WO2000062688A1 - Apparatus and method for tuning ultrasonic transducers - Google Patents
Apparatus and method for tuning ultrasonic transducers Download PDFInfo
- Publication number
- WO2000062688A1 WO2000062688A1 PCT/US2000/005964 US0005964W WO0062688A1 WO 2000062688 A1 WO2000062688 A1 WO 2000062688A1 US 0005964 W US0005964 W US 0005964W WO 0062688 A1 WO0062688 A1 WO 0062688A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- ultrasonic transducer
- transducer
- resonant frequency
- tuning
- threaded portion
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 59
- 230000008569 process Effects 0.000 claims abstract description 20
- 238000004519 manufacturing process Methods 0.000 claims abstract description 13
- 238000003780 insertion Methods 0.000 claims description 4
- 230000037431 insertion Effects 0.000 claims description 4
- 235000011890 sandwich Nutrition 0.000 claims 5
- 239000000463 material Substances 0.000 abstract description 10
- 238000009966 trimming Methods 0.000 abstract description 6
- 239000012636 effector Substances 0.000 description 12
- 230000000712 assembly Effects 0.000 description 6
- 238000000429 assembly Methods 0.000 description 6
- 230000006835 compression Effects 0.000 description 5
- 238000007906 compression Methods 0.000 description 5
- 230000003247 decreasing effect Effects 0.000 description 5
- 230000000694 effects Effects 0.000 description 5
- 230000026683 transduction Effects 0.000 description 5
- 238000010361 transduction Methods 0.000 description 5
- 239000007787 solid Substances 0.000 description 3
- 229910052782 aluminium Inorganic materials 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- 230000008878 coupling Effects 0.000 description 2
- 238000010168 coupling process Methods 0.000 description 2
- 238000005859 coupling reaction Methods 0.000 description 2
- 238000006073 displacement reaction Methods 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 230000003321 amplification Effects 0.000 description 1
- FFBHFFJDDLITSX-UHFFFAOYSA-N benzyl N-[2-hydroxy-4-(3-oxomorpholin-4-yl)phenyl]carbamate Chemical compound OC1=C(NC(=O)OCC2=CC=CC=C2)C=CC(=C1)N1CCOCC1=O FFBHFFJDDLITSX-UHFFFAOYSA-N 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- NKZSPGSOXYXWQA-UHFFFAOYSA-N dioxido(oxo)titanium;lead(2+) Chemical compound [Pb+2].[O-][Ti]([O-])=O NKZSPGSOXYXWQA-UHFFFAOYSA-N 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012212 insulator Substances 0.000 description 1
- HFGPZNIAWCZYJU-UHFFFAOYSA-N lead zirconate titanate Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[Ti+4].[Zr+4].[Pb+2] HFGPZNIAWCZYJU-UHFFFAOYSA-N 0.000 description 1
- 229910052451 lead zirconate titanate Inorganic materials 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000002324 minimally invasive surgery Methods 0.000 description 1
- 238000003199 nucleic acid amplification method Methods 0.000 description 1
- 230000008520 organization Effects 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
- 239000010937 tungsten Substances 0.000 description 1
- 238000002604 ultrasonography Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61B—DIAGNOSIS; SURGERY; IDENTIFICATION
- A61B17/00—Surgical instruments, devices or methods, e.g. tourniquets
- A61B17/32—Surgical cutting instruments
- A61B17/320068—Surgical cutting instruments using mechanical vibrations, e.g. ultrasonic
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B06—GENERATING OR TRANSMITTING MECHANICAL VIBRATIONS IN GENERAL
- B06B—METHODS OR APPARATUS FOR GENERATING OR TRANSMITTING MECHANICAL VIBRATIONS OF INFRASONIC, SONIC, OR ULTRASONIC FREQUENCY, e.g. FOR PERFORMING MECHANICAL WORK IN GENERAL
- B06B1/00—Methods or apparatus for generating mechanical vibrations of infrasonic, sonic, or ultrasonic frequency
- B06B1/02—Methods or apparatus for generating mechanical vibrations of infrasonic, sonic, or ultrasonic frequency making use of electrical energy
- B06B1/06—Methods or apparatus for generating mechanical vibrations of infrasonic, sonic, or ultrasonic frequency making use of electrical energy operating with piezoelectric effect or with electrostriction
- B06B1/0607—Methods or apparatus for generating mechanical vibrations of infrasonic, sonic, or ultrasonic frequency making use of electrical energy operating with piezoelectric effect or with electrostriction using multiple elements
