WO2001023061A3 - Recovery process for volatile compounds from solids in aqueous solution - Google Patents

Recovery process for volatile compounds from solids in aqueous solution Download PDF

Info

Publication number
WO2001023061A3
WO2001023061A3 PCT/US2000/026940 US0026940W WO0123061A3 WO 2001023061 A3 WO2001023061 A3 WO 2001023061A3 US 0026940 W US0026940 W US 0026940W WO 0123061 A3 WO0123061 A3 WO 0123061A3
Authority
WO
WIPO (PCT)
Prior art keywords
solids
volatile compounds
aqueous solution
recovery process
volatile
Prior art date
Application number
PCT/US2000/026940
Other languages
French (fr)
Other versions
WO2001023061A2 (en
Inventor
F Glenn Gallagher
George Schurr
Original Assignee
Du Pont
F Glenn Gallagher
George Schurr
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Du Pont, F Glenn Gallagher, George Schurr filed Critical Du Pont
Priority to CA002379624A priority Critical patent/CA2379624A1/en
Priority to DE60035701T priority patent/DE60035701D1/en
Priority to JP2001526267A priority patent/JP2003510170A/en
Priority to KR1020027004100A priority patent/KR100632323B1/en
Priority to MXPA02003242A priority patent/MXPA02003242A/en
Priority to EP00967155A priority patent/EP1216083B1/en
Priority to BRPI0014578-5A priority patent/BR0014578B1/en
Publication of WO2001023061A2 publication Critical patent/WO2001023061A2/en
Publication of WO2001023061A3 publication Critical patent/WO2001023061A3/en
Priority to NO20021336A priority patent/NO20021336L/en
Priority to HK02106359.0A priority patent/HK1044499A1/en

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B25/00—Details of general application not covered by group F26B21/00 or F26B23/00
    • F26B25/005—Treatment of dryer exhaust gases
    • F26B25/006—Separating volatiles, e.g. recovering solvents from dryer exhaust gases
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/16—Evaporating by spraying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/16—Evaporating by spraying
    • B01D1/18—Evaporating by spraying to obtain dry solids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/06—Flash distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0057—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes
    • B01D5/006—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes with evaporation or distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Physical Water Treatments (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)

Abstract

Volatile compounds may be economically recovered from solids present in aqueous solution by subjecting the solution to rapid separation where the volatilization occurs in a flash, spray, or fluid bed, or mechanically agitated dryers. Rapidly separating the solids from the volatile compound greatly simplifies the isolation of the volatile compounds from water. The methods have utility for fermentation processes, solids management, and recycling processes.
PCT/US2000/026940 1999-09-30 2000-09-29 Recovery process for volatile compounds from solids in aqueous solution WO2001023061A2 (en)

Priority Applications (9)

Application Number Priority Date Filing Date Title
CA002379624A CA2379624A1 (en) 1999-09-30 2000-09-29 Recovery process for volatile compounds from solids in aqueous solution
DE60035701T DE60035701D1 (en) 1999-09-30 2000-09-29 RECOVERY METHOD FOR VOLATILE COMPOUNDS OF SOLIDS-CONTAINING AQUEOUS SOLUTIONS
JP2001526267A JP2003510170A (en) 1999-09-30 2000-09-29 Recovery of volatile compounds from solids in aqueous solution.
KR1020027004100A KR100632323B1 (en) 1999-09-30 2000-09-29 Recovery method of volatile compounds from solids in aqueous solution
MXPA02003242A MXPA02003242A (en) 1999-09-30 2000-09-29 Recovery process for volatile compounds from solids in aqueous solution.
EP00967155A EP1216083B1 (en) 1999-09-30 2000-09-29 Recovery process for volatile compounds from solids in aqueous solution
BRPI0014578-5A BR0014578B1 (en) 1999-09-30 2000-09-29 process for the recovery of volatile solids compounds present in an aqueous solution.
NO20021336A NO20021336L (en) 1999-09-30 2002-03-18 Recovery process of volatiles from solids in aqueous solution
HK02106359.0A HK1044499A1 (en) 1999-09-30 2002-08-28 Recovery process for volatile compounds from solids in aqueous solution

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US15686399P 1999-09-30 1999-09-30
US60/156,863 1999-09-30

Publications (2)

Publication Number Publication Date
WO2001023061A2 WO2001023061A2 (en) 2001-04-05
WO2001023061A3 true WO2001023061A3 (en) 2001-10-25

Family

ID=22561413

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2000/026940 WO2001023061A2 (en) 1999-09-30 2000-09-29 Recovery process for volatile compounds from solids in aqueous solution

Country Status (14)

Country Link
US (1) US6538164B1 (en)
EP (1) EP1216083B1 (en)
JP (1) JP2003510170A (en)
KR (1) KR100632323B1 (en)
CN (1) CN1377292A (en)
AT (1) ATE367851T1 (en)
BR (1) BR0014578B1 (en)
CA (1) CA2379624A1 (en)
DE (1) DE60035701D1 (en)
HK (1) HK1044499A1 (en)
MX (1) MXPA02003242A (en)
NO (1) NO20021336L (en)
TR (1) TR200200822T2 (en)
WO (1) WO2001023061A2 (en)

