WO1993020153A1 - System for the production of carbon black - Google Patents
System for the production of carbon black Download PDFInfo
- Publication number
- WO1993020153A1 WO1993020153A1 PCT/NO1993/000057 NO9300057W WO9320153A1 WO 1993020153 A1 WO1993020153 A1 WO 1993020153A1 NO 9300057 W NO9300057 W NO 9300057W WO 9320153 A1 WO9320153 A1 WO 9320153A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- reactor
- carbon black
- gas
- hydrogen
- plasma
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/44—Carbon
- C09C1/48—Carbon black
- C09C1/487—Separation; Recovery
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
- C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
- C01B3/22—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by decomposition of gaseous or liquid organic compounds
- C01B3/24—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by decomposition of gaseous or liquid organic compounds of hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/44—Carbon
- C09C1/48—Carbon black
- C09C1/485—Preparation involving the use of a plasma or of an electric arc
Definitions
- the invention relates to a system for the production of carbon black and hydrogen by the decomposition of hydrocarbons.
- the object of the present invention is to provide a system for the production of carbon black and hydrogen by decomposition of hydrocarbon gas, which can be operated in a continuous process and where it is possible to preset the process conditions in such a way that a carbon black can be produced with predeter ⁇ mined physical properties.
- This object is achieved with a system which is characterized by the features in the patent claims presented.
- the main section of the system comprises a plasma torch 1 wit an attached reactor chamber 2.
- the plasma torch is supplied with plasma gas which may be hydrogen through a pipe 12 and hydrocarbon gas, e.g. methane, from a storage tank 16 or directly from a gas pipeline through a pipe 17.
- plasma gas which may be hydrogen through a pipe 12 and hydrocarbon gas, e.g. methane, from a storage tank 16 or directly from a gas pipeline through a pipe 17.
- hydrocarbon gas e.g. methane
- the hydrocarbon gas is decomposed, in the example methane is decomposed into carbon black and hydrogen, which are further processed in the reactor 2 in order to obtain the desired physical properties for the resulting carbon black.
- This is done by controlling the temperature of zones in the reactor and a controlled supply o methane resp. admixtures through branch pipes which lead into the reactor chamber and which are schematically indicated by 18.
- the reactor design is described in more detail in the applicant's copending patent application 92 1360.
- the produc carbon black is passed from the reactor together with the hydrogen, the carbon black now having predetermined physical properties, through a pipe cooler 3 and on to separation equipment which, e.g., may consist of a cyclone arrangement 4, 5, where coarse particles are separated if these are not want for the further processing.
- the tempera ture is reduced from an exit temperature from the reactor whi can be between, e.g. 800 and 1600° C, to a temperature of, e. 50-160° C.
- the heat which is removed from the product stream can be heat exchanged at 19 with the feed gas and plasma gas for energy optimization.
- the exit temperature from the plasma torch in the reactor is of the order of 3000-8000° C.
- the hydrogen and carbon black are passed on through the pipe 6 to a main filter 7 which filters off additional components, so that in the filter silo 8 there is collected only carbon black with a particle size within a desired, defined range and with a special structure which is achieved in the reactor section.
- the special carbon black can then be removed from the filter silo 8 for further processing.
- Remaining hydrogen can be recovered from the filters and combined with the hydrogen from the pipe.
- the hydrogen can either be supplied directly to a chemical processing industry or stored for later use, it can be used as an energy carrier and employed, e.g., in power production, and a desired portion is returned through the pipe 11 to the plasma torch and used as plasma gas there. For reasons of safety the system is connected to a flame stack 10 where the gas can be burned off.
- the hydrogen gas which is used as plasma gas can in addition be supplied with hydrocarbon gas, which can have a favourable effect in connection with the combustion or the consumption of the electrodes, which will thereby be less rapidly consumed.
- the control of the hydrogen supply to the plasma torch is provided by means of a control valve which is linked to the conditions in the plasma arc.
