WO1998050219A1 - Method and apparatus for producing stretch wrap plastic film - Google Patents
Method and apparatus for producing stretch wrap plastic film Download PDFInfo
- Publication number
- WO1998050219A1 WO1998050219A1 PCT/AU1998/000314 AU9800314W WO9850219A1 WO 1998050219 A1 WO1998050219 A1 WO 1998050219A1 AU 9800314 W AU9800314 W AU 9800314W WO 9850219 A1 WO9850219 A1 WO 9850219A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- film
- elastic deformation
- stretched
- stretching
- stretch
- Prior art date
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C55/00—Shaping by stretching, e.g. drawing through a die; Apparatus therefor
- B29C55/02—Shaping by stretching, e.g. drawing through a die; Apparatus therefor of plates or sheets
- B29C55/04—Shaping by stretching, e.g. drawing through a die; Apparatus therefor of plates or sheets uniaxial, e.g. oblique
- B29C55/06—Shaping by stretching, e.g. drawing through a die; Apparatus therefor of plates or sheets uniaxial, e.g. oblique parallel with the direction of feed
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/03—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor characterised by the shape of the extruded material at extrusion
- B29C48/09—Articles with cross-sections having partially or fully enclosed cavities, e.g. pipes or channels
- B29C48/10—Articles with cross-sections having partially or fully enclosed cavities, e.g. pipes or channels flexible, e.g. blown foils
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01F—PROCESSING OF HARVESTED PRODUCE; HAY OR STRAW PRESSES; DEVICES FOR STORING AGRICULTURAL OR HORTICULTURAL PRODUCE
- A01F15/00—Baling presses for straw, hay or the like
- A01F15/07—Rotobalers, i.e. machines for forming cylindrical bales by winding and pressing
- A01F15/071—Wrapping devices
- A01F2015/0745—Special features of the wrapping material for wrapping the bale
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
Definitions
- the present invention relates to a method and process for producing stretch wrap plastic film and in particular, the storage of such plastic film which has undergone stretching prior to storage on a roll.
- German laid open specification P3409117 there is disclosed a process for wrapping packaged goods in a web shaped stretch film wherein the film is provided in an already stretched state rolled up under tension; with the stretching taking place during the actual manufacture or as an intermediate step after processing of the film.
- the film in any film that has been stretched before storage, it is possible to store the film in its tensioned stretch state without allowing it to relax.
- the film it is possible for the film to do work so that the retained tension in the film will act on a load or package with the film relaxing to a steady state when wrapped around a load or package.
- the relatively high stored tension in the roll may cause the core of the roll to collapse.
- 55564/94 there is disclosed the provision of a roll of stretched plastics material film which has an embossed surface for trapping air so as to facilitate unwinding of the roll of stretched film for wrapping pallet loads.
- the film is totally relaxed prior to winding on to the storage roll.
- the present invention seeks to minimise the perceived disadvantages of the known prior art and has as its primary objective the provision of a method and apparatus for making stretched film product wherein the film is pre-stretched to provide a predetermined significant amount of memory, i.e. elastic deformation or recoverable strain in the film as distinct from non-recoverable plastic deformation of the film.
- the stretching of the film is carried out at the point of manufacture of the film in an extrusion machine so that the film is stored for later use in a stretched condition or at least partially stretched condition.
- the stretching and prior to storage it is necessary to trim the edges of the film to remove distortion at the marginal edge portions of the film which tend to form thickened areas compared with the main body of the stretched film web.
- the amount of recoverable strain retained in the film falls within the range of about 20% to a maximum of about 80% of the total memory in the film.
- the lower limit represents the minimum amount of useable stretch being retained for effective wrapping of a load and the upper limit represents the maximum amount of stretch that can be retained and yet avoiding damage to supporting cores and telescoping of the film during storage.
- the film is produced as a tube in an extruder of known construction and procedure and after cooling is stretched prior to cutting the tube to form webs of predetermined width and at predetermined retained memory in the stretch procedure which can then be stored for later re-use.
- the present invention also anticipates providing a stretch plastics material film made by any of the aforesaid methods.
- a method of making stretch film including the steps of stretching the film beyond its yield point to an elongation greater than 100%, removing opposed edge zones of the stretched film to produce a film having a substantially uniform thickness, allowing the film to partially relax to release part of the elastic deformation component in the film to retain between about 20% and 80% of the elastic deformation, and storing the partially relaxed film for future use in the partially relaxed state.
- a method of wrapping a load with plastics material film including providing plastics material film stretched beyond its yield point which in a stored state retains between 20% and 80% of the film's elastic deformation capability, and thereafter wrapping said film about said load.
