WO1998039077A1 - Downcomer for chemical process tower - Google Patents

Downcomer for chemical process tower Download PDF

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Publication number
WO1998039077A1
WO1998039077A1 PCT/US1998/003920 US9803920W WO9839077A1 WO 1998039077 A1 WO1998039077 A1 WO 1998039077A1 US 9803920 W US9803920 W US 9803920W WO 9839077 A1 WO9839077 A1 WO 9839077A1
Authority
WO
WIPO (PCT)
Prior art keywords
downcomer
tray
outlet
wall
liquid
Prior art date
Application number
PCT/US1998/003920
Other languages
French (fr)
Inventor
Adam T. Lee
Kuang Wu
Larry Burton
Leon Fan
Original Assignee
Koch Enterprises, Inc.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US08/811,434 external-priority patent/US6003847A/en
Application filed by Koch Enterprises, Inc. filed Critical Koch Enterprises, Inc.
Priority to AU63429/98A priority Critical patent/AU716737B2/en
Priority to EP98907678A priority patent/EP0964732A1/en
Priority to JP53861498A priority patent/JP2001513701A/en
Priority to CA002278756A priority patent/CA2278756A1/en
Priority to BR9807643-4A priority patent/BR9807643A/en
Publication of WO1998039077A1 publication Critical patent/WO1998039077A1/en

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/32Packing elements in the form of grids or built-up elements for forming a unit or module inside the apparatus for mass or heat transfer
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14Fractional distillation or use of a fractionation or rectification column
    • B01D3/16Fractionating columns in which vapour bubbles through liquid
    • B01D3/18Fractionating columns in which vapour bubbles through liquid with horizontal bubble plates
    • B01D3/20Bubble caps; Risers for vapour; Discharge pipes for liquid