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Inorganic Chemistry (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
- Carbon And Carbon Compounds (AREA)
- Breeding Of Plants And Reproduction By Means Of Culturing (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Abstract
Description
Claims
Priority Applications (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP5517332A JP2588840B2 (en) | 1992-04-07 | 1993-04-05 | System for the production of carbon black |
EP93909087A EP0635044B1 (en) | 1992-04-07 | 1993-04-05 | System for the production of carbon black |
DE69301541T DE69301541T2 (en) | 1992-04-07 | 1993-04-05 | PLANT FOR THE PRODUCTION OF RUSS |
GR960400544T GR3019120T3 (en) | 1992-04-07 | 1996-02-28 | System for the production of carbon black. |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
NO921359 | 1992-04-07 | ||
NO921359A NO176968C (en) | 1992-04-07 | 1992-04-07 | Carbon production plant |
Publications (1)
Publication Number | Publication Date |
---|---|
WO1993020153A1 true WO1993020153A1 (en) | 1993-10-14 |
Family
ID=19895049
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/NO1993/000057 WO1993020153A1 (en) | 1992-04-07 | 1993-04-05 | System for the production of carbon black |
Country Status (17)
Country | Link |
---|---|
EP (1) | EP0635044B1 (en) |
JP (1) | JP2588840B2 (en) |
CN (1) | CN1047609C (en) |
AT (1) | ATE133989T1 (en) |
AU (1) | AU3962693A (en) |
CA (1) | CA2133770C (en) |
CZ (1) | CZ287533B6 (en) |
DE (1) | DE69301541T2 (en) |
DK (1) | DK0635044T3 (en) |
EG (1) | EG20260A (en) |
ES (1) | ES2083858T3 (en) |
GR (1) | GR3019120T3 (en) |
HU (1) | HU217032B (en) |
MA (1) | MA22862A1 (en) |
MY (1) | MY107778A (en) |
NO (1) | NO176968C (en) |
WO (1) | WO1993020153A1 (en) |
Cited By (25)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5484978A (en) * | 1994-03-11 | 1996-01-16 | Energy Reclamation, Inc. | Destruction of hydrocarbon materials |
DE19827154A1 (en) * | 1998-06-18 | 1999-12-23 | Irt Innovative Recycling Techn | Production of methanol from biogas |
WO2007095563A2 (en) | 2006-02-15 | 2007-08-23 | Egt Enterprises, Inc. | Electric reaction technology for fuels processing |
CN102108216A (en) * | 2010-12-03 | 2011-06-29 | 苏州纳康纳米材料有限公司 | Method for preparing conductive carbon black and hydrogen by plasma technology |
RU2505586C2 (en) * | 2012-01-10 | 2014-01-27 | Федеральное Государственное Бюджетное Образовательное Учреждение Высшего Профессионального Образования "Дагестанский Государственный Технический Университет" (Дгту) | Light-duty plant for disposal of resources of small natural gas fields |
US8871173B2 (en) | 2010-02-19 | 2014-10-28 | Cabot Corporation | Method for carbon black production using preheated feedstock and apparatus for same |
DE102013010034A1 (en) | 2013-06-17 | 2014-12-18 | Evonik Industries Ag | Plant and method for the efficient use of excess electrical energy |
WO2015116811A1 (en) * | 2014-01-31 | 2015-08-06 | Monolith Materials, Inc. | Plasma reactor |
US10100200B2 (en) | 2014-01-30 | 2018-10-16 | Monolith Materials, Inc. | Use of feedstock in carbon black plasma process |
US10138378B2 (en) | 2014-01-30 | 2018-11-27 | Monolith Materials, Inc. | Plasma gas throat assembly and method |
US10337110B2 (en) | 2013-12-04 | 2019-07-02 | Covestro Deutschland Ag | Device and method for the flexible use of electricity |
US10370539B2 (en) | 2014-01-30 | 2019-08-06 | Monolith Materials, Inc. | System for high temperature chemical processing |
US10618026B2 (en) | 2015-02-03 | 2020-04-14 | Monolith Materials, Inc. | Regenerative cooling method and apparatus |
