WO1999063146A1 - Improved method of dyeing hydrophobic textile fibers with colorant material in supercritical fluid carbon dioxide - Google Patents

Improved method of dyeing hydrophobic textile fibers with colorant material in supercritical fluid carbon dioxide Download PDF

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Publication number
WO1999063146A1
WO1999063146A1 PCT/US1999/010172 US9910172W WO9963146A1 WO 1999063146 A1 WO1999063146 A1 WO 1999063146A1 US 9910172 W US9910172 W US 9910172W WO 9963146 A1 WO9963146 A1 WO 9963146A1
Authority
WO
WIPO (PCT)
Prior art keywords
temperature
scf
dyeing
colorant material
density
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/US1999/010172
Other languages
English (en)
French (fr)
Inventor
Carl Brent Smith
Gerardo A. Montero
Walter A. Hendrix
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
North Carolina State University
Original Assignee
North Carolina State University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by North Carolina State University filed Critical North Carolina State University
Priority to EP99922889A priority Critical patent/EP1210477A1/en
Priority to JP2000552334A priority patent/JP2002517619A/ja
Priority to KR1020007013657A priority patent/KR20010052517A/ko
Priority to AU39784/99A priority patent/AU3978499A/en
Publication of WO1999063146A1 publication Critical patent/WO1999063146A1/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/94—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dyes dissolved in solvents which are in the supercritical state
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B19/00—Treatment of textile materials by liquids, gases or vapours, not provided for in groups D06B1/00 - D06B17/00
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B23/00—Component parts, details, or accessories of apparatus or machines, specially adapted for the treating of textile materials, not restricted to a particular kind of apparatus, provided for in groups D06B1/00 - D06B21/00
    • D06B23/20—Arrangements of apparatus for treating processing-liquids, -gases or -vapours, e.g. purification, filtration or distillation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S8/00—Bleaching and dyeing; fluid treatment and chemical modification of textiles and fibers
    • Y10S8/92—Synthetic fiber dyeing
    • Y10S8/922—Polyester fiber

Definitions

  • Figure 6 is a graph which shows an exemplary temperature control profile for a dyeing run.
  • T dy ⁇ ng (°C) Temperature in higher temperature range at which dyeing is initiated.
  • t Time elapsed during dyeing process.
  • liquid C0 2 leaving mixer 38 enters electrical pre-heater 40 where its temperature is increased. Heated and pressurized C0 2 may enter the dyeing subsystem B through needle valve 66 and into dye-add vessel 70; through needle valve 64 and into dyeing vessel 106; orthrough both of these paths. Typically, dyeing subsystem B is filled and pressurized simultaneously through both the dye-add and dyeing vessels 70 and 106, respectively.
  • the complete dyeing cycle achieves a dye uptake of about 99%, and takes the heat-up time plus 30 minutes (running at 130°C) with reverse flows, 2 (I) times 2.5 (O), at 1 to 6 gpm per lb of yam.
  • a lower rate of temperature rise (start from about 40 °C to about 130 °C) favors more even uptake of dye before sorption equilibrium is set up.
  • the dyeing cycle time increases as compared to the embodiment presented above, which also benefits levelness.

Landscapes

  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Coloring (AREA)
PCT/US1999/010172 1998-06-03 1999-05-10 Improved method of dyeing hydrophobic textile fibers with colorant material in supercritical fluid carbon dioxide Ceased WO1999063146A1 (en)

Priority Applications (4)

Application Number Priority Date Filing Date Title
EP99922889A EP1210477A1 (en) 1998-06-03 1999-05-10 Improved method of dyeing hydrophobic textile fibers with colorant material in supercritical fluid carbon dioxide
JP2000552334A JP2002517619A (ja) 1998-06-03 1999-05-10 超臨界流体二酸化炭素中での染料物質による疎水性繊維の改良された染色方法
KR1020007013657A KR20010052517A (ko) 1998-06-03 1999-05-10 초임계 유체 이산화탄소내에 착색제로 소수성 직물 섬유를염색시키는 향상된 방법
AU39784/99A AU3978499A (en) 1998-06-03 1999-05-10 Improved method of dyeing hydrophobic textile fibers with colorant material in supercritical fluid carbon dioxide

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US8963998A 1998-06-03 1998-06-03
US09/089,639 1998-09-29
US09/162,817 US6048369A (en) 1998-06-03 1998-09-29 Method of dyeing hydrophobic textile fibers with colorant materials in supercritical fluid carbon dioxide
US09/162,817 1998-09-29

Publications (1)

Publication Number Publication Date
WO1999063146A1 true WO1999063146A1 (en) 1999-12-09

Family

ID=26780794

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US1999/010172 Ceased WO1999063146A1 (en) 1998-06-03 1999-05-10 Improved method of dyeing hydrophobic textile fibers with colorant material in supercritical fluid carbon dioxide

Country Status (7)

Country Link
US (1) US6048369A (https=)
EP (1) EP1210477A1 (https=)
JP (1) JP2002517619A (https=)
KR (1) KR20010052517A (https=)
CN (1) CN1309735A (https=)
AU (1) AU3978499A (https=)
WO (1) WO1999063146A1 (https=)