Definitions

  • the present invention relates to chemical process towers and, more particularly, but not by way of limitation, to a downcomer-tray assembly for maximizing
  • Distillation columns are utilized to separate selected components from a multi component stream. Successful fractionation in the column is dependent upon intimate contact between liquid and vapor phases. Some columns use vapor and liquid
  • the above-referenced trays are generally installed on support rings within the tower and have a solid tray or deck with a plurality of apertures in an "active" area. Liquid is directed onto the tray by means of a vertical channel from the tray above.
  • the liquid moves across the active area and
  • Vapor ascends through the apertures in the trays and contacts the
  • the liquid moving across the tray The liquid and vapor mix in the active area and fractionation occurs. It is the active area of the tray that is of critical concern.
  • the maximum fractionation capacity of the tray generally increases with
  • the liquid is the driving force to effect mass transfer. Said concentration-difference can be
  • Liquid entrainment is, in one sense, a dynamic flow condition.
  • High velocity vapor flow can suspend descending liquid droplets and prevent their
  • process column is allowed to by-pass the active area of a tray.
  • Efficiency of the active area in a tray is also influenced by the flow of
  • the flow of the liquid is not typically a flow characteristic that provides
  • the present invention relates to the chemical process tower downcomer
  • one aspect of the present invention comprises a
  • the downcomer disposed above a chemical process tower tray.
  • the downcomer. is formed
  • the downcomer outlet is formed by the lower edge of the wall
  • the lower edge of the wall region is closer to the wall of the process tower at
  • a discharge plate is disposed
  • the apertures are formed of such a size and spacing
  • the wall region includes semi-conical walls that
  • the wall region comprises a smooth curved edge.
  • the lower edge of the wall region comprises multiple straight lines connected
  • the present invention comprises an improved
  • the improvement comprising the steps of supporting the tray in the process column with a tray support located below a tray support area, forming a downcomer outlet having a
  • FIG. 1 is a perspective view of a packed column with various sections cut
  • FIG. 2 is an enlarged, fragmentary, perspective view of the downcomer-
  • FIG. 3 is an enlarged, fragmentary, perspective view of the downcomer
  • FIG. 4 is a diagrammatic, side-elevational, cross-sectional view of the
  • FIG. 5 A is an enlarged, fragmentary top view of one embodiment of the
  • FIG. 5B is an enlarged, fragmentary top view of another embodiment of
  • FIG. 5 C is an enlarged, fragmentary top view of another embodiment of
  • FIG. 6 is a top plan, diagrammatic view of a prior art tray illustrating the
  • FIG. 7A is an enlarged, fragmentary top view of an embodiment of a
  • FIG. 7B is an enlarged, fragmentary top view of another embodiment of
  • FIG. 7C is an enlarged, fragmentary top view of another embodiment of
  • FIG. 8 is a top plan, diagrammatic view of a tray illustrating the liquid
  • FIG. 1 there is shown a fragmentary, perspective view
  • FIG. 1 comprises a cylindrical tower 12 having packing beds 38 and 39, and
  • the tower 12 of the column 10 includes a skirt 28 for the support of
  • a plurality of manways 16 are constructed for facilitating access to the
  • a stream vapor feed line or reboiler return line 32 is
  • a vapor outlet or overhead line 26 is
  • a reflex return line 34 is provided in an upper portion of the tower 12.
  • the liquid 13 is depleted of some material which is gained by the vapor 15 as they
  • the vapor 15 is depleted of some material which is gained by the liquid 13.
  • upper packing bed 38 are shown for the purpose of illustration and include a liquid collector 40 disposed beneath a support grid 41 in support of the upper structured packing
  • a liquid distributor 42 adapted for redistributing liquid 13, is likewise disposed
  • a second type of distributor 42a is shown below the cut-line and disposed
  • FIGS. 2 and 3 there are shown two fragmentary
  • FIG. 1 perspective views of the downcomer-tray assembly 100 in FIG. 1 taken from opposite
  • first tray 110 connected to a first downcomer 120, and a second tray 130
  • the trays 110 and 130 are generally planer
  • the outlet weirs 112 and 132 are
  • the downcomers 120 and 140 have semi-record data. Still referring to FIGS. 2 and 3, the downcomers 120 and 140 have semi-record data.
  • 121 and 141 of the downcomers 120 and 140 are preferably formed from flat plates 121a-
  • side walls may be modified with more downcomer sections or with fewer downcomer
  • Downcomer outlets 122 and 142 are formed between the bottom of the walls 121 and 141 and the inner surface of the tower
  • the downcomer outlets 122 and 142 are positioned directly
  • the tray 130 has an inlet weir 133
  • the inlet weir 133 has a vertical height that extends above the position of
  • the lower portion of the downcomer 120 is supported by
  • the tray 130 includes a plurality of venting
  • the venting chambers 135 have a
  • the liquid 13 exits the downcomer 120 through the outlet 122 and accumulates on the
  • chambers 135 imparts a horizontal flow vector to the liquid 13 spilling over the inlet weir
  • the tray 130 engages vapor 15 ascending through the active area 131.
  • the froth or "foam" is a region of aeration
  • the froth 61 extends with a relatively
  • the length of the active area 131 of the tray 130 is governed by the distance between the
  • FIG. 5 A there is shown a top view of the tray 110 and
  • the downcomer 120 illustrated in FIGS. 2, 3, and 4. The downcomer 120 is separated from
  • the downcomer 120 is a chordal downcomer characterized by the
  • FIG. 5B there is illustrated a top view of another
  • the downcomer 120' is a swept downcomer (or multi-
  • chordal downcomer and is characterized by the outlet weir 112' having many, segments.
  • the outlet weir 112' has first and second segments 112a' and 112b' that are positioned in
  • FIG. 5C there is shown a top of view of yet another
  • the downcomer 120 is defined by the outlet weir
  • the outlet weir 112" is characterized by arcuate section that is semi-circular
  • outlet 122 is narrower than the upper region of the downcomer 120, causing a build up
  • a pool of liquid 13 from the downcomer 120 is created between the inlet weir 133
  • outlet 122 will be immersed in the pool of liquid accumulated between the inlet
  • the tray 130 has a support ring
  • the tray 130 also has a tray inlet area 138 located
  • outlet 122 first contacts the tray 130. Due to the flow of liquid 13 from the downcomer
  • the tray inlet area 138 of the tray 130 cannot readily be used as an active area
  • the tray inlet area 138 is substantially within the
  • tray 130 substantially within the support ring region 137, the area of the tray 130
  • downcomer outlet 122 and corresponding tray inlet area 138 of the tray 130 can vary
  • tray active area 131 inwardly of the tray support ring region
  • FIG. 6 there is shown a flow diagram across a
  • the prior art tray 950 is illustrated herein as a round tray having a first
  • a second downcomer 954 carries
  • FIG. 7A there is shown a top view of an embodiment
  • Downcomer 174 is formed by semi-conical wall 176 and the inside surface of wall 11 of
  • Semi-conical wall 176 is formed from plates 176a-e, respectively, that are
  • the downcomer outlet 180 is
  • downcomer outlet 180 is characterized
  • outlet portions 180a-e respectively, with the size of outlet portions 180a-e increasing
  • liquid 13 is therefore allowed to flow from and through outlet portions 180a, 180b, 180d
  • 176a-b and 176d-e respectively, is positioned further away from the inner surface of wall
  • 11 as lower edge 178 is formed from plate 176c to plate 176a and from plate 176c to
  • outlet 180 will flow onto tray inlet area 152 and over the inlet weir 146 (see FIG. 8) of
  • FIG. 7B there is shown a top view of another
  • Downcomer 188 is separated from the active area 171 of upper tray 170 by the outlet weir
  • Downcomer 188 is formed by semi-conical wall 190 and the inside surface of wall
  • Semi-conical wall 190 is formed from plates 190a-h, respectively, that
  • the downcomer outlet 194 is
  • outlet portions 194a-h characterized by outlet portions 194a-h, respectively, with the size of outlet portions
  • tray 170 will flow across tray 216 as uniform flow, as illustrated by a plurality of
  • FIG. 7C there is shown a top view of an additional item
  • Downcomer 198 is separated from the active area 171 of tray 170 by the outlet weir 172.
  • Downcomer 198 is formed by semi-conical wall 200 and the inside surface of wall 11 or
  • Semi-conical wall 200 is formed from plates 200a-f, respectively, that are
  • the downcomer outlet 204 is
  • Discharge plate 202 is formed by discharge apertures 204a-f formed in discharge plate 202. Discharge plate 202
  • downcomer outlet 204 is characterized by
  • apertures 204a and 204b than from discharge aperture 204c and also apertures 204e and
  • tray 216 in a uniform manner, effectively approximating flow in a generally rectangular
  • FIG. 8 there is shown a flow diagram across a tray 216
  • arrows 208 illustrate the uniform flow of liquid across tray 216 which essentially

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Organic Chemistry (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Extraction Or Liquid Replacement (AREA)

Abstract

An improved downcomer for vapor liquid contact towers. The downcomer is formed between generally semi-conical walls and the wall of the tower. The downcomer outlet is formed by the lower edge of the generally semi-conical walls and the wall of the tower with the lower edge of the generally semi-conical walls being closer to the wall of the tower at the center of the downcomer outlet than at the opposing end portions of the downcomer outlet so that more liquid flows through the opposing end portions of the downcomer outlet than through the center of the downcomer outlet thereby providing a substantially uniform flow of liquid across the tray adjacent the downcomer.