- B06B1/0611—Methods or apparatus for generating mechanical vibrations of infrasonic, sonic, or ultrasonic frequency making use of electrical energy operating with piezoelectric effect or with electrostriction using multiple elements in a pile
- B06B1/0618—Methods or apparatus for generating mechanical vibrations of infrasonic, sonic, or ultrasonic frequency making use of electrical energy operating with piezoelectric effect or with electrostriction using multiple elements in a pile of piezo- and non-piezoelectric elements, e.g. 'Tonpilz'
Definitions
- the present invention relates, in general, to apparatus and methods for manufacturing high power sandwich type ultrasonic transducers and, more particularly, to a new method of tuning high power sandwich type ultrasonic transducers.
- Ultrasonic instruments including both hollow core and solid core instruments, are used for the safe and effective treatment of many medical conditions.
- Ultrasonic instruments, and particularly solid core ultrasonic instruments are advantageous because they may be used to cut and/or coagulate organic tissue using energy in the form of mechanical vibrations transmitted to a surgical end-effector at ultrasonic frequencies.
- Ultrasonic vibrations when transmitted to organic tissue at suitable energy levels and using a suitable end-effector, may be used to cut, dissect, or cauterize tissue.
- Ultrasonic instruments utilizing solid core technology are particularly advantageous because of the amount of ultrasonic energy that may be transmitted from the ultrasonic transducer through the waveguide to the surgical end-effector.
- Such instruments are particularly suited for use in minimally invasive procedures, such as endoscopic or laparoscopic procedures, wherein the end-effector is passed through a trocar to reach the surgical site.
- Ultrasonic vibration is induced in the surgical end-effector by, for example, electrically exciting a transducer which may be constructed of one or more piezoelectric or magnetostrictive elements in the instrument handpiece. Vibrations generated by the transducer section are transmitted to the surgical end-effector via an ultrasonic waveguide extending from the transducer section to the surgical end-effector.
- Sandwich type ultrasonic transducers also called Langevin transducers, are well known and established for the production of high intensity ultrasonic motion. In United Kingdom Patent No. 145,691. issued in 1921, P.
- High-intensity ultrasonic transducers of the composite or sandwich type typically include front and rear mass members with alternating annular piezoelectric elements and electrodes stacked therebetween. Most such high-intensity transducers are of the pre- stressed type. They employ a compression bolt that extends axially through the stack to place a static bias of about one-half of the compressive force that the piezoelectric transducers can tolerate. When the transducers operate they are designed to always remain in compression, swinging from a minimum compression of nominally zero to a maximum peak of no greater than the maximum compressive strength of the material.
- Threaded studs are also known in the prior art for attaching and detaching transmission components to the transducer assembly. See, for example, US Patent Nos. 5,324,299 and 5,746,756. Such bolts and studs are utilized to maintain acoustic coupling between elements of the sandwich type transducer or any attached acoustic assembly. Coupling is important to maintain tuning of the assembly, allowing the assembly to be driven in resonance.
- Sandwich type transducers are relatively high Q devices, and during operation are driven at resonance, and maintained within a relatively narrow frequency range by feedback control methods known in the art. See, for example. US Patents No. 5,630,420 and 5.026,387 which describe systems incorporating and controlling sandwich type transducers.
- the invention is a method along with the attendant apparatus for manufacturing high power sandwich type ultrasonic transducers and, more particularly, a new method of tuning high power sandwich type ultrasonic transducers without the need for a trimming process.