DE102018132661A1 (en) * | 2018-12-18 | 2020-06-18 | Thyssenkrupp Ag | METHOD FOR HYDROCARBON PYROLYSIS WITH A SPACIFIED HEATING AND REACTION ZONE WITHIN THE REACTOR ROOM |
US10808097B2 (en) | 2015-09-14 | 2020-10-20 | Monolith Materials, Inc. | Carbon black from natural gas |
US11149148B2 (en) | 2016-04-29 | 2021-10-19 | Monolith Materials, Inc. | Secondary heat addition to particle production process and apparatus |
US11304288B2 (en) | 2014-01-31 | 2022-04-12 | Monolith Materials, Inc. | Plasma torch design |
US11453784B2 (en) | 2017-10-24 | 2022-09-27 | Monolith Materials, Inc. | Carbon particles having specific contents of polycylic aromatic hydrocarbon and benzo[a]pyrene |
US11492496B2 (en) | 2016-04-29 | 2022-11-08 | Monolith Materials, Inc. | Torch stinger method and apparatus |
US11665808B2 (en) | 2015-07-29 | 2023-05-30 | Monolith Materials, Inc. | DC plasma torch electrical power design method and apparatus |
US11760884B2 (en) | 2017-04-20 | 2023-09-19 | Monolith Materials, Inc. | Carbon particles having high purities and methods for making same |
US11926743B2 (en) | 2017-03-08 | 2024-03-12 | Monolith Materials, Inc. | Systems and methods of making carbon particles with thermal transfer gas |
US11939477B2 (en) | 2014-01-30 | 2024-03-26 | Monolith Materials, Inc. | High temperature heat integration method of making carbon black |
US11987712B2 (en) | 2015-02-03 | 2024-05-21 | Monolith Materials, Inc. | Carbon black generating system |
US12030776B2 (en) | 2017-08-28 | 2024-07-09 | Monolith Materials, Inc. | Systems and methods for particle generation |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP4516091B2 (en) * | 2007-04-23 | 2010-08-04 | 株式会社東芝 | Nanocarbon generator |
EP2623564A1 (en) * | 2012-02-03 | 2013-08-07 | Omya International AG | Installation for the purification of minerals, pigments and/or fillers and/or the preparation of precipitated earth alkali carbonate |
CN113897077A (en) * | 2021-11-16 | 2022-01-07 | 航天环境工程有限公司 | Continuous purification device of pyrolysis carbon black high temperature plasma |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB1150362A (en) * | 1965-05-31 | 1969-04-30 | Roger Morel | Improvements in the Production of Carbon-Black |
GB1492346A (en) * | 1975-06-30 | 1977-11-16 | Vnii Tekh Ugleroda | Process for the production of carbon black |
US4213939A (en) * | 1977-07-01 | 1980-07-22 | Sid Richardson Carbon & Gasoline Co. | Double venturi carbon black reactor system |
EP0315442A2 (en) * | 1987-11-04 | 1989-05-10 | Witco Corporation | Process and apparatus for producing improved carbon blacks and resultant product |
EP0392121A2 (en) * | 1989-04-10 | 1990-10-17 | Columbian Chemicals Company | Carbon black reactor with an elongated choke and method for producing carbon black therewith |
-
1992
- 1992-04-07 NO NO921359A patent/NO176968C/en not_active IP Right Cessation
-
1993
- 1993-04-01 MA MA23153A patent/MA22862A1/en unknown
- 1993-04-05 AU AU39626/93A patent/AU3962693A/en not_active Abandoned
- 1993-04-05 CA CA002133770A patent/CA2133770C/en not_active Expired - Fee Related
- 1993-04-05 DE DE69301541T patent/DE69301541T2/en not_active Expired - Fee Related
- 1993-04-05 ES ES93909087T patent/ES2083858T3/en not_active Expired - Lifetime
- 1993-04-05 DK DK93909087.4T patent/DK0635044T3/en active
- 1993-04-05 CZ CZ19942490A patent/CZ287533B6/en not_active IP Right Cessation
- 1993-04-05 WO PCT/NO1993/000057 patent/WO1993020153A1/en active IP Right Grant
- 1993-04-05 AT AT93909087T patent/ATE133989T1/en not_active IP Right Cessation