Description

DOWNCOMER FOR CHEMICAL PROCESS TOWER
Background of the Invention
Field of the Invention
The present invention relates to chemical process towers and, more particularly, but not by way of limitation, to a downcomer-tray assembly for maximizing
efficiency in a trayed tower. History of Related Art
Distillation columns are utilized to separate selected components from a multi component stream. Successful fractionation in the column is dependent upon intimate contact between liquid and vapor phases. Some columns use vapor and liquid
contact devices such as trays.
The above-referenced trays are generally installed on support rings within the tower and have a solid tray or deck with a plurality of apertures in an "active" area. Liquid is directed onto the tray by means of a vertical channel from the tray above. This
channel is referred to as the downcomer. The liquid moves across the active area and
exits through a similar downcomer. The location of the downcomers determine the flow
pattern of the liquid. Vapor ascends through the apertures in the trays and contacts the
liquid moving across the tray. The liquid and vapor mix in the active area and fractionation occurs. It is the active area of the tray that is of critical concern. The maximum fractionation capacity of the tray generally increases with
an increase in the active or bubbling area. Maximum utilization of active area of a tray
is an important consideration to chemical process tower design. Regions of the tray which are not effectively used for vapor-liquid contact can reduce the fractionation capacity and efficiency of the tray. Therefore, there is a need for devices and methods
that optimize the active area of a fractionation tray in a chemical process tower.
It is well known that the concentration-difference between the vapor and
the liquid is the driving force to effect mass transfer. Said concentration-difference can
be effected in many ways; some reducing fractionation efficiency. When operating
pressure is such as to produce a vapor density above about 1.0 lbs/cu. ft., there is the
possibility that some amount of vapor bubbles are commingled or entrained with the
downcomer incoming liquid. For example, as operating pressure increases due to an
increase in the vapor concentration, descending liquid begins to absorb vapor as it moves
across a tray. This is above that normally associated as dissolved gas as governed by
Henry's Law and represents much larger amounts of vapor bubbles that are commingled
or "entrained" with the liquid. This vapor is not firmly held and is released within the
downcomer, and, in fact, the majority of said vapor must be released, otherwise the
downcomer can not accommodate the liquid/vapor mixture and will flood thus preventing
successful tower operation.
Similarly, an exothermic reaction in the downcomer will generate vapors
from the equilibrium mixture, which also will be released. For conventional trays, the
released vapor will oppose the descending frothy vapor/liquid mixture flowing into the
downcomer. In many cases, such opposition leads to poor tower operation and premature
flooding. Therefore, there is a need for devices and methods that facilitate the release of
vapor entrained in the liquid within a downcomer of a chemical process tower.
Another serious problem which manifests itself in such operational
applications is entrainment of liquid droplets in the ascending vapor. This phenomenon,
which is virtually the opposite of the above vapor entrainment, can prevent effective vapor liquid contact. Liquid entrainment is, in one sense, a dynamic flow condition.
High velocity vapor flow can suspend descending liquid droplets and prevent their
effective passage through the underlying froth mixture zone. It is particularly difficult
to prevent this problem when the tower applications require high volume vapor flow in
a direction virtually opposite to that of high volume, descending liquid flow. Therefore,
there is a need for devices and methods that will reduce the liquid entrained in the vapor
within a chemical process tower.
Efficiency of a tray is also reduced when vapor ascending through the
process column is allowed to by-pass the active area of a tray. One area where vapor can
bypass the active area of a tray is the downcomer. When vapor intended for the active
area of the tray unintentionally passes through the downcomer the efficiency of the active
area in the tray is reduced. Also, vapor unintentionally passing through the downcomer
will reduce the flow of liquid through the downcomer and potentially cause a backup of
the liquid flowing through the process column. Therefore, there is a need for devices and
methods that reduce the amount of vapor that flows through a downcomer.
Efficiency of the active area in a tray is also influenced by the flow of
liquid across the active area. At the initial point of contact of liquid from a downcomer
onto the tray, the flow of the liquid is not typically a flow characteristic that provides
optimum efficiency for the active area of a tray. Therefore, there is a need for devices
and methods that assist in the change of flow characteristics of fluid from a downcomer
onto the active area of a tray and also across the active area of a tray. The present
invention provides such a method and apparatus for maximizing mass transfer efficiency
in chemical process towers. Summary of the Invention
The present invention relates to the chemical process tower downcomer
configuration. More particularly, one aspect of the present invention comprises a
downcomer disposed above a chemical process tower tray. The downcomer. is formed
by a wall region and the wall of the chemical process tower and has an outlet for the flow
of liquid therefrom. The downcomer outlet is formed by the lower edge of the wall
region and the wall of the chemical process tower and has a center and opposing end
portions. The lower edge of the wall region is closer to the wall of the process tower at
the center than at the opposing end portions so that more liquid flows through the
opposing end portions than through the center of the downcomer outlet thereby creating a more uniform flow of liquid.
In another aspect of the present invention, a discharge plate is disposed
across the downcomer outlet and the discharge plate has a predetermined number of
apertures formed therethrough. The apertures are formed of such a size and spacing
between the apertures that more liquid flows into the tray inlet area through the apertures
formed in the opposing end portions of the discharge plate than through the center of the
discharge plate thereby providing a uniform flow of liquid across the tower tray. In
another aspect of the present invention, the wall region includes semi-conical walls that
taper to the downcomer outlet. In another aspect of the present invention, the lower edge
of the wall region comprises a smooth curved edge. In another aspect of the present
invention, the lower edge of the wall region comprises multiple straight lines connected
end-to-end. In another embodiment, the present invention comprises an improved
method of mixing a gas with a liquid from a downcomer in a process tower using a tray,
the improvement comprising the steps of supporting the tray in the process column with a tray support located below a tray support area, forming a downcomer outlet having a
center and opposing end portions with the lower edge of the wall region being closer to
the wall of the chemical process tower at the center than at the opposing end portions so
that more liquid would flow through the opposing end portions of the downcomer outlet
