WO1996016318A1

WO1996016318A1 - Sensor for radiation-pyrometric temperature measurement at high ambient temperatures

Info

Publication number: WO1996016318A1
Application number: PCT/EP1995/004038
Authority: WO
Inventors: Ralf Pleva; Harry Pleva; Wilfried LÖBEL
Original assignee: Pleva Gmbh
Priority date: 1994-11-19
Filing date: 1995-10-13
Publication date: 1996-05-30
Also published as: US5921680A; EP0792443A1; DE4441257A1; DE59505931D1; EP0792443B1; ATE180052T1

Abstract

The invention relates to a sensor for the radiation-pyrometric measurement of the temperature of an object in high ambient temperatures inside a drier or the like. The sensor consists of a heat-conducting housing (1) with a window (2) transparent to heat radiation and at least one thermopile (3, 33) in the housing (1) consisting of thermocouples (18) of interconnected elements (18a, 18b) of mutually thermo-electrically active materials. A first radiation-sensitive connection (4, 34) between the elements (18a, 18b) faces the window (2) and they are distributed over a basic surface (25) of a substrate (5) facing the window (2). The substrate (5) consists of a heat-resistant and insulating material and has through apertures (19) in the basic area (25), each of which accepts an element (18a, 18b) of the thermocouples (18). The second reference connections (6, 36) of the thermocouples (18) are in a region shielded from the heat radiation.

Description

Sensor for radiation pyrometric temperature measurement at high ambient temperature

The invention relates to a sensor for the radiation pyrometric determination of the temperature of a measurement object, in particular under conditions of high ambient temperatures in the interior of a dryer or the like. According to the preamble of claim 1.

With such sensors, a non-contact measurement of the surface temperature of a measurement object, for. B. of solid materials, materials and products in hot air dryers and heat treatment systems possible. With several sensors arranged as close as possible to the surface to be measured, it is possible to determine a spatial and temporal temperature profile of the treated material, which, in addition to other process parameters, is an important prerequisite for optimized process management with regard to economy and quality assurance. Such heat treatment plants are used in the textile industry, the paper industry, the wood industry, the furniture industry and also in the production of gypsum boards or the like.

It is known to provide a radiation pyrometer outside the system and to aim at the measurement object or its surface and to measure the temperature through an opening or a window that is permeable to heat radiation. Only if it is optical and transparent to radiation If there is line of sight, the measurement can be sufficiently accurate. However, if there is a relatively large distance between the test object and the pyrometer, the measurement is considerably disturbed by radiation-absorbing gases, vapors or aerosols. Other disturbing factors can be the emissivity of the test object with regard to the reflection of external radiation or - if windows are used - their

spectral absorption properties. The arrangement of the radiation pyrometers requires the installation of a cross air barrier and cooling devices to prevent condensation and sublimation effects and to protect the pyrometer optics and pyrometer electronics from heat. The use of several pyrometers, as is necessary to measure a temperature profile, is hardly economically justifiable due to the effort involved.

It is also known (Textilbetrieb 1981, Issue 4, page 55), several simple for process control in web dryers

Temperature sensors e.g. B. as thermocouples along the track one after the other directly on the track grinding at a short distance above or in the exhaust air flow. This enables a tendency to control the temperature; however, the temperature profile that is important for certain chemical or physico-chemical processes cannot be measured with sufficient accuracy.

From DE-A 41 02 524 a sensor for measuring radiation temperature in the infrared spectral range is known, which is constructed as a miniaturized thermopile manufactured in thin-film technology. However, this sensor does not withstand the temperatures inside heat treatment plants. Known resistance thermometers (DE-A 35 36 133) cannot be used with sufficient accuracy in the area of high ambient temperatures. The invention has for its object to provide a sensor for radiation temperature measurement, which allows an accurate temperature measurement of a measurement object in its immediate vicinity even at high ambient temperatures.

The object is achieved according to the characterizing features of claim 1.

The sensor according to the invention allows measurement in the immediate vicinity of the measurement object in the interior of a hot air dryer or a heat treatment system. This is made possible by the use of materials and compounds which are resistant to high temperatures (for example up to 400 °), so that the mechanical properties of the sensor are appropriate for the application. Surprisingly, it has been found that the sensor structure according to the invention the temperature of the measurement object can be determined very precisely, the simple construction of the sensor making it economically feasible to use it several times in a heat treatment system, so that temperature profiles can be created at a reasonable cost and at low cost. It is essential that the D rante emente the thermocouples in the passage opening. lie so that they are shielded in terms of temperature. and the thermocouple emits a high temperature voltage. For this purpose, the comparison connection points must be shielded from the heat radiation, which is achieved either by arranging the comparison connection points on the back of the support body or by a shield that is impermeable to heat radiation, behind which the comparison connection points after the wire elements have been carried through the support body to the back and lie back.