- 1993-04-05 HU HU9402779A patent/HU217032B/en not_active IP Right Cessation
- 1993-04-05 JP JP5517332A patent/JP2588840B2/en not_active Expired - Lifetime
- 1993-04-05 EP EP93909087A patent/EP0635044B1/en not_active Expired - Lifetime
- 1993-04-06 EG EG20893A patent/EG20260A/en active
- 1993-04-06 CN CN93105483A patent/CN1047609C/en not_active Expired - Fee Related
- 1993-04-07 MY MYPI93000635A patent/MY107778A/en unknown
-
1996
- 1996-02-28 GR GR960400544T patent/GR3019120T3/en unknown
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB1150362A (en) * | 1965-05-31 | 1969-04-30 | Roger Morel | Improvements in the Production of Carbon-Black |
GB1492346A (en) * | 1975-06-30 | 1977-11-16 | Vnii Tekh Ugleroda | Process for the production of carbon black |
US4213939A (en) * | 1977-07-01 | 1980-07-22 | Sid Richardson Carbon & Gasoline Co. | Double venturi carbon black reactor system |
EP0315442A2 (en) * | 1987-11-04 | 1989-05-10 | Witco Corporation | Process and apparatus for producing improved carbon blacks and resultant product |
EP0392121A2 (en) * | 1989-04-10 | 1990-10-17 | Columbian Chemicals Company | Carbon black reactor with an elongated choke and method for producing carbon black therewith |
Cited By (36)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5484978A (en) * | 1994-03-11 | 1996-01-16 | Energy Reclamation, Inc. | Destruction of hydrocarbon materials |
DE19827154A1 (en) * | 1998-06-18 | 1999-12-23 | Irt Innovative Recycling Techn | Production of methanol from biogas |
DE19827154C2 (en) * | 1998-06-18 | 2003-01-30 | Irt Innovative Recycling Techn | Process for the production of methanol from biogas and an apparatus for carrying out the process |
WO2007095563A2 (en) | 2006-02-15 | 2007-08-23 | Egt Enterprises, Inc. | Electric reaction technology for fuels processing |
EP1991348A2 (en) * | 2006-02-15 | 2008-11-19 | EGT Enterprises Inc. | Electric reaction technology for fuels processing |
EP1991348A4 (en) * | 2006-02-15 | 2010-08-04 | Egt Entpr Inc | Electric reaction technology for fuels processing |
US8871173B2 (en) | 2010-02-19 | 2014-10-28 | Cabot Corporation | Method for carbon black production using preheated feedstock and apparatus for same |
US9574087B2 (en) | 2010-02-19 | 2017-02-21 | Cabot Corporation | Method for carbon black production using preheated feedstock and apparatus for same |
CN102108216A (en) * | 2010-12-03 | 2011-06-29 | 苏州纳康纳米材料有限公司 | Method for preparing conductive carbon black and hydrogen by plasma technology |
RU2505586C2 (en) * | 2012-01-10 | 2014-01-27 | Федеральное Государственное Бюджетное Образовательное Учреждение Высшего Профессионального Образования "Дагестанский Государственный Технический Университет" (Дгту) | Light-duty plant for disposal of resources of small natural gas fields |
WO2014202314A1 (en) | 2013-06-17 | 2014-12-24 | Evonik Industries Ag | Plant and process for the efficient utilization of excess electric energy |
DE102013010034A1 (en) | 2013-06-17 | 2014-12-18 | Evonik Industries Ag | Plant and method for the efficient use of excess electrical energy |
US10337110B2 (en) | 2013-12-04 | 2019-07-02 | Covestro Deutschland Ag | Device and method for the flexible use of electricity |
US11866589B2 (en) | 2014-01-30 | 2024-01-09 | Monolith Materials, Inc. | System for high temperature chemical processing |
US10138378B2 (en) | 2014-01-30 | 2018-11-27 | Monolith Materials, Inc. | Plasma gas throat assembly and method |
US10100200B2 (en) | 2014-01-30 | 2018-10-16 | Monolith Materials, Inc. | Use of feedstock in carbon black plasma process |