than through the center of the downcomer outlet, and positioning the downcomer outlet
over the tray inlet area so liquid from the downcomer outlet will approximate the flow
of liquid across a rectangular tray.
Brief Description of the Drawings
For a more complete understanding of the present invention and for further
objects and advantages thereof, reference may now be had to the following description
taken in conjunction with the accompanying drawings in which:
FIG. 1 is a perspective view of a packed column with various sections cut
away for illustrating a variety of tower internals and one embodiment of a downcomer-
tray assembly constructed in accordance with the principles of the present invention
disposed therein;
FIG. 2 is an enlarged, fragmentary, perspective view of the downcomer-
tray assembly in FIG. 1, with portions of the tower cut away and illustrating the
construction of the downcomer and tray of the present invention;
FIG. 3 is an enlarged, fragmentary, perspective view of the downcomer
tray assembly of FIG. 2, taken from the inside of the tower;
FIG. 4 is a diagrammatic, side-elevational, cross-sectional view of the
downcomer-tray assembly of FIGS. 2 and 3 illustrating the principles of operation
thereof; FIG. 5 A is an enlarged, fragmentary top view of one embodiment of the
downcomer tray assembly of FIGS. 2 and 3;
FIG. 5B is an enlarged, fragmentary top view of another embodiment of
the downcomer-tray assembly of FIGS. 2 and 3;
FIG. 5 C is an enlarged, fragmentary top view of another embodiment of
the downcomer-tray assembly of FIG. 2 and 3;
FIG. 6 is a top plan, diagrammatic view of a prior art tray illustrating the
liquid flow thereacross;
FIG. 7A is an enlarged, fragmentary top view of an embodiment of a
downcomer constructed in accordance with the principles of the present invention for
maximizing mass transfer efficiency in chemical process towers;
FIG. 7B is an enlarged, fragmentary top view of another embodiment of
a downcomer constructed in accordance with the principles of the present invention for
maximizing mass transfer efficiency in chemical process towers;
FIG. 7C is an enlarged, fragmentary top view of another embodiment of
a downcomer constructed in accordance with the principles of the present invention for
maximizing mass transfer efficiency in chemical process towers; and
FIG. 8 is a top plan, diagrammatic view of a tray illustrating the liquid
flow thereacross in accordance with the principles of the present invention for
maximizing mass transfer efficiency in chemical process tower.
Detailed Description
Referring first to FIG. 1, there is shown a fragmentary, perspective view
of an illustrative packed exchange tower or column with various sections cut away for showing a variety of tower internals and the utilization of one embodiment of the
improved downcomer-tray assembly of the present invention. The exchange column 10
of FIG. 1 comprises a cylindrical tower 12 having packing beds 38 and 39, and
downcomer tray assembly 100 incorporating the principles of the present invention
disposed therein. The tower 12 of the column 10 includes a skirt 28 for the support of
the tower 12. A plurality of manways 16 are constructed for facilitating access to the
internal region of the tower 12. A stream vapor feed line or reboiler return line 32 is
provided in a lower portion of the tower 12 and a vapor outlet or overhead line 26 is
provided in an upper portion of the tower 12. A reflex return line 34 is provided in an
upper portion of the tower 12 and a bottom stream draw off line 30 is provided at the
bottom of the tower 12. Also provided are a side stream draw off line 20 and a liquid
side feed line 18 in the tower 12.
Referring still to FIG. 1, in operation, vapor 15 is fed into the tower 12
through the return line 32 and liquid 13 is fed into the tower 12 through the reflux return
line 34 and the side stream feed input feed line 18. The vapor 15 flows upwardly through
the column 10 and ultimately leaves the tower 12 through the vapor outlet 26. The liquid
13 flows downwardly through the column 10 and ultimately leaves the tower 12 either
at the side stream draw off 20, or at the bottom stream draw offline 30. In its downward
flow, the liquid 13 is depleted of some material which is gained by the vapor 15 as they
pass through the tray assembly 100 and the packing beds 38, 39 of the column 10, and
the vapor 15 is depleted of some material which is gained by the liquid 13.
Referring still to FIG. 1, it may be seen that the upper packing bed 38 is
of the structured packing variety. The regions of the exchange column 10 beneath the
upper packing bed 38 are shown for the purpose of illustration and include a liquid collector 40 disposed beneath a support grid 41 in support of the upper structured packing
38. A liquid distributor 42, adapted for redistributing liquid 13, is likewise disposed
there-beneath. A second type of distributor 42a is shown below the cut-line and disposed
above the lower packing bed 39. The internal arrangement of the column 10 is
diagrammatical only and is provided for referencing various component arrays therein.
Referring now to FIGS. 2 and 3, there are shown two fragmentary
perspective views of the downcomer-tray assembly 100 in FIG. 1 taken from opposite
angles relative to the tower 12. In this embodiment, the downcomer tray assembly 100
includes a first tray 110 connected to a first downcomer 120, and a second tray 130
connected to a second downcomer 140. The trays 110 and 130 are generally planer
panels that have central active areas 111 and 131, respectively. The trays 110 and 130
are supported by support rings 98 and 99, respectively, of the tower 12. Outlet weirs 112
and 132 are disposed of on the first and second trays 110 and 130, respectively, adjacent
to the downcomers 120 and 140, respectively. The outlet weirs 112 and 132 are
preferably an upright plate or strip welded to the planer panels of the trays 120 and 140.
Still referring to FIGS. 2 and 3, the downcomers 120 and 140 have semi-
conical walls 121 and 141, respectively, that taper from the outlet weirs 112 and 132 of
the trays 110 and 130, downwardly towards the inner surface of the tower 12. The walls
121 and 141 of the downcomers 120 and 140 are preferably formed from flat plates 121a-
d and 141 a-d, respectively, that are welded together in a configuration shown herein. The
actual construction of the downcomer may vary in accordance with the principles of the
present invention. For example, the segmented-angled construction of the downcomer
side walls may be modified with more downcomer sections or with fewer downcomer
sections and an arcuate or curved construction. Downcomer outlets 122 and 142 are formed between the bottom of the walls 121 and 141 and the inner surface of the tower
12. In one embodiment, the downcomer outlets 122 and 142 are positioned directly
above the tray support rings 98 and 99 of the tower 12 and have an opening area that is
contained substantially within the area directly above the tray support rings 98 and 99.
Referring still to FIGS. 2 and 3, the tray 130 has an inlet weir 133
positioned around the area directly below the downcomer outlet 122. The inlet weir 133
is preferably an upright plate or strip welded to the planar panel of the tray 130. In one
embodiment, the inlet weir 133 has a vertical height that extends above the position of
the downcomer outlet 122. The lower portion of the downcomer 120 is supported by
clips 134 that are welded to the inlet weir 133 and bolted to the lower portion of the
downcomer 130.
Still referring to FIGS. 2 and 3, the tray 130 includes a plurality of venting
chambers 135 that are disposed in the area of the tray 130 located on the opposite side of