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6261326B1 (en) 2000-01-13 2001-07-17 North Carolina State University Method for introducing dyes and other chemicals into a textile treatment system
JP2001316988A (ja) * 2000-02-16 2001-11-16 Stork Brabant Bv 超臨界流体中において繊維材料を染色する方法
US6676710B2 (en) 2000-10-18 2004-01-13 North Carolina State University Process for treating textile substrates
US20160244911A1 (en) * 2015-02-20 2016-08-25 Nike, Inc. Supercritical fluid material finishing
CN106757918A (zh) * 2016-11-21 2017-05-31 大连工业大学 一种可换色工程化超临界二氧化碳流体无水染整系统及其方法
CN107419462A (zh) * 2017-08-08 2017-12-01 百事基材料（青岛）股份有限公司 一种超临界二氧化碳染色系统及染色工艺
US10519594B2 (en) 2015-02-20 2019-12-31 Nike, Inc. Supercritical fluid material scouring
US10731291B2 (en) 2015-02-20 2020-08-04 Nike, Inc. Supercritical fluid rolled or spooled material finishing
TWI741210B (zh) * 2018-08-31 2021-10-01 流亞科技股份有限公司 以染色殘液為控制要素的染色機控制系統

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US6517589B1 (en) * 2000-11-14 2003-02-11 China Textile Institute Manufacturing method of coloring and lustering substance
US7771818B2 (en) * 2002-09-20 2010-08-10 Bha Group, Inc. Treatment of porous article
US7407703B2 (en) * 2002-09-20 2008-08-05 Bha Group, Inc. Composite membrane having oleophobic properties
US7794742B2 (en) * 2005-02-08 2010-09-14 University Of Washington Devices for promoting epithelial cell differentiation and keratinization
US20070044817A1 (en) * 2005-08-30 2007-03-01 San-Lung Chen Wafer protection system employed in chemical stations
KR101487534B1 (ko) * 2008-09-12 2015-01-28 엘지전자 주식회사 세탁물 처리기기
WO2012018351A1 (en) * 2010-08-06 2012-02-09 Empire Technology Development Llc Supercritical noble gases and coloring methods
WO2012081745A1 (ko) 2010-12-16 2012-06-21 볼보 컨스트럭션 이큅먼트 에이비 굴삭기의 엔진 공회전 제어 장치 및 그 방법
CN102535068B (zh) * 2012-02-24 2013-12-04 广东出色无水印染科技有限公司 染色小样机及其染色方法
CN102877329A (zh) * 2012-08-29 2013-01-16 昆山铁牛衬衫厂 一种超临界二氧化碳染色方法
CN103726351B (zh) * 2013-12-30 2016-01-20 成都纺织高等专科学校 一种超临界co2流体还原染料染色方法
CN103741523B (zh) * 2013-12-30 2016-04-20 成都纺织高等专科学校 一种超临界co2流体分散染料增溶染色方法
CN103806234B (zh) * 2014-02-25 2015-11-18 中国科学院福建物质结构研究所 超临界co2无水旋转经轴卧式染色釜及其染色系统
CN103866515B (zh) * 2014-03-27 2015-09-30 山东大学 一种超临界流体喷染用喷射器
CN103981661B (zh) * 2014-06-04 2016-01-20 山东大学 一种超临界流体喷染用喷射器
CN104195854A (zh) * 2014-09-11 2014-12-10 马燕 一种零排放的染整工艺
CN106245385B (zh) * 2016-08-22 2018-06-08 闽江学院 一种光致发光纤维的染色方法
US11015289B2 (en) * 2016-10-27 2021-05-25 Swapneshu Ashok Baser Process for dyeing of textile materials using supercritical fluid
CN106757915B (zh) * 2016-12-02 2019-03-26 青岛即发集团股份有限公司 一种筒纱无水染色设备、染色方法及产品
US10550513B2 (en) 2017-06-22 2020-02-04 Hbi Branded Apparel Enterprises, Llc Fabric treatment compositions and methods
KR102002836B1 (ko) 2018-08-14 2019-07-24 아크로마코리아 주식회사 초임계 이산화탄소 염색을 위한 염료 조성물
KR102105582B1 (ko) 2019-05-08 2020-04-28 아크로마코리아 주식회사 이산화탄소 초임계 하에서 폴리아미드 섬유의 흑색 염색을 위한 분산염료 조성물
TWI811654B (zh) * 2021-03-31 2023-08-11 財團法人紡織產業綜合研究所 紡織品的雙面均染方法及使用其製造而成的多彩紗線
CN114606692B (zh) * 2022-03-25 2022-12-06 东华大学 提高超临界二氧化碳流体中染化料的溶解度和溶解速率的方法
CN114592365B (zh) * 2022-03-25 2023-04-07 青岛即发集团股份有限公司 一种分散染料上染率高的超临界二氧化碳流体染色方法
CN115182161A (zh) * 2022-07-08 2022-10-14 浙江英玛特生物科技有限公司 采用scf技术将羟基酸酯低聚物固着在纤维表面的方法及抗菌抗病毒产品
CN117779497B (zh) * 2023-12-27 2025-09-23 清源创新实验室 一种聚苯砜亚砜纤维的无水染色方法

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Cited By (16)

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US6261326B1 (en) 2000-01-13 2001-07-17 North Carolina State University Method for introducing dyes and other chemicals into a textile treatment system
US6615620B2 (en) 2000-01-13 2003-09-09 North Carolina State University Method for introducing dyes and other chemicals into a textile treatment system
JP2001316988A (ja) * 2000-02-16 2001-11-16 Stork Brabant Bv 超臨界流体中において繊維材料を染色する方法
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JP2002517619A (ja) 2002-06-18
US6048369A (en) 2000-04-11
AU3978499A (en) 1999-12-20

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