WO2000007194A8 - Preparation of tungsten bronzes for nuclear waste storage forms and electronic materials - Google Patents

Preparation of tungsten bronzes for nuclear waste storage forms and electronic materials

Info

Publication number
WO2000007194A8
WO2000007194A8 PCT/US1999/016869 US9916869W WO0007194A8 WO 2000007194 A8 WO2000007194 A8 WO 2000007194A8 US 9916869 W US9916869 W US 9916869W WO 0007194 A8 WO0007194 A8 WO 0007194A8
Authority
WO
WIPO (PCT)
Prior art keywords
preparation
electronic materials
waste storage
temperature
nuclear waste
Prior art date
Application number
PCT/US1999/016869
Other languages
French (fr)
Other versions
WO2000007194A9 (en
WO2000007194A1 (en
Inventor
Michael T Pope
Knut Wasserman
Original Assignee
Univ Georgetown
Michael T Pope
Knut Wasserman
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Univ Georgetown, Michael T Pope, Knut Wasserman filed Critical Univ Georgetown
Publication of WO2000007194A1 publication Critical patent/WO2000007194A1/en
Publication of WO2000007194A8 publication Critical patent/WO2000007194A8/en
Publication of WO2000007194A9 publication Critical patent/WO2000007194A9/en

Links

Classifications

    • GPHYSICS
    • G21NUCLEAR PHYSICS; NUCLEAR ENGINEERING
    • G21FPROTECTION AGAINST X-RADIATION, GAMMA RADIATION, CORPUSCULAR RADIATION OR PARTICLE BOMBARDMENT; TREATING RADIOACTIVELY CONTAMINATED MATERIAL; DECONTAMINATION ARRANGEMENTS THEREFOR
    • G21F9/00Treating radioactively contaminated material; Decontamination arrangements therefor
    • G21F9/28Treating solids
    • G21F9/30Processing
    • G21F9/301Processing by fixation in stable solid media
    • G21F9/302Processing by fixation in stable solid media in an inorganic matrix
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G41/00Compounds of tungsten
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G41/00Compounds of tungsten
    • C01G41/006Compounds containing, besides tungsten, two or more other elements, with the exception of oxygen or hydrogen
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G43/00Compounds of uranium
    • C01G43/006Compounds containing, besides uranium, two or more other elements, with the exception of oxygen or hydrogen
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/70Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/70Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/77Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by unit-cell parameters, atom positions or structure diagrams
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/80Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/86Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by NMR- or ESR-data
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/80Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/88Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by thermal analysis data, e.g. TGA, DTA, DSC
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/10Particle morphology extending in one dimension, e.g. needle-like
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/20Particle morphology extending in two dimensions, e.g. plate-like
    • C01P2004/22Particle morphology extending in two dimensions, e.g. plate-like with a polygonal circumferential shape
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/60Optical properties, e.g. expressed in CIELAB-values
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/80Compositional purity

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Engineering & Computer Science (AREA)
  • General Engineering & Computer Science (AREA)
  • High Energy & Nuclear Physics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Processing Of Solid Wastes (AREA)

Abstract

A process for preparing a lanthanide or actinide-containing tungsten bronze including: (a) heating a solid composition containing a lanthanide or actinide-containing polyoxotungstate in the presence of a reducing agent until the temperature of said solid composition reaches a first predetermined temperature to form a reduced composition; (b) heating said reduced composition in the presence of an inert gas until the temperature of said reduced composition reaches a second predetermined temperature; and (c) maintaining said reduced composition at said second temperature for a predetermined period of time.
PCT/US1999/016869 1998-07-27 1999-07-27 Preparation of tungsten bronzes for nuclear waste storage forms and electronic materials WO2000007194A1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US9423398P 1998-07-27 1998-07-27
US60/094,233 1998-07-27

Publications (3)

Publication Number Publication Date
WO2000007194A1 WO2000007194A1 (en) 2000-02-10
WO2000007194A8 true WO2000007194A8 (en) 2000-07-20
WO2000007194A9 WO2000007194A9 (en) 2000-08-24

Family

ID=22243923

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US1999/016869 WO2000007194A1 (en) 1998-07-27 1999-07-27 Preparation of tungsten bronzes for nuclear waste storage forms and electronic materials

Country Status (1)

Country Link
WO (1) WO2000007194A1 (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102006039341B4 (en) 2006-08-22 2009-11-26 Werner Schmidt Power system
CN109803941B (en) * 2016-10-17 2022-01-11 昭荣化学工业株式会社 Dielectric ceramic composition and ceramic electronic component
CN107256726B (en) * 2017-07-03 2019-04-30 中国工程物理研究院材料研究所 A kind of preparation method of metal reinforced uranium dioxide fuel ball

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4032417A (en) * 1974-09-03 1977-06-28 Hooker Chemicals & Plastics Corporation Electrolytic processes
US4339424A (en) * 1981-03-20 1982-07-13 Exxon Research & Engineering Co. Method of preparing W or Mo metal oxides
US4634502A (en) * 1984-11-02 1987-01-06 The Standard Oil Company Process for the reductive deposition of polyoxometallates
GB8906189D0 (en) * 1989-03-17 1989-05-04 Johnson Matthey Plc Improvements in chemical compounds
US5364568A (en) * 1992-07-08 1994-11-15 Georgetown University Compounds and methods for separation and molecular encapsulation of metal ions

Also Published As

Publication number Publication date
WO2000007194A9 (en) 2000-08-24
WO2000007194A1 (en) 2000-02-10

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