the inlet weir 133 from the downcomer outlet 122. The venting chambers 135 have a
plurality of apertures 135a for using the vapor 15 to impart a horizontal flow to the liquid
13 spilling over the inlet weir 133.
Referring now to FIG. 4, liquid 13 crossing the active area 111 of the tray
110 engages vapor 15 ascending through the active area 111. The outlet weir 112
controls the flow of liquid 13 that passes from the active area 111 of the tray 110 into the
downcomer 120. Liquid 13 flowing over the outlet weir 112 of the tray 110 passes
downwardly between wall 121 of the downcomer 120 and the inner wall of the tower 12.
The liquid 13 exits the downcomer 120 through the outlet 122 and accumulates on the
tray 130 in an area between the inlet weir 133 and the inner wall of the tower 12. Still referring to FIG. 4, once the level of liquid 13 accumulating in the
area of the tray 130 between inner wall of the tower 12 and the inlet weir 133 reaches the
height of the inlet weir 133, additional liquid 13 exiting the downcomer outlet 122 will
cause liquid 13 to pass or spill over the inlet weir 133. Some of the vapor J5 passing
upward in the column 10 flows through the apertures 135a in the vent chambers 135 and
engages the liquid 13 spilling over the inlet weir 133. The vapor 15 from the venting
chambers 135 imparts a horizontal flow vector to the liquid 13 spilling over the inlet weir
133 across the active area 131 of the tray 130. The liquid 13 passing over the active area
131 of the tray 130 engages vapor 15 ascending through the active area 131.
Referring still to FIG. 4, the engagement of the liquid 13 passing across
the active area 131 of the tray 130 with the vapor 15 ascending through the active area
131 creates the froth 61. As previously stated, the froth or "foam" is a region of aeration
in which the phase of the liquid 13 is continuous. The froth 61 extends with a relatively
uniform height, shown in phantom by line 63, across the active area 131 of the tray 130.
The length of the active area 131 of the tray 130 is governed by the distance between the
inlet weir 133 and the outlet weir 132. The outlet weir 132 also controls the flow of froth
61 or liquid 13 that passes from the active area 131 of the tray 130 into the downcomer
140, where the fluid exits the tray 130 for the next process in the column 10.
Referring now to FIG. 5 A, there is shown a top view of the tray 110 and
downcomer 120 illustrated in FIGS. 2, 3, and 4. The downcomer 120 is separated from
the active area 111 of the tray 110 by the outlet where weir 112. In the embodiment
illustrated in FIG. 5 A, the downcomer 120 is a chordal downcomer characterized by the
linear outlet weir 112 of the tray 110 defining the edge of the tray 110 in a chordal
manner. Referring now to FIG. 5B, there is illustrated a top view of another
embodiment of the tray 110 and downcomer 120 from FIGS. 2, 3, and 4. In the
embodiment illustrated in FIG. 5B, the downcomer 120' is a swept downcomer (or multi-
chordal downcomer) and is characterized by the outlet weir 112' having many, segments.
The outlet weir 112' has first and second segments 112a' and 112b' that are positioned in
a co-linear chordal fashion. A third section 112c' 15 parallel to the first and second
sections 112a' and 112b', but is disposed centered between the first and second sections
112a' and 112b', and offset towards the tower 12. Fourth and fifth sections 112d' and
112e' of the outlet weir 112' connect the third section 112c' with the first section 112a'
and the second section 112b', respectively.
Referring now to FIG. 5C, there is shown a top of view of yet another
embodiment of the tray 110 and downcomer 120 illustrated in FIGS. 2, 3, and 4. In the
embodiment illustrated in FIG. 5C, the downcomer 120 is defined by the outlet weir
112". The outlet weir 112" is characterized by arcuate section that is semi-circular
extending towards the downcomer 120.
Referring now to FIGS.2, 3, 4, and 5A-C in combination, the downcomer
outlet 122 is narrower than the upper region of the downcomer 120, causing a build up
in the region of the downcomer outlet 122 of liquid 13 flowing through the downcomer
120. The build up of liquid 13 in the region of the downcomer outlet 122 causes a
dynamic seal that prevents vapor 15 ascending through the column 10 from passing
through the downcomer 120 instead of the tray 110. A seal is also created by relative
vertical heights of the outlet 122 for the downcomer 120 and the inlet weir 133 of the tray
130. A pool of liquid 13 from the downcomer 120 is created between the inlet weir 133
and the inner wall of the tower 12. When the vertical height of the outlet 122 for the downcomer 120 is located near or below the vertical height of the inlet weir 133 for the
tray 130, outlet 122 will be immersed in the pool of liquid accumulated between the inlet
weir 133 and the inner surface of the tower 12. Because the outlet 122 of the downcomer
120 is at or below the level of a pool of liquid accumulated between the inlet weir 133
of the tray 130 and the inner surface of the tower 12, vapor 15 ascending through the
column 10 will be inhibited from flowing through the downcomer 120 and by-passing
the tray 110.
Still referring to FIGS. 2, 3, 4, and 5A-C, the tray 130 has a support ring
region 137 on a top side 130a of the tray 130 directly above location where the support
ring 98 engages the tray 130. Due to structural constraints, support ring region 137 of
conventional support rings cannot ordinarily be used as an active area for the mixing of
liquid 13 and vapor 15. (This aspect is addressed in U.S. Pat. No. 5,547,617 assigned to
the assignee of the present invention.) The tray 130 also has a tray inlet area 138 located
at the position on the top side 130a of the tray 130 where liquid 13 from the downcomer
outlet 122 first contacts the tray 130. Due to the flow of liquid 13 from the downcomer
outlet 122, the tray inlet area 138 of the tray 130 cannot readily be used as an active area
for the mixing of liquid 13 and vapor 15. Because the downcomer outlet 122 has an area
contained above the tray support ring 98, the tray inlet area 138 is substantially within the
support ring region 137 of the tray 130. By consolidating the tray inlet area 138 of the
tray 130 substantially within the support ring region 137, the area of the tray 130
available for use as the active area 131 is increased over conventional tray assemblies that
either do not position the tray inlet area substantially within the support ring region of the
tray 130 or otherwise address this issue. Referring still to FIGS. 2, 3, 4, and 5A-C, because the support ring 98 is
a narrow band around the inner circumference of the tower 12, the support ring region
137 of the tray 130 will be a long narrow region. In order for the tray inlet area 138 to
be substantially within the support ring region 137, the downcomer outlet 122 will
usually need to be longer than conventional downcomers to accommodate the liquid 13
flowing through the downcomer 120. However, as shown herein, the length of the
downcomer outlet 122 and corresponding tray inlet area 138 of the tray 130, can vary
significantly within the tray support ring region 137 of the tray 130 without having any
affect on the availability of tray active area 131 inwardly of the tray support ring region
137.
Referring now to FIG. 6, there is shown a flow diagram across a
conventional tray. The prior art tray 950 is illustrated herein as a round tray having a first
conventional downcomer for feeding liquid upon a solid, underlying panel or fray inlet
area 952 and then over inlet weir 946 to tray 950. A second downcomer 954 carries