- a method in accordance with the present invention includes the steps of assembling a sandwich type ultrasonic transducer, measuring the resonant frequency of the ultrasonic transducer, and selecting from a plurality of tuning elements, whereby a specific tuning element alters the measured resonant frequency of the ultrasonic transducer to a desired resonant frequency after assembly with the ultrasonic transducer.
- the tuning element is a connecting stud that is also used to connect an ultrasonic acoustic assembly to an end-effector.
- FIGURE 1 illustrates a perspective view of an ultrasonic signal generator with a sectioned plan view of a sandwich type ultrasonic transducer and housing in accordance with the present invention
- FIGURE 2 illustrates an exploded perspective view of a sandwich type ultrasonic transducer and housing in accordance with the present invention:
- FIGURE 3 illustrates a sectioned plan view of the distal-end of an acoustic assembly along with a plurality of attachment studs of differing lengths in accordance with the present invention:
- FIGURE 4 is a flow chart of an embodiment of an ultrasonic transducer assembly or tuning method in accordance with the present invention:
- FIGURE 5 is a flow chart of an embodiment of an ultrasonic transducer assembly or tuning method in accordance with the present invention
- FIGURE 6 is a perspective view of an alternate embodiment of a tuning stud in accordance with the present invention.
- FIG. 1 illustrates a perspective view of an ultrasonic signal generator 15 with a sectioned plan view of a sandwich type ultrasonic transducer S2 and housing 20 in accordance with the present invention.
- the transducer 82 which is known as a -5-
- Langevin stack generally includes a transduction portion 90. a first resonator or end- bell 92, and a second resonator or fore-bell 94.
- the transducer 82 is preferably an integral number of one-half system wavelengths (n ⁇ /2) in length as will be described in more detail later.
- An acoustic assembly 80 includes the transducer 82, mount 36, velocity transformer 64 and distal-end 95.
- the distal end of end-bell 92 is connected to the proximal end of transduction section 90, and the proximal end of fore-bell 94 is connected to the distal end of transduction portion 90.
- the first and second resonators 92 and 94 are preferably fabricated from titanium, aluminum, stainless steel, or any other suitable material.
- Fore- bell 94 and end-bell 92 have a length determined by a number of variables, including the thickness of the transduction section 90, the density and modulus of elasticity of material used end-bell 92 and fore-bell 94, and the resonant frequency of the transducer 82.
- the fore-bell 94 may be tapered inwardly from its proximal end to its distal end to amplify the ultrasonic vibration amplitude as velocity transformer 64, or alternately may have no amplification.
- the transduction portion 90 of the transducer 82 preferably comprises a piezoelectric section of alternating positive electrodes 96 and negative electrodes 98 (see Figure 2), with piezoelectric elements 100 alternating between the electrodes 96 and 98.
- the piezoelectric elements 100 may be fabricated from any suitable material, such as, for example, lead zirconate-titanate. lead meta-niobate, lead titanate, or other piezoelectric crystal material.
- Each of the positive electrodes 96, negative electrodes 98, and piezoelectric elements 100 have a bore extending through the center.
- the positive and negative electrodes 96 and 98 are electrically coupled to wires 102 and 104, respectfully. Wires 102 and 104 are encased within cable 25 and electrically connectable to generator 15 of ultrasonic system 10.
- the transducer 82 of the acoustic assembly 80 converts the electrical signal from generator 15 into mechanical energy that results in longitudinal vibratory motion of the ultrasonic transducer 82 and any attached end-effector at ultrasonic frequencies.
- a vibratory motion standing wave is generated through the acoustic assembly 80.
- the amplitude of the vibratory motion at any point along the acoustic assembly 80 depends on the location along the acoustic assembly 80 at which the vibratory motion is measured.
- a minimum or zero crossing in the vibratory motion standing wave is generally referred to as a node (i.e. , where motion is usually minimal), and an absolute value maximum or peak in the standing wave is generally referred to as an anti-node.