- the load may be any product or material that requires wrapping but can include pallet wrapping, vegetation material during the production of silage, and bundle wrapping applications such as timber lengths, cans including drink cans and any other similar product. Wrapping of the load may be achieved by storing the plastics material on a roll capable of use in either a manually handled wrapping machine, or a powered wrapping machine of any conventional configuration. The advantage achieved is that the force required to establish a required elastic loading on the load to be wrapped is substantially reduced because of the retained elastic deformation levels in the plastics film.
- a method of dispensing a plastics material film including providing a plastics material film stretched beyond its yield point which in a stored state retains between 20% and 80% of the film's elastic deformation capability, and thereafter dispensing said film from the stored state.
- the plastics material film prior to being stored in said stored state is stretched beyond its yield point in the range of about 100% to 400% elongation.
- Figure 1 shows schematically a stretch film production machine using an extrusion method, and a means for modifying this conventional arrangement to achieve in-line stretching of the film;
- Figure 2 shows in side elevation details of apparatus for stretching plastics material film as may be used in this invention.
- Figure 3 shows schematically a non-in-line arrangement for stretching plastics material film in accordance with this invention.
- an extruder 1 operates in known manner to generate an inflated film "bubble" 1 which is drawn up from the extruder to a great height in a cooling phase and then passed through a primary nip formed by nip rollers 2 to collapse the "bubble" whence it is passed to a secondary nip formed by nip rollers 7 via a film trimming and/or splitting station 8 or alternatively, to a stretching station A-AA comprised of several stretching and, if desired, web width adjustment rollers.
- the extrusion line including the extruder 1 (a) operates in a substantially continuous manner as a blown film line where film is fed to the secondary nip rollers 7 running at approximately the same speed as the primary nip rollers 2.
- an inline stretching unit 1 1 is provided as shown at A-AA of Figure 1.
- the unit 1 1 may be interposed after the primary nip rollers 2 and before the secondary nip rollers 7 as shown.
- the stretch unit may be an optional add on feature of a conventional extrusion machine and the unit is suitable for dual operation with or without in-line stretch of the film.
- the film is threaded around the low speed stretching roll 3, the high speed stretching roll 4 and then back to the idler rolls 10 and thence to the secondary nip rollers 7.
- the idler nip rolls 6 in the stretch unit are adjustable to an open position 6(a) to allow easy threading of the film therethrough.
- the nip rolls 6 may be left in the open disengaged position 6(a) whilst the extruded "bubble" of film is established and correct film thickness of say 25 microns at a lay flat tube width of 1 ,900 mms is produced.
- the idler roll 6 can then be moved to the closed or engaged position with the low speed stretch roll 3 and the high speed stretch roll 4.
- a web width adjustment roller 5 may also be provided which is adjustable between various positions, for example as shown at 5(a). The adjustment is dependent upon the amount of "neck down” imparted to the film which in turn impacts directly upon the properties of the stretched film.
- a non-in-line stretching unit which may take a roll of plastics material stretch film 9 such as might be produced by a conventional extrusion line shown schematically in Figure 1 and at any time there after stretch same as illustrated schematically in Figure 3.
- the film is passed through a stretching unit 11 which may be similar to that shown in Figures 1 and 2.
- the unit 11 includes a low speed roller 3 and a high speed roller 4 with stretching of the film 9 beyond its yield point generally occurring between these two rollers.
- the secondary nip rollers 7 are driven at a speed similar to the high speed roller 4 with partial relaxation occurring between the rollers 7 and a wind-up roller 19 such that partial elastic deformation in the range of between 20% and 80% is retained in the film.
- a preferred aspect of this invention is to remove these thickened edge portions to provide a film web of substantially reduced and uniform thickness across its width.
- a cutting station 18 is provided to remove the edge regions of the stretched film. If it is desired to cut the film into a number of strands of different widths, this may also occur at the cutting station 18 or at a subsequent cutting station before the wind-up roller 19.
- the approximate speed of the film travel is 100 metres per minute producing a 25 micron film thickness at a lay flat tube width of 1 ,900 mm.
- the primary nip rollers 2 and the low and high speed stretch rollers 3, 4 initially are operated at the same speed of approximately 100 metres per minute. In this format, the tube is wound on the wind up rolls 9 after the edges are trimmed at edge trim station 8.
- the stretching operation can now be commenced with the low speed stretch roller 3 maintaining a similar speed as primary nip rollers 2 and the high speed stretch roller 4 and following secondary nip rollers 7 and the winding rollers 9 accelerating to the desired speed to achieve the predetermined amount of stretch and relaxation desired.