liquid over outlet weir 948 and away from the fray 950. A plurality of arrows 156
illustrate the non-uniform flow 960 of liquid 913 across a conventional tray 950 with the
pattern producing retrograde, as manifest by recirculation cells 958. Said recirculation
cells are shown to be formed on both sides of the fray lateral to the direction of flow of
liquid 913. The formation of these retrograde flow areas, or recirculation cells 958,
decreases the efficiency of the tray. These recirculation cells are the result of retrograde
flow near the wall of tower 912 and this backflow problem becomes more pronounced
as the diameter of the column increases. With the increase in retrograde flow and the
resultant stagnation effect from the recirculation cells, concentration-difference driving
force for mass transfer between the counter-flowing streams is reduced. The reduction in concentration-difference driving force will result in more contact or height requirement
for a given separation in the column. Although back mixing is but a single aspect of tray
efficiency, the reduction thereof is provided concurrently with the other advantages
hereof.
Referring now to FIG. 7A, there is shown a top view of an embodiment
of a downcomer constructed in accordance with the principles of the present invention
for maximizing mass transfer efficiency in chemical process towers. Downcomer 174
is separated from the active area 171 of upper tray 170 by the outlet weir 172.
Downcomer 174 is formed by semi-conical wall 176 and the inside surface of wall 11 of
tower 12. Semi-conical wall 176 is formed from plates 176a-e, respectively, that are
connected together in a configuration shown herein. The downcomer outlet 180 is
formed by the curved lower edge 178 of plates 176a-e, respectively and the inner surface
of wall 11 of tower 12. It will be appreciated that downcomer outlet 180 is characterized
by outlet portions 180a-e, respectively, with the size of outlet portions 180a-e increasing
from 180c (the center) to 180a (end portion) and from 180c to 180e (end portion). More
liquid 13 is therefore allowed to flow from and through outlet portions 180a, 180b, 180d
and 180e than from and through outlet portion 180c because the lower edge 178 of plates
176a-b and 176d-e, respectively, is positioned further away from the inner surface of wall
11 as lower edge 178 is formed from plate 176c to plate 176a and from plate 176c to
plate 176e. It will be appreciated that the liquid 13 which flows through downcomer
outlet 180 will flow onto tray inlet area 152 and over the inlet weir 146 (see FIG. 8) of
lower tray 216 (see FIG. 8) and will flow across the lower tray 216 in a uniform flow, as
illustrated by a plurality of arrows 208. This uniform flow is the result of more liquid 13
being introduced onto the portions of tray 216 which are located nearest the wall of tower 12 than is being introduced onto the center portion of tray 216. This uniform flow
essentially eliminates the recirculation cells or retrograde flow areas.
Referring now to FIG. 7B, there is shown a top view of another
embodiment of a downcomer constructed in accordance with the principles of the present
invention for maximizing mass transfer efficiency in chemical process towers.
Downcomer 188 is separated from the active area 171 of upper tray 170 by the outlet weir
172. Downcomer 188 is formed by semi-conical wall 190 and the inside surface of wall
11 of tower 12. Semi-conical wall 190 is formed from plates 190a-h, respectively, that
are connected together in a configuration shown herein. The downcomer outlet 194 is
formed by the segmented lower edge 192 of plates 190a-h, respectively and the inner
surface of wall 11 of tower 12. It will be appreciated that downcomer outlet 194 is
characterized by outlet portions 194a-h, respectively, with the size of outlet portions
194a-h increasing from center 194' to 194a (end portion) and from center 194' to 194h
(end portion). More liquid 13 is therefore allowed to flow from and through outlet
portions 194a, 194b, 194c, 194f, 194g and 194h than from and through outlet portions
194d and 194e because the lower edge 192 of plates 190a-c and 190e-h, respectively, is
positioned further away from the inner surface of wall 11 as lower edge 192 is formed
from plate 190d to plate 190a and from plate 190e to plate 190h. It will be appreciated
that the liquid 13 which flows through downcomer outlet 194 will flow into tray inlet
area 152 and over the inlet weir 146 (see FIG. 8) of lower tray 216 (see FIG. 8) below
tray 170 and will flow across tray 216 as uniform flow, as illustrated by a plurality of
arrows 208. This uniform flow is the result of more liquid 13 being introduced onto the
portions of fray 216 which are located nearest the wall of tower 12 than is being introduced onto the center portion of tray 216 and which essentially eliminates the
recirculation cells or retrograde flow areas.
Referring now to FIG. 7C, there is shown a top view of an additional
embodiment of a downcomer constructed in accordance with the principles of the present
invention for maximizing mass transfer efficiency in chemical process towers.
Downcomer 198 is separated from the active area 171 of tray 170 by the outlet weir 172.
Downcomer 198 is formed by semi-conical wall 200 and the inside surface of wall 11 or
tower 12. Semi-conical wall 200 is formed from plates 200a-f, respectively, that are
connected together in a configuration shown herein. The downcomer outlet 204 is
formed by discharge apertures 204a-f formed in discharge plate 202. Discharge plate 202
extends from the lower edge of plates 200a-f to the inner surface of wall 11 of tower 12
so that any liquid 13 which exits from downcomer 198 can only exit through discharge
apertures 204a-f. It will be appreciated that downcomer outlet 204 is characterized by
the size and number of discharge apertures increasing from 204c to 204a and from 204d
to 204f. More liquid 13 is therefore allowed to flow from and through discharge
apertures 204a and 204b than from discharge aperture 204c and also apertures 204e and
204f than from discharge aperture 204d. At will be appreciated that the liquid 13 which
flows through discharge apertures 204a-f will flow into fray inlet area 152 and over the
inlet weir 146 (see FIG. 8) of fray 216 (see FIG. 8) below fray 170 and will flow across
tray 216 in a uniform manner, effectively approximating flow in a generally rectangular
tower as illustrated by a plurality of arrows 208. This uniform flow is the result of more
liquid 13 being introduced onto the portions of tray 216 which are located nearest the
wall of tower 12 than is being introduced onto the center portion of fray 216 and which
essentially eliminates the recirculation cells or retrograde flow areas. Referring now to FIG. 8, there is shown a flow diagram across a tray 216
which receives liquid from the present inventive downcomer after the liquid has been fed
to the tray inlet area 152 and then over the inlet weir 146 to tray 216. A plurality of
arrows 208 illustrate the uniform flow of liquid across tray 216 which essentially
eliminates the recirculation cells or retrograde flow areas and thereby enhancing
interaction of vapor and liquid passing in counter-current flow through the tower 12.
It is thus believed that the operation and construction of the present
invention will be apparent from the foregoing description. While the method and
apparatus shown or described has been characterized as being preferred it will be obvious
that various changes and modifications may be made therein without departing from the
spirit and scope of the invention as defined in the following claims.