To compensate for interference, a further thermocouple can be arranged to determine the temperature gradient, its radiation-sensitive connection point on the side the base area and its comparison connection points is located on the rear side of the support body, the radiation-sensitive connection point being arranged behind a shield impermeable to heat radiation. The output signal obtained in this way provides information about the non-radiation-related temperature difference between the groups of connection points and can therefore be used to correct the temperature difference indicated by the thermopiles.

A plurality of further thermocouples are preferably combined to form a second thermopile, which has the same structure and the same arrangement as the first thermopile. The radiation-sensitive connection points of the second thermopile are located behind the heat radiation-impermeable shield. The second thermopile is connected in series with the first thermopile so that thermoelectric currents cancel each other out that have no radiation-related cause for the temperature difference.

In order to ensure an exact temperature measurement of the opera area of a measurement object under extreme conditions of use, the radiation of the base of the support body facing the window is expediently symmetrical in the same sectors, e.g. B. 2, 4, 6, 8 sectors divided and provided in the sectors identically designed and arranged thermopiles. The thermopiles are connected in opposite polarity in series, which eliminates false signals and provides a highly accurate output signal.

In order to obtain a better adjustment of the comparison connection points to the intrinsic temperature of the sensor which corresponds to the ambient temperature and thus the

Sensitivity should be increased by increasing the temperature difference between the groups of connection points the comparison connection points are connected to one another in a heat-conducting manner, preferably with a heat-conducting washer.

By arranging a radiation-reflecting layer on the base surface of the support body facing the heat-radiation-permeable window, on the one hand a better radiation exchange between the radiation-sensitive connection points and the measurement object is achieved and on the other hand radiation-related heating of the support body is prevented.

In order to enlarge the radiation-sensitive areas and thus to increase the sensitivity, the radiation-sensitive connection points are connected to, in particular, metallic surface elements that absorb heat radiation and are oriented towards the measurement object.

To determine the object temperature from the measured radiation-related and corrected signal of the temperature difference between the two groups of connection points, knowledge of the intrinsic temperature of the sensor is additionally required. Their determination is also carried out thermoelectrically by a at any connection point of a measuring line led out of the housing

Compensation line is connected from a thermoelectrically active material to the measuring line and is led out of the housing.

To evaluate the temperature difference signal is the

Knowledge of the temperature of the sensor in the area of the radiation-sensitive connection points is expedient, which is why a temperature sensor, e.g. B. a thermocouple is arranged.

The design of each thermocouple of the thermopile is such that the ratio of the wire diameter to the wire length between two connection points is greater than about 1: 100, the wire element made of the material having higher thermal conductivity having a relatively smaller diameter. This minimizes the radiation-related influence on the temperature of the comparison junction by heat conduction via the wire elements, since the heat flow flowing from the wire surface to the surrounding air in the through-opening or the support body is greater than that between the junction points.

Further features of the invention result from the further claims, the description and the drawing, in which exemplary embodiments of the invention described in detail below are shown. Show it:

1 shows in section a schematic structure of a sensor according to the invention,

2 shows in section another structure of a sensor in a representation according to FIG. 1,

3 shows in section a further structure of a sensor in a representation according to FIG. 1,

4 is a plan view of a base of a support body of the sensor with two thermopiles,

5 shows a plan view of the base area according to FIG. 4 with four thermopiles,

Fig. 6 in section, a fourth structure of a sensor in

a representation according to FIG. 1.

The sensor for radiation pyrometric determination of the temperature of a measurement object shown in FIG. 1 is particularly suitable for use at high ambient temperatures provided as it exists in the interior of a dryer, a heat treatment system or the like.

In the exemplary embodiment, the sensor consists of a heat-conducting housing 1, which can preferably be made of aluminum, steel or copper. If the cylindrical housing 1 is made of steel, a wall thickness of 2 mm can be expedient. On one end face 20 of the cylindrical housing 1, a circular opening is provided, which advantageously has a diameter of 25 mm. This opening forms a window 2, which is covered by a preferably 2 mm thick, radiation-permeable pane 21. The disk consists in particular of barium fluoride (BaF ₂ ); it is permeable to the long-wave infrared range, i.e. to heat radiation. Germanium, silicon or the like can also be expedient as material for the pane.