- the distance between an anti- node and its nearest node is one-quarter wavelength ( ⁇ 14).
- FIG. 2 illustrates an exploded perspective view of a handpiece assembly 70 including the ultrasonic transducer 82 and housing 20 in accordance with the present invention.
- Handpiece assembly 70 includes cable 25, housing 20, acoustic assembly 80, and a selected stud 50.
- Housing 20 includes proximal portion 22, distal portion 24, nose-cone 34, and O-rings 21. 23. and 32.
- Acoustic assembly 80 includes transducer 82 described above, and ancillar. components including acoustic isolator 26, electrode assembly 30, bolt 106, positi ⁇ e electrodes 96, negative electrodes 98, and insulator 28.
- wires 102 and 104 transmit the electrical signal from the generator 15 to electrodes 96 and 98.
- the piezoelectric elements 100 are energized by an electrical signal supplied from the generator 15 in response to a foot switch 118 to produce an acoustic standing wave in the acoustic assembly 80.
- the electrical signal causes disturbances in the piezoelectric elements 100 in the form of repeated small displacements resulting in large compression forces within the material.
- the repeated small displacements cause the piezoelectric elements 100 to expand and contract in a continuous manner along the axis of the voltage gradient, producing longitudinal waves of ultrasonic energy.
- the ultrasonic energy is transmitted through the acoustic assembly 80 to the end-effector.
- the piezoelectric elements 100 are conventionally held in compression between end-bell 92 and fore-bell 94 by a bolt 106.
- the bolt 106 preferably has a head, a shank, and a threaded distal end.
- the bolt 106 is inserted from the proximal end of end-bell 92 through the bores of end-bell 92. the electrodes 96 and 98, and piezoelectric elements 100.
- the threaded distal end of the bolt 106 is screwed into a threaded bore in the proximal end of fore-bell 94.
- the distal end of the transducer 82 may be acoustically coupled to the proximal end of an ultrasonic end-effector by a threaded connection such as stud 50.
- the components of the acoustic assembly 80 are preferably acoustically tuned such that the length of any assembly is an integral number of one-half wavelengths (n ⁇ 12), where the wavelength ⁇ is the wavelength of a pre-selected or operating longitudinal vibration drive frequency f d of the acoustic assembly 80. and where n is any positive integer. It is also contemplated that the acoustic assembly 80 may incorporate any suitable arrangement of acoustic elements.
- Figure 3 illustrates a sectioned plan view of the distal-end 95 of acoustic assembly 80 along with the plurality of attachment studs 50 of differing lengths in accordance with the present invention.
- Distal-end 95 includes bore 110, threaded portion 111, and terminal face 112. Studs 50 may be so ⁇ ed by size or mass such as, for example, PI through P5 as described below in Table 1.
- acoustic assembly 80 may be designed to have an acoustic length (n ⁇ .2). "Stack-up" resonant frequency discrepancies of acoustic assembly 80 may be corrected by proper selection of a tuning element such as, for example, stud 50. when the relationship between stud size or mass and the frequency effect on acoustic assembly 80 of insertion of stud 50 into threaded portion 111 of bore 110 is understood.
- tuning elements may be utilized to correct for resonant frequency variations, such as, for example, selection from a plurality of fore-bells 94, end bells 92, or other ancillary components, each of which having varying masses.
- Table 1 is provided as an example of frequency ranges and stud 50 lengths for an embodiment of the present invention.
- a measured transducer S2 frequency is shown in the first row, along with a frequency deviation range correctable by the stud 50 disclosed in each column.
- a transducer 82 may be designed to have a resonant frequency of 55,540 Hertz, corresponding to the column containing P Level (P3). If the measured resonant frequency during assembly is within +/- 60 Hertz of 55,540 Hertz, then a 0.445 inch smd may be inserted to keep transducer 82 within its design limits for frequency. As the measured resonant frequency of transducer 82 deviates above or below the designed frequency, an appropriare stud 50 length may be selected from Table 1 to compensate for the deviation and bring transducer 82 within the desired resonant frequency range.