Families Citing this family (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101105957B1 (en) * 2003-05-06 2012-01-18 테이트 앤드 라일 인그레디언츠 아메리카스, 인크. Purification of biologically-produced 1,3-propanediol
US7323539B2 (en) 2003-05-06 2008-01-29 E. I. Du Pont De Nemours And Company Polytrimethylene ether glycol and polytrimethylene ether ester with excellent quality
US20050089979A1 (en) * 2003-09-18 2005-04-28 Ezeji Thaddeus C. Process for continuous solvent production
US7695594B2 (en) * 2003-09-30 2010-04-13 Clark Arthur F Method for separating volatile components by dilutive distillation
DE102005056669A1 (en) * 2005-11-28 2007-05-31 Basf Ag Fermentative preparation of organic compounds, useful for making, e.g. amino acids or enzymes, using a starch source from which non-starch solids have not been removed, hydrolyzed and enzymatically converted to monosaccharides
US20070203323A1 (en) * 2006-02-10 2007-08-30 Gyorgyi Fenyvesi Food compositions comprising biologically-based biodegradable 1,3-propanediol esters
US8163826B2 (en) 2006-11-21 2012-04-24 Schlumberger Technology Corporation Polymeric acid precursor compositions and methods
FR2913974A1 (en) * 2007-03-19 2008-09-26 Arkema France GLYCEROL VAPORIZATION PROCESS
US20090198088A1 (en) * 2008-02-01 2009-08-06 Lanxess Sybron Chemicals Inc. Process for the purification of crude glycerin utilizing ion exclusion chromatorgraphy and glycerin concentration
EP2402423B8 (en) * 2009-02-26 2014-03-26 S.T. Corporation Method for producing monoterpene component-rich essential oil
US20110127254A1 (en) * 2009-11-30 2011-06-02 Cypress Technology Llc Electric Heating Systems and Associated Methods
CN102666651B (en) * 2009-12-21 2014-09-10 纳幕尔杜邦公司 Processes for producing polytrimethylene ether glycol and copolymers thereof
JP6081690B2 (en) * 2009-12-22 2017-02-15 花王株式会社 Liquid cooling method
WO2011077652A1 (en) * 2009-12-22 2011-06-30 花王株式会社 Liquid cooling method
KR101376159B1 (en) 2011-11-28 2014-03-20 대상 주식회사 Method for recoverying diols from fermentation broth
KR102547252B1 (en) * 2016-01-08 2023-06-23 에스케이이노베이션 주식회사 Method for Manufacturing Vapor Dehydration Reaction Feed of Organic Material
WO2018009762A1 (en) * 2016-07-07 2018-01-11 Waters Technologies Corporation Venturi method of low pressure recycling of co2
SG11201905673RA (en) 2017-03-20 2019-10-30 Lanzatech Inc A process and system for product recovery and cell recycle
JP6643637B2 (en) 2017-06-06 2020-02-12 パナソニックＩｐマネジメント株式会社 VOC refining equipment
CA3129223C (en) 2019-02-08 2023-07-11 Lanzatech, Inc. Process for recovering close boiling products
CN110585749B (en) * 2019-08-26 2022-04-19 浙江工业大学 Device and method for separating viscous solid-liquid mixture
CN110773079B (en) * 2019-11-18 2022-03-01 江苏博迁新材料股份有限公司 Method for preparing superfine powder balls by ultrasonic spraying method
CN116712742B (en) * 2023-08-11 2024-02-02 黑龙江飞鹤乳业有限公司 Industrial open type spray multistage drying system

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB737570A (en) * 1952-06-23 1955-09-28 Ici Ltd Improvements in or relating to the recovery of glycerol from industrial liquors by evaporation
US4497838A (en) * 1982-02-17 1985-02-05 Tropicana Products, Inc. Process for the production of useful products from orange peel
DE4030331A1 (en) * 1990-09-25 1992-03-26 Beister Heinz J Dr METHOD AND DEVICE FOR THE DISPOSAL OF GLYCOL-CONTAINING OPERATING LIQUIDS
US5904321A (en) * 1992-08-19 1999-05-18 Glyrecsys, Inc. Deicing fluid recovery system especially adapted for aircraft deicing apparatus

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
LU48718A1 (en) * 1964-06-01 1965-12-01
US5158651A (en) * 1990-06-11 1992-10-27 Hoechst Celanese Corporation Process of centrifugally removing inorganic compounds from polyester glycol recovery bottoms
US6165962A (en) * 1997-07-31 2000-12-26 E. I. Du Pont De Nemours And Comapny Aqueous microemulsions

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB737570A (en) * 1952-06-23 1955-09-28 Ici Ltd Improvements in or relating to the recovery of glycerol from industrial liquors by evaporation
US4497838A (en) * 1982-02-17 1985-02-05 Tropicana Products, Inc. Process for the production of useful products from orange peel
DE4030331A1 (en) * 1990-09-25 1992-03-26 Beister Heinz J Dr METHOD AND DEVICE FOR THE DISPOSAL OF GLYCOL-CONTAINING OPERATING LIQUIDS
US5904321A (en) * 1992-08-19 1999-05-18 Glyrecsys, Inc. Deicing fluid recovery system especially adapted for aircraft deicing apparatus

Also Published As

Publication number Publication date
CN1377292A (en) 2002-10-30
DE60035701D1 (en) 2007-09-06
BR0014578A (en) 2002-06-18
MXPA02003242A (en) 2002-10-31
EP1216083B1 (en) 2007-07-25
KR100632323B1 (en) 2006-10-11
JP2003510170A (en) 2003-03-18
HK1044499A1 (en) 2002-10-25
US6538164B1 (en) 2003-03-25
CA2379624A1 (en) 2001-04-05
EP1216083A2 (en) 2002-06-26
KR20020043598A (en) 2002-06-10
WO2001023061A2 (en) 2001-04-05
TR200200822T2 (en) 2002-06-21
ATE367851T1 (en) 2007-08-15
NO20021336L (en) 2002-05-28
NO20021336D0 (en) 2002-03-18
BR0014578B1 (en) 2010-02-09

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