Claims

What is Claimed is:
1. An apparatus for facilitating enhanced interaction of vapor and
liquid passing in counter-current flow through a process tower having a wall, said
apparatus comprising: an outlet weir having a plurality of segments arranged. in a multi-
chordal configuration; a downcomer disposed below said outlet weir, said downcomer
having a downcomer outlet and a downcomer wall tapering from said outlet weir
downwardly towards the wall of said process tower and said downcomer outlet, wherein
said downcomer outlet includes a center opening section and opposing edge opening
sections, and wherein said opposing edge opening portions are greater than said center
opening section; and a fray having an inlet area disposed below said downcomer outlet
and a second tray area.
2. The apparatus according to claim 1 , wherein said downcomer wall
is a semi-conical wall.
3. The apparatus according to claim 1, further including a support
ring supporting said tray, and wherein said inlet area is located above said support ring.
4. The apparatus according to claim 1, wherein said tray further
includes an inlet weir separating said inlet area from said second fray area.
5. The apparatus according to claim 4, wherein said inlet weir extends
above said downcomer outlet.
6. The apparatus according to claim 4, wherein said tray further
includes a plurality of venting chambers disposed on said tray adjacent to said inlet weir
and opposite of said inlet area.
7. An apparatus for facilitating enhanced interaction of vapor and
liquid passing in counter-current flow through a process tower having a wall, said apparatus comprising: an outlet weir having an arcuate section extending towards said
wall of said tower; a downcomer disposed below said outlet weir, said downcomer
having a downcomer outlet and a downcomer wall tapering from said outlet weir
downwardly towards the wall of said process tower and said downcomer outlet, wherein
said downcomer outlet has a center opening section and opposing edge opening sections,
and wherein said opposing edge opening sections are greater than said center opening
section; and a fray having an inlet area disposed below said downcomer outlet and a
second fray area.
8. The apparatus according to claim 7, wherein said arcuate section
of said outlet weir is a semi-circular shape extending towards said wall of said process
tower.
9. The apparatus according to claim 7, wherein said downcomer wall
is a semi-conical wall.
10. The apparatus according to claim 7, further including a support
ring supporting said tray, and wherein said inlet area is located above said support ring.
11. The apparatus according to claim 7, wherein said tray further
includes an inlet weir separating said inlet area from said second tray area.
12. The apparatus according to claim 11, wherein said inlet weir
extends above said downcomer outlet.
13. The apparatus according to claim 11, wherein said tray further
includes a plurality of venting chambers disposed on said tray adjacent to said inlet weir
and opposite of said inlet area.
14. An apparatus for facilitating enhanced interaction of vapor and
liquid passing counter-current flow through a process tower having a wall, said apparatus comprising: an outlet weir; a downcomer disposed below said outlet weir, said
downcomer having a downcomer wall tapering from said outlet weir downwardly
towards the wall of said process tower and to a discharge plate, wherein said discharge
plate includes a center and opposing end portions and a plurality of. apertures
therethrough, and wherein the size and spacing of said apertures in said discharge plate
is such that more liquid flowing through said downcomer flows through the apertures in
the end portions of said discharge plates than through the apertures in the center section
of the discharge plate; and a tray having an inlet area disposed below said discharge plate
of said downcomer and a second tray area.
15. The apparatus according to claim 14, wherein said downcomer
wall is a semi-conical wall.
16. The apparatus according to claim 14, further including a support
ring supporting said tray, and wherein said inlet area is located above said support ring.
17. The apparatus according to claim 14, wherein said tray further
includes an inlet weir separating said inlet area from said second tray area.
18. The apparatus according to claim 17, wherein said tray further
includes a plurality of venting chambers disposed on said tray adjacent to said inlet weir
and opposite of said inlet area.
19.. Apparatus for facilitating enhanced interaction of vapor and liquid
passing in counter-current flow through a process tower having a wall and having at least
one tray supported therein which has a tray inlet area and a tray outlet area, said apparatus
comprising: a downcomer disposed above said at least one fray; said downcomer being
formed between a wall region and the wall of said process tower and having an outlet for
the flow of liquid therefrom; said downcomer outlet disposed above said tray inlet area, said downcomer outlet being formed by the lower edge of the wall region and the wall
of said process tower and having a center and opposing end portions; a discharge plate
disposed across said downcomer outlet, said discharge plate having a center and opposing
end portions; and said discharge plate having a predetermined number of apertures
formed therethrough, said apertures being formed of such a size and spacing between the
apertures that more liquid flows into the tray inlet area through the apertures formed in
the opposing end portions of the discharge plate than through the center of the discharge
plate thereby providing a uniform flow of liquid across said fray.
20. The apparatus as set forth in claim 19, wherein said wall region
includes semi-conical walls that taper to said downcomer outlet.
21. The apparatus as set forth in claim 19, wherein said lower edge of
the wall region comprises a smooth curved edge.
22. The apparatus as set forth in claim 19, wherein said lower edge of
the wall region comprises multiple straight lines connected end-to-end.
23. A method of mixing a gas with a liquid discharged from a
downcomer onto a tray in a chemical process tower, the method comprising the steps
of: supporting the fray in the process column with a tray support below a tray support
region of the fray; forming a downcomer between a wall region and a wall of the
chemical process tower; forming a downcomer outlet between the lower edge of the wall
region and the wall of the chemical process tower with said downcomer outlet having a
center and opposing end portions; forming a discharge plate across said downcomer
outlet with said discharge plate having a center and opposing end portions; forming a
predetermined number of apertures through said discharge plate with said apertures being
formed of such a size and spacing between the apertures that more liquid would flow through the apertures formed in the opposing end portions of the discharge plate than
through the center of the discharge plate; and positioning the discharge plate substantially
over said tray support area to define a tray inlet area of the fray so liquid from the
downcomer outlet will provide a uniform flow of the liquid across said fray..
24. The method as set forth to claim 23, including the step of forming
the wall region with semi-conical walls that taper to said downcomer outlet
25. The method as set forth in claim 23, including the step of forming
the lower edge of the wall region into a smooth curved edge.
26. The method as set forth in claim 23, including the step of forming
the lower edge of the wall region into multiple sfraight lines connected end-to-end.
PCT/US1998/003920 1997-03-03 1998-02-27 Downcomer for chemical process tower WO1998039077A1 (en)