- pre-stretching the film to 200% elongation with approximately 50% of elastic deformation being left on the roll is achieved by accelerating the high speed roller 4 to 300 metres per minute with the film winding roller 9 being accelerated to a lesser extent of approximately 270 metres per minute.
- Total Deformation Plastic deformation and elastic deformation.
- Low speed stretch roller 3 100 metres / minute ⁇ 1 - 2%
- High speed stretch roller 4 300 metres / minute
- High speed stretch roller 4 245 metres / minute giving a 250% elongation
- partially relaxed film 1 metre to 3 metre stretch relaxed to 2.4 metres (totally relaxed) to stretch back to 3 metres requires a force of X plus Y which force is greater than force X.
- Production of partially relaxed film will impart greater versatility and breadth of application to various loads.
- Such a partially relaxed film may be wrapped around a desired product or load without further stretching at the point of wrapping and in which case the retained elastic capability can be used to provide the required retaining force for the load.
- a partially relaxed film in accordance with the present invention may be further stretched (or restretched) to attain the original level of stretching or in some cases even beyond the original level of stretching but this will require more force than that which would have been required during the original stretching process.
- the stretched film can be used in various non wrapping applications, for example police tape where tension in the film would be a clear advantage.
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Shaping By String And By Release Of Stress In Plastics And The Like (AREA)
- Laminated Bodies (AREA)
- Manufacture Of Macromolecular Shaped Articles (AREA)
- Basic Packing Technique (AREA)
- Wrappers (AREA)
- Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)
Abstract
Description
Claims
Priority Applications (10)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CA002288903A CA2288903C (en) | 1997-05-01 | 1998-05-01 | Method and apparatus for producing stretch wrap plastic film |
DE69824869T DE69824869T2 (en) | 1997-05-01 | 1998-05-01 | METHOD FOR PRODUCING EXPRESSIVE PACKAGING FOILS |
JP54753698A JP4435310B2 (en) | 1997-05-01 | 1998-05-01 | Method for producing stretched film, stretched film produced according to the method, and method for packaging luggage |
EP98916670A EP1015228B1 (en) | 1997-05-01 | 1998-05-01 | Method for producing stretch wrap plastic film |
AU70172/98A AU726288B2 (en) | 1997-05-01 | 1998-05-01 | Method and apparatus for producing stretch wrap plastic film |
US09/403,960 US6383430B1 (en) | 1997-05-01 | 1998-05-01 | Method for producing stretch wrap plastic film |
AT98916670T ATE270181T1 (en) | 1997-05-01 | 1998-05-01 | METHOD FOR PRODUCING STRETCHABLE PACKAGING FILM |
BRPI9809357-6A BR9809357B1 (en) | 1997-05-01 | 1998-05-01 | manufacturing process of stretch film and stretch film. |
NZ500876A NZ500876A (en) | 1997-05-01 | 1998-05-01 | Method and apparatus for producing stretch wrap plastic film |
NO995278A NO316613B1 (en) | 1997-05-01 | 1999-10-28 | Plastic stretch film and process for the production of plastic stretch film |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
AUPO6563A AUPO656397A0 (en) | 1997-05-01 | 1997-05-01 | Improvements relating to method and apparatus for producing stretch wrap plastic film |
AUPO6563 | 1997-05-01 |
Publications (1)
Publication Number | Publication Date |
---|---|
WO1998050219A1 true WO1998050219A1 (en) | 1998-11-12 |
Family
ID=3800855
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/AU1998/000314 WO1998050219A1 (en) | 1997-05-01 | 1998-05-01 | Method and apparatus for producing stretch wrap plastic film |
Country Status (15)
Country | Link |
---|---|
US (1) | US6383430B1 (en) |
EP (1) | EP1015228B1 (en) |
JP (1) | JP4435310B2 (en) |