A support body 5 is arranged in the interior 22 of the metallic housing, which is expediently located at all sides from the walls of the housing 1. The support body 5 is cylindrical in accordance with the cylindrical housing 1, the axial end faces 25, 26 approximately

lie parallel to the end faces of the housing 1. The supporting body 5 consists of a poorly heat-conducting or heat-insulating material; In the exemplary embodiment shown, the support body 5 consists of a cement-bound, light silicate foam material with a thermal conductivity of approximately 0.1 W / km. The diameter and the height of the body are preferably the same; in the exemplary embodiment they are 30 mm.

In the axial direction of the support body 5, openings 19 are provided as through bores, in each of which a wire element 18a, 18b of a thermocouple 18 is arranged in the exemplary embodiment. The wire elements 18a and 18b of a plurality of thermocouples 18 are interconnected to form a thermopile 3, which is symmetrical on the axial end face of the support body forming a flat base surface 25

5 are distributed. 1, the thermopile 3 consists of thirty thermocouples 18 of the material combination nickel-chromium / nickel. The wire elements 18a have a diameter of 0.2 mm (nickel-chrome); the

Wire elements 18b have a diameter of 0.1 mm (Ni). The ratio of the wire diameter D or d to the wire length L or 1 between two connection points 4 and 6 is greater than approximately 1: 100. The wire element 18b made of the material with higher thermal conductivity has a relatively smaller diameter.

The first radiation-sensitive or hot connection points 4 of the thermopile 3 are arranged symmetrically distributed on the flat base surface 25 facing the window 2; the second, cold comparison junctions

6 lie on the rear side 26 of the support body 5 facing away from the base side 25. As shown in FIG. 1, the comparison connection points 6 are connected to one another in a heat-conducting manner via a disk 7, the disk 7 being an electrical insulator to avoid electrical short-circuits. In the same way, the support body 5 consists of an electrically insulating material.

Another thermocouple 17 is suitably arranged to compensate for radiation-related interference. The thermocouple 17 lies with its radiation-sensitive connection point 16 preferably in the center of the base area 25 behind a shield 9 which is impermeable to heat radiation and which is expediently fastened on the pane 21 of the window 2. The shield 9 is connected to the disk 21 in a heat-transferring manner and is advantageously mirrored on the side 9a facing the measurement object. In order to obtain the most accurate possible detection of the temperature on the side of the base area 25 ten, the radiation-sensitive connection point 16 can be of metallic bare or mirrored design.

In order to achieve a high degree of efficiency at the radiation-sensitive connection points 4 of the thermopile 3, the flat base surface 25 can be made bare or metallically mirrored. The radiation-sensitive connection points 4 are expediently designed to absorb heat radiation; z. B. blackened with a radiation absorbing pigment. In another embodiment, the radiation-sensitive connection points can be connected to surface radiation elements which absorb heat radiation and are oriented, in particular metallic, to the measurement object.

The comparison connection point 15 of the thermocouple 17 is preferably connected in a heat-transferring manner to the comparison connection points 6 of the thermopile 3, for which purpose the comparison connection point 15 is preferably fastened on the heat-conducting, electrically insulating disk 7. The

Disc 7 expediently has the same diameter as the supporting body 5.

In order to also receive a signal representing the temperature on the rear side 26 of the support body 5, a compensation line 11 is expediently connected to a connection point 27 of a measuring line 10, which consists of a thermoelectrically active material compared to the measuring line 10 and, like the measuring lines 10, from the housing 1 is brought out.

With the sensor according to the invention, output signals (thermal voltage) can be tapped on the measuring lines 10, 11, which allow a precise determination of the heat radiation entering through the window 2 and thus a determination of the surface temperature of the measuring object targeted by the sensor. The sensor according to the invention can directly are used inside the heat treatment systems, i.e. in the area of high ambient temperatures of up to 400'C. All materials used are resistant to the high temperatures. It can be assumed that the sensor temperature under such conditions is generally above the temperature of the object to be measured, and that the measurement signal is triggered by cooling the radiation-sensitive connection points of the thermopile.

The basic structure of the sensor according to the exemplary embodiment according to FIG. 2 corresponds to that according to FIG. 1, which is why the same reference numerals are used for the same parts. In a deviation from FIG. 1, a second thermopile 33 is arranged on the support body 5 symmetrically to a central plane 30 lying perpendicular to the base surface 25, the radiation-sensitive connection points 34 of which lie behind a shield 31 which covers half of the window 2 impermeably against heat radiation. As already described above, the shield 31 is preferably mirrored on the outside facing the measurement object and is in heat-conducting connection with the window 2 carrying it. The comparison connection points connection points 36, like the comparison connection points 6 of the first thermopile 3, are on the heat-conducting one , electrically insulating disc 7 attached so that the comparison junctions 6 and 36 of the two thermopiles 3 and 33 are at the same temperature level. The thermopiles 3 and 33 are connected in opposite polarity in series, so that thermoelectric currents cancel each other out that have no radiation-related cause for the temperature difference.