Priority Applications (5)

Application Number Priority Date Filing Date Title
AU63429/98A AU716737B2 (en) 1997-03-03 1998-02-27 Downcomer for chemical process tower
EP98907678A EP0964732A1 (en) 1997-03-03 1998-02-27 Downcomer for chemical process tower
JP53861498A JP2001513701A (en) 1997-03-03 1998-02-27 Downcomer for chemical process tower
CA002278756A CA2278756A1 (en) 1997-03-03 1998-02-27 Downcomer for chemical process tower
BR9807643-4A BR9807643A (en) 1997-03-03 1998-02-27 Apparatus intended to facilitate improved interaction of vapor and liquid that pass in counter-current flow through a processing tower, and process of mixing a gas with liquid discharged from a descending tube over a tray in a tower chemical processing

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US08/811,434 US6003847A (en) 1996-10-30 1997-03-03 Downcomer for chemical process tower
US08/811,434 1997-03-03

Publications (1)

Publication Number Publication Date
WO1998039077A1 true WO1998039077A1 (en) 1998-09-11

Family

ID=25206548

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US1998/003920 WO1998039077A1 (en) 1997-03-03 1998-02-27 Downcomer for chemical process tower

Country Status (12)

Country Link
EP (1) EP0964732A1 (en)
JP (1) JP2001513701A (en)
KR (1) KR20000075884A (en)
AR (1) AR011917A1 (en)
AU (1) AU716737B2 (en)
BR (1) BR9807643A (en)
CA (1) CA2278756A1 (en)
CO (1) CO4761079A1 (en)
ID (1) ID20927A (en)
TW (1) TW438616B (en)
WO (1) WO1998039077A1 (en)
ZA (1) ZA981737B (en)

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US6460833B2 (en) 2000-02-16 2002-10-08 Shell Oil Company Gas-liquid contacting column
WO2004011119A2 (en) * 2002-07-29 2004-02-05 Koch-Glitsch, Lp Vapor-liquid contact trays and method employing same

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KR100759193B1 (en) * 2005-08-30 2007-09-14 주식회사 엘지화학 Manufacturing method of multi-layered printed circuit board and multi-layered printed circuit board manufactured by the same
CN108310921A (en) * 2018-03-29 2018-07-24 杭州众盛新科技有限公司 Oval ripple sieve-plate tower
KR20210084901A (en) * 2019-12-30 2021-07-08 한화솔루션 주식회사 tray-type distillation apparatus

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JPS5549101A (en) * 1978-10-03 1980-04-09 Mitsubishi Heavy Ind Ltd Vapor-liquid contact apparatus
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Cited By (3)

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Publication number Priority date Publication date Assignee Title
US6460833B2 (en) 2000-02-16 2002-10-08 Shell Oil Company Gas-liquid contacting column
WO2004011119A2 (en) * 2002-07-29 2004-02-05 Koch-Glitsch, Lp Vapor-liquid contact trays and method employing same
WO2004011119A3 (en) * 2002-07-29 2005-02-24 Koch Glitsch Lp Vapor-liquid contact trays and method employing same

Also Published As

Publication number Publication date
EP0964732A1 (en) 1999-12-22
TW438616B (en) 2001-06-07
BR9807643A (en) 2000-02-22
AR011917A1 (en) 2000-09-13
JP2001513701A (en) 2001-09-04
ID20927A (en) 1999-03-25
KR20000075884A (en) 2000-12-26
ZA981737B (en) 1998-08-21
CA2278756A1 (en) 1998-09-11
CO4761079A1 (en) 1999-04-27
AU6342998A (en) 1998-09-22
AU716737B2 (en) 2000-03-02

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