CN (1) | CN1084663C (en) |
AT (1) | ATE270181T1 (en) |
AU (2) | AUPO656397A0 (en) |
BR (1) | BR9809357B1 (en) |
CA (1) | CA2288903C (en) |
DE (1) | DE69824869T2 (en) |
ES (1) | ES2224376T3 (en) |
ID (1) | ID22882A (en) |
NO (1) | NO316613B1 (en) |
NZ (1) | NZ500876A (en) |
RU (1) | RU2191694C2 (en) |
WO (1) | WO1998050219A1 (en) |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1999067080A1 (en) * | 1998-06-23 | 1999-12-29 | First Green Park Pty Ltd. | Orientation of films to improve barrier and uv stability |
EP1125718A2 (en) * | 2000-02-09 | 2001-08-22 | Itw Mima Films Llc | Stretch wrap film |
WO2007093280A1 (en) * | 2006-02-15 | 2007-08-23 | Kverneland Asa | Wrapping of agricultural bales of rectangular cross section |
EP2164770B1 (en) | 2007-06-21 | 2016-03-30 | Combipac BV | Prestretched film |
US9358760B2 (en) | 2007-09-28 | 2016-06-07 | Combipac Bv | Prestretched agricultural stretch wrap film |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US9676507B2 (en) * | 2008-07-23 | 2017-06-13 | Best Packaging, Inc. | Stretch wrapping system and process |
EP2335906A1 (en) | 2009-12-21 | 2011-06-22 | Trioplast AB | Prestretched film |
AU2013395445B2 (en) | 2013-07-26 | 2018-11-08 | Tama group | Wrapping web assembly and wrapping method |
AU2014308544B2 (en) * | 2013-08-20 | 2017-02-23 | Tama group | A wrapping material and method of manufacture for baled harvested agricultural materials |
MX2018013749A (en) * | 2016-05-10 | 2019-05-13 | Michael Trenchard Douglas | A solar reactive mulch film. |
CN110524854B (en) * | 2019-08-30 | 2023-09-29 | 重庆和泰润佳股份有限公司 | Blow molding breathable film production line |
JP7251662B2 (en) * | 2019-12-20 | 2023-04-04 | 東洋紡株式会社 | Laser-printable film and package using the same |
CN115771224B (en) * | 2022-10-28 | 2023-07-04 | 宁波鄞州晟瑜橡塑制品有限公司 | Automobile shock absorber piston rubber coating equipment and production process thereof |
Citations (3)
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US4436888A (en) * | 1982-10-05 | 1984-03-13 | E. I. Du Pont De Nemours And Company | Method for making balanced low shrink tension polyolefin film |
AU1950192A (en) * | 1991-09-06 | 1993-03-11 | Illinois Tool Works Inc. | Method for making prestretched film |
AU5556494A (en) * | 1992-05-19 | 1995-06-06 | Saltech Inc. | Stretch film |
Family Cites Families (13)
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US2307056A (en) | 1940-08-03 | 1943-01-05 | Henry D Minich | Film |
US4387548A (en) * | 1979-11-21 | 1983-06-14 | Lantech, Inc. | Power assisted roller-stretch wrapping process |
US4712686A (en) | 1980-09-08 | 1987-12-15 | Lantech, Inc. | Power assisted roller-stretch apparatus and process |
US4413463A (en) | 1980-10-23 | 1983-11-08 | Lantech, Inc. | Roller stretch pass through stretching apparatus and process |
US4816094A (en) * | 1984-05-01 | 1989-03-28 | Kimberly-Clark Corporation | Method of producing a heat shrinkable elastomer and articles utilizing the elastomer |
GB8800670D0 (en) | 1988-01-13 | 1988-02-10 | Drg Uk Ltd | Thin plastics film for packaging |
JPH0830765B2 (en) * | 1988-09-26 | 1996-03-27 | 富士写真フイルム株式会社 | Method of manufacturing retardation film |
JPH0542592A (en) * | 1991-08-09 | 1993-02-23 | Shin Etsu Chem Co Ltd | Manufacture of polyvinylidene fluoride resin oriented film |
FR2695102B1 (en) | 1992-08-25 | 1994-11-04 | Newtec Int | Method for overpacking loads using stretch film, machine and film for its implementation. |
EP0614810A1 (en) | 1993-02-26 | 1994-09-14 | Mobil Oil Corporation | Stretch wrap film rolls |
FR2718414B1 (en) | 1994-04-07 | 1996-05-15 | Newtec Int | Optimized process for overpacking and transporting an overpackaged load. |
DE19515599A1 (en) * | 1995-05-02 | 1996-11-07 | Hoechst Ag | Process for the production of polypropylene films and their use |
FR2748734B1 (en) * | 1996-05-06 | 1998-07-31 | Thimon | OVERPACKING FILM, FILM PRE-STRETCHING DEVICE AND OVERPACKING PROCESS |