FIG. 3 shows a further exemplary embodiment of a sensor according to the invention, which corresponds in its basic structure to that according to FIG. 2. The same reference numerals are used for the same parts. In the exemplary embodiment according to FIG. 3, the heat-conducting disc is for the comparative connection digits 6 and 36 are omitted. The shield 31 is applied to the side of the disk 21 facing the base surface 25, the side facing the measurement object being mirrored. The shield 31 can consist of a film which is in heat-transferring connection with the window 2.

The base surface 25 of the supporting body 5 facing the window 2 is divided into two sectors 40, 41 according to FIG. 3, fifteen radiation-sensitive connection points 4 and 34 being provided in each sector. The wire elements run - as already described above - in the axial direction of the support body 5 through axially parallel bores to the rear 26 of the support body 5. The radiation-sensitive connection points 4, 34 are arranged symmetrically to the plane 30, which is perpendicular to the base surface 25, and the sectors 40 , 41 separates from each other.

The thermopiles 3, 33 are connected in opposite polarity in series, so that a compensated output signal is present on the measuring lines 10. For further compensation, a thermocouple 50 is arranged in the sector 40 exposed to heat radiation. Its output signal indicates the actual temperature on the base side 25 of the body 5.

An output signal largely cleaned up even with diffuse heat radiation from interference radiation is obtained if the base area 25 of the supporting body 5 is divided into four identical sectors 40a, 40b, 41a, 41b. Six radiation-sensitive connection points 4a, 4b and 34a, 34b are arranged in each sector, the radiation-sensitive connection points 34a and 34b being located behind a shield 31a and 31b, respectively. The sectors are provided such that the sectors 40a and 40b exposed to heat radiation and the sectors 41a, 41b shielded by the heat-impermeable shield 31a, 31b in the circumferential direction switch. The sectors of FIGS. 4 and 5 form circular segments (quarter circle, semicircle), the thermopile exposed to thermal radiation being connected in series with the thermopile arranged behind a shield in an antipolar manner. It has been shown that when four thermopiles are arranged in the manner shown in FIG. 5, a very precise output signal is achieved with a sensor according to FIG. 3. The radiation-sensitive connection points 4a, 4b and 34a, 34b of the four thermopiles according to FIG. 5 are axially symmetrical to the vertical axis 29, which is preferably the cylinder axis of the cylindrical support body 5. It may be expedient to design the support body 5 as a cuboid.

6 corresponds in its basic structure to that of FIG. 1, which is why the same reference numerals are used for the same parts. 4, the base area 25 can be divided into two sectors 40, 41 by the plane 30. The radiation-sensitive connection points 4 of a thermopile 3, whose comparison connection points 6 are located on the side of the base area 25 in the heat radiation-impermeable sector 41, lie in the heat radiation-permeable sector 40. The wire elements 18a, 18b of each thermocouple 18 run through a bore 19 in the support body 5 from the base 25 from the sector 40 to the rear 26 and from there through a further bore 19 back to the base 25 into the radiation-opaque sector 41. With such an arrangement a separate thermopile for compensation can be omitted. A corresponding arrangement is also possible with a division into four sectors (FIG. 5) with one or two thermopiles, which are then connected in series in opposite polarity. A thermopile with radiation-sensitive connection points 4a lies in the sector 40a; the comparison junctions of the same thermopile are in the adjacent, covered sector 41. The groups of junctions are corresponding place the second thermopile in sectors 40b and 41b.

Claims

Expectations

1. Sensor for radiation pyrometric determination of

Temperature of a test object, especially below

Conditions of high ambient temperatures in the interior of a dryer or the like, consisting of a heat-conducting housing (1) with a heat-radiation-permeable window (2) and at least one thermopile (3, 33) arranged in the housing (1), which are made of thermocouples (18) from one another connected elements (18a, 18b) of mutually thermoelectrically active

Materials, with a first,

radiation-sensitive connection point (4, 34) of the

Elements (18a, 18b) face the window (2), characterized in that the strand-sensitive connection points (4, 34) are distributed over a base area (25) of a supporting body (5) facing the window (2) such that the supporting body (5th ) consists of a heat-resistant, heat-insulating material that the support body (5) from the base (25)

has outgoing through openings (19) which each receive an element (18a, 18b) of the thermocouples (18), the second comparison connecting points (6, 36) of the thermocouples (18) being in a region covered by the thermal radiation.

