US5720551A (en) * | 1994-10-28 | 1998-02-24 | Shechter; Tal | Forming emulsions |
US5852076A (en) * | 1994-11-13 | 1998-12-22 | Minnesota Mining And Manufacturing Company | Process for preparing a dispersion of hard particles in solvent |
EP0787035B1 (en) * | 1994-11-14 | 2001-08-16 | Minnesota Mining And Manufacturing Company | Process and apparatus for preparing a dispersion of hard particles in solvent |
DE19536845A1 (en) * | 1995-10-02 | 1997-04-03 | Bayer Ag | Method and device for producing finely divided solid dispersions |
DE19617086A1 (en) * | 1996-04-29 | 1997-10-30 | Bayer Ag | Process for the preparation of aqueous coating compositions for stove enamels |
US6227694B1 (en) * | 1996-12-27 | 2001-05-08 | Genus Corporation | High speed collision reaction method |
DE19700810A1 (en) * | 1997-01-13 | 1998-07-16 | Bayer Ag | Method and device for homogenizing milk |
DE19708606A1 (en) * | 1997-03-03 | 1998-09-10 | Bayer Ag | Process for the production of stable, finely divided polymer dispersions |
CA2299284C (en) * | 1997-08-05 | 2008-07-08 | Mfic Corporation | Multiple stream high pressure mixer/reactor |
US5931771A (en) * | 1997-12-24 | 1999-08-03 | Kozyuk; Oleg V. | Method and apparatus for producing ultra-thin emulsions and dispersions |
US6365555B1 (en) * | 1999-10-25 | 2002-04-02 | Worcester Polytechnic Institute | Method of preparing metal containing compounds using hydrodynamic cavitation |
-
2002
- 2002-04-22 US US10/131,512 patent/US20030199595A1/en not_active Abandoned
-
2003
- 2003-04-22 DE DE60323480T patent/DE60323480D1/en not_active Expired - Fee Related
- 2003-04-22 CA CA002482459A patent/CA2482459A1/en not_active Abandoned
- 2003-04-22 AT AT03726399T patent/ATE407732T1/en not_active IP Right Cessation
- 2003-04-22 MX MXPA04010449A patent/MXPA04010449A/en active IP Right Grant
- 2003-04-22 WO PCT/US2003/012410 patent/WO2003089122A1/en not_active Application Discontinuation
- 2003-04-22 AU AU2003228638A patent/AU2003228638A1/en not_active Abandoned
- 2003-04-22 EP EP03726399A patent/EP1501626B1/en not_active Expired - Lifetime
-
2004
- 2004-01-16 US US10/760,606 patent/US20040246815A1/en not_active Abandoned
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3849074A (en) * | 1972-12-07 | 1974-11-19 | Du Pont | Apparatus for mixing quickly reactive materials |
US4996004A (en) * | 1982-08-14 | 1991-02-26 | Bayer Aktiengesellschaft | Preparation of pharmaceutical or cosmetic dispersions |
US5723518A (en) * | 1994-06-03 | 1998-03-03 | Bayer Aktiengesellschaft | Aqueous two-component polyurethane coating compositions and a method for their preparation |
Also Published As
Publication number | Publication date |
---|---|
US20030199595A1 (en) | 2003-10-23 |
ATE407732T1 (en) | 2008-09-15 |
EP1501626A4 (en) | 2007-08-15 |
AU2003228638A1 (en) | 2003-11-03 |
DE60323480D1 (en) | 2008-10-23 |
US20040246815A1 (en) | 2004-12-09 |
MXPA04010449A (en) | 2005-02-24 |
EP1501626A1 (en) | 2005-02-02 |
CA2482459A1 (en) | 2003-10-30 |
EP1501626B1 (en) | 2008-09-10 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
US6749329B2 (en) | Processing product components | |
US5931771A (en) | Method and apparatus for producing ultra-thin emulsions and dispersions | |
KR950011425B1 (en) | In-line dispersion of gas in liquid | |
US5205648A (en) | Method and device for acting upon fluids by means of a shock wave | |
US5492654A (en) | Method of obtaining free disperse system and device for effecting same | |
US7762715B2 (en) | Cavitation generator | |
US6042089A (en) | Foam generating device | |
US7086777B2 (en) | Device for creating hydrodynamic cavitation in fluids | |
US5061406A (en) | In-line gas/liquid dispersion | |
CA2320450C (en) | Method and apparatus of producing liquid disperse systems in liquid | |
JP2006503227A (en) | Jet pump | |
WO2001045830A1 (en) | Rotating membrane | |
US9776159B2 (en) | Device for conducting sonochemical reactions and processing liquids | |
CN112755826B (en) | Device and method for enhancing liquid-liquid emulsification | |
JP2013530033A (en) | Method and apparatus for cavitation generation for mixing and emulsification | |
US20030199595A1 (en) | Device and method of creating hydrodynamic cavitation in fluids | |
RU1773469C (en) | Rotary apparatus | |
CA2056418A1 (en) | Apparatus and method for sparging a gas into a liquid | |
US10639599B2 (en) | Method and device for cavitationally treating a fluid | |
SU1549570A1 (en) | Hydrodynamic homogenizer/mixer | |
CA3082103C (en) | Multilobular supersonic gas nozzles for liquid sparging | |
SU1176933A1 (en) | Cavitation mixer | |
SU820892A1 (en) | Method and apparatus for dispersing liquid | |
WO2009154587A1 (en) | Device for mixing fluid media |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
AK | Designated states |
Kind code of ref document: A1 Designated state(s): AE AG AL AM AT AU AZ BA BB BG BR BY BZ CA CH CN CO CR CU CZ DE DK DM DZ EC EE ES FI GB GD GE GH GM HR HU ID IL IN IS JP KE KG KP KR KZ LC LK LR LS LT LU LV MA MD MG MK MN MW MX MZ NO NZ PL PT RO RU SD SE SG SK SL TJ TM TR TT TZ UA UG US UZ VN YU ZA ZW |
|
AL | Designated countries for regional patents |
Kind code of ref document: A1 Designated state(s): GH GM KE LS MW MZ SD SL SZ TZ UG ZM ZW AM AZ BY KG KZ MD RU TJ TM AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HU IE IT LU MC NL PT RO SE SI SK TR BF BJ CF CG CI CM GA GN GQ GW ML MR NE SN TD TG |
|
121 | Ep: the epo has been informed by wipo that ep was designated in this application | ||
WWE | Wipo information: entry into national phase |
Ref document number: 2482459 Country of ref document: CA |
|
WWE | Wipo information: entry into national phase |
Ref document number: PA/a/2004/010449 Country of ref document: MX |
|
WWE | Wipo information: entry into national phase |
Ref document number: 2003726399 Country of ref document: EP |
|
WWP | Wipo information: published in national office |
Ref document number: 2003726399 Country of ref document: EP |
|
NENP | Non-entry into the national phase |
Ref country code: JP |
|
WWW | Wipo information: withdrawn in national office |
Country of ref document: JP |