US10370539B2 (en) | 2014-01-30 | 2019-08-06 | Monolith Materials, Inc. | System for high temperature chemical processing |
US11939477B2 (en) | 2014-01-30 | 2024-03-26 | Monolith Materials, Inc. | High temperature heat integration method of making carbon black |
US11203692B2 (en) | 2014-01-30 | 2021-12-21 | Monolith Materials, Inc. | Plasma gas throat assembly and method |
US11591477B2 (en) | 2014-01-30 | 2023-02-28 | Monolith Materials, Inc. | System for high temperature chemical processing |
WO2015116811A1 (en) * | 2014-01-31 | 2015-08-06 | Monolith Materials, Inc. | Plasma reactor |
US11304288B2 (en) | 2014-01-31 | 2022-04-12 | Monolith Materials, Inc. | Plasma torch design |
US10618026B2 (en) | 2015-02-03 | 2020-04-14 | Monolith Materials, Inc. | Regenerative cooling method and apparatus |
US11998886B2 (en) | 2015-02-03 | 2024-06-04 | Monolith Materials, Inc. | Regenerative cooling method and apparatus |
US11987712B2 (en) | 2015-02-03 | 2024-05-21 | Monolith Materials, Inc. | Carbon black generating system |
US11665808B2 (en) | 2015-07-29 | 2023-05-30 | Monolith Materials, Inc. | DC plasma torch electrical power design method and apparatus |
US10808097B2 (en) | 2015-09-14 | 2020-10-20 | Monolith Materials, Inc. | Carbon black from natural gas |
US11492496B2 (en) | 2016-04-29 | 2022-11-08 | Monolith Materials, Inc. | Torch stinger method and apparatus |
US11149148B2 (en) | 2016-04-29 | 2021-10-19 | Monolith Materials, Inc. | Secondary heat addition to particle production process and apparatus |
US12012515B2 (en) | 2016-04-29 | 2024-06-18 | Monolith Materials, Inc. | Torch stinger method and apparatus |
US11926743B2 (en) | 2017-03-08 | 2024-03-12 | Monolith Materials, Inc. | Systems and methods of making carbon particles with thermal transfer gas |
US11760884B2 (en) | 2017-04-20 | 2023-09-19 | Monolith Materials, Inc. | Carbon particles having high purities and methods for making same |
US12030776B2 (en) | 2017-08-28 | 2024-07-09 | Monolith Materials, Inc. | Systems and methods for particle generation |
US11453784B2 (en) | 2017-10-24 | 2022-09-27 | Monolith Materials, Inc. | Carbon particles having specific contents of polycylic aromatic hydrocarbon and benzo[a]pyrene |
DE102018132661B4 (en) * | 2018-12-18 | 2020-10-01 | Thyssenkrupp Ag | Process for hydrocarbon pyrolysis with spatially separated heating and reaction zones within the reactor space |
DE102018132661A1 (en) * | 2018-12-18 | 2020-06-18 | Thyssenkrupp Ag | METHOD FOR HYDROCARBON PYROLYSIS WITH A SPACIFIED HEATING AND REACTION ZONE WITHIN THE REACTOR ROOM |
Also Published As
Publication number | Publication date |
---|---|
EG20260A (en) | 1998-05-31 |
DE69301541T2 (en) | 1996-09-05 |
EP0635044A1 (en) | 1995-01-25 |
HU217032B (en) | 1999-11-29 |
MA22862A1 (en) | 1993-12-31 |
CN1047609C (en) | 1999-12-22 |
HUT67854A (en) | 1995-05-29 |
CA2133770C (en) | 1998-01-06 |
DK0635044T3 (en) | 1996-05-20 |
CZ249094A3 (en) | 1995-06-14 |
NO176968B (en) | 1995-03-20 |
AU3962693A (en) | 1993-11-08 |
HU9402779D0 (en) | 1995-01-30 |
JPH07508543A (en) | 1995-09-21 |
MY107778A (en) | 1996-06-15 |
ATE133989T1 (en) | 1996-02-15 |
NO176968C (en) | 1995-06-28 |
CN1082571A (en) | 1994-02-23 |
NO921359D0 (en) | 1992-04-07 |
EP0635044B1 (en) | 1996-02-07 |
JP2588840B2 (en) | 1997-03-12 |
CZ287533B6 (en) | 2000-12-13 |
ES2083858T3 (en) | 1996-04-16 |
GR3019120T3 (en) | 1996-05-31 |
DE69301541D1 (en) | 1996-03-21 |
NO921359L (en) | 1993-10-08 |
CA2133770A1 (en) | 1993-10-14 |
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