- FIG 4 is a flow chart of an embodiment of ultrasonic transducer 82 assembly or tuning method in accordance with the present invention.
- Acoustic assembly 80 may be designed to have a resonant frequency f d , and an effective acoustic length of (n ⁇ 12). However, tolerance "stack-up " variations in material properties of components, or other aspects of the assembly may cause acoustic assembly 80 to deviate from its designed resonant frequency as shown above in Table 1.
- ultrasonic transducer 82 or the entire acoustic assembly 80 may be measured for resonant frequency. Deviations from the desired resonant frequency may be corrected by proper selection and insertion of a tuning stud 50.
- the flow chart of Figure 4 includes the steps of:
- studs 50 of equal size but varying densities may be used.
- studs PI through P3 may be of equal length, but stud PI may be manufactured from Aluminum, stud P2 may be manufactured from stainless steel, and stud P3 may be manufactured from Tungsten.
- the assembly or tuning process may select from one of the three studs of different densities to compensate for differences in resonant frequency.
- a further embodiment of the present invention may be appreciated when considering a simple resonator model.
- the ability of a mass located around an anti-node of vibration to alter resonant frequency may be envisioned as analogous to a mass hanging at the end of a spring. If the mass is displaced and released, the mass spring system will vibrate at a resonant frequency. If the mass is increased, the resonant frequency will decrease. If the mass is decreased, the resonant frequency will increase.
- the overall resonant frequency of acoustic assembly 80 may be decreased from a measured resonant frequency to a desired resonant frequency within a range useable to correct for manufacturing variations. Likewise as the mass selected is decreased, the resonant frequency would be increased.
- the ability of an added mass to alter the frequency of an acoustic assembly 80 changes as the mass deviates from an anti-node of acoustic vibration. If a mass is added at a node of vibration its effect on the resonant frequency is due primarily to any stiffness it adds near the node. In the spring / mass analogy, the added mass at a node is analogous to increasing the spring rate. Alternately, if that same mass is located at an anti-node of vibration, its effect on the resonant frequency is due to the increased mass in the mass / spring analogy.
- studs PI through P5 have centers of mass Cl through C5 respectively. If stud 50 is inserted into threaded portion 111 of bore 110 such that smd 50 extends from terminal face 112 at a consistent length regardless of which smd PI through P5 is selected, then the location of the center of mass of stud 50 within distal-end 95 will vary as the length of smd 50 varies, as illustrated in Figure 3.
- FIG. 5 is a flow chart of an embodiment of an ultrasonic transducer assembly or tuning method in accordance with the present invention.
- the flow chart of Figure 5 includes the steps of selecting at least one piezoelectric element, wherein the piezoelectric element includes a central opening, designated as process 121: selecting an end-bell, wherein the end-bell includes a central opening, designated as process 120; selecting a fore-bell, the fore-bell including: a proximal surface; a distal surface; and a body separating the proximal surface and the distal surface; wherein the proximal surface includes a first threaded bore, and wherein the distal surface includes a second threaded bore, designated as process 1 19: selecting ancillary pieces, designated as process 123; assembling a transducer sandwich, designated as process 124: measuring the resonant frequency, designated as process 125; determining the appropriate range, designated as decisions 126 through 130; selecting from a plurality of studs according to the measured frequency range
- FIG. 6 is a perspective view of an alternate embodiment of a tuning stud 120 in accordance with the present invention.
- Tuning smd 120 comprises a proximal threaded portion 122, a central non-threaded portion 126, and a distal threaded portion 124.
- Central non-threaded portion 126 may be altered in length or diameter to vary the amount of resonant frequency shift desired when tuning smd 120 is inserted into threaded portion 111 of bore 1 10 illustrated in Figure 3.
- Central non-threaded portion 126 may also comprise materials of differing density, thereby altering the mass of tuning s d 120. It can be appreciated that central non-threaded portion 126 may also be a washer placed onto smd 50 to perform as tuning smd 120.