2. Sensor according to claim 1,

characterized in that the comparison Joints are covered by the support body (9) and lie on the back (26).

3. Sensor according to claim 1,

characterized in that each element (18a, 18b) of the thermocouples (18) is guided through the support body (5) to its rear side (26) and through a further through opening (19) from the rear side (26) back to the base surface (25) , wherein the comparison connection points (6, 36) lie on the base (25) behind a radiation-opaque shield (9, 39).

4. Sensor according to one of claims 1 to 3,

characterized in that the supporting body (5) has approximately the shape of a cylinder, cuboid or the like. With flat sides facing away from one another and lying approximately parallel to one another, which form the base surface (25) and the rear side (26).

5. Sensor according to one of claims 1 to 4,

characterized in that the base (25) is flat.

6. Sensor according to one of claims 1 to 5,

characterized in that at least one further thermocouple (17) is arranged, the radiation-sensitive connection point (16) on the side of the

Base area (25) and its comparison connection point (15) is located on the rear side (26) of the supporting body (5), the radiation-sensitive connection point (16) being arranged behind a shield (9) which is impervious to heat radiation.

7. Sensor according to claim 6,

characterized in that several further thermocouples form a second thermopile (33) which has the same structure and the same arrangement as the first thermopile (3), the radiation-sensitive hot junctions (34) of the second thermopile (33) being located behind the heat radiation-impermeable shield (31), and that the second thermopile (33) with the first thermopile (3) in opposite polarity in series

is switched.

8. Sensor according to claim 6 or 7,

characterized in that the shield (9, 31) is coated on its side facing the measurement object in a radiation-reflecting manner.

9. Sensor according to one of claims 6 to 8,

characterized in that the shield (9, 31) is arranged on the window (2) and is thermally conductively connected to the window (2).

10. Sensor according to one of claims 1 to 9,

characterized in that the comparison junctions (6, 15, 36), preferably all

Comparison connection points are connected to each other in a heat-conducting manner.

11. Sensor according to one of claims 1 to 10,

characterized in that the base area (25) is divided into m identical sectors (40, 41) and a group of connecting points (4, 6) is arranged in each sector (40, 41).

12. Sensor according to claim 11,

characterized in that the sectors (40, 41) have the same area and are equipped with identically designed and arranged thermopiles (3, 33).

13. Sensor according to claim 11 or 12,

characterized in that the sectors (40a and 40b) exposed to heat radiation and the sectors (41a, 41b) shielded by a heat-impermeable shield (31) alternate.

14. Sensor according to one of claims 11 to 13,

characterized in that the sectors (40, 40a, 40b, 41, 41a, 41b) are circular segments.

15. Sensor according to one of claims 1 to 14,

characterized in that the thermopiles (3, 33) arranged on a support body (9) are axially symmetrical to a vertical axis (29) of the support body (5) which is perpendicular to the base surface (25).

16. Sensor according to one of claims 1 to 15,

characterized in that the base surface (25) of the support body (9) facing the heat-radiation-permeable window (2) is a radiation-reflecting element

Layer (25a) carries.

17. Sensor according to one of claims 1 to 16,

characterized in that the radiation-sensitive connection points (4, 34) are coated in a radiation-absorbing manner, in particular with a

radiation-absorbing pigment are blackened.

18. Sensor according to one of claims 1 to 17,

characterized in that the radiation-sensitive connection points (4, 34) are connected to in particular metallic surface elements (14) which absorb heat radiation and are oriented towards the object to be measured.

19. Sensor according to one of claims 1 to 18,

characterized in that the from the shield (9, 31) covered connection points (16, 34) are designed to reflect radiation, in particular are mirrored.

20. Sensor according to one of claims 1 to 19,

characterized in that in a region (40, 40a, 40b) of the base (25) exposed to heat radiation a temperature sensor (50), e.g. B. a thermocouple is arranged.

21. Sensor according to one of claims 1 to 20,

characterized in that at the connection point (27) of a measuring line (10) led out of the housing (1) a compensation line (11) made of a thermoelectrically active material with respect to the measuring line (10) is connected and led out of the housing (1).

22. Sensor according to one of claims 1 to 21,

characterized in that the supporting body (5) and the disc (7) consist of an electrically insulating material.

23. Sensor according to one of claims 1 to 22,

characterized in that the housing (1) consists of a metal, in particular aluminum or copper.

24. Sensor according to one of claims 1 to 23,

characterized in that the ratio of the wire diameter to the wire length between two connection points (46, 34, 36) is greater than approximately 1: 100 and the wire element (18b) made of the material of higher thermal conductivity has a relatively smaller diameter.