-
1997
- 1997-05-01 AU AUPO6563A patent/AUPO656397A0/en not_active Abandoned
-
1998
- 1998-05-01 ES ES98916670T patent/ES2224376T3/en not_active Expired - Lifetime
- 1998-05-01 BR BRPI9809357-6A patent/BR9809357B1/en not_active IP Right Cessation
- 1998-05-01 CN CN98805749A patent/CN1084663C/en not_active Expired - Lifetime
- 1998-05-01 CA CA002288903A patent/CA2288903C/en not_active Expired - Lifetime
- 1998-05-01 NZ NZ500876A patent/NZ500876A/en not_active IP Right Cessation
- 1998-05-01 ID IDW991487A patent/ID22882A/en unknown
- 1998-05-01 JP JP54753698A patent/JP4435310B2/en not_active Expired - Lifetime
- 1998-05-01 RU RU99125548/12A patent/RU2191694C2/en not_active IP Right Cessation
- 1998-05-01 AT AT98916670T patent/ATE270181T1/en active
- 1998-05-01 AU AU70172/98A patent/AU726288B2/en not_active Expired
- 1998-05-01 DE DE69824869T patent/DE69824869T2/en not_active Expired - Lifetime
- 1998-05-01 US US09/403,960 patent/US6383430B1/en not_active Expired - Lifetime
- 1998-05-01 WO PCT/AU1998/000314 patent/WO1998050219A1/en active IP Right Grant
- 1998-05-01 EP EP98916670A patent/EP1015228B1/en not_active Expired - Lifetime
-
1999
- 1999-10-28 NO NO995278A patent/NO316613B1/en not_active IP Right Cessation
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4436888A (en) * | 1982-10-05 | 1984-03-13 | E. I. Du Pont De Nemours And Company | Method for making balanced low shrink tension polyolefin film |
AU1950192A (en) * | 1991-09-06 | 1993-03-11 | Illinois Tool Works Inc. | Method for making prestretched film |
AU5556494A (en) * | 1992-05-19 | 1995-06-06 | Saltech Inc. | Stretch film |
Cited By (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1999067080A1 (en) * | 1998-06-23 | 1999-12-29 | First Green Park Pty Ltd. | Orientation of films to improve barrier and uv stability |
EP1105282A1 (en) * | 1998-06-23 | 2001-06-13 | First Green Park Pty. Ltd. | Orientation of films to improve barrier and uv stability |
EP1105282A4 (en) * | 1998-06-23 | 2005-06-22 | Illinois Tool Works | Orientation of films to improve barrier and uv stability |
US7396498B1 (en) | 1998-06-23 | 2008-07-08 | Integrated Packaging Australia Pty. Ltd. | Orientation of films to improve barrier and UV stability |
EP1125718A2 (en) * | 2000-02-09 | 2001-08-22 | Itw Mima Films Llc | Stretch wrap film |
EP1125718A3 (en) * | 2000-02-09 | 2001-12-05 | Itw Mima Films Llc | Stretch wrap film |
WO2007093280A1 (en) * | 2006-02-15 | 2007-08-23 | Kverneland Asa | Wrapping of agricultural bales of rectangular cross section |
US8276349B2 (en) | 2006-02-15 | 2012-10-02 | Kuhn-Geldrop B.V. | Wrapping of agricultural bales of rectangular cross section |
EP2164770B1 (en) | 2007-06-21 | 2016-03-30 | Combipac BV | Prestretched film |
EP2164770B2 (en) † | 2007-06-21 | 2019-10-09 | Combipac BV | Prestretched film |
US9358760B2 (en) | 2007-09-28 | 2016-06-07 | Combipac Bv | Prestretched agricultural stretch wrap film |
Also Published As
Publication number | Publication date |
---|---|
AUPO656397A0 (en) | 1997-05-29 |
AU7017298A (en) | 1998-11-27 |
EP1015228A4 (en) | 2002-06-12 |
NO995278D0 (en) | 1999-10-28 |
EP1015228B1 (en) | 2004-06-30 |
DE69824869D1 (en) | 2004-08-05 |
CN1084663C (en) | 2002-05-15 |
BR9809357B1 (en) | 2009-01-13 |
RU2191694C2 (en) | 2002-10-27 |
NO316613B1 (en) | 2004-03-08 |
ID22882A (en) | 1999-12-16 |
NZ500876A (en) | 2001-03-30 |
CA2288903A1 (en) | 1998-11-12 |
JP4435310B2 (en) | 2010-03-17 |
JP2001522327A (en) | 2001-11-13 |
AU726288B2 (en) | 2000-11-02 |
CA2288903C (en) | 2008-01-22 |
BR9809357A (en) | 2000-07-04 |
ES2224376T3 (en) | 2005-03-01 |
DE69824869T2 (en) | 2005-03-17 |
CN1259077A (en) | 2000-07-05 |
EP1015228A1 (en) | 2000-07-05 |
US6383430B1 (en) | 2002-05-07 |
ATE270181T1 (en) | 2004-07-15 |
NO995278L (en) | 1999-12-15 |
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