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- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Surgery (AREA)
- Mechanical Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Molecular Biology (AREA)
- General Health & Medical Sciences (AREA)
- Biomedical Technology (AREA)
- Heart & Thoracic Surgery (AREA)
- Medical Informatics (AREA)
- Dentistry (AREA)
- Animal Behavior & Ethology (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Apparatuses For Generation Of Mechanical Vibrations (AREA)
- Transducers For Ultrasonic Waves (AREA)
- Control Of Motors That Do Not Use Commutators (AREA)
- Investigating Or Analyzing Materials By The Use Of Ultrasonic Waves (AREA)
- Fuel-Injection Apparatus (AREA)
Abstract
Description
Claims
Priority Applications (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CA002370128A CA2370128C (en) | 1999-04-15 | 2000-03-07 | Apparatus and method for tuning ultrasonic transducers |
JP2000611827A JP2002542690A (en) | 1999-04-15 | 2000-03-07 | Apparatus and method for tuning an ultrasonic transducer |
DE60040788T DE60040788D1 (en) | 1999-04-15 | 2000-03-07 | METHOD FOR TUNING ULTRASOUND TRANSFORMERS |
AU36191/00A AU773135B2 (en) | 1999-04-15 | 2000-03-07 | Apparatus and method for tuning ultrasonic transducers |
EP00914856A EP1173100B1 (en) | 1999-04-15 | 2000-03-07 | Method for tuning ultrasonic transducers |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US29244199A | 1999-04-15 | 1999-04-15 | |
US09/292,441 | 1999-04-15 |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2000062688A1 true WO2000062688A1 (en) | 2000-10-26 |
Family
ID=23124692
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/US2000/005963 WO2000062678A1 (en) | 1999-04-15 | 2000-03-07 | Ultrasonic transducer with improved compressive loading |
PCT/US2000/005964 WO2000062688A1 (en) | 1999-04-15 | 2000-03-07 | Apparatus and method for tuning ultrasonic transducers |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/US2000/005963 WO2000062678A1 (en) | 1999-04-15 | 2000-03-07 | Ultrasonic transducer with improved compressive loading |
Country Status (7)
Country | Link |
---|---|
US (1) | US6491708B2 (en) |
EP (2) | EP1173100B1 (en) |
JP (2) | JP4545323B2 (en) |
AU (2) | AU773135B2 (en) |
CA (2) | CA2370076C (en) |
DE (2) | DE60043192D1 (en) |
WO (2) | WO2000062678A1 (en) |
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ES2339626A1 (en) * | 2007-11-06 | 2010-05-21 | Zunibal, S.L. | Perfected ultrasonic transducer. (Machine-translation by Google Translate, not legally binding) |
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Also Published As
Publication number | Publication date |
---|---|
CA2370128A1 (en) | 2000-10-26 |
AU3619100A (en) | 2000-11-02 |
DE60040788D1 (en) | 2008-12-24 |
JP2002542690A (en) | 2002-12-10 |
EP1182971B1 (en) | 2009-10-21 |
CA2370076A1 (en) | 2000-10-26 |
WO2000062678A1 (en) | 2000-10-26 |
EP1182971A4 (en) | 2005-04-27 |
EP1173100A4 (en) | 2005-04-27 |
AU773135B2 (en) | 2004-05-20 |
AU4449200A (en) | 2000-11-02 |
EP1173100B1 (en) | 2008-11-12 |
EP1182971A1 (en) | 2002-03-06 |
JP4545323B2 (en) | 2010-09-15 |
DE60043192D1 (en) | 2009-12-03 |
US6491708B2 (en) | 2002-12-10 |
JP2002542005A (en) | 2002-12-10 |
AU774545B2 (en) | 2004-07-01 |
EP1173100A1 (en) | 2002-01-23 |
CA2370128C (en) | 2008-05-13 |
CA2370076C (en) | 2007-11-13 |
US20010001123A1 (en) | 2001-05-10 |
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